CN112680279A - Natural medicinal fragrant plant composite essential oil and essential oil soap with sterilizing and anti-inflammation functions and preparation method thereof - Google Patents

Natural medicinal fragrant plant composite essential oil and essential oil soap with sterilizing and anti-inflammation functions and preparation method thereof Download PDF

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Publication number
CN112680279A
CN112680279A CN202011425416.XA CN202011425416A CN112680279A CN 112680279 A CN112680279 A CN 112680279A CN 202011425416 A CN202011425416 A CN 202011425416A CN 112680279 A CN112680279 A CN 112680279A
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essential oil
parts
soap
chrysanthemum
pepper
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Inventor
晏家瑛
陈岩冰
陈娅
何天平
曾维友
周於强
池浩
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CHONGQING INSTITUTE OF DAILY-USED CHEMICAL INDUSTRY
Chongqing Academy of Science and Technology
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CHONGQING INSTITUTE OF DAILY-USED CHEMICAL INDUSTRY
Chongqing Academy of Science and Technology
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Abstract

The invention belongs to the field of daily-use cleaning products, and particularly relates to natural medicine-fragrance plant composite essential oil and essential oil soap with functions of sterilization and inflammation diminishing and a preparation method thereof. The natural medicine-fragrance plant composite essential oil is prepared from 1-5 parts of sweet wormwood, 1-5 parts of pepper, 2-5 parts of chrysanthemum and 1-5 parts of honeysuckle. The method comprises the steps of firstly, crushing and mixing sweet wormwood, pepper, chrysanthemum and honeysuckle, and distilling to obtain the composite medicine fragrance plant essential oil; heating the soap in water bath at 50-70 deg.C until the soap base is completely melted to obtain liquid soap base; and adding the composite medicinal fragrant plant essential oil into the liquid soap base according to the weight ratio, and uniformly mixing to obtain the essential oil soap. The prepared essential oil soap has natural herbal fragrance, is mild and non-irritant to skin, has the effects of inhibiting bacteria, killing bacteria and moistening skin, and can effectively inhibit the formation of bacteria on the surface of the skin.

Description

Natural medicinal fragrant plant composite essential oil and essential oil soap with sterilizing and anti-inflammation functions and preparation method thereof
Technical Field
The invention belongs to the field of daily-use cleaning products, and particularly relates to natural medicine-fragrance plant composite essential oil and essential oil soap capable of sterilizing and diminishing inflammation and a preparation method thereof.
Background
Along with the development of social economy, the living standard of people is increasingly improved, and higher requirements on the quality of life are also put forward. Particularly, in the past, people have higher requirements on daily cleaning products, and the soap not only meets the cleaning function of the soap, but also hopes to clean the skin and simultaneously have the effects of sterilizing, inhibiting bacteria, moistening the skin, diminishing inflammation and the like. The essential oil soap is a perfumed soap containing natural plant essential oil. The natural plant essential oil is an active component aromatic substance extracted from flowers, leaves, stems, roots or fruits of plants by steam distillation, extrusion, cold soaking or solvent extraction. The natural plant extract has the effects of resisting bacteria and viruses, diminishing inflammation, soothing the nerves, restoring consciousness and the like, and can meet the pursuit of people for high-quality life. The medicinal fragrant plant refers to a Chinese medicinal material with double effects of fragrance and drug effect, and can be used as spice and medicinal material. The herb fragrance plant extract is processed by cold pressing or distillation, which is different from the common traditional Chinese medicine processing method, and other common traditional Chinese medicines are processed by decoction method. The odor of the medicinal fragrant plant extract is more easily accepted by people, so the clinical application effect of the medicinal fragrant plant extract is stronger than that of common traditional Chinese medicines.
The invention discloses CN201510571492.4 natural plant flower fragrance type essential oil soap with an antibacterial function, which comprises rosemary essential oil, marigold essential oil, lavender essential oil, rose essential oil, vetiver essential oil and soap base. The essential oil soap has strong fragrance and lasting fragrance, has the effects of inhibiting bacteria and killing bacteria, can improve the mental state of a user, and has an excitation effect. The invention mainly uses the flower fragrance type essential oil, mainly highlights the mental excitation effect of the fragrance to users, and only has the secondary auxiliary effect of bacteriostasis and sterilization.
