CN103710177B - One is gone acne, is removed acne Herba Pogostemonis essential oil handmade soap and preparation method thereof - Google Patents
One is gone acne, is removed acne Herba Pogostemonis essential oil handmade soap and preparation method thereof Download PDFInfo
- Publication number
- CN103710177B CN103710177B CN201410014761.2A CN201410014761A CN103710177B CN 103710177 B CN103710177 B CN 103710177B CN 201410014761 A CN201410014761 A CN 201410014761A CN 103710177 B CN103710177 B CN 103710177B
- Authority
- CN
- China
- Prior art keywords
- essential oil
- herba pogostemonis
- acne
- pogostemonis essential
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Detergent Compositions (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to one to go acne, remove acne Herba Pogostemonis essential oil handmade soap and preparation method thereof.It is by: Herba Pogostemonis essential oil, sweet oil, Zoomeric acid sodium, soap flakes, glycerine, Oleum Cocois, shea butter, Viscotrol C, deionized water are prepared from by certain weight ratio.Making method: 1) sweet oil, Zoomeric acid sodium, soap flakes, glycerine, Oleum Cocois, shea butter, Viscotrol C, deionized water are mixed in proportion, is heated to dissolve completely, stirs, is cooled to 50-55 DEG C; 2) in above-mentioned mixing oil, add Herba Pogostemonis essential oil, stir; 3) pour into mold curing; 4) demoulding, packaging gets product.Herba Pogostemonis essential oil handmade soap, can be used for whole skin and cleans, there are acne, go acne, sterilization, anti-inflammatory, antipyretic, moisturizing, moisturizing, nourishing skin, desalination spot effect, and the fragrance of Wrinkled Gianthyssop Herb can mood placating, release the pressure and eliminate uneasiness.The present invention adopts natural plant Normal juice, to skin without any stimulation, is a kind of environmental protection of life-time service can washing and protect product.
Description
Technical field
The invention belongs to daily washing product technical field, be specifically related to one and go acne, remove acne Herba Pogostemonis essential oil handmade soap and preparation method thereof.
Background technology
The skin clean perfumed soap sold in the market, the synthesis of many employings chemical substance is obtained, the reasons such as Chang Yin " alkalinity grease grade that is too high, that include is not high, glycerine is pulled out, with the addition of sanitising agent or composite reactive agent ", after using, easily cause skin dry and astringent, coarse, cleaning effect is also undesirable, also may work the mischief to skin and environment.Still more, in recent years along with part big and medium-sized cities air-polluting is serious, acne, small pox etc. frequently occur.People, particularly women not only rests on clean aspect to the requirement of washing product, more wish that it has acne, goes acne, nourish skin, desalination spot, sterilization, anti-inflammatory, antipyretic, moisturizing, the function such as moisturizing, to promote quality of life, therefore, washing product that is natural, healthy and environmental protection is anxious waits to develop.
Wrinkled Gianthyssop Herb [
pogostemon cablin(Blanco) Benth.] be that Labiatae thorn stamen grass belongs to herbaceous plant, slightly warm in nature, taste are pungent, have eliminating dampness with aromatics, the preventing or arresting vomiting that whets the appetite, deliver effect of relieving summer-heat.The main raw material of more than 30 kind of Chinese patent medicine is not only by Wrinkled Gianthyssop Herb, and with the Herba Pogostemonis essential oil that it extracts, or the important source material of medicine and light industry industry (be used as preparation pellet, cream, ball, fall apart and makeup, fixative and agrochemical), among the peoplely also decocts drink with Wrinkled Gianthyssop Herb leaf and avoids heat wet.The main component detected in Herba Pogostemonis essential oil has Patchoulicalcohol, pogostone, α-different guaiene, α-pinene, limonene, phenyl aldehyde, cloves alkene, Eugenol, allylguaiacol, cinnamic aldehyde, patchouli pyridine, sesquiterpene etc. 191 kinds, and thus Herba Pogostemonis essential oil has antibacterial, desinsection, analgesia, antipyretic, anti-inflammatory, antitumor, resisting pathogenic microbes and immunomodulatory isoreactivity.Having had the application report of patchouli oil as germicide for skin in prior art, is the Chinese patent of CN1174724A see publication number.
