CN108531321A - A kind of preparation method of tea fruit handmade soap - Google Patents
A kind of preparation method of tea fruit handmade soap Download PDFInfo
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- CN108531321A CN108531321A CN201810571879.3A CN201810571879A CN108531321A CN 108531321 A CN108531321 A CN 108531321A CN 201810571879 A CN201810571879 A CN 201810571879A CN 108531321 A CN108531321 A CN 108531321A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/16—Emollients or protectives, e.g. against radiation
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/10—Antimycotics
Abstract
The present invention provides a kind of preparation method of tea fruit handmade soap, is related to daily necessities processing technique field, and the preparation method of tea fruit handmade soap of the invention includes the following steps：(1) preparation of raw material, (2) tea fruit pretreatment, (3) prepare soap lye, (4) prepare handmade soap；The present invention uses the preparation of the tea oil progress handmade soap extracted in tea fruit, in combination with homemade neat soap and flavouring additives, antipruritic auxiliary agent, the handmade soap processed is green safe, and character is mild, suitable for all ages, not only clean skin ability is good, moreover it is possible to enhance the cell viability of skin, inhibit fungi, improve the anti-infection ability of skin, it deeply solves the problems, such as pruitus, and the handmade soap fragrant taste is pleasant, there is the effect of relieving mental strain and helping sleep.
Description
【Technical field】
The present invention relates to daily necessities processing technique fields, and in particular to a kind of preparation method of tea fruit handmade soap.
【Background technology】
Rich in oleic acid, protein, starch, Tea Saponin, flavones, polyphenol, VE etc., the monounsaturated fatty acid of tea-seed oil in tea fruit
Acid content is up to 80%, be current edible oil most, be referred to as beauty acid；And rich in vitamin E, Rosmarinus officinalis extract spiny dogfish
The specific physiological activator such as alkene, camellianin has sun-proof, moisturizing, moist, antibacterial, anti-inflammatory and other effects, is first choice of improving looks
Raw material；Studies have shown that Tea Saponin also has antibacterial and antioxidation.
Traditional perfumed soap is mostly that chemical raw material is prepared, and due to chemical compositions complexity, is easy to occur with skin anti-
Answer, cause the discomfort of skin, cause allergy during use, it is dry the problems such as.With the improvement of living standards, people are to strong
The requirement of health and environmental protection is also higher and higher, and the washing product with natural component is increasingly pursued by people.Handmade soap is
In recent years more popular a kind of washing product, you can as washing one's face, remove ornaments and formal dress, and can be used as taking a shower.Due to being pure hand-made, at
Point in combination with needing to add various natural materials, make handmade soap that there is different effects.Handmade soap not only various shapes, Er Qiegong
Can be also numerous, gradually liked in recent years by people.
【Invention content】
In view of this, the purpose of the present invention is to provide a kind of preparation method of tea fruit handmade soap, the present invention uses tea fruit
The middle preparation extracted obtained tea oil and carry out handmade soap, in combination with homemade neat soap and flavouring additives, antipruritic auxiliary agent, processing
Obtained handmade soap is green safe, and character is mild, is suitable for all ages, not only clean skin ability is good, moreover it is possible to enhance the thin of skin
Born of the same parents' vigor inhibits fungi, improves the anti-infection ability of skin, deeply solve the problems, such as pruitus, and the handmade soap fragrant taste
It is pleasant, there is the effect of relieving mental strain and helping sleep.
