CN103565700A - Lycium ruthenicum mill whitening and moisturizing facial cleanser and preparation method of facial cleanser - Google Patents
Lycium ruthenicum mill whitening and moisturizing facial cleanser and preparation method of facial cleanser Download PDFInfo
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- CN103565700A CN103565700A CN201310557908.8A CN201310557908A CN103565700A CN 103565700 A CN103565700 A CN 103565700A CN 201310557908 A CN201310557908 A CN 201310557908A CN 103565700 A CN103565700 A CN 103565700A
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- fructus lycii
- black fructus
- skin
- cleansing milk
- preserving moisture
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- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 1
- 210000001519 tissue Anatomy 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 235000010374 vitamin B1 Nutrition 0.000 description 1
- 239000011691 vitamin B1 Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
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- Cosmetics (AREA)
Abstract
The invention provides a lycium ruthenicum mill whitening and moisturizing facial cleanser and a preparation method of the facial cleanser. The lycium ruthenicum mill whitening and moisturizing facial cleanser is simple in preparation technology, pure in color, simple and elegant in fragrance, fine and smooth in texture, rich in foam, safe to use and free from stimulation, sensitization and toxic and side effects; after being used, the lycium ruthenicum mill whitening and moisturizing facial cleanser enables the skin not to have a tight feeling, is good in moisture retention, can enable spots to be gradually faded and removed, and has the effects of cleaning the skin, removing acnes, resisting bacteria, shrinking pores, moistening, whitening, moisturizing and keeping water as well as preventing the skin aging. A lycium ruthenicum mill extract is combined with a facial cleanser matrix and is even in distribution, so that the functions of the effective components in the natural products can be fully exerted.
Description
Technical field
The present invention relates to a kind of black Fructus Lycii whitening skin and preserving moisture cleansing milk and preparation method thereof.
Background technology
Skin clean is the first step of skin care.Due to the physiological action of human body, as smegma sebum finally becomes through being subject to air oxidation and bacterial decomposition for a long time the material that is harmful to skin; Sweat gland secretion perspiration can remain in skin surface by salinity and carbamide etc. after moisture evaporation; The metabolism of human body, as the pus the cell coming off from human body, secretions and skin, crust, serum transudate etc.; Residual cosmetics and dust, antibacterial etc., greatly reduce texture and the vigor of skin.If cleared up not in time, can further cutaneous physiologically active.Only carry out the follow-up skin protection work of cleaning guarantee of skin, therefore cleansing milk has been subject to the parent of consumer, look at.At present, the cleansing milk on market is numerous in variety, and function is also varied.
Summary of the invention
The object of the present invention is to provide a kind of whitening skin and preserving moisture cleansing milk that natural biological extract is active component and preparation method thereof of take.
The invention provides a kind of black Fructus Lycii whitening skin and preserving moisture cleansing milk, it is that supplementary material by following weight percentage is prepared from:
Wherein, described black Fructus Lycii fruit powder extracting solution is the water extract of black Fructus Lycii fruit powder; Preferably, the preparation method of black Fructus Lycii extracting solution is as follows: precision takes the dried powder of 5g black Fructus Lycii, add 50mL deionized-distilled water, in 50 ℃ of water-baths, extract 2 times, each 15 minutes, after filtration, residue is added to water 100mL extracts 2 times at 75 ℃, each 15 minutes, merge extracted twice liquid, filter, be evaporated to 10g/mL, obtain black Fructus Lycii extracting solution.
Wherein, Flos Matricariae chamomillae extracting solution preparation method is as follows: after Flos Matricariae chamomillae is pulverized, soak 1-3 hour, the 10-20 that the addition of water is Flos Matricariae chamomillae doubly, ultrasonic extraction 10-15 minute, filters again, centrifugal, discard precipitation, supernatant concentration, to concentration 10g/mL, is obtained to Flos Matricariae chamomillae extracting solution.
Wherein, Aloe extraction solution preparation method is as follows: get the clean aloe leaf chopping that 200g is fresh, after grinding 0.5h, put into iodine flask, adding 100mL ether to soak 5h decolours, sucking filtration (recovery ether), adds 300mL volume fraction and is distilling under reduced pressure after 95% soak with ethanol 24h, and residual ether and excessive ethanol low temperature are steamed, be concentrated into 10g/mL, obtain Aloe extraction solution.
But the extracting method of various extracts is not limited to said method, the disclosed extracting method of manufacturing cosmetics-stage extract of all prior aries is all applicable to the present invention.
Wherein, described anion surfactant is selected from one or more in polyoxyethylenated alcohol sodium sulfate (AES), sodium lauryl sulphate, ammonium lauryl sulfate, amide groups polyoxyethylene ether magnesium sulfate, 1-isobutyl-3,5-dimethylhexylphosphoric acid potassium salt, Dodecyl Polyoxyethylene Ether sulfosuccinic acid diesters.