CN201410355444.7 the invention relates to microcapsule plant essential oils and also to essential oil soaps containing plant microcapsules. In addition, the preparation method of the microcapsule plant essential oil and the preparation method of the essential oil soap are also provided. The microcapsule plant essential oil takes plant essential oil as a core, and at least three layers of coating layers are coated outside the plant essential oil, so that the original state and properties of the plant essential oil can be kept. The invention mainly discloses a special plant essential oil structure and an essential oil soap combined with a soap base. The microstructure of the essential oil soap is mainly highlighted, and a specific essential oil formula and the efficacy thereof are not disclosed.
CN201210516639.6 discloses an essential oil soap with sterilization and bacteriostasis functions, which mainly comprises sweet almond oil, wheat germ oil, tea tree essential oil, patchouli essential oil, melaleuca viridis essential oil, vetiver essential oil, myrrh essential oil, cedar essential oil and soap base.
CN101157884A discloses a soap containing plant essential oil, which comprises 1-3 parts of geranium essential oil, 1-3 parts of chamomile essential oil, 1-3 parts of honeysuckle essential oil, 1-3 parts of citronella essential oil, 3-6 parts of thyme essence and 82-93 parts of soap matrix. The patent only describes the function of sterilizing and relieving itching in the specification, but does not describe the specific effect. Moreover, in this patent, relatively irritant essential oils such as citronella essential oil are used, and the amount of the essential oil used is 3%, which irritates the skin.
CN200810095533.7 discloses a health soap which is prepared by mixing concentrated solution prepared by using traditional Chinese medicines of radix isatidis, ginger, radix scutellariae, houttuynia cordata, dandelion, honeysuckle and pepper as main raw materials with a certain proportion of cleaning and decontamination components and carrying out modern production process. The soap of the patent contains a plurality of chemical raw materials, and the production process is complex, and the soap is specifically explained about the sterilization effect.
CN108770880A discloses a natural Chinese herbal medicine mixed antibacterial and degerming agent, which comprises the following components in parts by weight: 15-22 parts of honeysuckle, 12-18 parts of fructus forsythiae, 23-30 parts of folium artemisiae argyi, 11-16 parts of golden cypress, 8-14 parts of selfheal, 3-10 parts of burdock, 2-8 parts of cocklebur fruit, 10-15 parts of radix isatidis and 1-6 parts of houttuynia cordata. The patent only describes the sterilization effect in the specification, but does not specifically describe the sterilization effect.
Therefore, in order to overcome the defects of the technologies, it is necessary to develop an essential oil soap which has natural fragrance, good skin cleaning effect, mild and no stimulation to skin, and has the effects of bacteriostasis, sterilization and skin moistening.
Disclosure of Invention
In view of the above, the invention provides a natural medicinal fragrant plant composite essential oil with sterilization and inflammation diminishing functions. The plant composite essential oil is not added with other flavoring agents and bactericides, namely any chemical raw material, and achieves the purposes of sterilization and aroma enhancement by the natural bacteriostasis and sterilization effects and the fragrance of each plant component of the composite essential oil.
The natural medicine-fragrance plant composite essential oil is prepared by mixing sweet wormwood, pepper, chrysanthemum and honeysuckle and extracting.
The herba Artemisiae Annuae has antibacterial, antiviral, antioxidant, insecticidal, and mosquito repellent effects; the pricklyash peel has the functions of sterilization, bacteriostasis, inflammation diminishing, calming and the like; the flos Chrysanthemi has antiinflammatory, antibacterial, and antiallergic effects; the flos Lonicerae has effects of reducing inflammation, keeping moisture, caring skin and caring skin.
Further, by weight, 1-5 parts of sweet wormwood, 1-5 parts of pepper, 1-3 parts of chrysanthemum and 1-5 parts of honeysuckle.