In order to solve the above-mentioned technical problem, present invention employs the following technical solutions：
A kind of preparation method of tea fruit handmade soap, includes the following steps：
(1) preparation of raw material：Prepare following raw material according to parts by weight：35-48 parts of tea fruit, 20-35 parts of neat soap, flavouring help
40-60 parts of 5-10 parts of agent, auxiliary agent 5-10 parts antipruritic, 5-10 parts of sodium hydroxide, 3-9 parts of stearic acid and deionized water；
(2) tea fruit pre-processes：By tea fruit decladding, tea seed kernel is taken to crush, the tea seed kernel after crushing, which is carried out microwave, to be done
The frequency of dry processing, first time microwave drying is 800-1000MHz, drying time 90-130s；The frequency of second of microwave drying
Rate is 900-950MHz, drying time 65-100s；It is 1 that solid-to-liquid ratio, that is, w/v will be pressed in tea seed kernel after microwave drying:
The ratio of 2-6 is added a concentration of 20-50% ethanol solutions and is used as extracting solution, is homogenized, and slurries is carried out heating water bath, in centrifuging and taking
It is spare to obtain tea oil for layer edible vegetable oil, vacuum drying；
(3) soap lye is prepared：Sodium hydroxide is slowly added into deionized water, is quickly stirred with alkaline-resisting blender while adding
It mixes, sodium hydroxide is dissolved completely in water postcooling to 40-45 DEG C, obtains aqueous slkali；By stearic acid, tea oil, neat soap, antipruritic help
Agent, flavouring additives, which are added in oil phase pot, is heated to 70-90 DEG C, stirs evenly, obtains mixed liquor A；Aqueous slkali is poured slowly into dress
It in the container of mixed liquor A, while quickly being stirred with alkaline-resisting blender, is until mixed solution A surface can mark complete 8 word
Only, you can obtain soap lye；
(4) handmade soap is prepared：Mold clean is clean, an olive oil is dipped in brush time inside mold with brush, and soap lye is fallen
Enter mold, then mold is covered with plastic film, in being placed 1-2 days in 30-38 DEG C of incubator, takes out, be placed on shady and cool ventilation
Four to eight weeks put for, you can obtain handmade soap finished product in place.
In the present invention, further, bath temperature is 70-100 DEG C in the step (2), water bath time 0.5-2.0h.
In the present invention, further, the neat soap is made of the raw material of following parts by weight：10-20 parts of aliphatic acid, palm kernel
3-9 parts oily, 2-8 parts of propylene glycol, 2-8 parts of zeolite powder, 0.1-0.3 parts of chelating agent, 1-3 parts of sodium chloride, 3-10 parts of Radix Glycyrrhizae, soapberry
3-9 parts of fruit.
In the present invention, further, the neat soap obtains by the following method：
A. it is pre-mixed：The aliphatic acid of the parts by weight, propylene glycol and palm-kernel oil are pre-mixed, are pre-mixed
Liquid；
B. Chinese medicine extract is prepared：Dry Radix Glycyrrhizae and soapberry fruit are taken, the temperature for being equivalent to 5-10 times of its weight is added
Water impregnates, and then boils extraction, until the proportion of gained extracting solution is 1.0-1.2, stops extraction, filtering carries to get to Chinese medicine
Take liquid；
C. saponification：Premix is heated to 80-85 DEG C, then the sodium chloride, chelating agent and Chinese medicine of above-mentioned parts by weight are carried
It takes liquid to be added in mixed liquor after mixing, carries out saponification, reaction time 12-18min waits for that saponification is complete
Afterwards, the zeolite powder of above-mentioned parts by weight is added, is uniformly mixed, obtains soap base；
D. neat soap is molded：By soap base after vacuum spray drying, extruding, homogeneous, refined and pelletizing, you can obtain neat soap.
In the present invention, further, the flavouring additives are made of the raw material of following parts by weight：5-10 parts of sweet osmanthus, yesterday
3-8 parts fragrant, 3-8 parts of lemon grass (Cymbopogon citratus), 2-6 parts of bean cotyledon perfume (or spice), 2-4 parts of sodium alginate, 12-22 parts of ethyl alcohol and distillation appropriate amount of water.
In the present invention, further, the antipruritic auxiliary agent is made of the raw material of following parts by weight：3-8 parts of rhizoma zingiberis, asarum 3-
5-9 parts of 8 parts, deep 6-12 parts of knuckle-tooth violet, 5-10 parts of folium artemisiae argyi, 4-9 parts of Herba Andrographitis and olive oil.
In conclusion by adopting the above-described technical solution, the beneficial effects of the invention are as follows：
1. the present invention is used as the preparation that raw material carries out tea fruit handmade soap by extracting the oily substance in tea fruit, tea fruit is day
Right raw material, have the characteristics that weak-alkaline and weak-acidic, small to the irritation of skin, tea oil can nourishes rough skin, used neat soap is
Homemade neat soap, materials safety, preparation process is simple, has biocidal efficacies, and propylene glycol, which is added, in neat soap is mainly used for emulsifying
The wetting agent of product and various flowing products, moisturizer, play the effect of antifreezing agent in neat soap so that neat soap has preferable
Antifreezing function；It also added flavouring additives and antipruritic auxiliary agent in handmade soap, be made of natural herbal raw material, not only to energy
The problems such as effectively inhibiting skin surface fungi, solving dermatitis, pruitus, while the handmade soap of the present invention also distributes pleasant perfume (or spice)
Gas can alleviate pressure, relaxation body and mind, have good effect for insomnia.