Wherein, described amphoteric surfactant is selected from one or more in cocamido propyl betaine, coconut oleoyl amine dipropyl betanin, fatty alcohol-polyoxyethylene ether disodium sulfosuccinate, empgen BB, dodecyldimethylammonium hydroxide inner salt.
Wherein, described non-ionic surface active agent is selected from one or more in fatty monoethanol amide, fatty acid distribution of coconut oil diglycollic amide, alkyl polyglucoside.
Preferably, it is that supplementary material by following weight percentage is prepared from:
In the present invention, multiple natural extract is used in combination, has brought into play clean more good skin care activity, for market provides clean better, safe skin care item of a kind of skin effect.
The present invention also provides the preparation method of above-mentioned black Fructus Lycii whitening skin and preserving moisture cleansing milk, and it comprises the steps:
(1) guar gum, disodiumedetate are dissolved in suitable quantity of water, at 70 ℃ ± 5 ℃, fully dissolve, obtain the mixed liquor of clarification;
(2) allantoin, cetostearyl alcohol, Jojoba oil, anion surfactant, amphoteric surfactant, non-ionic surface active agent are joined in above-mentioned mixed liquor, add remaining water, 70 ℃ ± 5 ℃ stirring and dissolving;
(3) glycol distearate is joined to mixed liquor in (2), it is dissolved completely, obtain the mixed liquor of transparent clarification;
(4) get citric acid and be added to mixed liquor in (3);
(5) WSR-205 is added after dissolving with glycerol, then join in the solution in (4);
(6) 10% sodium chloride solution is joined in (5) middle solution, stir;
(7) to be cooled during to 40～50 ℃, add Glydant PLUS and essence, stir;
(8) add again black Fructus Lycii extracting solution, Flos Matricariae chamomillae extracting solution, Aloe extraction solution, cooling standing after stirring, obtain black Fructus Lycii whitening skin and preserving moisture cleansing milk.
Wherein, black Fructus Lycii extracting solution is the water extract of black Fructus Lycii fruit powder.The composition such as rich in proteins, aminoacid, flavone, procyanidin, fat, polysaccharide, vitamin E in lycium ruthenicum fruit.Protein is the structural material of human body skin, gives skin with nutrition, can make impaired cell, tissue obtain timely high-quality repairing, makes the high resilience of skin gloss, delaying senility.In lycium ruthenicum fruit, contain 17 seed amino acids except tryptophan, aminoacid is form organism protein and with one of closely bound up base substance of vital movement, nutrition can be provided, promote growth, maintain normal metabolism.Assessment of Pigment of Lycium ruthenicum Murr is anthocyanin class and flavone compound, and its non-oxidizability is obviously better than than vitamin E, and visible ray and ultraviolet are had to Stabilization.The non-oxidizability of flavone is mainly manifested in aspects such as removing free radical and anti-peroxidation.
Flos Matricariae chamomillae extracting solution contains the effective ingredient such as aminoacid, flavonoid, vitamin A, vitamin B1, there is powerful broad-spectrum antiviral, antibiotic effect, also there is good Shu Min, the responsive skin of maintenance, reduce thin red blood streak, reduce rubescent, the unequal effect of the adjustment colour of skin, also there is the effect of repairing laceration of skin, moisturizing, releive calm skin pore refining.It makes an addition in cosmetics, can not only balanced fat secretion, press down the anti-pox of fat, and prevent acne, eliminate black speck, skin whitening, and some skin pathogenicity fungus is had and suppressed and bactericidal action.It is rich in flavonoid active component, has antioxidation, anti-angiogenic hypertrophy, antiinflammatory, anti-allergy and antiviral effect.
The aloin that Aloe extraction solution contains, Aloe resin B, have certain effect at aspect tools such as moisturizing, antiinflammatory, antibacterial, antipruritic, antiallergic, softening skin, anti-acne, antiperspirant deodorant, and ultraviolet is had to strong Absorption, prevents skin burn.The composition that Aloe contains multiple elimination superoxide radical, as superoxide dismutase (SOD), catalase.Wherein superoxide dismutase is the enzyme with catalysis superoxide anion dismutation reaction function, effectively remove superfluous oxygen-derived free radicals, under physiological conditions, maintain dynamic equilibrium, there is the damage, speckle dispelling, wrinkle removal, the antidotal effect that prevent radical pair human body, can make skin delicate, flexible, there is the effects such as anticorrosion and slow down aging.Aloe glue is natural sun-prevention component, can effectively suppress the ultraviolet in daylight, prevents pigmentation, keeps whitening skin.