Preferably, the sweet wormwood herb is 1-5 parts, the pepper is 1-5 parts, and the honeysuckle is 2-5 parts by weight.
Preferably, the traditional Chinese medicine composition comprises, by weight, 5 parts of sweet wormwood, 1-5 parts of pepper, 1-3 parts of chrysanthemum and 1-5 parts of honeysuckle.
Preferably, the sweet wormwood herb is 1-5 parts, the pepper is 5 parts, the chrysanthemum is 1-3 parts, and the honeysuckle is 1-5 parts by weight.
Preferably, the sweet wormwood herb is 1-5 parts, the pepper is 1-5 parts, the chrysanthemum is 2 parts, and the honeysuckle is 1-5 parts by weight.
Preferably, the sweet wormwood herb is 1-5 parts, the pepper is 1-5 parts, the chrysanthemum is 1-3 parts, and the honeysuckle is 3 parts by weight.
Preferably, the Chinese herbal medicine comprises, by weight, 5 parts of sweet wormwood, 5 parts of pepper, 2 parts of chrysanthemum and 3 parts of honeysuckle.
Preferably, the sweet wormwood is unitary yang sweet wormwood, the pepper is Jiangjin pepper, the chrysanthemum is Hangzhou white chrysanthemum, and the honeysuckle is Xiushan honeysuckle. The medicine fragrance plants protected by national geographical sign products are obtained from unitary yang sweet wormwood herb, Jiangjin pricklyash peel, Xiushan honeysuckle flower and the like.
Preferably, the sweet wormwood, the pepper, the chrysanthemum and the honeysuckle are all dried.
Further, the extraction and preparation method of the natural medicinal fragrant plant composite essential oil comprises the following steps: pulverizing and uniformly mixing the sweet wormwood, the pepper, the chrysanthemum and the honeysuckle to obtain a mixture, taking 1-2 parts of the mixture, adding 5-10 parts of deionized water, distilling, and collecting essential oil.
Preferably, the sweet wormwood, the pepper, the chrysanthemum and the honeysuckle are crushed and uniformly mixed to obtain a mixture, 1-2 parts of the mixture is taken, 5-10 parts of deionized water is added, and distillation is carried out after soaking for 30-60 minutes.
Further, the distillation is specifically: heating to 50-70 deg.C, controlling temperature, heating for 10-15 min, heating to 100 deg.C, distilling, and collecting essential oil.
The invention also provides natural medicinal fragrant plant composite essential oil which comprises sweet wormwood herb essential oil, pepper essential oil, chrysanthemum essential oil and honeysuckle essential oil.
The invention also aims to provide the essential oil soap containing the natural medicinal fragrant plant composite essential oil. The essential oil soap not only has the common cleaning function, but also has the natural medicinal fragrance and the functions of sterilization, bacteriostasis, skin refreshment and inflammation diminishing. Moreover, the essential oil soap does not contain any chemical raw material and does not irritate the skin.
According to the invention, the unitary yang sweet wormwood, Jiangjin pricklyash peel, Xiushan honeysuckle and the like are innovatively used for obtaining the medicine fragrance plants protected by national geographic marking products, natural plant essential oil is extracted, and the prepared medicine fragrance plant essential oil soap has natural medicinal material fragrance, also has remarkable effects of sterilization, bacteriostasis, skin moistening, inflammation diminishing and the like, has a better effect than a single-component essential oil soap, is convenient to use and has a wide market prospect.
Further, the essential oil soap comprises, by weight, 5-10 parts of the natural medicinal fragrant plant composite essential oil and 90-100 parts of soap base.
Preferably, the essential oil soap comprises 5 parts by weight of the natural medicinal fragrant plant compound essential oil and 95 parts by weight of soap base.
Preferably, the essential oil soap comprises 8 parts by weight of the natural medicinal fragrant plant composite essential oil and 92 parts by weight of soap base.
