CN113186045A - Preparation method of sweet wormwood essential oil soap - Google Patents
Preparation method of sweet wormwood essential oil soap Download PDFInfo
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- CN113186045A CN113186045A CN202110432169.4A CN202110432169A CN113186045A CN 113186045 A CN113186045 A CN 113186045A CN 202110432169 A CN202110432169 A CN 202110432169A CN 113186045 A CN113186045 A CN 113186045A
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- parts
- essential oil
- soap
- sweet wormwood
- oil soap
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- 239000000344 soap Substances 0.000 title claims abstract description 70
- 239000000341 volatile oil Substances 0.000 title claims abstract description 39
- 235000001405 Artemisia annua Nutrition 0.000 title claims abstract description 38
- 240000000011 Artemisia annua Species 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 33
- KJXSIXMJHKAJOD-LSDHHAIUSA-N (+)-dihydromyricetin Chemical compound C1([C@@H]2[C@H](C(C3=C(O)C=C(O)C=C3O2)=O)O)=CC(O)=C(O)C(O)=C1 KJXSIXMJHKAJOD-LSDHHAIUSA-N 0.000 claims abstract description 30
- 239000002502 liposome Substances 0.000 claims abstract description 16
- 235000011034 Rubus glaucus Nutrition 0.000 claims abstract description 15
- 244000235659 Rubus idaeus Species 0.000 claims abstract description 15
- 235000009122 Rubus idaeus Nutrition 0.000 claims abstract description 15
- KQILIWXGGKGKNX-UHFFFAOYSA-N dihydromyricetin Natural products OC1C(=C(Oc2cc(O)cc(O)c12)c3cc(O)c(O)c(O)c3)O KQILIWXGGKGKNX-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000012046 mixed solvent Substances 0.000 claims abstract description 13
- 241000157282 Aesculus Species 0.000 claims abstract description 12
- 229960003333 chlorhexidine gluconate Drugs 0.000 claims abstract description 12
- YZIYKJHYYHPJIB-UUPCJSQJSA-N chlorhexidine gluconate Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O.C1=CC(Cl)=CC=C1NC(=N)NC(=N)NCCCCCCNC(=N)NC(=N)NC1=CC=C(Cl)C=C1 YZIYKJHYYHPJIB-UUPCJSQJSA-N 0.000 claims abstract description 12
- 235000010181 horse chestnut Nutrition 0.000 claims abstract description 12
- 235000021122 unsaturated fatty acids Nutrition 0.000 claims abstract description 12
- 150000004670 unsaturated fatty acids Chemical class 0.000 claims abstract description 12
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims abstract description 11
- 244000248021 Vitex negundo Species 0.000 claims abstract description 11
- 235000013427 Vitex negundo var incisa Nutrition 0.000 claims abstract description 11
- 235000014961 Vitex negundo var negundo Nutrition 0.000 claims abstract description 11
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 11
- 235000014956 negundo chastetree Nutrition 0.000 claims abstract description 11
- 239000000600 sorbitol Substances 0.000 claims abstract description 11
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 10
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 9
- 244000068988 Glycine max Species 0.000 claims abstract description 9
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 9
- GOMNOOKGLZYEJT-UHFFFAOYSA-N isoflavone Chemical compound C=1OC2=CC=CC=C2C(=O)C=1C1=CC=CC=C1 GOMNOOKGLZYEJT-UHFFFAOYSA-N 0.000 claims abstract description 9
- CJWQYWQDLBZGPD-UHFFFAOYSA-N isoflavone Natural products C1=C(OC)C(OC)=CC(OC)=C1C1=COC2=C(C=CC(C)(C)O3)C3=C(OC)C=C2C1=O CJWQYWQDLBZGPD-UHFFFAOYSA-N 0.000 claims abstract description 9
- 235000008696 isoflavones Nutrition 0.000 claims abstract description 9
- 239000012141 concentrate Substances 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims description 25
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 10
- 239000012188 paraffin wax Substances 0.000 claims description 8
- 238000007789 sealing Methods 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical group OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 238000007599 discharging Methods 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000009423 ventilation Methods 0.000 claims description 5
- 244000269722 Thea sinensis Species 0.000 claims description 4
- 150000007513 acids Chemical class 0.000 claims description 4
- ONJQDTZCDSESIW-UHFFFAOYSA-N polidocanol Chemical compound CCCCCCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO ONJQDTZCDSESIW-UHFFFAOYSA-N 0.000 claims description 4
- 239000003963 antioxidant agent Substances 0.000 claims description 3
- 230000003078 antioxidant effect Effects 0.000 claims description 3
- 235000006708 antioxidants Nutrition 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- JQWAHKMIYCERGA-UHFFFAOYSA-N (2-nonanoyloxy-3-octadeca-9,12-dienoyloxypropoxy)-[2-(trimethylazaniumyl)ethyl]phosphinate Chemical compound CCCCCCCCC(=O)OC(COP([O-])(=O)CC[N+](C)(C)C)COC(=O)CCCCCCCC=CCC=CCCCCC JQWAHKMIYCERGA-UHFFFAOYSA-N 0.000 claims description 2
