CN103045419A - Handmade soap composition, handmade soap and preparation method thereof - Google Patents
Handmade soap composition, handmade soap and preparation method thereof Download PDFInfo
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- CN103045419A CN103045419A CN201310027821XA CN201310027821A CN103045419A CN 103045419 A CN103045419 A CN 103045419A CN 201310027821X A CN201310027821X A CN 201310027821XA CN 201310027821 A CN201310027821 A CN 201310027821A CN 103045419 A CN103045419 A CN 103045419A
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Abstract
The invention relates to a handmade soap composition which is characterized by comprising the following components in percentage by weight: 70-77 percent of vegetable fat, 9.5-12.5 percent of sodium hydroxide, 0.5-3 percent of dry fruit jelly and the balance of water. The handmade soap prepared from the handmade soap composition is prepared by long-term slow saponification of multiple plant oil and sodium hydroxide at low temperature being less than 40 DEG C. The handmade soap contains high-content natural glycerin, and natural vitamins, mineral substances, polysaccharide and other nutritional ingredients in the plant oil and fruits are kept to the greatest degree, so that the product has a cleaning function, has excellent moisturizing and skin-care effects and is long in quality guarantee period.
Description
Technical field
The invention belongs to daily washing product technical field, be specifically related to a kind of handmade soap, relate to more specifically a kind of handmade soap composition that contains the fruit jelly dry fruit, handmade soap and preparation method thereof.
Background technology
Perfumed soap is to take a shower in people's daily life and clean product commonly used, preferably cleaning effect is arranged, but humidity-holding effect is not good, to tight, the dry and astringent sense of people, adds that alkalescence is large after using, and life-time service will make the skin degrease drying that excessively becomes coarse.Rise gradually in recent years a kind of new perfumed soap---handmade soap, handmade soap uses natural plant grease and alkali generation saponification reaction to make, the tensio-active agent lathering property that saponification generates is good, and foam is fine and smooth abundant, and the natural glycerin that reaction generates also has good humidity-holding effect.For further strengthening the skin care characteristic of product, part handmade soap on sale is added with plant extraction liquid, plant petals etc. on the market.Although above-mentioned handmade soap moisturizing, skin care performance make moderate progress, but have following shortcoming for the handmade soap that adds plant extraction liquid: 1) plant extraction liquid can only extract the part effective constituent of plant, all nutritive ingredients that can not the preserve characteristic plant, make its most of nutrient loss, can not well be utilized; 2) conventional decocting method and circumfluence method utilization ratio is low, so that the biological activity of heat-sensitive substance and working substance is affected; 3) solvent that uses in the leaching process also can bring pollution to product.
Summary of the invention
In order to solve the shortcomings and deficiencies that exist in the above-mentioned prior art, better use sensation and effect are provided, the invention provides a kind of handmade soap composition that contains the fruit jelly dry fruit, handmade soap and preparation method thereof.Handmade soap of the present invention by various plants oil and sodium hydroxide (be lower than 40 ℃) at low temperatures through for a long time slowly saponification reaction make.It contains the natural glycerin (reaching 20%～30%) of high-content, and unsaturated fatty acids and the nutritive ingredients such as the natural complex group in the fruit, mineral substance, carbohydrate, fruit oil and pulp in the vegetables oil have been kept to greatest extent, make product when playing cleaning action, possess excellent cleaning, moisturizing, skin care and certain result for the treatment of, and the quality guarantee period is longer, and use procedure has more the advantages such as enjoyment.
In order to overcome above-mentioned technical problem, the present invention is achieved through the following technical solutions:
A kind of handmade soap composition is characterized in that, by weight percentage, described handmade soap composition contains: 70-77% Vegetable oil lipoprotein, 9.5-12.5% sodium hydroxide, 0.5-5% fruit jelly dry fruit, surplus are water.
Fruit involved in the present invention includes but not limited to pawpaw, strawberry, pineapple, blueberry, raspberry, pumpkin, mango, tomato, lemon.Rich vitamin in the fruit (A, B, B1, B2, C), several mineral materials (such as iron, calcium, zinc), protein, amino acid, fructose and organic acid etc., different fruit makes an addition to can play whitening in the washing product, reduce wrinkle of skin, exfoliation, the Shujin that dries, and the effect such as stimulate circulation.
Term of the present invention " Vacuum Freezing ﹠ Drying Technology " is called for short freeze drying technology, is the technological measure that a kind of material of rising in 20th century dehydrates.Its principle is to utilize the distillation principle of water, and distillation becomes water vapor and removes without melting directly to make the moisture that is frozen in advance in the material, finally obtains the method for drying products.