Preferably, the essential oil soap comprises 10 parts by weight of the natural medicinal fragrant plant compound essential oil and 90 parts by weight of soap base.
Further, the soap base may be an existing product on the market, or may be a soap base prepared by any existing technique.
The invention also aims to provide a preparation method of the essential oil soap. The preparation method has simple process and mild conditions, and is suitable for industrial production.
The preparation method comprises the following steps:
(1) pulverizing herba Artemisiae Annuae, fructus Zanthoxyli, flos Chrysanthemi and flos Lonicerae, mixing, and distilling to obtain composite medicinal plant essential oil; heating the soap in water bath at 50-70 deg.C until the soap base is completely melted to obtain liquid soap base;
(2) and adding the composite medicinal fragrant plant essential oil into the liquid soap base according to the weight ratio, and uniformly mixing to obtain the essential oil soap.
Further, the essential oil soap is poured into a mold, is demoulded and taken out after being cooled and formed, and can be used after being placed in a shady and cool windproof place for two weeks.
The invention has the beneficial effects that:
(1) the essential oil soap contains various high-efficiency natural medicinal fragrant plant essential oils, and no chemical raw materials are added; wherein the herba Artemisiae Annuae essential oil has antibacterial, antiviral, antioxidant, insecticidal, and mosquito repellent effects; the essential oil of the pepper has the functions of sterilization, bacteriostasis, inflammation diminishing, tranquilization and the like; the chrysanthemum essential oil has the functions of diminishing inflammation, resisting bacteria, resisting allergy and the like; the flos Lonicerae essential oil has effects of reducing inflammation, keeping moisture, caring skin, etc.
(2) The natural medicinal-fragrance compound plant essential oil provided by the invention contains various medicinal-fragrance plant essential oils, has natural and fragrant medicinal fragrance, obvious sterilization and bacteriostasis effects, is natural and green, and is harmless to human bodies.
(3) The preparation process of the natural medicine-fragrance composite plant essential oil and the natural medicine-fragrance composite plant essential oil soap provided by the invention is simple, the equipment investment is low, the production process is easy to control, the large-scale production is easy, the finished product can directly act on skin, and the use is convenient.
Detailed Description
The examples are given for the purpose of better illustration of the invention, but the invention is not limited to the examples. Therefore, those skilled in the art should make insubstantial modifications and adaptations to the embodiments of the present invention in light of the above teachings and remain within the scope of the invention.
Example 1
(1) Formulation of
Compound medicinal fragrant plant essential oil: is prepared by mixing 2 parts of sweet wormwood herb, 2 parts of pepper, 2 parts of chrysanthemum and 2 parts of honeysuckle.
The essential oil soap containing the compound medicinal fragrant plant essential oil comprises the following components: 5 parts of compound medicinal fragrant plant essential oil and 95 parts of soap base.
(2) Preparation method
a. The dried sweet wormwood, the pepper, the chrysanthemum and the honeysuckle are crushed and mixed according to the proportion, and then the mixture is distilled to extract the essential oil.
b. Firstly, heating the soap on the basis of a water bath at 50-70 ℃ until the soap base is completely melted;
c. b, adding the composite medicinal fragrant plant essential oil obtained in the step a into the mixture obtained in the step b according to the weight ratio, mixing and uniformly stirring;
d. and c, pouring the product obtained in the step c into a mold, demolding and taking out after cooling and molding, and placing the product in a shady and cool windproof place for two weeks for use.
Example 2
(1) Formulation of
Compound medicinal fragrant plant essential oil: is prepared by mixing 3 parts of sweet wormwood herb, 3 parts of pepper, 2 parts of chrysanthemum and 2 parts of honeysuckle.
The essential oil soap containing the compound medicinal fragrant plant essential oil comprises the following components: 8 parts of compound medicinal fragrant plant essential oil and 92 parts of soap base.