2. tea fruit handmade soap material composition safety of the present invention, process is simple, and contamination-free generates, environmentally protective, symbol
Close the ecological economy industrial policy of country；And the handmade soap is easy to use, while being suitable for men and women, old and young, crowd is extensive, is easy to
It promotes, great market prospects.
【Specific implementation mode】
The following examples can help those skilled in the art that the present invention is more fully understood, but cannot be with any
Mode limits the present invention.
Embodiment 1
The present embodiment provides a kind of preparation methods of tea fruit handmade soap, include the following steps：
(1) preparation of raw material：Prepare following raw material according to parts by weight：35 parts of tea fruit, 20 parts of neat soap, 5 parts of flavouring additives,
40 parts of 5 parts of antipruritic auxiliary agent, 5 parts of sodium hydroxide, 3 parts of stearic acid and deionized water；Wherein, flavouring additives by following parts by weight original
Material composition：5 parts of sweet osmanthus, 3 parts of cordate telosma, 3 parts of lemon grass (Cymbopogon citratus), 2 parts of bean cotyledon perfume, 2 parts of sodium alginate, 12 parts of ethyl alcohol and distilled water are suitable
Amount；Antipruritic auxiliary agent is made of the raw material of following parts by weight：3 parts of rhizoma zingiberis, 3 parts of asarum, deep 6 parts of knuckle-tooth violet, 5 parts of folium artemisiae argyi, punching
5 parts of 4 parts of lotus and olive oil；Neat soap is made of the raw material of following parts by weight：10 parts of aliphatic acid, 3 parts of palm-kernel oil, 2 parts of propylene glycol,
2 parts of zeolite powder, 0.1 part of chelating agent, 1 part of sodium chloride, 3 parts of Radix Glycyrrhizae, 3 parts of soapberry fruit；Neat soap obtains by the following method：a.
Premixing：The aliphatic acid of the parts by weight, propylene glycol and palm-kernel oil are pre-mixed, premix is obtained；B. in preparing
Medicament extracting solution：Dry Radix Glycyrrhizae and soapberry fruit are taken, the warm water immersion for being equivalent to 5 times of its weight is added, then boils extraction,
Until the proportion of gained extracting solution is 1.0, stop extraction, filtering is to get to Chinese medicine extract；C. saponification：By premix plus
Heat is added in mixed liquor after mixing to 80 DEG C, then by the sodium chloride, chelating agent and Chinese medicine extract of above-mentioned parts by weight, into
The zeolite powder of above-mentioned parts by weight is added after saponification is complete in row saponification, reaction time 12min, is uniformly mixed,
Obtain soap base；D. neat soap is molded：By soap base after vacuum spray drying, extruding, homogeneous, refined and pelletizing, you can obtain neat soap；
(2) tea fruit pre-processes：By tea fruit decladding, tea seed kernel is taken to crush, the tea seed kernel after crushing, which is carried out microwave, to be done
The frequency of dry processing, first time microwave drying is 800MHz, drying time 90s；The frequency of second of microwave drying is
900MHz, drying time 65s；It is 1 that solid-to-liquid ratio, that is, w/v will be pressed in tea seed kernel after microwave drying:2 ratio is added dense
It spends for 20% ethanol solution as extracting solution, slurries are carried out heating water bath by homogenate, and bath temperature is 70 DEG C, and water bath time is
0.5h；Centrifuging and taking upper layer edible vegetable oil, vacuum drying, it is spare to obtain tea oil；
(3) soap lye is prepared：Sodium hydroxide is slowly added into deionized water, is quickly stirred with alkaline-resisting blender while adding
It mixes, sodium hydroxide is dissolved completely in water postcooling to 40 DEG C, obtains aqueous slkali；By stearic acid, tea oil, neat soap, antipruritic auxiliary agent, increasing
Fragrant auxiliary agent is added in oil phase pot and is heated to 70 DEG C, stirs evenly, obtains mixed liquor A；Aqueous slkali is poured slowly into dress mixed liquor A
It in container, while quickly being stirred with alkaline-resisting blender, until mixed solution A surface can mark complete 8 word, you can
To soap lye；
(4) handmade soap is prepared：Mold clean is clean, an olive oil is dipped in brush time inside mold with brush, and soap lye is fallen
Enter mold, then mold is covered with plastic film, in being placed 1 day in 30 DEG C of incubators, takes out, be placed at shady and cool ventilation, put
Four to eight weeks, you can obtain handmade soap finished product.