China's Wrinkled Gianthyssop Herb is used as medicine with top dryly, and root system rots usually in soil, in order to make full use of this precious resources, turns waste into wealth, and the present invention extracts the essential oil in Wrinkled Gianthyssop Herb root system, as the component of handmade soap.Through GC-MS test,
The essential oil that Wrinkled Gianthyssop Herb root system and overground part extract, chemical composition and content very nearly the same, be suitable for the component being used as handmade soap.
State Intellectual Property Office also discloses one " a kind of pure plant essential oil shampoo soap " by name, number of patent application is the patent of invention of 201210526180.8, it is hair soap Herba Lysimachiae foenumgraeci quintessence oil, orange essential oil, Herba Pogostemonis essential oil, loose essential oil, lemongrass essential oil, lemon quintessence oil, elemi essential oil, citral, Geraniol, Linaool, gardenia jasminoides extraction liquid, flores anthemidis extraction liquid made, the disclosure patent only writes it in the description of specification sheets antipruritic effect, but just concrete effect is not described, and does not also introduce the effect of Herba Pogostemonis essential oil.In addition, there is certain deficiency in this publication, the production cycle is long, and only the curing time needs 25-28 days.
State Intellectual Property Office also discloses one " a kind of soap containing plants essential oil " by name, number of patent application is the patent of invention of 200710177304.5, it is that Geranium Essential, chamomile essential oil, Japanese Honeysuckle essential oil, oil of Cymbopogon winterianus and thyme oil are added the essential oil soap made in soap matrix, the disclosure patent only writes effect that it has sterilizing and itch-relieving in the description of specification sheets, but is not described with regard to concrete effect.
State Intellectual Property Office also discloses one " a kind of essential oil soap with bactericidal function " by name, number of patent application is the patent of invention of 201210516639.6, it is essential oil soap sweet almond oil, wheatgerm oil, tea tree ethereal oil, Herba Pogostemonis essential oil, Australian broad leared tea tree essential oil, Vetiveria zizanoides essential oil, myrrh essential oil and cdear essential oil made, the disclosure patent only writes effect that it has bactericidal in the description of specification sheets, but not clear and definite effect degree of Herba Pogostemonis essential oil in this essential oil soap.
In order to overcome the deficiency of above technology, exploitation is a kind of is main effect component with Herba Pogostemonis essential oil, to human body without any stimulation, goes acne, goes acne, nourishes skin, the essential oil soap product of desalination spot successful is extremely necessary.
Summary of the invention
The present invention is directed to the deficiency of perfumed soap in prior art, provide a kind of pure home built Herba Pogostemonis essential oil soap and preparation method thereof, the glycerine of " natural moisture preserving moisturizing agent " is introduced in Herba Pogostemonis essential oil handmade soap by this method, during use, will nourish skin, desalination spot; Adopt pure natural raw material to extract obtained Herba Pogostemonis essential oil, fragrance is pleasant, there is antibacterial, desinsection, anti-inflammatory isoreactivity, there are acne, go acne, sterilization, anti-inflammatory effect.
To achieve these goals, the present invention adopts following technical scheme: a kind of Herba Pogostemonis essential oil handmade soap, and the mass fraction of each component is: Herba Pogostemonis essential oil 1.8-4.2 part, sweet oil 1.5-2.0 part, Zoomeric acid sodium 8.5-17 part, soap flakes 5-9 part, glycerine 17.5-26 part, Oleum Cocois 16.5-25 part, shea butter 12-17 part, Viscotrol C 3.5-7 part, balance deionized water are formulated.