(2) Preparation method
a. The dried sweet wormwood, the pepper, the chrysanthemum and the honeysuckle are crushed and mixed according to the proportion, and then the mixture is distilled to extract the essential oil.
b. Firstly, heating the soap on the basis of a water bath at 50-70 ℃ until the soap base is completely melted;
c. b, adding the composite medicinal fragrant plant essential oil obtained in the step a into the mixture obtained in the step b according to the weight ratio, mixing and uniformly stirring;
d. and c, pouring the product obtained in the step c into a mold, demolding and taking out after cooling and molding, and placing the product in a shady and cool windproof place for two weeks for use.
Example 3
(1) Formulation of
Compound medicinal fragrant plant essential oil: is prepared by mixing 5 parts of sweet wormwood, 5 parts of pepper, 2 parts of chrysanthemum and 3 parts of honeysuckle.
The essential oil soap containing the compound medicinal fragrant plant essential oil comprises the following components: 10 parts of compound medicinal fragrant plant essential oil and 90 parts of soap base.
(2) Preparation method
a. The dried sweet wormwood, the pepper, the chrysanthemum and the honeysuckle are crushed and mixed according to the proportion, and then the mixture is distilled to extract the essential oil.
b. Firstly, heating the soap on the basis of a water bath at 50-70 ℃ until the soap base is completely melted;
c. b, adding the composite medicinal fragrant plant essential oil obtained in the step a into the mixture obtained in the step b according to the weight ratio, mixing and uniformly stirring;
d. and c, pouring the product obtained in the step c into a mold, demolding and taking out after cooling and molding, and placing the product in a shady and cool windproof place for two weeks for use.
Comparative example 1
(1) Formulation of
Medicinal fragrant plant essential oil: is prepared from 2 parts of chrysanthemum.
Essential oil soap containing medicinal fragrant plant essential oil: 5 parts of medicinal fragrant plant essential oil and 95 parts of soap base.
(2) Preparation method
a. The dried chrysanthemum is crushed according to the proportion and distilled to extract the essential oil.
b. Firstly, heating the soap on the basis of a water bath at 50-70 ℃ until the soap base is completely melted;
c. adding the chrysanthemum essential oil obtained in the step a into the chrysanthemum essential oil obtained in the step b according to the weight ratio, mixing and uniformly stirring;
d. and c, pouring the product obtained in the step c into a mold, demolding and taking out after cooling and molding, and placing the product in a shady and cool windproof place for two weeks for use.
Comparative example 2
Certain brand flower fragrance type degerming soap is sold in the market.
Test of use effects experiment:
1. sensory and efficacy evaluation test
The present invention is further illustrated by the following detailed description and functional studies.
The essential oil soaps of examples 1 to 3 and comparative examples 1 to 2 were tried by testers, respectively, who consisted of 50 persons and were aged between 25 and 60 years.
The testers firstly moisten the skins of the face and the hands by water, wet the essential oil soap on the palms, rub and foam the palms, slowly make a circle on the face and rub the two sides of the skins of the hands, and mark the skins after the skins are washed clean by clear water.
According to the evaluation of the testers on the smell, the use comfort and the skin appearance after use, the evaluation is carried out at room temperature, the evaluation is recorded, and the average value is taken. The evaluation criteria are as follows:
regarding odor (30 points): the smell is not pungent, and the natural fragrance is better; the smell is pungent, and the strong flavor is not good;
regarding comfort (30 points): the feeling is not irritating to the skin, the skin is smooth, and the washing is easy and clean; the skin is slightly irritated in feeling, the washing is not clean, and the feeling of residue is not good;
skin feel after use (40 points): after the skin care product is used, the skin feels clean and is not tight; after the skin cleansing cream is used, the skin cleansing effect is poor, and the skin is not tight;
the results are shown in Table 1.
TABLE 1 statistics of the effectiveness of the trials of essential oil soaps
Figure RE-GDA0002938328050000101
As can be seen from the above table, examples 1 and 3 and comparative example 2 are relatively good in terms of odor, but according to the ingredient table of comparative example 2, a floral essence is added thereto, which is pleasant in odor but not a natural odor, and is not beneficial to the human body. The former is superior to the latter in the effect of comparative example 1 and comparative example 2, but is inferior to examples 1 to 3, both of which contain the complex medicinal plant essential oil. Among them, example 3 is most effective in terms of odor, skin comfort, and the like.