Embodiment 2
The present embodiment provides a kind of preparation methods of tea fruit handmade soap, include the following steps：
(1) preparation of raw material：Prepare following raw material according to parts by weight：41 parts of tea fruit, 28 parts of neat soap, 7 parts of flavouring additives,
50 parts of 7 parts of antipruritic auxiliary agent, 7 parts of sodium hydroxide, 7 parts of stearic acid and deionized water；Wherein, flavouring additives by following parts by weight original
Material composition：7 parts of sweet osmanthus, 6 parts of cordate telosma, 6 parts of lemon grass (Cymbopogon citratus), 4 parts of bean cotyledon perfume, 3 parts of sodium alginate, 17 parts of ethyl alcohol and distilled water are suitable
Amount；Antipruritic auxiliary agent is made of the raw material of following parts by weight：6 parts of rhizoma zingiberis, 6 parts of asarum, deep 9 parts of knuckle-tooth violet, 7 parts of folium artemisiae argyi, punching
7 parts of 7 parts of lotus and olive oil；Neat soap is made of the raw material of following parts by weight：15 parts of aliphatic acid, 6 parts of palm-kernel oil, 5 parts of propylene glycol,
5 parts of zeolite powder, 0.2 part of chelating agent, 2 parts of sodium chloride, 7 parts of Radix Glycyrrhizae, 6 parts of soapberry fruit；Neat soap obtains by the following method：a.
Premixing：The aliphatic acid of the parts by weight, propylene glycol and palm-kernel oil are pre-mixed, premix is obtained；B. in preparing
Medicament extracting solution：Dry Radix Glycyrrhizae and soapberry fruit are taken, the warm water immersion for being equivalent to 7 times of its weight is added, then boils extraction,
Until the proportion of gained extracting solution is 1.1, stop extraction, filtering is to get to Chinese medicine extract；C. saponification：By premix plus
Heat arrives 80-85 DEG C, then the sodium chloride, chelating agent and Chinese medicine extract of above-mentioned parts by weight are added to mixed liquor after mixing
In, saponification is carried out, the zeolite powder of above-mentioned parts by weight is added after saponification is complete in reaction time 15min, mixes
Uniformly, soap base is obtained；D. neat soap is molded：By soap base after vacuum spray drying, extruding, homogeneous, refined and pelletizing, you can obtain
Neat soap；
(2) tea fruit pre-processes：By tea fruit decladding, tea seed kernel is taken to crush, the tea seed kernel after crushing, which is carried out microwave, to be done
The frequency of dry processing, first time microwave drying is 900MHz, drying time 115s；The frequency of second of microwave drying is
920MHz, drying time 80s；It is 1 that solid-to-liquid ratio, that is, w/v will be pressed in tea seed kernel after microwave drying:4 ratio is added dense
It spends for 35% ethanol solution as extracting solution, slurries are carried out heating water bath by homogenate, and bath temperature is 85 DEG C, and water bath time is
1.2h；Centrifuging and taking upper layer edible vegetable oil, vacuum drying, it is spare to obtain tea oil；
(3) soap lye is prepared：Sodium hydroxide is slowly added into deionized water, is quickly stirred with alkaline-resisting blender while adding
It mixes, sodium hydroxide is dissolved completely in water postcooling to 42 DEG C, obtains aqueous slkali；By stearic acid, tea oil, neat soap, antipruritic auxiliary agent, increasing
Fragrant auxiliary agent is added in oil phase pot and is heated to 80 DEG C, stirs evenly, obtains mixed liquor A；Aqueous slkali is poured slowly into dress mixed liquor A
It in container, while quickly being stirred with alkaline-resisting blender, until mixed solution A surface can mark complete 8 word, you can
To soap lye；
(4) handmade soap is prepared：Mold clean is clean, an olive oil is dipped in brush time inside mold with brush, and soap lye is fallen
Enter mold, then mold is covered with plastic film, in being placed 1 day in 34 DEG C of incubators, takes out, be placed at shady and cool ventilation, put
Four to eight weeks, you can obtain handmade soap finished product.