- 238000001027 hydrothermal synthesis Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 229940057838 polyethylene glycol 4000 Drugs 0.000 claims description 2
- 239000003755 preservative agent Substances 0.000 claims description 2
- 230000002335 preservative effect Effects 0.000 claims description 2
- 235000003687 soy isoflavones Nutrition 0.000 claims description 2
- 241000049464 Artemisia apiacea Species 0.000 claims 6
- 235000011570 Artemisia caruifolia var apiacea Nutrition 0.000 claims 6
- 230000000694 effects Effects 0.000 abstract description 4
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 3
- 230000028327 secretion Effects 0.000 abstract description 2
- 238000005406 washing Methods 0.000 abstract description 2
- 208000013738 Sleep Initiation and Maintenance disease Diseases 0.000 abstract 1
- 230000003385 bacteriostatic effect Effects 0.000 abstract 1
- 239000004519 grease Substances 0.000 abstract 1
- 239000005556 hormone Substances 0.000 abstract 1
- 229940088597 hormone Drugs 0.000 abstract 1
- 206010022437 insomnia Diseases 0.000 abstract 1
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 8
- 210000003491 skin Anatomy 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 239000010410 layer Substances 0.000 description 5
- 241000588807 Bordetella Species 0.000 description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- 229960001484 edetic acid Drugs 0.000 description 4
- 239000000049 pigment Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 230000007547 defect Effects 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- 230000035699 permeability Effects 0.000 description 3
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 2
- 239000012466 permeate Substances 0.000 description 2
- 239000004408 titanium dioxide Substances 0.000 description 2
- 230000002087 whitening effect Effects 0.000 description 2
- 208000020154 Acnes Diseases 0.000 description 1
- 208000032544 Cicatrix Diseases 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- YJPIGAIKUZMOQA-UHFFFAOYSA-N Melatonin Natural products COC1=CC=C2N(C(C)=O)C=C(CCN)C2=C1 YJPIGAIKUZMOQA-UHFFFAOYSA-N 0.000 description 1
- 235000006679 Mentha X verticillata Nutrition 0.000 description 1
- 235000002899 Mentha suaveolens Nutrition 0.000 description 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 1
- IKMDFBPHZNJCSN-UHFFFAOYSA-N Myricetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC(O)=C(O)C(O)=C1 IKMDFBPHZNJCSN-UHFFFAOYSA-N 0.000 description 1
- 241001018563 Nekemias grossedentata Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 244000223014 Syzygium aromaticum Species 0.000 description 1
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 244000172533 Viola sororia Species 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 230000037336 dry skin Effects 0.000 description 1
- 230000003670 easy-to-clean Effects 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- DRLFMBDRBRZALE-UHFFFAOYSA-N melatonin Chemical compound COC1=CC=C2NC=C(CCNC(C)=O)C2=C1 DRLFMBDRBRZALE-UHFFFAOYSA-N 0.000 description 1
- 229960003987 melatonin Drugs 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229940116852 myricetin Drugs 0.000 description 1
- PCOBUQBNVYZTBU-UHFFFAOYSA-N myricetin Natural products OC1=C(O)C(O)=CC(C=2OC3=CC(O)=C(O)C(O)=C3C(=O)C=2)=C1 PCOBUQBNVYZTBU-UHFFFAOYSA-N 0.000 description 1
- 235000007743 myricetin Nutrition 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 238000010606 normalization Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 231100000241 scar Toxicity 0.000 description 1
- 230000037387 scars Effects 0.000 description 1
- 210000004927 skin cell Anatomy 0.000 description 1
- 230000005808 skin problem Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/045—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
Abstract
The invention provides a preparation method of sweet wormwood essential oil soap, and relates to the technical field of washing and caring articles. The sweet wormwood essential oil soap comprises the following components in parts by weight: 2-3 parts of sweet wormwood herb essential oil, 15-20 parts of unsaturated fatty acid, 10-15 parts of mixed solvent, 3-5 parts of sodium hydroxide, 1-2 parts of complex, 10-15 parts of nonionic surfactant, 0.1-0.5 part of chlorhexidine gluconate, 3-5 parts of multi-vesicular dihydromyricetin liposome, 1-2 parts of raspberry concentrate, 1-2 parts of soybean isoflavone, 1-2 parts of negundo chastetree fruit essence, 1-2 parts of horse chestnut essence, 0.5-1 part of bristlet flower extract, 3-5 parts of sorbitol and 0.5-1.5 parts of other auxiliary agents. The invention has outstanding antibacterial and bacteriostatic effects and long effective time, can improve hormone secretion and reduce grease generation, has sleep-aiding effect, can promote insomnia patients to gradually improve, and is very suitable for night use.
