CN105112180A - Natural plant flower fragrance type essential oil soap having bacteriostatic function and producing method thereof - Google Patents
Natural plant flower fragrance type essential oil soap having bacteriostatic function and producing method thereof Download PDFInfo
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Abstract
The invention discloses a natural plant flower fragrance type essential oil soap having a bacteriostatic function. The natural plant flower fragrance type essential oil soap comprises compound essential oil and a soap base, wherein the compound essential oil contains, by volume, 1-4 parts of essential oil of rosemary, 2-5 parts of essential oil of marigold, 2-5 parts of essential oil of lavender, 1-5 parts of essential oil of palmarosa, 1-3 parts of essential oil of vetiver and 78-93 parts of natural soap base. The essential oil soap contains herbs and warm flowery fragrance, is rich, natural and lasting in fragrance, rich in bubble, exquisite in hand feel and good in washing effect, a soap body is resistant to dry cracking and is good in stability, and the essential oil soap has the bacteriostatic and bactericidal effects, can effectively inhibit bacterial formation on the skin surface and treat skin inflammations, is mild and stimulation-free to the skin, can improve the skin condition and moisturize and enhance the skin elasticity after being used for a long period of time, can improve the mental state of a user, inspire enthusiasm and enhance vigor and has the incentive effect.
Description
Technical field
The present invention relates to cosmetics of everyday use field, refer to a kind of essential oil soap especially.
Background technology
Perfumed soap is a kind of common daily necessities, and in recent years, along with the raising of people's living standard, the outburst of the extensive transmissible disease caused by bacteriological infection especially, more exacerbates people to the demand with antibacterial type perfumed soap.Sterilant conventional in perfumed soap has sulphur, chloride sterilant is as triclosan etc., research is had to compare the bacteria resistance function of current common commercially available perfumed soap, find to indicate that the perfumed soap (sulphur, triclocarban, parachlormetaxylenol etc.) with degerming composition all has fungistatic effect in various degree in commercially available prod, be significantly higher than conventional toilet soaps (not containing degerming composition).These chemotype sterilant also have its disadvantageous one side, such as parachlormetaxylenol, the irritant and corrodibility to oral cavity, throat and stomach.In order to overcome these problems, people attempt the use carrying out alternative chemosynthesis product with natural plant extracts, as functional additive in perfumed soap and natural spices.
Plants essential oil (Essentialoil, EO) is if root, stem, leaf, flower, fruit, seed, limb or secretory product are the general name with fragrance and (or fragrance) volatility oily liquid substance that raw material extracts from plant different tissues.Usually, plants essential oil is used to prepare essence and flavoring agent, but the research of nearly decades finds, essential oil and single component have very strong suppression or kill the characteristic of the microorganism such as bacterium and fungi.Under the situation that the current disease caused by bacterium, fungi infestation is aggravated increasingly, plants essential oil is as a kind of natural phant sterilant of efficient, security, and application prospect is very wide.
The use of compound essential oil is with a long history, usually it is believed that essential oil can bring the lifting of allomeric function time used in combination.Found by current literature search, in treatment bacteriological infection, the combination of essential oil more than 600 kinds, and combine the effect brought also be divided into collaborative, be added, irrelevant and antagonism four kinds of situations.
A kind of essential oil soap of bactericidal function of CN201210516639.6 disclosure of the invention, it is by sweet almond oil and wheatgerm oil, put into a container and stir, then add tea tree ethereal oil, Herba Pogostemonis essential oil, Australian broad leared tea tree essential oil, Vetiveria zizanoides essential oil, myrrh essential oil and cdear essential oil, and stir; Again by cold soap soap base, cool after being heated to melt completely, when soap base temperature is cooled to about 50 DEG C, adds deployed essential oil solution, and stir, finally pour in the mould of soapmaking, take out after being cooled to room temperature.
A kind of soap containing plants essential oil of CN200710177304.5 disclosure of the invention, it is made according to adding soap matrix after the mixing of certain ratio primarily of Geranium Essential, chamomile essential oil, Japanese Honeysuckle essential oil, oil of Cymbopogon winterianus, Thymus vulgaris essence etc.The soap of this invention can be clearing heat and detoxicating, sterilizing and itch-relieving, Clean Living profit body.
