CN103710177A - Patchouli essential oil handmade soap for removing comedos and acnes and fabrication method thereof - Google Patents
Patchouli essential oil handmade soap for removing comedos and acnes and fabrication method thereof Download PDFInfo
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- CN103710177A CN103710177A CN201410014761.2A CN201410014761A CN103710177A CN 103710177 A CN103710177 A CN 103710177A CN 201410014761 A CN201410014761 A CN 201410014761A CN 103710177 A CN103710177 A CN 103710177A
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- essential oil
- herba pogostemonis
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- pogostemonis essential
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Abstract
The invention relates to a piece of patchouli essential oil handmade soap for removing comedos and acnes and a fabrication method thereof. The patchouli essential oil handmade soap is prepared from the following raw materials: patchouli essential oil, olive oil, sodium palmate, flaked soap, glycerinum, coconut oil, shea butter, castor oil and deionized water according to certain weight ratio. The fabrication method comprises the following steps: (1) mixing the olive oil, the sodium palmate, the flaked soap, the glycerinum, the coconut oil, the shea butter, the castor oil and the deionized water according to the ratio; heating until the mixture is completely dissolved, stirring and cooling the mixture to 50-55 DEG C; (2) adding patchouli essential oil to the mixed oil and evenly stirring; (3) pouring into a die for solidifying; (4) demolding and packaging to obtain the product. The patchouli essential oil handmade soap can be used for cleaning the skin of the overall body, and has the effects of removing comedos and acnes, sterilizing, diminishing inflammation, cooling down, moisturizing, supplying water, nourishing the skin, and whitening spots. The flavor of pogostemon cablin can be used for soothing feeling, relieving pressure and removing anxiety. The patchouli essential oil handmade soap adopts pure natural plant juice, is free of stimulation to skin, and is an environmental bath product which can be used for a long period of time.
Description
Technical field
The invention belongs to daily washing product technical field, be specifically related to a kind ofly go acne, remove acne Herba Pogostemonis essential oil handmade soap and preparation method thereof.
Background technology
The skin clean perfumed soap of selling in the market, synthetic the making of many employing chemical substances, the reasons such as Chang Yin " alkalinity grease grade too high, that include is not high, glycerine is pulled out, added sanitising agent or composite reactive agent ", after use, easily cause skin dry and astringent, coarse, cleaning effect is also undesirable, also may work the mischief to skin and environment.Still more, in recent years along with part big and medium-sized cities air-polluting is serious, acne, small pox etc. are frequent to be occurred.People, particularly women not only rests on clean aspect to the requirement of washing product, more wish that it has acne, goes acne, nourishes the functions such as skin, desalination spot, sterilization, anti-inflammatory, antipyretic, moisturizing, moisturizing, to promote quality of life, therefore, the washing product of natural, health and environmental protection is anxious waits to develop.
Wrinkled Gianthyssop Herb [
pogostemon cablin(Blanco) Benth.] be that Labiatae thorn stamen grass belongs to herbaceous plant, slightly warm in nature, taste are pungent, have eliminating dampness with aromatics, the preventing or arresting vomiting that whets the appetite, deliver the effect of relieving summer-heat.Wrinkled Gianthyssop Herb is not only the main raw material of more than 30 kind of Chinese patent medicine, and with the Herba Pogostemonis essential oil of its extraction, or medicine and the important source material of light industry industry (as preparation pellet, cream, ball, fall apart and makeup, fixative and agrochemical), among the people also with Wrinkled Gianthyssop Herb leaf decoct drink avoid heat wet.The main component having detected in Herba Pogostemonis essential oil has 191 kinds of Patchoulicalcohol, pogostone, α-different guaiene, α-pinene, limonene, phenyl aldehyde, cloves alkene, Eugenol, allylguaiacol, cinnamic aldehyde, patchouli pyridine, sesquiterpenes etc., thereby Herba Pogostemonis essential oil has antibacterial, desinsection, analgesia, antipyretic, anti-inflammatory, antitumor, resisting pathogenic microbes and immunomodulatory isoreactivity.In prior art, there is the application report using patchouli oil as germicide for skin, the Chinese patent that is CN1174724A referring to publication number.
China's Wrinkled Gianthyssop Herb is used as medicine with top dryly, and root system rots conventionally in soil, in order to make full use of this precious resources, turns waste into wealth, and the present invention extracts the essential oil in Wrinkled Gianthyssop Herb root system, as the component of handmade soap.Through GC-MS test,
The essential oil that Wrinkled Gianthyssop Herb root system and overground part extract, chemical composition and content thereof are very nearly the same, the suitable component as handmade soap.