The preparation method of Herba Pogostemonis essential oil is as follows: the over-ground part of Wrinkled Gianthyssop Herb plant takes root system after tapping, and cleans, dries to constant weight, be ground into powder at 50-55 DEG C, and Herba Pogostemonis essential oil adopts wet distillation to extract or supercritical CO
2extract two kinds of methods: 1) wet distillation extraction method is: the water adding Wrinkled Gianthyssop Herb powder 7-8 times of quality, soak 4-5 hour, pour in volatile oil is drawn glass device, ebuillition of heated, extract 4-5 hour, collect Herba Pogostemonis essential oil-water mixture, remove moisture with Sodium Thio Sulphate(Anhydrous), namely obtain Herba Pogostemonis essential oil; 2) supercritical CO
2extraction process: Wrinkled Gianthyssop Herb powder is placed in supercritical CO after crossing 40-60 mesh sieve
2in extraction plant, extracting pressure 18-20 megapascal (MPa), extraction time 2.0-2.5 hour, extraction temperature is 40-42 DEG C, that is obtains Herba Pogostemonis essential oil.
A preparation method for Herba Pogostemonis essential oil handmade soap, its step is as follows:
The first step, is mixed in proportion sweet oil, Zoomeric acid sodium, soap flakes, glycerine, Oleum Cocois, shea butter, Viscotrol C, deionized water, and heating in water bath, to dissolving completely, stirs, is cooled to 50-55 DEG C of insulation;
Second step, adds Herba Pogostemonis essential oil, stirs in above-mentioned mixing oil;
3rd step, pours mold curing 12-24 hour into;
4th step, the demoulding after soap lye solidifies, is placed in shady and cool ventilation drying place 3-5 days, gets product after finishing packaging.
One as Herba Pogostemonis essential oil handmade soap making method of the present invention is improved, and adds Herba Pogostemonis essential oil, after stirring, need spray a small amount of alcohol froth breaking in second step.
The invention has the advantages that: 1) the present invention is with the root system usually rotted in soil for starting material, extracts Wrinkled Gianthyssop Herb root system essential oil, and obtained Herba Pogostemonis essential oil handmade soap, reaches the object turned waste into wealth; 2) Herba Pogostemonis essential oil handmade soap, according to difform mould, its moulding is also rich and varied; 3) making method of the present invention is adopted, do not need the high temperature of more than 80 DEG C in handmade soap preparation process, remain effect and the nutritive ingredient of each component to greatest extent, make it have and nourish skin preferably, desalination spot, go acne, go acne, sterilization, the effect such as moisturizing; 4) compared with prior art, the manufacture craft of Herba Pogostemonis essential oil handmade soap of the present invention is simple and safe, there is no chemical additive, can be used for whole skin and clean, because glycerine is intactly retained in perfumed soap, with Herba Pogostemonis essential oil, there is synergy, not only there is nourishing skin whitening, desalination spot, the effects such as bright color, also can be used for acne, go acne, sterilization, anti-inflammatory, antipyretic, moisturizing effect, and the fragrance of Wrinkled Gianthyssop Herb can mood placating, release the pressure and eliminate uneasiness.Main ingredient of the present invention adopts natural plant Normal juice, to skin without any stimulation, is a kind of environmental protection of life-time service can washing and protect product.
Embodiment
Embodiment 1
Prepare Herba Pogostemonis essential oil handmade soap in accordance with the following steps: 1) take each component according to the formula of the embodiment 1 shown in table 1; 2) sweet oil, Zoomeric acid sodium, soap flakes, glycerine, Oleum Cocois, shea butter, Viscotrol C, deionized water are mixed in proportion, heating in water bath, to dissolving completely, stirs, is cooled to 50-55 DEG C of insulation; 3) in above-mentioned mixing oil, add Herba Pogostemonis essential oil, stir; 4) mold curing 12-24 hour is poured into; 5) demoulding after soap lye solidifies, is placed in shady and cool ventilation drying place 3-5 days, gets product after finishing packaging.
Embodiment 2
Take each component according to the formula of the embodiment 2 shown in table 1, all the other steps are identical with embodiment 1.
Embodiment 3
Take each component according to the formula of the embodiment 3 shown in table 1, all the other steps are identical with embodiment 1.
Comparative example 1
Take each component according to the formula of embodiment 1 shown in table 1, but do not have glycerin component, all the other steps are identical with embodiment 1.