CN201310577658.4 discloses a kind of beauty treatment antibacterial toilet soap, and the feed composition of this perfumed soap comprises: Oleum Cocois 10-13%, plam oil 20-23%, sweet oil 21-38.3%, sodium hydroxide 8.5-9%, water 20-23%, bighead atractylodes rhizome decocting liquid 1-3%, the ultrasonic alcohol extract 1-3% of the root of Dahurain angelica, Radix Asparagi decocting liquid 1-3%, tea tree ethereal oil 0.2-2%.
CN201210459852.8 discloses a kind of antibacterial cold-resistant perfumed soap, its major ingredient is fresh Conditions of Onion Juice, Rhizoma Zingiberis Recens, add the concentrated solution of the Chinese medicines such as tarragon, Japanese Honeysuckle, Leaf of Indigowoad, taraxacum, Turkey-galls, sodium hydroxide, jojoba oil and water are according to the mixing of certain ratio, and through stirring, solidifying, the demoulding forms.
Summary of the invention
In order to solve the problem, the invention provides a kind of natural plant essential oils soap with bacteria resistance function and preparation method thereof.
A kind of natural phant floral type essential oil soap with bacteria resistance function, it comprises composite essential oil and soap base, described composite essential oil is part meter by volume, comprise following component: rosemary ethereal oil 1-4 part, Flower of Aztec Marigold essential oil 2-5 part, Herba Lysimachiae foenumgraeci quintessence oil 2-5 part, rusha grass essential oil 1-5 part, Vetiveria zizanoides essential oil 1-3 part, natural soap base 78-93 part.
In one embodiment of the invention, described composite essential oil is part meter by volume, comprise following component: rosemary ethereal oil 2-4 part, Flower of Aztec Marigold essential oil 2-4 part, Herba Lysimachiae foenumgraeci quintessence oil 2-4 part, rusha grass essential oil 1-3 part, Vetiveria zizanoides essential oil 1-3 part, natural soap base 82-92 part.
In a preferred embodiment of the present invention, described composite essential oil is part meter by volume, comprises following component: rosemary ethereal oil 4 parts, Flower of Aztec Marigold essential oil 3 parts, Herba Lysimachiae foenumgraeci quintessence oil 2 parts, rusha grass essential oil 1 part, Vetiveria zizanoides essential oil 2 parts, natural soap base 88 parts.
The present invention also provides the preparation method of described essential oil soap, and it comprises the steps:
1) rosemary ethereal oil, Flower of Aztec Marigold essential oil, Herba Lysimachiae foenumgraeci quintessence oil, rusha grass essential oil, Vetiveria zizanoides essential oil are mixed by proportioning, ultrasonic oscillation 5-15S, obtains composite essential oil;
2) by soap base in 50-60 DEG C of heating in water bath, after soap base dissolves, by volume soap base and composite essential oil are mixed, pour in mould, after cooling and get final product.
The rosemary ethereal oil used in the present invention is the extraction of Labiatae Rosmarinus officinalis complete stool.Essential oil has biological activity and the value medical health care such as antibacterial, anti-oxidant, anti-inflammatory analgesic significantly, restraining effect is had, the clean and converging action to skin tool, energy consolidation skin to various bacteria such as intestinal bacteria, streptococcus aureus, vibrio cholerae, recover elasticity of skin, Ginseng Extract.The rosemary ethereal oil for India's plantation extraction selected in the present invention.
The Flower of Aztec Marigold essential oil used in the present invention is the extraction of composite family Flower of Aztec Marigold flower.Flower of Aztec Marigold essential oil can process the infection of bacterium or virus initiation, effectively can promote wound healing, and anti-inflammatory effects is obvious, also can remove the symptom of fungal infection.Tool softens skin effect, can be used for skin care, especially the nursing of brothers.
The Herba Lysimachiae foenumgraeci quintessence oil used in the present invention extracted for Labiatae lavandula angustifolia ' capital smokes No. 3 ' Hua Sui, and this kind lavandula angustifolia is self-fertile kind, by the forest variety certification council of State Administration of Forestry breeding authorization in 2014.Herba Lysimachiae foenumgraeci quintessence oil is the most ancient in aromatotherapy, purposes essential oil the most widely, and character is gentle, is applicable to any skin quality, is also that minority can directly and one of the essential oil of skin contact.Can equilibrium state be rebuild, make the body & mind of people all be in harmonious equilibrium state, loosened completely.To streptococcus aureus and Resistant strain thereof, pneumobacillus, Candida albicans, there is certain restraining effect.