Term of the present invention " fruit jelly dry fruit " refers to fruit piece or the fruit grain of fruit after Vacuum Freezing ﹠ Drying Technology is processed.In the vacuum lyophilization process, because fruit dries out under low temperature, anoxic and lucifuge condition, dried fruit jelly dry fruit has kept color, shape and the most effective constituent of fresh prod basically, such as VITAMIN, polysaccharide, mineral substance etc., some volatile thermo-sensitivity effective constituents particularly, keep to greatest extent whole nutrition, effectively prevent the oxidation in the drying process, conversion and the change of state of nutritive ingredient.Freeze-dried products becomes piece/granular, and fabulous without drying shrinkage, rehydration, water content is few, and long-time storage and transport at normal temperatures after the packing are easy to use.
The dispersion of fruit jelly dry fruit involved in the present invention is, is that 4～15 ℃ deionized water soaks with fruit jelly dry fruit piece temperature, uses high speed shear clarifixator (3000 rev/mins) that it is separated into uniform paste or thinner particle again.Can avoid like this can producing heat under high-speed stirring and the shearing and cause local temperature higher, keep to greatest extent the biological activity of fruit jelly dry fruit.
In preferred implementation of the present invention, described Vegetable oil lipoprotein is selected from least a in Oleum Cocois, plam oil, sweet oil, sweet almond oil and the shea butter.
In preferred implementation of the present invention, described Vegetable oil lipoprotein is comprised of 10-30% Oleum Cocois, 10-35% plam oil, 15-40% sweet oil, 10-25% sweet almond oil and 5-15% shea butter by weight percentage.
Utilize above-mentioned handmade soap composition to prepare the method for handmade soap, it is characterized in that, comprise the steps:
1) add described Vegetable oil lipoprotein in reactor, after stirring, be warming up to 30～40 degree, constant temperature is stand-by;
2) be that the aqueous sodium hydroxide solutions of 30～40 degree add in the solution of step 1) with temperature, rapid stirring is until soap lye thickens (viscosity 6000mPa.s～8000mPa.s);
The fruit jelly dry fruit adding step 2 of 3) water in advance being disperseed) in the soap lye that obtains, and stirs;
4) soap lye of step 3) is poured in the preprepared mould, put into temperature and be 30～40 ℃ insulation can, after soap lye solidifies fully, the demoulding, then be put under the Air drying environment to place and treat its fully matured 4-8 week (soap blank is stiff, PH is weakly alkaline, PH7～9), obtain containing the handmade soap of fruit jelly dry fruit.。
In above-mentioned preparation method, in order to keep the biological activity of fruit jelly dry fruit, need until vegetables oil with add again after alkali reaction becomes starchiness, stir.
The handmade soap that makes according to aforesaid method.
The handmade soap that the present invention makes after one month on probation, reflects all that result of use is very dry and comfortable through 100 people, and without tight sense, humidity-holding effect is good, and facial skin becomes more fine and smooth glossy after use for some time.
Compared with prior art, handmade soap composition of the present invention has kept the nutritive ingredients such as natural complex in vegetables oil and the fruit to greatest extent, makes product possess good moisturizing, skin-care effect when playing cleaning action, and the quality guaranteed period limit for length.
Embodiment
To of the present invention for a more detailed description, but embodiments of the present invention are not limited to this below in conjunction with embodiment, for processing parameter or the condition do not indicated especially, can carry out with reference to routine techniques.
Embodiment 1
A kind of handmade soap composition, its component by following weight percent forms:
Above-mentioned Oleum Cocois, plam oil, sweet oil, sweet almond oil, shea butter are dropped in the reactor successively, and turn on agitator (10rpm) stirs, and is warmed up to 31 ℃, heat preservation for standby use;
Under rapid stirring (30rpm), sodium hydroxide is dissolved in an amount of water, after the dissolving, be cooled to 31 ℃ fully;
Above-mentioned sodium hydroxide solution slowly adds in the reactor, and rapid stirring (30rpm) is until soap lye thickens (viscosity 6000mPa.s～8000mPa.s);
Pawpaw freezed dry really with after the remaining deionized water dispersion, is added it in reactor, stir;
Soap lye is poured in the preprepared mould, build mould with plastics film after, put into 31 ℃ of insulation cans and leave standstill;
Carry out the demoulding after 48 hours, then be put into to place under the Air drying environment and treat its fully matured (soap blank is stiff, PH is weakly alkaline, PH7～9) 4-8 week, obtain containing the handmade soap of pawpaw freezed dry fruit.