Table 1: formula table (in mass fraction)
In order to verify that whether embodiment of the present invention 1-3 sample is irritant to skin, first, with 6 regular grade New Zealand white rabbit for study subject, after using 7 days continuously, all occur without red and swollen, oedema phenomenon, this shows: inventive samples nonirritant material.Then, in the nonirritant of the enterprising step card inventive samples of human body skin, test every day once, continuously tested 7 days, test process and the results are shown in Table 2.
Table 2: the test process of inventive samples on human body skin and result
" to go acne, go acne " effect detection: carry out effect detection with reference to " Chinese medical disease Standardization of diagnosis and curative effect ".Recovery from illness: conscious acne, small pox transference cure; Effective: conscious acne, small pox obviously alleviate; Effective: conscious acne, small pox alleviate to some extent; Invalid: conscious acne, small pox alleviate not obvious.With the Herba Pogostemonis essential oil handmade soap that embodiment 1-2 in the present invention and comparative example 1 prepare, after having the human consumer of 17-25 one full year of life of acne, small pox to try out 60 days continuously on the face through 320, all feedback is gone acne, is gone acne respond well, and Detection results is in table 3.
Table 3: effect detection is added up
According to table 3 effect detection statistic data, we find in Herba Pogostemonis essential oil handmade soap of the present invention, have synergy, for going acne, going acne to have unexpected effect under Herba Pogostemonis essential oil and glycerine exist simultaneously.
According to the above description book announcement and describe; those skilled in the art in the invention also can carry out suitable change and amendment to above-mentioned embodiment; therefore; the present invention is not limited to embodiment disclosed and described above; also should fall in the protection domain of the claims in the present invention modifications and changes more of the present invention; comprise and extract Herba Pogostemonis essential oil from Wrinkled Gianthyssop Herb over-ground part, obtained Herba Pogostemonis essential oil handmade soap, also in the protection domain of the claims in the present invention.
Claims (1)
1. a making method for Herba Pogostemonis essential oil handmade soap, is characterized in that, the mass fraction of each component is:
Herba Pogostemonis essential oil 1.8-4.2 part, sweet oil 1.5-2.0 part, Zoomeric acid sodium 8.5-17 part, soap flakes 5-9 part, glycerine 17.5-26 part, Oleum Cocois 16.5-25 part, shea butter 12-17 part, Viscotrol C 3.5-7 part, balance deionized water;
Comprise the following steps:
The first step, is mixed in proportion sweet oil, Zoomeric acid sodium, soap flakes, glycerine, Oleum Cocois, shea butter, Viscotrol C, deionized water, and heating in water bath, to dissolving completely, stirs, is cooled to 50-55 DEG C of insulation;
Second step, adds Herba Pogostemonis essential oil, stirs in above-mentioned mixing oil; Add Herba Pogostemonis essential oil in second step, after stirring, spray a small amount of alcohol froth breaking;
3rd step, pours mold curing 12-24 hour into;
4th step, the demoulding after soap lye solidifies, is placed in shady and cool ventilation drying place 3-5 days, gets product after finishing packaging;
The preparation method of described Herba Pogostemonis essential oil is as follows:
The over-ground part of Wrinkled Gianthyssop Herb plant takes root system after tapping, and cleans, dries to constant weight, be ground into powder at 50-55 DEG C, and Herba Pogostemonis essential oil adopts wet distillation to extract or supercritical CO
2extract two kinds of methods: 1) wet distillation extraction method is: the water adding Wrinkled Gianthyssop Herb powder 7-8 times of quality, soak 4-5 hour, pour in volatile oil is drawn glass device, ebuillition of heated, extract 4-5 hour, collect Herba Pogostemonis essential oil-water mixture, remove moisture with Sodium Thio Sulphate(Anhydrous), namely obtain Herba Pogostemonis essential oil; 2) supercritical CO
2extraction process: Wrinkled Gianthyssop Herb powder is placed in supercritical CO after crossing 40-60 mesh sieve
