CN105567474A - Delavay falsepanax herb essential oil soap and preparation method thereof - Google Patents
Delavay falsepanax herb essential oil soap and preparation method thereof Download PDFInfo
- Publication number
- CN105567474A CN105567474A CN201610090821.8A CN201610090821A CN105567474A CN 105567474 A CN105567474 A CN 105567474A CN 201610090821 A CN201610090821 A CN 201610090821A CN 105567474 A CN105567474 A CN 105567474A
- Authority
- CN
- China
- Prior art keywords
- oil
- essential oil
- parts
- soap
- perfumed soap
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
Abstract
The invention discloses delavay falsepanax herb essential oil soap and a preparation method thereof. The delavay falsepanax herb essential oil soap is prepared from delavay falsepanax herb essential oil, shea butter, prinsepia utilis seed oil, coconut oil, palm oil, olive oil, sodium hydroxide and water. The preparation technology is simple and safe, natural plant effective ingredients are added, the quality of the soap is improved, skin can be cleaned, the soap can achieve the antibacterial, anti-inflammation and skin lubricating effects, fragrance lasts long, and use experience and feel are unique.
Description
Technical field
The invention belongs to fine chemistry industry daily necessities technical field, what be specifically related to is a kind of Essential Oil From Nothopanax Delavayi perfumed soap and preparation method thereof.
Background technology
Herba seu Radix Nothopanacis delavayi is complete stool or the root of Araliaceae Nothopanax.Herba seu Radix Nothopanacis delavayi be distributed in the limes marginis of Yunnan height above sea level 1600 ~ 2500 meters, Schattenseite shrub from and forest.Recording Herba seu Radix Nothopanacis delavayi in " Yunnan herbal medicine " and " Kunming conventional herbal medicine among the people " can " clearing heat and detoxicating, relaxing muscles and tendons of regulating the flow of vital energy " and " heat clearing and inflammation relieving, antidiarrheal of promoting the production of body fluid ".Be commonly used to control throat heat pain, acute pharyngitis, maldigestion, menoxenia, wound and lumbago, skelalgia of rheumatism.
The people such as Hu Yingjie have delivered the research of the chemical composition about Essential Oil From Nothopanax Delavayi in " chemistry of forest product and industry ", point out that its main component is monoterpenes and sesquiterpenoids, as: α-pinene, myrcene, β-phellandrene, α-terpinene, α-thujene, amphene, terpenes-4-alcohol etc.And such material has the effect of antisepsis and anti-inflammation.In addition, this paper also points out that Essential Oil From Nothopanax Delavayi has strong aromatic odour, and its diluent also keeps lasting delicate fragrance; Herba seu Radix Nothopanacis delavayi is strong to environmental compatibility, extraction process is simple, oil yield is high, in spices, makeup and air freshener, have application prospect.
Perfumed soap is a kind of traditional personal cleansing articles for use, forms primarily of animal-plant oil saponification.Compare other cleaning products, especially strong, the skin care of natural component perfumed soap cleaning force, noresidue and being easily degraded, can not cause water pollution.Therefore, the pursuit that plant perfumed soap is more and more subject to people is held in both hands with heat.But, there is no the report of a Essential Oil From Nothopanax Delavayi perfumed soap at present.
Summary of the invention
Object of the present invention is just to provide a kind of Essential Oil From Nothopanax Delavayi perfumed soap, and this perfumed soap can effectively clean, lubricate the skin and muscle, bacteriostasis antibiosis and lasting delicate fragrance.
Technical scheme provided by the invention:
A kind of Essential Oil From Nothopanax Delavayi perfumed soap, by weight, the raw material of described Essential Oil From Nothopanax Delavayi perfumed soap comprises: Essential Oil From Nothopanax Delavayi 1-3 part, shea butter 3-9 part, prinsepia utilis royle oil 5-12 part, Oleum Cocois 8-15 part, plam oil 12-18 part, sweet oil 14-20 part, sodium hydroxide 12-18 part, water 30-50 part.
Preferably, by weight, the raw material of described Essential Oil From Nothopanax Delavayi perfumed soap comprises: Essential Oil From Nothopanax Delavayi 1.3 parts, shea butter 6.4 parts, prinsepia utilis royle oil 9.6 parts, Oleum Cocois 11.5 parts, plam oil 15.4 parts, 17.9 parts, sweet oil, 15.8 parts, sodium hydroxide, 40 parts, water.