State Intellectual Property Office also discloses one " a kind of pure plants essential oil hair washing soap " by name, number of patent application is 201210526180.8 patent of invention, it is the hair washing soap that Herba Lysimachiae foenumgraeci quintessence oil, orange essential oil, Herba Pogostemonis essential oil, loose essential oil, lemongrass essential oil, lemon quintessence oil, elemi essential oil, citral, Geraniol, Linaool, gardenia jasminoides extraction liquid, flores anthemidis extraction liquid are made, the disclosure patent is only write it in the description of specification sheets antipruritic effect, but just not concrete effect describes, and does not also introduce the effect of Herba Pogostemonis essential oil.In addition, there is certain deficiency in this publication, and the production cycle is long, and only the curing time needs 25-28 days.
State Intellectual Property Office also discloses one " a kind of soap that contains plants essential oil " by name, number of patent application is 200710177304.5 patent of invention, it is that Flos Pelargonii essential oil, Flos Matricariae chamomillae essential oil, Japanese Honeysuckle essential oil, oil of Cymbopogon winterianus and thyme oil are added to the essential oil soap of making in soap matrix, the disclosure patent is only write the effect that it has sterilizing and itch-relieving in the description of specification sheets, but just not concrete effect describes.
State Intellectual Property Office also discloses one " a kind of essential oil soap with bactericidal function " by name, number of patent application is 201210516639.6 patent of invention, it is the essential oil soap that sweet almond oil, wheatgerm oil, tea tree ethereal oil, Herba Pogostemonis essential oil, Australian broad leared tea tree essential oil, Vetiveria zizanoides essential oil, myrrh essential oil and cdear essential oil are made, the disclosure patent is only write the effect that it has bactericidal in the description of specification sheets, but the clear and definite effect degree of Herba Pogostemonis essential oil in this essential oil soap not.
In order to overcome the deficiency of above technology, develop and a kind ofly take Herba Pogostemonis essential oil as main effect component, human body, without any stimulation, is gone acne, goes acne, nourishes skin, the essential oil soap product of desalination spot successful is extremely necessary.
Summary of the invention
The present invention is directed to the deficiency of perfumed soap in prior art, a kind of pure home built Herba Pogostemonis essential oil soap and preparation method thereof is provided, this method is introduced the glycerine of " natural moisture preserving moisturizing agent " in Herba Pogostemonis essential oil handmade soap, during use, will nourish skin, desalination spot; Adopt pure natural raw material to extract the Herba Pogostemonis essential oil making, fragrance is pleasant, has antibacterial, desinsection, anti-inflammatory isoreactivity, has acne, goes acne, the effect of sterilization, anti-inflammatory.
To achieve these goals, the present invention adopts following technical scheme: a kind of Herba Pogostemonis essential oil handmade soap, the mass fraction of each component is: Herba Pogostemonis essential oil 1.8-4.2 part, sweet oil 1.5-2.0 part, Zoomeric acid sodium 8.5-17 part, soap flakes 5-9 part, glycerine 17.5-26 part, Oleum Cocois 16.5-25 part, shea butter 12-17 part, Viscotrol C 3.5-7 part, surplus deionized water are formulated.
The preparation method of Herba Pogostemonis essential oil is as follows: the over-ground part of Wrinkled Gianthyssop Herb plant takes root system after tapping, and cleans, and dries to constant weight at 50-55 ℃, is ground into powder, and Herba Pogostemonis essential oil adopts wet distillation to extract or supercritical CO
2extract two kinds of methods: 1) wet distillation extraction method is: the water that adds 7-8 times of quality of Wrinkled Gianthyssop Herb powder, soak 4-5 hour, pouring volatile oil into extracts in glass device, ebuillition of heated, extract 4-5 hour, collect Herba Pogostemonis essential oil-water mixture, with Sodium Thio Sulphate(Anhydrous), remove moisture, obtain Herba Pogostemonis essential oil; 2) supercritical CO
2extraction process: Wrinkled Gianthyssop Herb powder is crossed after 40-60 mesh sieve, is placed in supercritical CO
2in extraction plant, extracting pressure 18-20 megapascal (MPa), extraction time 2.0-2.5 hour, extraction temperature is 40-42 ℃, that is obtains Herba Pogostemonis essential oil.
A preparation method for Herba Pogostemonis essential oil handmade soap, its step is as follows:
The first step, is mixed in proportion sweet oil, Zoomeric acid sodium, soap flakes, glycerine, Oleum Cocois, shea butter, Viscotrol C, deionized water, and heating in water bath, to dissolving completely, stirs, and is cooled to 50-55 ℃ of insulation;
Second step adds Herba Pogostemonis essential oil in above-mentioned mixing oil, stirs;
The 3rd step, pours curing 12-24 hour in mould into;
The 4th step, the demoulding after soap lye solidifies, is placed in the 3-5 days of the dry place of shady and cool ventilation, after finishing packing, gets product.