Embodiment 2
A kind of handmade soap composition, its component by following weight percent forms:
Above-mentioned Oleum Cocois, plam oil, sweet oil, sweet almond oil, shea butter are dropped in the reactor successively, and turn on agitator (10rpm) stirs, and is warmed up to 33 ℃, heat preservation for standby use;
Under rapid stirring (30rpm), sodium hydroxide is dissolved in an amount of water, after the dissolving, be cooled to 33 ℃ fully;
Above-mentioned sodium hydroxide solution slowly adds in the reactor, and rapid stirring (30rpm) is until soap lye thickens (viscosity 6000mPa.s～8000mPa.s);
After the strawberry jelly dry fruit disperseed with remaining deionized water, it is added in reactor, stir;
Soap lye is poured in the preprepared mould, build mould with plastics film after, put into 33 ℃ of insulation cans and leave standstill;
Carry out the demoulding after 48 hours, then be put into to place under the Air drying environment and treat its fully matured (soap blank is stiff, PH is weakly alkaline, PH7～9) 4-8 week, obtain containing the handmade soap of strawberry jelly dry fruit.
Embodiment 3
A kind of handmade soap composition, its component by following weight percent forms:
Above-mentioned Oleum Cocois, plam oil, sweet oil, sweet almond oil, shea butter are dropped in the reactor successively, and turn on agitator (10rpm) stirs, and is warmed up to 34 ℃, heat preservation for standby use;
Under rapid stirring (30rpm), sodium hydroxide is dissolved in an amount of water, after the dissolving, be cooled to 34 ℃ fully;
Above-mentioned sodium hydroxide solution slowly adds in the reactor, and rapid stirring (30rpm) is until soap lye thickens (viscosity 6000mPa.s～8000mPa.s);
The pumpkin freeze-drying really with after the remaining deionized water dispersion, is added it in reactor, stir;
Soap lye is poured in the preprepared mould, build mould with plastics film after, put into 34 ℃ of insulation cans and leave standstill;
Carry out the demoulding after 48 hours, then be put into to place under the Air drying environment and treat its fully matured (soap blank is stiff, PH is weakly alkaline, PH7～9) 4-8 week, obtain containing the handmade soap of pumpkin freeze-drying fruit.
Embodiment 4
A kind of handmade soap composition, its component by following weight percent forms:
Above-mentioned Oleum Cocois, plam oil, sweet oil, sweet almond oil, shea butter are dropped in the reactor successively, and turn on agitator (10rpm) stirs, and is warmed up to 35 ℃, heat preservation for standby use;
Under rapid stirring (30rpm), sodium hydroxide is dissolved in an amount of water, after the dissolving, be cooled to 35 ℃ fully;
Above-mentioned sodium hydroxide solution slowly adds in the reactor, and rapid stirring (30rpm) is until soap lye thickens (viscosity 6000mPa.s～8000mPa.s);
The blueberry freeze-drying really with after the remaining deionized water dispersion, is added it in reactor, stir;
Soap lye is poured in the preprepared mould, build mould with plastics film after, put into 35 ℃ of insulation cans and leave standstill;
Carry out the demoulding after 48 hours, then be put into to place under the Air drying environment and treat its fully matured (soap blank is stiff, PH is weakly alkaline, PH7～9) 4-8 week, obtain containing the handmade soap of blueberry freeze-drying fruit.
Embodiment 5
A kind of handmade soap composition, its component by following weight percent forms:
Above-mentioned Oleum Cocois, plam oil, sweet oil, sweet almond oil, shea butter are dropped in the reactor successively, and turn on agitator (10rpm) stirs, and is warmed up to 36 ℃, heat preservation for standby use;
Under rapid stirring (30rpm), sodium hydroxide is dissolved in an amount of water, after the dissolving, be cooled to 36 ℃ fully;
Above-mentioned sodium hydroxide solution slowly adds in the reactor, and rapid stirring (30rpm) is until soap lye thickens (viscosity 6000mPa.s～8000mPa.s);
The tomato freeze-drying really with after the remaining deionized water dispersion, is added it in reactor, stir;
Soap lye is poured in the preprepared mould, build mould with plastics film after, put into 36 ℃ of insulation cans and leave standstill;
Carry out the demoulding after 48 hours, then be put into to place under the Air drying environment and treat its fully matured (soap blank is stiff, the PH weakly alkaline, PH7～9) 4-8 week, obtain containing the handmade soap of tomato freeze-drying fruit.