The rusha grass essential oil used in the present invention is the extraction of Gramineae rusha grass herb, tool rose fragrance.Rusha grass essential oil is excellent antibacterium, Fungicide, and for skin and mucous membrane gentle, non-stimulated, there is anti-inflammatory effect, become the good medicine of curing acne, zoster, dermatitis, eczema and other skin inflammationes.
The Vetiveria zizanoides essential oil used in the present invention is the extraction of Gramineae Vetiveria zizanoides root, and fragrance is lasting, and smell is strong.Be strong effective tranquillizer, there is the function making skin dispel the heat and be humidified, for most of skin inflammation, as acne, dermatitis, acne, psoriasis and urticaria have therapeutic action.
In the present invention, the extraction process of various essential oil is this area routine techniques means.
Essential oil soap of the present invention has medicinal herbs and the warm fragrance of a flower concurrently, give off a strong fragrance, nature, lasting be lasting, product foaming abundancy, feel are fine and smooth, washing effect is good and soap body resists dry and cracked, good stability, there is effect of restraining and sterilizing bacteria, effectively can suppress the formation of skin surface bacterium, treatment skin inflammation, simultaneously gentle, non-stimulated to skin, life-time service can improve skin condition, moisturizing, enhancing elasticity of skin, the mental status of user can be improved simultaneously, inspire enthusiasm, dynamic, there is incentive action.
Embodiment
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
Embodiment 1
Get rosemary ethereal oil 4 parts, Flower of Aztec Marigold essential oil 3 parts, Herba Lysimachiae foenumgraeci quintessence oil 2 parts, rusha grass essential oil 1 part, Vetiveria zizanoides essential oil 2 parts mix in glass or stainless steel vessel, ultrasonic oscillation 10S, obtains mixed essential oil.
By soap base in 55 DEG C of heating in water bath, after soap base dissolves, get the mixed essential oil of 88ml soap base, 12ml, pour into after mixing in container in mould, the refrigerator after cooling the essential oil soap made being put into 4 DEG C saves backup.
Antibacterial Activity:
1.1 disk diffusion method
By bacterial classification to be measured, (intestinal bacteria EscherichiacoliATCC25922, staphylococcus aureus Staphylococcusaureussubsp.AureusATCC25923, Pseudomonas aeruginosa (Pseudomonasaeruginosa) ATCC27583 beef extract-peptone liquid nutrient medium cultivate, and with than turbid instrument, each bacterium liquid are diluted to 1 × 10 before using respectively
8cFUmL
-1.
The beef extract-peptone nutrient agar of sterilizing is poured in the culture dish of diameter 9cm, after culture medium solidifying, draws each bacterium liquid 100 μ l be spread evenly across on flat board with liquid-transfering gun, then gets the diameter 6mm filter paper after dry sterilization with tweezers smooth in dull and stereotyped central authorities.
In embodiment 1, often kind of folk prescription essential oil, mixed essential oil all cross 0.45 μm of millipore filtration, and liquid-transfering gun is drawn 10 μ l and dripped on filter paper, and each processes three repetitions.Distilled water is set and makes blank, penicillin, Streptomycin sulphate and ceftazime (1mgmL are respectively to positive control (microbiotic) selected by three kinds of bacteriums
-1).After essential oil is fully absorbed, is inverted cultivation 24 hours for 37 DEG C, measures antibacterial circle diameter, get three average value measured.
The bacteriostatic action (inhibition zone radius r=mm) of table 1 compound essential oil
Note: inhibition zone size unit is mm, tolerance range is 0.02mm
As can be seen from the above table, essential oil, when being used alone, has certain inhibition to intestinal bacteria, streptococcus aureus and Pseudomonas aeruginosa, and the inhibition of different essential oil exists significant difference.For intestinal bacteria (bacterium A), rusha grass essential oil inhibition is the most remarkable, and Flower of Aztec Marigold essential oil inhibition is poor, and the fungistatic effect of ' capital smokes No. 3 ' Herba Lysimachiae foenumgraeci quintessence oil is significantly better than lavandula angustifolia commercial variety; For streptococcus aureus (bacterium B), the fungistatic effect of ' capital smokes No. 3 ' lavandula angustifolia, rusha grass and rosemary ethereal oil is better, and the inhibition of Vetiveria zizanoides essential oil is poor; The better resistance of Pseudomonas aeruginosa (bacterium C), most essential oil is not ideal to its inhibition, but rosemary ethereal oil demonstrates and has stronger inhibition to it.