Description
Technical Field
The invention relates to the technical field of washing and caring articles, in particular to a preparation method of sweet wormwood essential oil soap.
Background
The sweet wormwood essential oil can quickly permeate into the surface layer of the skin, and can sterilize and diminish inflammation of the skin, clean the skin, whiten the skin, improve dry skin, reduce pores, remove acnes and scars and activate the skin.
The applicant finds that a Chinese patent discloses 'sweet wormwood soap and a preparation method thereof' through retrieval when applying the invention, the application number is '201711261525.0', the main components of the patent use titanium dioxide and pearl powder as whitening components, but the main effect is realized through external covering, and the titanium dioxide component is not easy to clean when being stained, but can not substantially lighten melanin. The application number of the artemisia annua handmade soap is 201911409862.9, although the ampelopsis grossedentata component in the main components of the artemisia annua handmade soap contains flavone such as myricetin and dihydromyricetin and polysaccharide antioxidant components, can remove free radicals in skin cells, particularly free radicals formed after hydroxyl loses an electron, and protects the skin from being damaged by carboxyl generated by the handmade soap, but the artemisia annua handmade soap has the defects of low water solubility, short biological half-life period and poor membrane permeability, and therefore innovative utilization of the artemisia annua handmade soap is needed.
Although some sweet wormwood essential oil soaps mainly used at night are added with clove, jasmine, rose, violet and mint to promote the relaxation of human bodies and improve sleep, the sweet wormwood essential oil soap mainly used at night is still lacked to regulate the sleep of the human bodies so as to naturally fade melanin and whiten the melanin.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a preparation method of sweet wormwood essential oil soap, which solves the problems that the vine tea ingredient in the prior art is low in water solubility, short in biological half-life period and poor in membrane permeability, and the market lacks of the special sweet wormwood essential oil soap at night.
(II) technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme: the preparation method of the sweet wormwood essential oil soap comprises the following steps of: 2-3 parts of sweet wormwood herb essential oil, 15-20 parts of unsaturated fatty acid, 10-15 parts of mixed solvent, 3-5 parts of sodium hydroxide, 1-2 parts of complex, 10-15 parts of nonionic surfactant, 0.1-0.5 part of chlorhexidine gluconate, 3-5 parts of multi-vesicular dihydromyricetin liposome, 1-2 parts of raspberry concentrate, 1-2 parts of soybean isoflavone, 1-2 parts of negundo chastetree fruit essence, 1-2 parts of horse chestnut essence, 0.5-1 part of bristlet flower extract, 3-5 parts of sorbitol and 0.5-1.5 parts of other auxiliary agents.
Preferably, the nonionic surfactant is any one of AES and AEO-9.
Preferably, the multivesicular dihydromyricetin liposome is prepared from vine tea components extracted by a hydrothermal method, egg yolk lecithin serving as a liposome template and polyethylene glycol 4000 serving as a modifying material.
Preferably, the mixed solvent is formed by mixing ethanol, propylene glycol and glycerol in equal amount.
Preferably, the unsaturated fatty acids are C18 acids and C14 acids in a ratio of 4: 1 are mixed to obtain the product.
Preferably, the complex is ethylenediaminetetraacetic acid.
Preferably, the other adjuvants are a kasone preservative and a BHT antioxidant in a ratio of 10: 1-2, and mixing.