Further, described Essential Oil From Nothopanax Delavayi perfumed soap has the effect of bacteriostasis antibiosis.
A kind of Essential Oil From Nothopanax Delavayi perfumed soap, its preparation method, comprises the following steps:
(1) water is poured in container, slowly add sodium hydroxide, add with alkaline-resisting agitator rapid stirring, after dissolving completely, be cooled to 45 DEG C, obtain alkaline solution;
(2) put into container, heating in water bath to 45 DEG C after shea butter, prinsepia utilis royle oil, Oleum Cocois, plam oil, sweet oil being weighed by weight, obtain mixing oil;
(3) mixing oil is slowly added in alkaline solution, add rapid stirring, until completely dissolved, then stir while oil is little by little added, stir 20 minutes with agitator, obtain soap lye;
(4) in soap lye, add Essential Oil From Nothopanax Delavayi while stirring, obtain mixing soap lye;
(5) leave standstill after 2 minutes, soap lye will be mixed and inject mould;
(6) original place left standstill after 1 ~ 2 day, then placed 1 ~ 2 day in warm place, Do not touch;
(7) perfumed soap is taken out in mould, be placed on shady and cool ventilation place, after one month, complete.
Beneficial effect of the present invention:
Manufacture craft of the present invention is simple and safe, adds active ingredient of natural plant, promotes perfumed soap quality, not only can cleaning skin, more can inhibiting bacteria and diminishing inflammation, lubricate the skin and muscle.In addition, plants essential oil perfumed soap delicate fragrance lasting, there is unique experience and impression.
Embodiment
Embodiment 1
A kind of Essential Oil From Nothopanax Delavayi perfumed soap, by weight, its raw material comprises: Essential Oil From Nothopanax Delavayi 1.3 parts, shea butter 6.4 parts, prinsepia utilis royle oil 9.6 parts, Oleum Cocois 11.5 parts, plam oil 15.4 parts, 17.9 parts, sweet oil, 15.8 parts, sodium hydroxide, 40 parts, water.
Its preparation method, comprises the following steps:
(1) water is poured in container, slowly add sodium hydroxide, add with alkaline-resisting agitator rapid stirring, after dissolving completely, be cooled to 45 DEG C, obtain alkaline solution;
(2) put into container, heating in water bath to 45 DEG C after shea butter, prinsepia utilis royle oil, Oleum Cocois, plam oil, sweet oil being weighed by weight, obtain mixing oil;
(3) mixing oil is slowly added in alkaline solution, add rapid stirring, until completely dissolved, then stir while oil is little by little added, stir 20 minutes with agitator, obtain soap lye;
(4) in soap lye, add Essential Oil From Nothopanax Delavayi while stirring, obtain mixing soap lye;
(5) leave standstill after 2 minutes, soap lye will be mixed and inject mould;
(6) original place left standstill after 1 ~ 2 day, then placed 1 ~ 2 day in warm place, Do not touch;
(7) perfumed soap is taken out in mould, be placed on shady and cool ventilation place, after one month, complete.
Embodiment 2
A kind of Essential Oil From Nothopanax Delavayi perfumed soap, by weight, its raw material comprises: Essential Oil From Nothopanax Delavayi 1 part, shea butter 3 parts, prinsepia utilis royle oil 5 parts, Oleum Cocois 8 parts, plam oil 12 parts, 14 parts, sweet oil, 12 parts, sodium hydroxide, 30 parts, water.
Its preparation method, comprises the following steps:
(1) water is poured in container, slowly add sodium hydroxide, add with alkaline-resisting agitator rapid stirring, after dissolving completely, be cooled to 45 DEG C, obtain alkaline solution;
(2) put into container, heating in water bath to 45 DEG C after shea butter, prinsepia utilis royle oil, Oleum Cocois, plam oil, sweet oil being weighed by weight, obtain mixing oil;
(3) mixing oil is slowly added in alkaline solution, add rapid stirring, until completely dissolved, then stir while oil is little by little added, stir 20 minutes with agitator, obtain soap lye;
(4) in soap lye, add Essential Oil From Nothopanax Delavayi while stirring, obtain mixing soap lye;
(5) leave standstill after 2 minutes, soap lye will be mixed and inject mould;
(6) original place left standstill after 1 ~ 2 day, then placed 1 ~ 2 day in warm place, Do not touch;
(7) perfumed soap is taken out in mould, be placed on shady and cool ventilation place, after one month, complete.