A kind of improvement as Herba Pogostemonis essential oil handmade soap making method of the present invention, adds Herba Pogostemonis essential oil in second step, after stirring, need to spray a small amount of alcohol froth breaking.
The invention has the advantages that: 1) to take the root system conventionally rotting in soil be starting material in the present invention, extracts Wrinkled Gianthyssop Herb root system essential oil, makes Herba Pogostemonis essential oil handmade soap, reaches the object turning waste into wealth; 2) Herba Pogostemonis essential oil handmade soap, according to difform mould, its moulding is also rich and varied; 3) adopt making method of the present invention, in handmade soap preparation process, do not need 80 ℃ of above high temperature, retained to greatest extent effect and the nutritive ingredient of each component, make it have good nourishing skin, desalination spot, goes acne, goes acne, the effect such as sterilization, moisturizing; 4) compared with prior art, the manufacture craft of Herba Pogostemonis essential oil handmade soap of the present invention is simple and safe, there is no chemical additive, can be used for whole skin clean, because glycerine is intactly retained in perfumed soap, there is synergy with Herba Pogostemonis essential oil, not only there is nourishing skin whitening, desalination spot, the effects such as bright color, also can be used for acne, go acne, the effect of sterilization, anti-inflammatory, antipyretic, moisturizing, and the fragrance of Wrinkled Gianthyssop Herb can mood placating, release the pressure and eliminate uneasiness.Main ingredient of the present invention adopts natural plant Normal juice, to skin, without any stimulation, is that a kind of environmental protection that can life-time service is washed and protected product.
Embodiment
Embodiment 1
Prepare in accordance with the following steps Herba Pogostemonis essential oil handmade soap: 1) according to the formula of the embodiment 1 shown in table 1, take each component; 2) sweet oil, Zoomeric acid sodium, soap flakes, glycerine, Oleum Cocois, shea butter, Viscotrol C, deionized water are mixed in proportion, heating in water bath, to dissolving completely, stirs, and is cooled to 50-55 ℃ of insulation; 3) in above-mentioned mixing oil, add Herba Pogostemonis essential oil, stir; 4) pour curing 12-24 hour in mould into; 5) demoulding after soap lye solidifies, is placed in the 3-5 days of the dry place of shady and cool ventilation, after finishing packing, gets product.
Embodiment 2
Formula according to the embodiment 2 shown in table 1 takes each component, and all the other steps are identical with embodiment 1.
Embodiment 3
Formula according to the embodiment 3 shown in table 1 takes each component, and all the other steps are identical with embodiment 1.
Comparative example 1
Formula according to embodiment shown in table 11 takes each component, but there is no glycerin component, and all the other steps are identical with embodiment 1.
Table 1: formula table (in mass fraction)
Whether irritant to skin in order to verify embodiment of the present invention 1-3 sample, first, 6 the regular grade New Zealand white rabbit of take are study subject, use continuously after 7 days, all without red and swollen, oedema phenomenon, occur, and this shows: sample nonirritant material of the present invention.Then, in the nonirritant of the enterprising step card of human body skin sample of the present invention, test once every day, continuously tested 7 days, test process and the results are shown in Table 2.
Table 2: test process and the result of sample of the present invention on human body skin
The effect detection of " going acne, go acne ": carry out effect detection with reference to < < traditional Chinese medical science disease Standardization of diagnosis and curative effect > >.Recovery from illness: conscious acne, small pox transference cure; Effective: conscious acne, small pox obviously alleviate; Effective: conscious acne, small pox alleviate to some extent; Invalid: conscious acne, small pox alleviate not obvious.The Herba Pogostemonis essential oil handmade soap preparing by embodiment 1-2 in the present invention and comparative example 1, through 320 continuous trying out after 60 days of human consumer that have on the face 17-25 one full year of life of acne, small pox, all feedback is gone acne, is gone acne respond well, detects effect in Table 3.
Table 3: effect detection statistics
According to table 3 effect detection statistic data, we find in Herba Pogostemonis essential oil handmade soap of the present invention, have synergy, for going acne, going acne to have unexpected effect when Herba Pogostemonis essential oil and glycerine exist down simultaneously.
The announcement of book and narration according to the above description; those skilled in the art in the invention also can carry out suitable change and modification to above-mentioned embodiment; therefore; the present invention is not limited to embodiment disclosed and described above; to modifications and changes more of the present invention, also should fall in the protection domain of the claims in the present invention; comprise from Wrinkled Gianthyssop Herb over-ground part and extract Herba Pogostemonis essential oil, the Herba Pogostemonis essential oil handmade soap making, also in the protection domain of the claims in the present invention.
Claims (4)
1. a Herba Pogostemonis essential oil handmade soap, is characterized in that, the mass fraction of each component is:
Herba Pogostemonis essential oil 1.8-4.2 part, sweet oil 1.5-2.0 part, Zoomeric acid sodium 8.5-17 part, soap flakes 5-9 part, glycerine 17.5-26 part, Oleum Cocois 16.5-25 part, shea butter 12-17 part, Viscotrol C 3.5-7 part, surplus deionized water.