Embodiment 3
The present embodiment provides a kind of preparation methods of tea fruit handmade soap, include the following steps：
(1) preparation of raw material：Prepare following raw material according to parts by weight：48 parts of tea fruit, 35 parts of neat soap, flavouring additives 10
Part, 10 parts of antipruritic auxiliary agent, 10 parts of sodium hydroxide, 9 parts of stearic acid and 60 parts of deionized water；Wherein, flavouring additives are by following weight
The raw material composition of part：10 parts of sweet osmanthus, 8 parts of cordate telosma, 8 parts of lemon grass (Cymbopogon citratus), 6 parts of bean cotyledon perfume, 4 parts of sodium alginate, 22 parts of ethyl alcohol and steaming
Appropriate distilled water；Antipruritic auxiliary agent is made of the raw material of following parts by weight：8 parts of rhizoma zingiberis, 8 parts of asarum, deep 12 parts of knuckle-tooth violet, folium artemisiae argyi 10
9 parts of part, 9 parts of Herba Andrographitis and olive oil；Neat soap is made of the raw material of following parts by weight：20 parts of aliphatic acid, 9 parts of palm-kernel oil, third
8 parts of glycol, 8 parts of zeolite powder, 0.3 part of chelating agent, 3 parts of sodium chloride, 10 parts of Radix Glycyrrhizae, 9 parts of soapberry fruit；Neat soap passes through with lower section
Method obtains：A. it is pre-mixed：The aliphatic acid of the parts by weight, propylene glycol and palm-kernel oil are pre-mixed, premix is obtained；
B. Chinese medicine extract is prepared：Dry Radix Glycyrrhizae and soapberry fruit are taken, the warm water immersion for being equivalent to 10 times of its weight is added, then
Extraction is boiled, until the proportion of gained extracting solution is 1.2, stops extraction, filtering is to get to Chinese medicine extract；C. saponification：It will be pre-
Mixed liquor is heated to 85 DEG C, then the sodium chloride, chelating agent and Chinese medicine extract of above-mentioned parts by weight is added to after mixing mixed
It closing in liquid, carries out saponification, the zeolite powder of above-mentioned parts by weight is added after saponification is complete in reaction time 18min,
It is uniformly mixed, obtains soap base；D. neat soap is molded：By soap base after vacuum spray drying, extruding, homogeneous, refined and pelletizing, you can
Obtain neat soap；
(2) tea fruit pre-processes：By tea fruit decladding, tea seed kernel is taken to crush, the tea seed kernel after crushing, which is carried out microwave, to be done
The frequency of dry processing, first time microwave drying is 1000MHz, drying time 130s；The frequency of second of microwave drying is
950MHz, drying time 100s；It is 1 that solid-to-liquid ratio, that is, w/v will be pressed in tea seed kernel after microwave drying:6 ratio is added
Slurries are carried out heating water bath by a concentration of 50% ethanol solution as extracting solution, homogenate, and bath temperature is 100 DEG C, water bath time
For 2.0h；Centrifuging and taking upper layer edible vegetable oil, vacuum drying, it is spare to obtain tea oil；
(3) soap lye is prepared：Sodium hydroxide is slowly added into deionized water, is quickly stirred with alkaline-resisting blender while adding
It mixes, sodium hydroxide is dissolved completely in water postcooling to 45 DEG C, obtains aqueous slkali；By stearic acid, tea oil, neat soap, antipruritic auxiliary agent, increasing
Fragrant auxiliary agent is added in oil phase pot and is heated to 90 DEG C, stirs evenly, obtains mixed liquor A；Aqueous slkali is poured slowly into dress mixed liquor A
It in container, while quickly being stirred with alkaline-resisting blender, until mixed solution A surface can mark complete 8 word, you can
To soap lye；
(4) handmade soap is prepared：Mold clean is clean, an olive oil is dipped in brush time inside mold with brush, and soap lye is fallen
Enter mold, then mold is covered with plastic film, in being placed 2 days in 38 DEG C of incubators, takes out, be placed at shady and cool ventilation, put
Four to eight weeks, you can obtain handmade soap finished product.