The essential oil of embodiment 1 all has good fungistatic effect to intestinal bacteria, staphylococcus aureus and Pseudomonas aeruginosa, and its antibacterial circle diameter is significantly greater than essential oil and is used alone and microbiotic control group, and synergy is remarkable.
1.2 staff tests
Experimenter is respectively with the essential oil soap of clear water, embodiment 1 and each finger of certain commercially available brand bacteriostatic soap cleaning right-hand man, with the non-woven fabrics wiping through autoclave sterilization after flowing water cleaning, spin cloth to the random swabing sampling of the finger of right-hand man within 1h, 2h, 3h, 4h time period with anhydrous respectively again after drying, afterwards by anhydrous spin cloth put into containing containing the Erlenmeyer flask of MH broth culture after constant incubator cultivates 18h with than turbid instrument record number of bacteria.The fungistatic effect of the essential oil soap of preparation is compared by the concentration of bacterium.
Study subject bacterial concentration (× 10 in table 24h
8cFUmL
-1) change
As can be seen from the above table, no matter be with the essential oil soap in embodiment 1 or certain commercially available brand bacteriostatic soap, along with time lengthening, experimenter's number of bacteria on hand all can showed increased, but its degree increased is different: for three experimenters, in test duration, essential oil soap continues fungistatic effect significantly, and number of bacteria is on hand significantly lower than certain brand perfumed soap experimental group commercially available.
Embodiment 2
Get rosemary ethereal oil 3ml, Flower of Aztec Marigold essential oil 2ml, Herba Lysimachiae foenumgraeci quintessence oil 3ml, rusha grass essential oil 2ml, Vetiveria zizanoides essential oil 1ml mix in glass or stainless steel vessel, ultrasonic oscillation 10S, obtains mixed essential oil.
By soap base in 60 DEG C of heating in water bath, after soap base dissolves, get the mixed essential oil of 89 parts of soap bases, 11ml, pour into after mixing in container in mould, the refrigerator after cooling the essential oil soap made being put into 4 DEG C saves backup.
Antibacterial Activity:
1.1 disk diffusion method
By bacterial classification to be measured, (intestinal bacteria EscherichiacoliATCC25922, staphylococcus aureus Staphylococcusaureussubsp.AureusATCC25923, Pseudomonas aeruginosa (Pseudomonasaeruginosa) ATCC27583 beef extract-peptone liquid nutrient medium cultivate, and with than turbid instrument, each bacterium liquid are diluted to 1x10 before using respectively
8cFUmL-1.
The beef extract-peptone nutrient agar of sterilizing is poured in the culture dish of diameter 9cm, after culture medium solidifying, draws each bacterium liquid 100 μ l be spread evenly across on flat board with liquid-transfering gun, then gets the diameter 6mm filter paper after dry sterilization with tweezers smooth in dull and stereotyped central authorities.
In embodiment 2, often kind of folk prescription essential oil, mixed essential oil all cross 0.45 μm of millipore filtration, and liquid-transfering gun is drawn 10 μ l and dripped on filter paper, and each processes three repetitions.Distilled water is set and makes blank, penicillin, Streptomycin sulphate and ceftazime (1mgmL are respectively to positive control (microbiotic) selected by three kinds of bacteriums
-1).After essential oil is fully absorbed, is inverted cultivation 24 hours for 37 DEG C, measures antibacterial circle diameter, get three average value measured.
The bacteriostatic action (inhibition zone radius r=mm) of table 3 compound essential oil
Note: inhibition zone size unit is mm, tolerance range is 0.02mm
The essential oil of embodiment 2 has good fungistatic effect to intestinal bacteria, and its antibacterial circle diameter is significantly greater than single essential oil and microbiotic control group; Microbiotic group is better than to the inhibition of streptococcus aureus, but is slightly weaker than the inhibition of ' capital smokes No. 3 ' lavandula angustifolia, illustrate that certain antagonistic action has appearred in this kind of essential oil proportioning; Single essential oil is better than to the inhibition of Pseudomonas aeruginosa, but is weaker than antibiotic inhibition.
1.2 staff tests
Experimenter is respectively with the essential oil soap of clear water, embodiment 2 and each finger of certain commercially available brand bacteriostatic soap cleaning right-hand man, with the non-woven fabrics wiping through autoclave sterilization after flowing water cleaning, spin cloth to the random swabing sampling of the finger of right-hand man within 1h, 2h, 3h, 4h time period with anhydrous respectively again after drying, afterwards by anhydrous spin cloth put into containing containing the Erlenmeyer flask of MH broth culture after constant incubator cultivates 18h with than turbid instrument record number of bacteria.The fungistatic effect of the essential oil soap of preparation is compared by the concentration of bacterium.