Embodiment 6
A kind of handmade soap composition, its component by following weight percent forms:
Above-mentioned Oleum Cocois, plam oil, sweet oil, sweet almond oil, shea butter are dropped in the reactor successively, and turn on agitator (10rpm) stirs, and is warmed up to 38 ℃, heat preservation for standby use;
Under rapid stirring (30rpm), sodium hydroxide is dissolved in an amount of water, after the dissolving, be cooled to 38 ℃ fully;
Above-mentioned sodium hydroxide solution slowly adds in the reactor, and rapid stirring (30rpm) is until soap lye thickens (viscosity 6000mPa.s～8000mPa.s);
After the pineapple jelly dry fruit disperseed with remaining deionized water, it is added in reactor, stir;
Soap lye is poured in the preprepared mould, build mould with plastics film after, put into 38 ℃ of insulation cans and leave standstill;
Carry out the demoulding after 48 hours, then be put into to place under the Air drying environment and treat its fully matured (soap blank is stiff, PH is weakly alkaline, PH7～9) 4-8 week, obtain containing the handmade soap of pineapple jelly dry fruit.
Embodiment 7
A kind of handmade soap composition, its component by following weight percent forms:
Above-mentioned Oleum Cocois, plam oil, sweet oil, sweet almond oil, shea butter are dropped in the reactor successively, and turn on agitator (10rpm) stirs, and is warmed up to 39 ℃, heat preservation for standby use;
Under rapid stirring (30rpm), sodium hydroxide is dissolved in an amount of water, after the dissolving, be cooled to 39 ℃ fully;
Above-mentioned sodium hydroxide solution slowly adds in the reactor, and rapid stirring (30rpm) is until soap lye thickens (viscosity 6000mPa.s～8000mPa.s);
The raspberry freeze-drying really with after the remaining deionized water dispersion, is added it in reactor, stir;
Soap lye is poured in the preprepared mould, build mould with plastics film after, put into 39 ℃ of insulation cans and leave standstill;
Carry out the demoulding after 48 hours, then be put into to place under the Air drying environment and treat its fully matured (soap blank is stiff, PH is weakly alkaline, PH7～9) 4-8 week, obtain containing the handmade soap of raspberry freeze-drying fruit.
The present invention is not limited to above-mentioned embodiment, and in the situation that does not break away from the spirit and scope of the present invention, various modifications and/or distortion that the present invention is made all belong to protection scope of the present invention.
Claims (6)
1. a handmade soap composition is characterized in that, by weight percentage, described handmade soap composition contains: 70-77% Vegetable oil lipoprotein, 9.5-12.5% sodium hydroxide, 0.5-5% fruit jelly dry fruit, surplus are water.
2. handmade soap composition according to claim 1 is characterized in that, described Vegetable oil lipoprotein is selected from least a in Oleum Cocois, plam oil, sweet oil, sweet almond oil and the shea butter.
3. handmade soap composition according to claim 2 is characterized in that, described Vegetable oil lipoprotein is comprised of 10-30% Oleum Cocois, 10-35% plam oil, 15-40% sweet oil, 10-25% sweet almond oil and 5-15% shea butter by weight percentage.
4. described handmade soap composition is characterized in that according to claim 1-3, and described fruit jelly dry fruit is pawpaw freezed dry fruit, strawberry jelly dry fruit, pumpkin freeze-drying fruit, blueberry freeze-drying fruit, tomato freeze-drying fruit, pineapple jelly dry fruit or raspberry freeze-drying fruit.
5. utilize each described handmade soap composition of claim 1-4 to prepare the method for handmade soap, it is characterized in that, comprise the steps:
1) add described Vegetable oil lipoprotein in reactor, after stirring, be warming up to 30-40 ℃, constant temperature is stand-by;
2) be that 30-40 ℃ aqueous sodium hydroxide solution adds in the solution of step 1) with temperature, rapid stirring is until soap lye thickens;
The fruit jelly dry fruit adding step 2 of 3) water in advance being disperseed) in the soap lye that obtains, and stirs;
4) soap lye of step 3) is poured in the preprepared mould, putting into temperature is the insulation can of 30～40 degree, after soap lye solidifies fully, and the demoulding, then be put into to place under the Air drying environment and 4-8 week treat its fully matured, obtain containing the handmade soap of fruit jelly dry fruit.
6. the handmade soap that makes of method according to claim 5.