2. Herba Pogostemonis essential oil handmade soap according to claim 1, is characterized in that, the preparation method of Herba Pogostemonis essential oil is as follows:
The over-ground part of Wrinkled Gianthyssop Herb plant takes root system after tapping, and cleans, and dries to constant weight at 50-55 ℃, is ground into powder, and Herba Pogostemonis essential oil adopts wet distillation to extract or supercritical CO
2extract two kinds of methods: 1) wet distillation extraction method is: the water that adds 7-8 times of quality of Wrinkled Gianthyssop Herb powder, soak 4-5 hour, pouring volatile oil into extracts in glass device, ebuillition of heated, extract 4-5 hour, collect Herba Pogostemonis essential oil-water mixture, with Sodium Thio Sulphate(Anhydrous), remove moisture, obtain Herba Pogostemonis essential oil; 2) supercritical CO
2extraction process: Wrinkled Gianthyssop Herb powder is crossed after 40-60 mesh sieve, is placed in supercritical CO
2in extraction plant, extracting pressure 18-20 megapascal (MPa), extraction time 2.0-2.5 hour, extraction temperature is 40-42 ℃, that is obtains Herba Pogostemonis essential oil.
3. the making method of Herba Pogostemonis essential oil handmade soap according to claim 1, is characterized in that, comprises the following steps:
The first step, is mixed in proportion sweet oil, Zoomeric acid sodium, soap flakes, glycerine, Oleum Cocois, shea butter, Viscotrol C, deionized water, and heating in water bath, to dissolving completely, stirs, and is cooled to 50-55 ℃ of insulation;
Second step adds Herba Pogostemonis essential oil in above-mentioned mixing oil, stirs;
The 3rd step, pours curing 12-24 hour in mould into;
The 4th step, the demoulding after soap lye solidifies, is placed in the 3-5 days of the dry place of shady and cool ventilation, after finishing packing, gets product.
4. the making method of Herba Pogostemonis essential oil handmade soap according to claim 3, is characterized in that: in second step, add Herba Pogostemonis essential oil, after stirring, spray a small amount of alcohol froth breaking.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410014761.2A CN103710177B (en) | 2014-01-13 | 2014-01-13 | One is gone acne, is removed acne Herba Pogostemonis essential oil handmade soap and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410014761.2A CN103710177B (en) | 2014-01-13 | 2014-01-13 | One is gone acne, is removed acne Herba Pogostemonis essential oil handmade soap and preparation method thereof |
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| Publication Number | Publication Date |
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| CN103710177A true CN103710177A (en) | 2014-04-09 |
| CN103710177B CN103710177B (en) | 2015-07-29 |
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| CN201410014761.2A Expired - Fee Related CN103710177B (en) | 2014-01-13 | 2014-01-13 | One is gone acne, is removed acne Herba Pogostemonis essential oil handmade soap and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106398870A (en) * | 2016-08-28 | 2017-02-15 | 广西灏源盛世生物科技有限公司 | Extraction method of pogostemon cablin essential oil |
| CN106520416A (en) * | 2016-10-28 | 2017-03-22 | 楚雄乌蛮渡农垦有限公司 | Elsholtzia rugulosa hemsl essential oil soap and preparing method thereof |
| CN112111345A (en) * | 2019-06-20 | 2020-12-22 | 杭州船王实业有限公司 | Man refreshing skin-care handmade soap and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103242991A (en) * | 2013-06-03 | 2013-08-14 | 湖北科技学院 | Osmanthus handmade soap and manufacturing method thereof |
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2014
- 2014-01-13 CN CN201410014761.2A patent/CN103710177B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103242991A (en) * | 2013-06-03 | 2013-08-14 | 湖北科技学院 | Osmanthus handmade soap and manufacturing method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 彩色小盐巴: "天然草本手作香皂-来自台湾的TICTACTOE", 《WWW.SZMAA.COM_THREAD-78819-1-1.HTML》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106398870A (en) * | 2016-08-28 | 2017-02-15 | 广西灏源盛世生物科技有限公司 | Extraction method of pogostemon cablin essential oil |
| CN106520416A (en) * | 2016-10-28 | 2017-03-22 | 楚雄乌蛮渡农垦有限公司 | Elsholtzia rugulosa hemsl essential oil soap and preparing method thereof |
| CN112111345A (en) * | 2019-06-20 | 2020-12-22 | 杭州船王实业有限公司 | Man refreshing skin-care handmade soap and preparation method thereof |
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| CN103710177B (en) | 2015-07-29 |
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Granted publication date: 20150729 Termination date: 20220113 |