Study subject bacterial concentration (× 10 in table 44h
8cFUmL
-1) change
As can be seen from the above table, no matter be with the essential oil soap in embodiment 2 or certain commercially available brand bacteriostatic soap, along with time lengthening, experimenter's number of bacteria on hand all can showed increased, but its degree increased is different: stage on-test, three experimenters use essential oil soap number of bacteria on hand a little more than certain brand perfumed soap experimental group commercially available, but along with time lengthening (in 2-4 hour), experimenter 1 uses essential oil soap number of bacteria on hand significantly lower than certain brand perfumed soap experimental group commercially available, continues bacteriostasis remarkable; Experimenter 2,3 uses essential oil soap number of bacteria on hand close to certain brand perfumed soap experimental group commercially available, and the two all has lasting bacteriostasis.
Embodiment 3
Get rosemary ethereal oil 2ml, Flower of Aztec Marigold essential oil 3ml, Herba Lysimachiae foenumgraeci quintessence oil 2ml, rusha grass essential oil 2ml, Vetiveria zizanoides essential oil 1ml mix in glass or stainless steel vessel, ultrasonic oscillation 10S, obtains mixed essential oil.
By soap base in 60 DEG C of heating in water bath, after soap base dissolves, get 90ml soap base, 10ml mixed essential oil, pour into after mixing in container in mould, the refrigerator after cooling the essential oil soap made being put into 4 DEG C saves backup.
Antibacterial Activity:
1.1 disk diffusion method
By bacterial classification to be measured, (intestinal bacteria EscherichiacoliATCC25922, staphylococcus aureus Staphylococcusaureussubsp.AureusATCC25923, Pseudomonas aeruginosa (Pseudomonasaeruginosa) ATCC27583 beef extract-peptone liquid nutrient medium cultivate, and with than turbid instrument, each bacterium liquid are diluted to 1x10 before using respectively
8cFUmL-1.
The beef extract-peptone nutrient agar of sterilizing is poured in the culture dish of diameter 9cm, after culture medium solidifying, draws each bacterium liquid 100 μ l be spread evenly across on flat board with liquid-transfering gun, then gets the diameter 6mm filter paper after dry sterilization with tweezers smooth in dull and stereotyped central authorities.
In embodiment 3, often kind of folk prescription essential oil, mixed essential oil all cross 0.45 μm of millipore filtration, and liquid-transfering gun is drawn 10 μ l and dripped on filter paper, and each processes three repetitions.Distilled water is set and makes blank, penicillin, Streptomycin sulphate and ceftazime (1mgmL are respectively to positive control (microbiotic) selected by three kinds of bacteriums
-1).After essential oil is fully absorbed, is inverted cultivation 24 hours for 37 DEG C, measures antibacterial circle diameter, get three average value measured.
The bacteriostatic action (inhibition zone radius r=mm) of table 5 compound essential oil
Note: inhibition zone size unit is mm, tolerance range is 0.02mm
The essential oil of embodiment 3 has good fungistatic effect to intestinal bacteria and streptococcus aureus, and its antibacterial circle diameter is significantly greater than single essential oil and microbiotic control group; Single essential oil is better than to the inhibition of Pseudomonas aeruginosa, but is weaker than antibiotic inhibition.
1.2 staff tests
Experimenter is respectively with the essential oil soap of clear water, embodiment 3 and each finger of certain commercially available brand bacteriostatic soap cleaning right-hand man, with the non-woven fabrics wiping through autoclave sterilization after flowing water cleaning, spin cloth to the random swabing sampling of the finger of right-hand man within 1h, 2h, 3h, 4h time period with anhydrous respectively again after drying, afterwards by anhydrous spin cloth put into containing containing the Erlenmeyer flask of MH broth culture after constant incubator cultivates 18h with than turbid instrument record number of bacteria.The fungistatic effect of the essential oil soap of preparation is compared by the concentration of bacterium.