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103215150A (en) * | 2013-04-28 | 2013-07-24 | 黑龙江省科学院火山与矿泉研究所 | Wudalianchi volcanic mud handmade soap and cold-making method thereof |
| CN103224848A (en) * | 2013-04-28 | 2013-07-31 | 广州丹奇日用化工厂有限公司 | Hand-made cold process soap and preparation method thereof |
| CN103289839A (en) * | 2013-06-28 | 2013-09-11 | 广州丹奇日用化工厂有限公司 | Breast-enhancing handmade soap |
| CN103540455A (en) * | 2013-10-11 | 2014-01-29 | 石云 | Natural fruit perfumed soap and preparation method thereof |
| CN104629952A (en) * | 2015-03-03 | 2015-05-20 | 上海制皂有限公司 | Cold soap |
| CN105132219A (en) * | 2015-09-29 | 2015-12-09 | 青岛海之源智能技术有限公司 | Perfumed soap for smoothing striae atrophicae and preparation method thereof |
| CN105567474A (en) * | 2016-02-18 | 2016-05-11 | 李金明 | Delavay falsepanax herb essential oil soap and preparation method thereof |
| CN108531321A (en) * | 2018-05-31 | 2018-09-14 | 广西浪伏茶业股份有限公司 | A kind of preparation method of tea fruit handmade soap |
| CN108531320A (en) * | 2018-05-22 | 2018-09-14 | 中北大学 | A kind of function perfumed soap and preparation method thereof |
| IT201700040115A1 (en) * | 2017-04-11 | 2018-10-11 | Idee Vulcaniche S R L | PREPARE FOR USE IN INDUSTRIAL APPLICATIONS AND THEIR PRODUCTION PROCEDURES |
| CN113493725A (en) * | 2021-06-21 | 2021-10-12 | 广东菁萃生物科技有限公司 | Mild non-irritating nursing handmade soap and preparation method thereof |
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| CN103224848A (en) * | 2013-04-28 | 2013-07-31 | 广州丹奇日用化工厂有限公司 | Hand-made cold process soap and preparation method thereof |
| CN103224848B (en) * | 2013-04-28 | 2015-01-14 | 广州丹奇日用化工厂有限公司 | Hand-made cold process soap and preparation method thereof |
| CN103215150A (en) * | 2013-04-28 | 2013-07-24 | 黑龙江省科学院火山与矿泉研究所 | Wudalianchi volcanic mud handmade soap and cold-making method thereof |
| CN103289839A (en) * | 2013-06-28 | 2013-09-11 | 广州丹奇日用化工厂有限公司 | Breast-enhancing handmade soap |
| CN103540455A (en) * | 2013-10-11 | 2014-01-29 | 石云 | Natural fruit perfumed soap and preparation method thereof |
| CN103540455B (en) * | 2013-10-11 | 2015-03-04 | 石云 | Natural fruit perfumed soap and preparation method thereof |
| CN104629952B (en) * | 2015-03-03 | 2018-01-23 | 上海制皂有限公司 | Cold process soap |
| CN104629952A (en) * | 2015-03-03 | 2015-05-20 | 上海制皂有限公司 | Cold soap |
| CN105132219A (en) * | 2015-09-29 | 2015-12-09 | 青岛海之源智能技术有限公司 | Perfumed soap for smoothing striae atrophicae and preparation method thereof |
| CN105567474A (en) * | 2016-02-18 | 2016-05-11 | 李金明 | Delavay falsepanax herb essential oil soap and preparation method thereof |
| IT201700040115A1 (en) * | 2017-04-11 | 2018-10-11 | Idee Vulcaniche S R L | PREPARE FOR USE IN INDUSTRIAL APPLICATIONS AND THEIR PRODUCTION PROCEDURES |
| WO2018189685A1 (en) * | 2017-04-11 | 2018-10-18 | Idee Vulcaniche S.R.L. | Preparations for industrial use and their production methods |
| US20220298074A1 (en) * | 2017-04-11 | 2022-09-22 | : Idee Vulcaniche S.R.L. | Preparations for industrial use and their production methods |
| US11787738B2 (en) * | 2017-04-11 | 2023-10-17 | Idee Vulcaniche S.R.L. | Preparations for industrial use and their production methods |
| CN108531320A (en) * | 2018-05-22 | 2018-09-14 | 中北大学 | A kind of function perfumed soap and preparation method thereof |
| CN108531320B (en) * | 2018-05-22 | 2020-11-24 | 中北大学 | Functional soap and preparation method thereof |
| CN108531321A (en) * | 2018-05-31 | 2018-09-14 | 广西浪伏茶业股份有限公司 | A kind of preparation method of tea fruit handmade soap |
| CN113493725A (en) * | 2021-06-21 | 2021-10-12 | 广东菁萃生物科技有限公司 | Mild non-irritating nursing handmade soap and preparation method thereof |
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Application publication date: 20130417 |