Compliance test result
In order to illustrate more clearly of the characteristic of the present invention, now divide 4 groups of progress or less comparative analysis and compliance test result：
First group：Handmade soap prepared by embodiment 2；
Second group：Self-control neat soap is changed to the common neat soap bought on the market, other modes are carried out in strict accordance with embodiment 2；
Third group：Flavouring additives are removed, other modes are carried out in strict accordance with embodiment 2；
4th group：Antipruritic auxiliary agent is removed, other modes are carried out in strict accordance with embodiment 2.
Test explanation：Subject is the women of routine use skin nursing products.40 subjects are randomly divided into 4
Group provides 0-10 points to indices, and 10 points of representatives are most satisfied, and 0 point of representative is dissatisfied；Test result is as shown in table 1.
1 handmade soap experience situation of table compares
| First group | Second group | Third group | 4th group | |
| Cleannes | 9.2 | 8.0 | 8.6 | 8.5 |
| With rear comfort level | 9.5 | 8.3 | 8.9 | 8.7 |
| Moisture retention | 8.9 | 7.8 | 8.8 | 8.7 |
| Fragrance | 9.4 | 9.3 | 7.9 | 9.0 |
| Antipruritic effect | 9.3 | 9.5 | 9.4 | 8.2 |
As can be drawn from Table 1, handmade soap of the invention has better maintenance effect to skin.
Although above the present invention is described in detail with a general description of the specific embodiments,
On the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Cause
This, these modifications or improvements, belong to the scope of protection of present invention without departing from theon the basis of the spirit of the present invention.
Claims (6)
1. a kind of preparation method of tea fruit handmade soap, which is characterized in that include the following steps：
(1) preparation of raw material：Prepare following raw material according to parts by weight：35-48 parts of tea fruit, 20-35 parts of neat soap, flavouring additives 5-
40-60 parts of 10 parts, auxiliary agent 5-10 parts antipruritic, 5-10 parts of sodium hydroxide, 3-9 parts of stearic acid and deionized water；
(2) tea fruit pre-processes：By tea fruit decladding, tea seed kernel is taken to crush, the tea seed kernel after crushing is carried out at microwave drying
The frequency of reason, first time microwave drying is 800-1000MHz, drying time 90-130s；The frequency of second of microwave drying is
900-950MHz, drying time 65-100s；It is 1 that solid-to-liquid ratio, that is, w/v will be pressed in tea seed kernel after microwave drying:2-6's
A concentration of 20-50% ethanol solutions are added as extracting solution in ratio, and slurries are carried out heating water bath, centrifuging and taking upper layer is clear by homogenate
Oil, vacuum drying, it is spare to obtain tea oil；
(3) soap lye is prepared：Sodium hydroxide is slowly added into deionized water, is quickly stirred with alkaline-resisting blender while adding,
Sodium hydroxide is dissolved completely in water postcooling to 40-45 DEG C, obtains aqueous slkali；By stearic acid, tea oil, neat soap, antipruritic auxiliary agent, increasing
Fragrant auxiliary agent is added in oil phase pot and is heated to 70-90 DEG C, stirs evenly, obtains mixed liquor A；Aqueous slkali is poured slowly into dress mixed liquor
It in the container of A, while quickly being stirred with alkaline-resisting blender, until mixed solution A surface can mark complete 8 word, i.e.,
Soap lye can be obtained；
(4) handmade soap is prepared：Mold clean is clean, an olive oil is dipped in brush time inside mold with brush, and soap lye is poured into mould
Tool, then covers mold with plastic film, in being placed 1-2 days in 30-38 DEG C of incubator, takes out, is placed at shady and cool ventilation, puts
Four to eight weeks, you can obtain handmade soap finished product.
2. a kind of preparation method of tea fruit handmade soap according to claim 1, which is characterized in that water in the step (2)
Bath temperature is 70-100 DEG C, water bath time 0.5-2.0h.
3. a kind of preparation method of tea fruit handmade soap according to claim 1, which is characterized in that the neat soap is by following heavy
Measure the raw material composition of part：10-20 parts of aliphatic acid, 3-9 parts of palm-kernel oil, 2-8 parts of propylene glycol, 2-8 parts of zeolite powder, chelating agent 0.1-
0.3 part, 1-3 parts of sodium chloride, 3-10 parts of Radix Glycyrrhizae, 3-9 parts of soapberry fruit.