A preparation method of sweet wormwood essential oil soap comprises the following preparation steps:
s1: adding unsaturated fatty acid into a container, adding a mixed solvent into the unsaturated fatty acid, and heating and stirring at 50-60 ℃ for 30-60 min to obtain a clear solution;
s2: after the solution is clarified, slowly adding sodium hydroxide, and after the reaction is completed, continuously stirring for 20 min;
s3: then adding a complex, a nonionic surfactant, sorbitol and other auxiliary agents, continuing stirring for 20min, then adding sweet wormwood herb essential oil, raspberry concentrated solution and chlorhexidine gluconate, continuing stirring for 25min, then cooling to 10-15 ℃, and adding the multi-vesicle dihydromyricetin liposome, soy isoflavone, negundo chastetree fruit essence, horse chestnut essence and bristlet flower extract, stirring for 5min, namely obtaining orange soap base:
s4: pouring the soap base into a transparent soap mould while the soap base is hot, cooling, forming, demoulding, discharging, modifying the uneven part of the soap block by using a blade, and removing the corner or the protruded grinding tool part;
s5: and (3) drying the demoulded soap block for 1d in a drying chamber with good ventilation and a temperature of 20min and a humidity of 40%, then attaching a layer of 0.2mm industrial paraffin on the surface of the prepared soap block, printing, bagging and sealing.
(III) advantageous effects
The invention provides a preparation method of sweet wormwood essential oil soap. The method has the following beneficial effects:
1. the sweet wormwood essential oil, the chlorhexidine gluconate, the multi-vesicular dihydromyricetin liposome and the raspberry concentrated solution have antibacterial effects, are also used as pigments, have the effects of resisting tumors and inflammation and remarkable antioxidation, and simultaneously overcome the defects of low water solubility, short biological half-life period and poor membrane permeability of the vine tea in the prior art and prolong the antibacterial time.
2. The horse chestnut essence can quickly permeate into a skin basal layer, activate cells, promote blood circulation, regulate skin metabolism normalization, improve tissue renewal capacity, and remarkably improve skin problems of rough skin, excessive oil secretion, darkness, no transparency and the like.
3. The components of the Bordetella extract in the invention volatilize along with use and can act on the central nerve of a user, the user can fall asleep quickly after using the Bordetella extract, and the generation of melatonin is promoted to lighten melanin after using the Bordetella extract, so that the whitening is realized, and the Bordetella extract is very suitable for night use.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
the embodiment of the invention provides a sweet wormwood essential oil soap which comprises the following components in parts by weight: 2 parts of sweet wormwood essential oil, 15 parts of unsaturated fatty acid, 10 parts of mixed solvent, 3 parts of sodium hydroxide, 1 part of complex, 10 parts of nonionic surfactant, 0.1 part of chlorhexidine gluconate, 3 parts of multi-vesicular dihydromyricetin liposome, 1 part of raspberry concentrate, 1 part of soybean isoflavone, 1 part of negundo chastetree fruit essence, 1 part of horse chestnut essence, 0.5 part of borlotte flower extract, 3 parts of sorbitol and 0.5 part of other auxiliary agents.
The preparation method of the sweet wormwood essential oil soap is characterized by comprising the following preparation steps:
s1: taking 4: adding C18 acid and C14 acid of 1 into a container, adding a mixed solvent formed by mixing ethanol and propylene glycol in equal amount, heating and stirring at 50 ℃ for 30min to obtain a clear solution;
s2: after the solution is clarified, slowly adding sodium hydroxide which is 15% solution prepared by adding pure water, and continuously stirring for 20min after the reaction is completed;
s3: then adding ethylene diamine tetraacetic acid, AES, sorbitol and 10: 1, continuously stirring for 20min, then adding sweet wormwood herb essential oil, raspberry concentrated solution and chlorhexidine gluconate, continuously stirring for 25min, then cooling to 10 ℃, and adding the multi-vesicle dihydromyricetin liposome, the soybean isoflavone, the negundo chastetree fruit essence, the horse chestnut essence and the bristlet flower extract, stirring for 5min, namely obtaining orange soap base, wherein the color is generated due to the pigment action of the raspberry concentrated solution:
s4: pouring the soap base into a transparent soap mould while the soap base is hot, cooling, forming, demoulding, discharging, modifying the uneven part of the soap block by using a blade, and removing the corner or the protruded grinding tool part;
s5: drying the demoulded soap block in a drying chamber with the temperature of 20min and the humidity of 40% and good ventilation for 1d, then attaching a layer of 0.2mm industrial paraffin on the surface of the prepared soap block, printing, bagging and sealing, wherein the reason for wrapping the industrial paraffin is to prevent the components of the extract of the bloom flower in the finished product from volatilizing to reduce the sleep-aiding performance, and the soap block is prevented from being directly subjected to high temperature after being unpacked and is suitable for being placed in a shade place for sealing.