Embodiment 3
A kind of Essential Oil From Nothopanax Delavayi perfumed soap, by weight, its raw material comprises: Essential Oil From Nothopanax Delavayi 3 parts, shea butter 9 parts, prinsepia utilis royle oil 12 parts, Oleum Cocois 15 parts, plam oil 18 parts, 20 parts, sweet oil, 18 parts, sodium hydroxide, 50 parts, water.
Its preparation method, comprises the following steps:
(1) water is poured in container, slowly add sodium hydroxide, add with alkaline-resisting agitator rapid stirring, after dissolving completely, be cooled to 45 DEG C, obtain alkaline solution;
(2) put into container, heating in water bath to 45 DEG C after shea butter, prinsepia utilis royle oil, Oleum Cocois, plam oil, sweet oil being weighed by weight, obtain mixing oil;
(3) mixing oil is slowly added in alkaline solution, add rapid stirring, until completely dissolved, then stir while oil is little by little added, stir 20 minutes with agitator, obtain soap lye;
(4) in soap lye, add Essential Oil From Nothopanax Delavayi while stirring, obtain mixing soap lye;
(5) leave standstill after 2 minutes, soap lye will be mixed and inject mould;
(6) original place left standstill after 1 ~ 2 day, then placed 1 ~ 2 day in warm place, Do not touch;
(7) perfumed soap is taken out in mould, be placed on shady and cool ventilation place, after one month, complete.
Embodiment 4: bacteriostatic experiment
(1) bacterial classification: intestinal bacteria CMCC (B) 44102, Salmonellas CMCC (B) 50094, Pseudomonas aeruginosa CMCC (B) 10104, streptococcus aureus CMCC (B) 26003; There is provided by institute for drug control, Kunming, Yunnan Province.
(2) perfumed soap liquid preparation: get the perfumed soap that example 1 is made, weighs 5g and puts into Erlenmeyer flask, add sterile distilled water 25mL, and 45 DEG C of water-bath vibrations are dissolved completely to sample, make the perfumed soap liquid of concentration 1:5.
(3) preparation of susceptibility sheet: the filter paper getting the aseptic drying of 6mm, every sheet drips perfumed soap liquid 20 μ L, is then lain against by filter paper in clean sterile petri dish, for subsequent use after dry;
(4) preparation of negative control sheet: get the aseptic dry filter paper sheet of 6mm, every sheet drips sterile distilled water 20 μ L, for subsequent use after dry.
(5) K-B Method of paper diffusion: dipping concentration with aseptic cotton carrier is 5 × 106cfu/ml test organisms suspension, tube wall squeezes and removes unnecessary bacterium liquid, be coated with whole nutrient agar planar surface, 3 times repeatedly; Often smear 1 time, dull and stereotyped rotation 60 degree, cotton swab evenly, is finally smeared one week around plate edge by coating; Build culture dish, put drying at room temperature 5min; Stick susceptibility sheet to be measured and negative control sheet, observe fungistatic effect after 37 DEG C of cultivation 16 ~ 24h, measure inhibition zone diameter.
Table 1:1:5 concentration perfumed soap liquid antibacterial experiment in vitro result (inhibition zone diameter mm)
Intestinal bacteria | 15.8 |
Salmonellas | 12.1 |
Pseudomonas aeruginosa | 10.5 |
Streptococcus aureus | 13.4 |
Table 1 illustrates that perfumed soap of the present invention has the effect of obvious bacteriostasis antibiosis.
Embodiment 5:
Because the too high meeting of essential oil concentration causes skin easily to be burnt, and strong and light quality and the experience that also directly can affect perfumed soap of fragrance.Therefore, the optimum quantum of utilization determining Essential Oil From Nothopanax Delavayi in perfumed soap is needed.Experimental technique: shea butter 6.4 parts pressed by other raw materials, prinsepia utilis royle oil 9.6 parts, Oleum Cocois 11.5 parts, plam oil 15.4 parts, 17.9 parts, sweet oil, 15.8 parts, sodium hydroxide, the proportioning that water is 40 parts makes perfumed soap, add Essential Oil From Nothopanax Delavayi 0 part more respectively, 0.5 part, 1.0 part, 1.3 part, 1.5 part, 2 parts, 2.5 part, 3 parts make 8 groups of perfumed soaps and carry out sensory testing, method is that random selecting 50 people forms test crowd, adopt the mode of blank marking to skin irritation sense, perfumed soap fragrance and use sense are given a mark by 4 indexs, mark is higher, represent that product quality is better, statistical study is carried out to use sense, result is as shown in table 2 below.