2in extraction plant, extracting pressure 18-20 megapascal (MPa), extraction time 2.0-2.5 hour, extraction temperature is 40-42 DEG C, that is obtains Herba Pogostemonis essential oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410014761.2A CN103710177B (en) | 2014-01-13 | 2014-01-13 | One is gone acne, is removed acne Herba Pogostemonis essential oil handmade soap and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410014761.2A CN103710177B (en) | 2014-01-13 | 2014-01-13 | One is gone acne, is removed acne Herba Pogostemonis essential oil handmade soap and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103710177A CN103710177A (en) | 2014-04-09 |
| CN103710177B true CN103710177B (en) | 2015-07-29 |
Family
ID=50403540
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410014761.2A Expired - Fee Related CN103710177B (en) | 2014-01-13 | 2014-01-13 | One is gone acne, is removed acne Herba Pogostemonis essential oil handmade soap and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103710177B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106398870A (en) * | 2016-08-28 | 2017-02-15 | 广西灏源盛世生物科技有限公司 | Extraction method of pogostemon cablin essential oil |
| CN106520416A (en) * | 2016-10-28 | 2017-03-22 | 楚雄乌蛮渡农垦有限公司 | Elsholtzia rugulosa hemsl essential oil soap and preparing method thereof |
| CN112111345A (en) * | 2019-06-20 | 2020-12-22 | 杭州船王实业有限公司 | Man refreshing skin-care handmade soap and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103242991A (en) * | 2013-06-03 | 2013-08-14 | 湖北科技学院 | Osmanthus handmade soap and manufacturing method thereof |
-
2014
- 2014-01-13 CN CN201410014761.2A patent/CN103710177B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103242991A (en) * | 2013-06-03 | 2013-08-14 | 湖北科技学院 | Osmanthus handmade soap and manufacturing method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 天然草本手作香皂-来自台湾的TICTACTOE;彩色小盐巴;《www.szmaa.com_thread-78819-1-1.html》;20090411;第1-17页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103710177A (en) | 2014-04-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102688163B (en) | Anti-skin aging skin care compound essential oil | |
| CN103446025B (en) | A kind of Traditional Chinese medicine plant liquid shampoo | |
| CN104382823A (en) | Camellia cleansing oil and preparation method thereof | |
| KR20160112865A (en) | Weak acidic soap powder composition, method for manufacturing weak acidic soap using the composition, and weak acidic soap manufacured by the method | |
| CN104164301A (en) | Functional lavender essence and preparation method thereof | |
| CN105342932B (en) | A kind of all natural multifunctional liquid soap and its production method containing carboxymethyl chitosan | |
| CN104928080A (en) | Method for preparing peppermint-green tea handmade soap | |
| CN103710177B (en) | One is gone acne, is removed acne Herba Pogostemonis essential oil handmade soap and preparation method thereof | |
| CN104367529A (en) | Mosquito repellent floral water for purifying air and preparation method of mosquito repellent floral water | |
| CN111840172A (en) | Skin-beautifying firming cream and preparation method thereof | |
| CN104814897A (en) | Natural shampoo soap | |
| CN102451111A (en) | Natural bacteriostasis hand cleanser and its preparation method | |
| CN104644535A (en) | Hair and body wash powder | |
| CN104745332A (en) | Condensed soap prepared by raw material of Yunnan big leaf species tea-seed oil | |
| CN104382824A (en) | Nourishing and moisturizing eye cream and preparation method thereof | |
| KR20100135576A (en) | An extract for functional cosmetic and a cosmetic utilizing the same | |
| CN104771346A (en) | Lemongrass liquid soap and preparation method thereof | |
| KR101161533B1 (en) | A Cleanser and A Manufacturing Method therefor | |
| CN102949308B (en) | Hair-care cosmetic containing acanthopanax trifoliatus extract | |
| CN106176516A (en) | One is calmed the nerves perfume | |
| CN111686016A (en) | Water-oil two-layer scalp care plant essential oil | |
| CN104305840A (en) | Costus root stick and preparation method thereof | |
| KR20210012144A (en) | Diy kit for manufacturing natural cosmetic | |
| CN104312790A (en) | Novel traditional Chinese herbal perfumed soap | |
| CN107412105A (en) | A kind of camellia oil emollient cream and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150729 Termination date: 20220113 |