Example two:
the embodiment of the invention provides a sweet wormwood essential oil soap which comprises the following components in parts by weight: 2 parts of sweet wormwood herb essential oil, 20 parts of unsaturated fatty acid, 12 parts of mixed solvent, 4 parts of sodium hydroxide, 1 part of complex, 12 parts of nonionic surfactant, 0.2 part of chlorhexidine gluconate, 4 parts of multi-vesicular dihydromyricetin liposome, 2 parts of raspberry concentrate, 1 part of soybean isoflavone, 1 part of negundo chastetree fruit essence, 2 parts of horse chestnut essence, 0.6 part of borlotte flower extract, 3 parts of sorbitol and 0.8 part of other auxiliary agents.
The preparation method of the sweet wormwood essential oil soap is characterized by comprising the following preparation steps:
s1: taking 4: adding C18 acid and C14 acid of 1 into a container, adding a mixed solvent formed by mixing ethanol and propylene glycol in equal amount, heating and stirring at 50 ℃ for 30min to obtain a clear solution;
s2: after the solution is clarified, slowly adding sodium hydroxide which is 15% solution prepared by adding pure water, and continuously stirring for 20min after the reaction is completed;
s3: then adding ethylene diamine tetraacetic acid, AEO-9, sorbitol and 10: 1, continuously stirring for 20min, then adding sweet wormwood herb essential oil, raspberry concentrated solution and chlorhexidine gluconate, continuously stirring for 25min, then cooling to 10 ℃, and adding the multi-vesicle dihydromyricetin liposome, the soybean isoflavone, the negundo chastetree fruit essence, the horse chestnut essence and the bristlet flower extract, stirring for 5min, namely obtaining orange soap base, wherein the color is generated due to the pigment action of the raspberry concentrated solution:
s4: pouring the soap base into a transparent soap mould while the soap base is hot, cooling, forming, demoulding, discharging, modifying the uneven part of the soap block by using a blade, and removing the corner or the protruded grinding tool part;
s5: drying the demoulded soap block in a drying chamber with the temperature of 20min and the humidity of 40% and good ventilation for 1d, then attaching a layer of 0.2mm industrial paraffin on the surface of the prepared soap block, printing, bagging and sealing, wherein the reason for wrapping the industrial paraffin is to prevent the components of the extract of the bloom flower in the finished product from volatilizing to reduce the sleep-aiding performance, and the soap block is prevented from being directly subjected to high temperature after being unpacked and is suitable for being placed in a shade place for sealing.
Example three:
the embodiment of the invention provides a sweet wormwood essential oil soap which comprises the following components in parts by weight: 3 parts of sweet wormwood essential oil, 15 parts of unsaturated fatty acid, 15 parts of mixed solvent, 5 parts of sodium hydroxide, 2 parts of complex, 15 parts of nonionic surfactant, 0.5 part of chlorhexidine gluconate, 5 parts of multi-vesicular dihydromyricetin liposome, 2 parts of raspberry concentrate, 2 parts of soybean isoflavone, 2 parts of negundo chastetree fruit essence, 2 parts of horse chestnut essence, 1.5 parts of borlotte flower extract, 3 parts of sorbitol and 0.8 part of other auxiliary agents.