4. a kind of preparation method of tea fruit handmade soap according to claim 3, which is characterized in that the neat soap passes through following
Method obtains：
A. it is pre-mixed：The aliphatic acid of the parts by weight, propylene glycol and palm-kernel oil are pre-mixed, premix is obtained；
B. Chinese medicine extract is prepared：Dry Radix Glycyrrhizae and soapberry fruit are taken, the warm water leaching for being equivalent to 5-10 times of its weight is added
Bubble, then boils extraction, until the proportion of gained extracting solution is 1.0-1.2, stops extraction, filters to get to Chinese medicine extract；
C. saponification：Premix is heated to 80-85 DEG C, then by the sodium chloride, chelating agent and Chinese medicine extract of above-mentioned parts by weight
It is added in mixed liquor after mixing, carries out saponification, reaction time 12-18min adds after saponification is complete
Enter the zeolite powder of above-mentioned parts by weight, is uniformly mixed, obtains soap base；
D. neat soap is molded：By soap base after vacuum spray drying, extruding, homogeneous, refined and pelletizing, you can obtain neat soap.
5. a kind of preparation method of tea fruit handmade soap according to claim 1, which is characterized in that the flavouring additives by with
The raw material of lower parts by weight forms：5-10 parts of sweet osmanthus, 3-8 parts of cordate telosma, 3-8 parts of lemon grass (Cymbopogon citratus), 2-6 parts of bean cotyledon perfume (or spice), sodium alginate 2-4
Part, 12-22 parts of ethyl alcohol and distillation appropriate amount of water.
6. a kind of preparation method of tea fruit handmade soap according to claim 1, which is characterized in that the antipruritic auxiliary agent by with
The raw material of lower parts by weight forms：3-8 parts of rhizoma zingiberis, 3-8 parts of asarum, deep 6-12 parts of knuckle-tooth violet, 5-10 parts of folium artemisiae argyi, Herba Andrographitis 4-9
5-9 parts of part and olive oil.
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| CN201810571879.3A CN108531321A (en) | 2018-05-31 | 2018-05-31 | A kind of preparation method of tea fruit handmade soap |
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| CN201810571879.3A CN108531321A (en) | 2018-05-31 | 2018-05-31 | A kind of preparation method of tea fruit handmade soap |
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| CN108531321A true CN108531321A (en) | 2018-09-14 |
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| CN201810571879.3A Pending CN108531321A (en) | 2018-05-31 | 2018-05-31 | A kind of preparation method of tea fruit handmade soap |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109112009A (en) * | 2018-09-25 | 2019-01-01 | 安顺市永烁科技有限公司 | A kind of detergent and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102311870A (en) * | 2011-08-30 | 2012-01-11 | 南昌大学 | Method for extracting tea oil, |
| CN103045419A (en) * | 2013-01-24 | 2013-04-17 | 广州丹奇日用化工厂有限公司 | Handmade soap composition, handmade soap and preparation method thereof |
| CN106867721A (en) * | 2017-03-31 | 2017-06-20 | 贵州省镇远县古镇米业有限责任公司 | A kind of camellia oil handmade soap and preparation method thereof |
| CN107164123A (en) * | 2017-05-27 | 2017-09-15 | 梁慰爱 | A kind of neat soap and the method that laundry soap is prepared using the neat soap |
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2018
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102311870A (en) * | 2011-08-30 | 2012-01-11 | 南昌大学 | Method for extracting tea oil, |
| CN103045419A (en) * | 2013-01-24 | 2013-04-17 | 广州丹奇日用化工厂有限公司 | Handmade soap composition, handmade soap and preparation method thereof |
| CN106867721A (en) * | 2017-03-31 | 2017-06-20 | 贵州省镇远县古镇米业有限责任公司 | A kind of camellia oil handmade soap and preparation method thereof |
| CN107164123A (en) * | 2017-05-27 | 2017-09-15 | 梁慰爱 | A kind of neat soap and the method that laundry soap is prepared using the neat soap |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109112009A (en) * | 2018-09-25 | 2019-01-01 | 安顺市永烁科技有限公司 | A kind of detergent and preparation method thereof |
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Application publication date: 20180914 |