2. Product testing
The essential oil soaps of examples 1-3 and comparative examples 1-2 were subjected to bacteriostatic performance tests, and the obtained test results are shown in table 2 with reference to QB/T2738-.
TABLE 2 results of the bacteriostatic properties test
Figure RE-GDA0002938328050000111
As can be seen from the above table, examples 1 to 3 have a good bacteriostatic effect, and comparative example 2 shows that the chemical bacteriostatic component is added according to the ingredient table of comparative example 2. The examples 1 to 3 all adopt the compound drug essential oil, and the bacteriostatic effect is better than that of the comparative example 1 (single essential oil).
Finally, the above embodiments are only for illustrating the technical solutions of the present invention and not for limiting, although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions may be made to the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention, and all of them should be covered in the claims of the present invention.

Claims (10)

1. The natural medicine-fragrance plant composite essential oil is characterized by being prepared by mixing sweet wormwood, pepper, chrysanthemum and honeysuckle and extracting.
2. The natural medicinal fragrant plant composite essential oil as claimed in claim 1, wherein the natural medicinal fragrant plant composite essential oil comprises, by weight, 1-5 parts of sweet wormwood herb, 1-5 parts of pepper, 1-3 parts of chrysanthemum and 1-5 parts of honeysuckle flower.
3. The natural medicinal fragrant plant composite essential oil as claimed in claim 1, wherein the natural medicinal fragrant plant composite essential oil comprises, by weight, 5 parts of sweet wormwood herb, 5 parts of pepper, 2 parts of chrysanthemum and 3 parts of honeysuckle flower.
4. The natural medicinal fragrant plant composite essential oil according to any one of claims 1 to 3, wherein the sweet wormwood is Yueyang sweet wormwood, the pepper is Jiangjin pepper, the chrysanthemum is Hangzhou white chrysanthemum, and the honeysuckle is Xiushan honeysuckle.
5. The natural medicinal fragrant plant composite essential oil according to any one of claims 1 to 3, wherein the sweet wormwood herb, the pepper, the chrysanthemum and the honeysuckle are all dried.
6. The natural medicinal fragrant plant composite essential oil according to any one of claims 1 to 3, wherein the natural medicinal fragrant plant composite essential oil is prepared by a specific method comprising the following steps: and (2) crushing and uniformly mixing the sweet wormwood, the pepper, the chrysanthemum and the honeysuckle to obtain a mixture, taking 1-2 parts of the mixture, adding 5-10 parts of deionized water, distilling, and collecting essential oil.
7. The natural medicine-fragrance plant composite essential oil is characterized by comprising sweet wormwood herb essential oil, pepper essential oil, chrysanthemum essential oil and honeysuckle essential oil.
8. An essential oil soap comprising the natural medicinal fragrant plant composite essential oil according to any one of claims 1 to 6.
9. The essential oil soap according to claim 8, wherein the essential oil soap comprises 5-10 parts by weight of the natural medicinal and fragrant plant composite essential oil and 90-100 parts by weight of soap base.
10. A process for the preparation of the essential oil soap according to any one of claims 8 to 9, characterized in that it comprises the following steps carried out:
(1) pulverizing herba Artemisiae Annuae, fructus Zanthoxyli, flos Chrysanthemi and flos Lonicerae, mixing, and distilling to obtain composite medicinal plant essential oil; heating the soap in water bath at 50-70 deg.C until the soap base is completely melted to obtain liquid soap base;
(2) and adding the composite medicinal fragrant plant essential oil into the liquid soap base according to the weight ratio, and uniformly mixing to obtain the essential oil soap.
CN202011425416.XA 2020-12-09 2020-12-09 Natural medicinal fragrant plant composite essential oil and essential oil soap with sterilizing and anti-inflammation functions and preparation method thereof Pending CN112680279A (en)

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Application publication date: 20210420