Study subject bacterial concentration (× 10 in table 64h
8cFUmL
-1) change
As can be seen from the above table, no matter be with the essential oil soap in embodiment 3 or certain commercially available brand bacteriostatic soap, along with time lengthening, experimenter's number of bacteria on hand all can showed increased, but its degree increased is different: stage on-test (in 1-2 hour), three experimenters use essential oil soap number of bacteria on hand higher than certain brand perfumed soap experimental group commercially available, illustrate essential oil soap in embodiment 3 in short-term bacteriostasis be weaker than commercially available prod; But along with time lengthening (in 2-4 hour), experimenter 1 uses essential oil soap number of bacteria on hand significantly lower than certain brand perfumed soap experimental group commercially available, continue bacteriostasis remarkable; Experimenter 2 used essential oil soap number of bacteria on hand close to certain brand perfumed soap experimental group commercially available in 4 hours, and the two all has lasting bacteriostasis; Experimenter 3 uses essential oil soap number of bacteria on hand to increases slowly, and illustrates that now fungistatic effect is better than certain brand perfumed soap experimental group commercially available.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (5)
1. one kind has the natural phant floral type essential oil soap of bacteria resistance function, it comprises composite essential oil and soap base, described composite essential oil is part meter by volume, comprise following component: rosemary ethereal oil 1-4 part, Flower of Aztec Marigold essential oil 2-5 part, Herba Lysimachiae foenumgraeci quintessence oil 2-5 part, rusha grass essential oil 1-5 part, Vetiveria zizanoides essential oil 1-3 part, natural soap base 78-93 part.
2. essential oil soap as claimed in claim 1, it is characterized in that, described composite essential oil is part meter by volume, comprises following component: rosemary ethereal oil 2-4 part, Flower of Aztec Marigold essential oil 2-4 part, Herba Lysimachiae foenumgraeci quintessence oil 2-4 part, rusha grass essential oil 1-3 part, Vetiveria zizanoides essential oil 1-3 part, natural soap base 82-92 part.
3. essential oil soap as claimed in claim 2, it is characterized in that, described composite essential oil is part meter by volume, comprises following component: rosemary ethereal oil 4 parts, Flower of Aztec Marigold essential oil 3 parts, Herba Lysimachiae foenumgraeci quintessence oil 2 parts, rusha grass essential oil 1 part, Vetiveria zizanoides essential oil 2 parts, natural soap base 88 parts.
4. the essential oil soap as described in any one of claim 1-3, is characterized in that, described Herba Lysimachiae foenumgraeci quintessence oil is that Labiatae lavandula angustifolia ' capital smokes No. 3 ' Hua Sui extracts.
5. the preparation method of the essential oil soap described in any one of claim 1-4, it comprises the steps:
1) rosemary ethereal oil, Flower of Aztec Marigold essential oil, Herba Lysimachiae foenumgraeci quintessence oil, rusha grass essential oil, Vetiveria zizanoides essential oil are mixed by proportioning, ultrasonic oscillation 5-15S, obtains composite essential oil;
2) by soap base in 50-60 DEG C of heating in water bath, after soap base dissolves, by volume soap base and composite essential oil are mixed, pour in mould, after cooling and get final product.
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| CN108379127A (en) * | 2018-04-26 | 2018-08-10 | 江西中医药大学 | Acne removal essential oil composition and its preparation method and application |
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| CN106318719A (en) * | 2016-08-23 | 2017-01-11 | 陕西师范大学 | Bacteriostatic salvia miltiorrhiza essential oil soap and producing method |
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| CN107557196A (en) * | 2017-08-25 | 2018-01-09 | 张悦健 | Liquid soap and preparation method thereof |
| CN108697629A (en) * | 2017-09-05 | 2018-10-23 | 拉芳家化股份有限公司 | A kind of plants essential oil preservative naturally substituted and the application in cosmetics |
| CN108379127B (en) * | 2018-04-26 | 2021-04-23 | 江西中医药大学 | Acne-removing essential oil composition and preparation method and application thereof |
| CN108379127A (en) * | 2018-04-26 | 2018-08-10 | 江西中医药大学 | Acne removal essential oil composition and its preparation method and application |
| CN110951553A (en) * | 2019-11-06 | 2020-04-03 | 海南大学 | Water lily compound essential oil handmade soap with anti-aging effect and preparation method thereof |
| CN111700825A (en) * | 2020-06-29 | 2020-09-25 | 上海中医药大学 | Oily composition for oral health care, preparation method and application thereof |
| CN111700825B (en) * | 2020-06-29 | 2022-07-01 | 上海中医药大学 | Oily composition for oral health care, preparation method and application thereof |
| CN111956687A (en) * | 2020-07-09 | 2020-11-20 | 上海军慧医疗管理有限公司 | Bacteriostatic foot care solution containing plant essential oil and preparation method of foot care solution |
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