Table 2 perfumed soap sensory evaluation scores summary sheet
Table 2 perfumed soap organoleptic test shows that group 3 Essential Oil From Nothopanax Delavayi perfumed soap has preferably experience, and pleasant, the lasting delicate fragrance of fragrance.
Claims (4)
1. an Essential Oil From Nothopanax Delavayi perfumed soap, it is characterized in that, by weight, the raw material of described Essential Oil From Nothopanax Delavayi perfumed soap comprises: Essential Oil From Nothopanax Delavayi 1-3 part, shea butter 3-9 part, prinsepia utilis royle oil 5-12 part, Oleum Cocois 8-15 part, plam oil 12-18 part, sweet oil 14-20 part, sodium hydroxide 12-18 part, water 30-50 part.
2. Essential Oil From Nothopanax Delavayi perfumed soap according to claim 1, it is characterized in that, by weight, the raw material of described Essential Oil From Nothopanax Delavayi perfumed soap comprises: Essential Oil From Nothopanax Delavayi 1.3 parts, shea butter 6.4 parts, prinsepia utilis royle oil 9.6 parts, Oleum Cocois 11.5 parts, plam oil 15.4 parts, 17.9 parts, sweet oil, 15.8 parts, sodium hydroxide, 40 parts, water.
3. the Essential Oil From Nothopanax Delavayi perfumed soap according to any one of claim 1-3, is characterized in that, described Essential Oil From Nothopanax Delavayi perfumed soap has the effect of bacteriostasis antibiosis.
4. the Essential Oil From Nothopanax Delavayi perfumed soap according to any one of claim 1-3, is characterized in that its preparation method comprises the following steps:
(1) water is poured in container, slowly add sodium hydroxide, add with alkaline-resisting agitator rapid stirring, after dissolving completely, be cooled to 45 DEG C, obtain alkaline solution;
(2) put into container, heating in water bath to 45 DEG C after shea butter, prinsepia utilis royle oil, Oleum Cocois, plam oil, sweet oil being weighed by weight, obtain mixing oil;
(3) mixing oil is slowly added in alkaline solution, add rapid stirring, until completely dissolved, then stir while oil is little by little added.Stir 20 minutes with agitator, obtain soap lye;
(4) in soap lye, add Essential Oil From Nothopanax Delavayi while stirring, obtain mixing soap lye;
(5) leave standstill after 2 minutes, soap lye will be mixed and inject mould;
(6) original place left standstill after 1 ~ 2 day, then placed 1 ~ 2 day in warm place, Do not touch;
(7) perfumed soap is taken out in mould, be placed on shady and cool ventilation place, after one month, complete.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610090821.8A CN105567474A (en) | 2016-02-18 | 2016-02-18 | Delavay falsepanax herb essential oil soap and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610090821.8A CN105567474A (en) | 2016-02-18 | 2016-02-18 | Delavay falsepanax herb essential oil soap and preparation method thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN105567474A true CN105567474A (en) | 2016-05-11 |
Family
ID=55878111
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610090821.8A Pending CN105567474A (en) | 2016-02-18 | 2016-02-18 | Delavay falsepanax herb essential oil soap and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN105567474A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107267314A (en) * | 2017-06-02 | 2017-10-20 | 张志杰 | Essential oil soap and preparation method thereof |
CN107737070A (en) * | 2017-11-16 | 2018-02-27 | 东兴市良佳优农林科技有限公司 | Sterilization, skin care hand cleaning liquid |
CN110591841A (en) * | 2019-09-11 | 2019-12-20 | 福建师范大学泉港石化研究院 | Antibacterial and anti-inflammatory handmade soap and preparation method thereof |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100837796B1 (en) * | 2007-12-06 | 2008-06-13 | 김홍열 | Neutral calcium-yellow soil soup and the producing method |
CN102002450A (en) * | 2010-12-05 | 2011-04-06 | 韩萍萍 | Essential oil soap and preparation method thereof |