The preparation method of the sweet wormwood essential oil soap is characterized by comprising the following preparation steps:
s1: taking 4: adding C18 acid and C14 acid of 1 into a container, adding a mixed solvent formed by mixing ethanol and propylene glycol in equal amount, heating and stirring at 50 ℃ for 30min to obtain a clear solution;
s2: after the solution is clarified, slowly adding sodium hydroxide which is 15% solution prepared by adding pure water, and continuously stirring for 20min after the reaction is completed;
s3: then adding ethylene diamine tetraacetic acid, AEO-9, sorbitol and 10: 1, continuously stirring for 20min, then adding sweet wormwood herb essential oil, raspberry concentrated solution and chlorhexidine gluconate, continuously stirring for 25min, then cooling to 10 ℃, and adding the multi-vesicle dihydromyricetin liposome, the soybean isoflavone, the negundo chastetree fruit essence, the horse chestnut essence and the bristlet flower extract, stirring for 5min, namely obtaining orange soap base, wherein the color is generated due to the pigment action of the raspberry concentrated solution:
s4: pouring the soap base into a transparent soap mould while the soap base is hot, cooling, forming, demoulding, discharging, modifying the uneven part of the soap block by using a blade, and removing the corner or the protruded grinding tool part;
s5: drying the demoulded soap block in a drying chamber with the temperature of 20min and the humidity of 40% and good ventilation for 1d, then attaching a layer of 0.2mm industrial paraffin on the surface of the prepared soap block, printing, bagging and sealing, wherein the reason for wrapping the industrial paraffin is to prevent the components of the extract of the bloom flower in the finished product from volatilizing to reduce the sleep-aiding performance, and the soap block is prevented from being directly subjected to high temperature after being unpacked and is suitable for being placed in a shade place for sealing.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. The sweet wormwood essential oil soap is characterized by comprising the following components in parts by weight: 2-3 parts of sweet wormwood herb essential oil, 15-20 parts of unsaturated fatty acid, 10-15 parts of mixed solvent, 3-5 parts of sodium hydroxide, 1-2 parts of complex, 10-15 parts of nonionic surfactant, 0.1-0.5 part of chlorhexidine gluconate, 3-5 parts of multi-vesicular dihydromyricetin liposome, 1-2 parts of raspberry concentrate, 1-2 parts of soybean isoflavone, 1-2 parts of negundo chastetree fruit essence, 1-2 parts of horse chestnut essence, 0.5-1 part of bristlet flower extract, 3-5 parts of sorbitol and 0.5-1.5 parts of other auxiliary agents.
2. The artemisia apiacea essential oil soap as set forth in claim 1, wherein: the non-ionic surfactant is any one of AES and AEO-9.
3. The artemisia apiacea essential oil soap as set forth in claim 1, wherein: the multi-vesicle dihydromyricetin liposome is prepared from vine tea components extracted by a hydrothermal method, egg yolk lecithin serving as a liposome template and polyethylene glycol 4000 serving as a modifying material.
4. The artemisia apiacea essential oil soap as set forth in claim 1, wherein: the mixed solvent is formed by mixing ethanol, propylene glycol and glycerol in equal amount.
5. The artemisia apiacea essential oil soap as set forth in claim 1, wherein: the unsaturated fatty acids are C18 acids and C14 acids in a ratio of 4: 1 are mixed to obtain the product.
6. The artemisia apiacea essential oil soap as set forth in claim 1, wherein: the complex is ethylenediamine tetraacetic acid.
7. The artemisia apiacea essential oil soap as set forth in claim 1, wherein: the other auxiliary agents are a kasong preservative and a BHT antioxidant, wherein the weight ratio of 10: 1-2, and mixing.
8. The method for preparing the sweet wormwood essential oil soap as claimed in claim 1, wherein the method comprises the following steps: the preparation method comprises the following preparation steps:
s1: adding unsaturated fatty acid into a container, adding a mixed solvent into the unsaturated fatty acid, and heating and stirring at 50-60 ℃ for 30-60 min to obtain a clear solution;
s2: after the solution is clarified, slowly adding sodium hydroxide, and after the reaction is completed, continuously stirring for 20 min;
s3: then adding a complex, a nonionic surfactant, sorbitol and other auxiliary agents, continuing stirring for 20min, then adding sweet wormwood herb essential oil, raspberry concentrated solution and chlorhexidine gluconate, continuing stirring for 25min, then cooling to 10-15 ℃, and adding the multi-vesicle dihydromyricetin liposome, soy isoflavone, negundo chastetree fruit essence, horse chestnut essence and bristlet flower extract, stirring for 5min, namely obtaining orange soap base:
s4: pouring the soap base into a transparent soap mould while the soap base is hot, cooling, forming, demoulding, discharging, modifying the uneven part of the soap block by using a blade, and removing the corner or the protruded grinding tool part;
s5: and (3) drying the demoulded soap block for 1d in a drying chamber with good ventilation and 20 ℃ of temperature and 40% of humidity, then attaching a layer of 0.2mm industrial paraffin on the surface of the prepared soap block, printing, bagging and sealing.
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Application publication date: 20210730 |