CN103045419A (en) * | 2013-01-24 | 2013-04-17 | 广州丹奇日用化工厂有限公司 | Handmade soap composition, handmade soap and preparation method thereof |
CN104293540A (en) * | 2014-10-10 | 2015-01-21 | 青岛润鑫伟业科贸有限公司 | Handmade soap |
-
2016
- 2016-02-18 CN CN201610090821.8A patent/CN105567474A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100837796B1 (en) * | 2007-12-06 | 2008-06-13 | 김홍열 | Neutral calcium-yellow soil soup and the producing method |
CN102002450A (en) * | 2010-12-05 | 2011-04-06 | 韩萍萍 | Essential oil soap and preparation method thereof |
CN103045419A (en) * | 2013-01-24 | 2013-04-17 | 广州丹奇日用化工厂有限公司 | Handmade soap composition, handmade soap and preparation method thereof |
CN104293540A (en) * | 2014-10-10 | 2015-01-21 | 青岛润鑫伟业科贸有限公司 | Handmade soap |
Non-Patent Citations (2)
Title |
---|
胡正海: "《药用植物的结构、发育与药用成分的关系》", 31 October 2014 * |
胡英杰: "良旺茶精油的化学成分", 《林产化学与工业》 * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107267314A (en) * | 2017-06-02 | 2017-10-20 | 张志杰 | Essential oil soap and preparation method thereof |
CN107737070A (en) * | 2017-11-16 | 2018-02-27 | 东兴市良佳优农林科技有限公司 | Sterilization, skin care hand cleaning liquid |
CN110591841A (en) * | 2019-09-11 | 2019-12-20 | 福建师范大学泉港石化研究院 | Antibacterial and anti-inflammatory handmade soap and preparation method thereof |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103589537B (en) | Beautifying and antibacterial toilet soap | |
CN105112180B (en) | Natural plants floral type essential oil soap with bacteria resistance function and preparation method thereof | |
KR101652700B1 (en) | Toilet paper with antimicrobial properties | |
CN103622865B (en) | A kind of medical handwashing liquid comprising plant extract quintessence oil and preparation method thereof | |
CN106259509A (en) | A kind of natural plant disinfectant and preparation method thereof | |
CN106900781A (en) | Antibacterial bacteriostatic liquid prepared by a kind of vegetable Chinese herbal medicine | |
CN102847028A (en) | Traditional Chinese medicine disinfectant and preparation method thereof | |
CN105567474A (en) | Delavay falsepanax herb essential oil soap and preparation method thereof | |
CN107737070A (en) | Sterilization, skin care hand cleaning liquid | |
CN105018254A (en) | Oil-control acne-removing cosmetic soap and preparation method therefor | |
CN103351962B (en) | A kind of artemisia annua health care toilet soap | |
CN106309174A (en) | Folium isatidis hand cleanser and preparation method thereof | |
CN105602768A (en) | Prinsepia utilis royle soap and preparation method thereof | |
CN105733853A (en) | Sun block and repair sea buckthorn fruit cold-processed handmade soap and preparing method thereof | |
CN109512741A (en) | A kind of essential oil is washed one's hands condensation and preparation method thereof | |
CN106305840A (en) | Plant disinfectant and preparation method thereof | |
CN104815454B (en) | Rosemary natural extract and utilize this extract to prepare antibacterial toilet soap and its preparation method and application | |
CN105154257A (en) | Faint-scent natural plant essential oil soap with bacteriostasis function and preparation method of faint-scent natural plant essential oil soap | |
CN103284896B (en) | Chimonanthus salicifolius sterilization hand washing solution and its preparation method | |
CN110484393A (en) | A kind of Cannador multifunctional manual soap and preparation method thereof | |
CN102166314A (en) | Oil in water type citionella oil nanoemulsion and preparation method thereof | |
Debnath et al. | Formulation and Evaluation of Liquid Soap Containing Herbal Antimicrobial Agent. | |
CN108671088B (en) | Chinese herbal medicine environment-friendly disinfectant for livestock and poultry breeding and preparation method and use method thereof | |
CN111686016A (en) | Water-oil two-layer scalp care plant essential oil | |
CN106635565A (en) | Cosmetic soap and preparation method thereof |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160511 |