Black Fructus Lycii whitening skin and preserving moisture cleansing milk preparation technology provided by the present invention is simple, color and luster is pure, fragrance is simple and elegant, exquisite quality, foam abundant, use safety, nonirritant, without sensitization, have no side effect, after use, can not make skin produce tight sense, moisture retention is good, can desalinate gradually, remove mottle, and there is cleaning skin, the pox that disappears is antibiotic, pore refining, moisten whitening, moisturizing lock water, prevent the effect of skin aging.The black Fructus Lycii extract adding is combined with cleansing milk substrate, is evenly distributed, and can make the effective ingredient in natural product play one's part to the full.
Below pass through the specific embodiment; scope of the present invention is further elaborated and is illustrated; but protection scope of the present invention is not limited to this; any those of ordinary skill in the art are in the disclosed technical scope of the present invention; can be without modification or the replacement of creative work, within all should being encompassed in protection scope of the present invention.
The specific embodiment
Flos Matricariae chamomillae extracting solution preparation method is as follows: after Flos Matricariae chamomillae is pulverized, soak 1-3 hour, the 10-20 that the addition of water is Flos Matricariae chamomillae doubly, ultrasonic extraction 10-15 minute, filters again, centrifugal, discard precipitation, supernatant concentration, to concentration 10g/mL, is obtained to Flos Matricariae chamomillae extracting solution.
Aloe extraction solution preparation method is as follows: get the clean aloe leaf chopping that 200g is fresh, after grinding 0.5h, put into iodine flask, adding 100mL ether to soak 5h decolours, sucking filtration (recovery ether), add 300mL volume fraction and be distilling under reduced pressure after 95% soak with ethanol 24h, residual ether and excessive ethanol low temperature are steamed, be concentrated into 10g/mL, obtain Aloe extraction solution.
The black Fructus Lycii extracting solution that the present invention uses is the water extract of black Fructus Lycii fruit powder, its concrete preparation method can be: precision takes the dried powder of 5g black Fructus Lycii, add 50mL deionized-distilled water, in 50 ℃ of water-baths, extract 2 times, each 15 minutes, after filtration, residue is added to water 100mL extracts 2 times at 75 ℃, each 15 minutes, merge extracted twice liquid, filter, be evaporated to 10g/mL, obtain black Fructus Lycii extracting solution.
Concentration after concentrated in the present invention is all with the mass/volume of concentrated solution, to calculate the ratio of gained.
The using method of cleansing milk of the present invention: with warm water moistening face, make the abundant diastole of pore, get appropriate this product and play foam at the palm of the hand, evenly be applied in face, the massage 1～2 minute of looping gently of Yong Shou face, then cleans with clear water, then with the cold water portion of washing one's face of raising.
In the embodiment of the present invention, each component is listed in table 1, and proportional quantity is with mass percent example.
Table 1
The preparation method of the embodiment of the present invention is all according to following steps:
(1) guar gum, disodiumedetate are dissolved in suitable quantity of water, at 70 ℃ ± 5 ℃, fully dissolve, obtain the mixed liquor of clarification;
(2) allantoin, cetostearyl alcohol, Jojoba oil, anion surfactant, amphoteric surfactant, non-ionic surface active agent are joined in above-mentioned mixed liquor, add remaining water, 70 ℃ ± 5 ℃ stirring and dissolving;
(3) glycol distearate is joined to mixed liquor in (2), it is dissolved completely, obtain the mixed liquor of transparent clarification;
(4) get citric acid and be added to mixed liquor in (3);
(5) WSR-205 is added after dissolving with glycerol, then join in the solution in (4);
(6) 10% sodium chloride solution is joined in (5) middle solution, stir;
(7) to be cooled during to 40～50 ℃, add Glydant PLUS and essence, stir;
(8) add again black Fructus Lycii extracting solution, Flos Matricariae chamomillae extracting solution, Aloe extraction solution, cooling standing after stirring, obtain black Fructus Lycii whitening skin and preserving moisture cleansing milk.
By effect comparison, the prescription best results of embodiment 4.Product used in Application Example 1～3 is according to the prepared product of the prescription of embodiment 4.
Embodiment 7
The Detection of Stability of the embodiment of the present invention 4 products:
1, pH value is 6.2.
2, heat resistant test, puts into calorstat (40 ± 1) ℃ one bottle of sample of Packing Intact and keeps 24h, returns to after room temperature without oil-water separation phenomenon.
3, low temperature resistant test, puts into refrigerator-5～-10 ℃ one bottle of sample of Packing Intact and places 24h, returns to after room temperature without layering, coarse, metachromatism.
4, centrifugal test, places in centrifuge one bottle of sample of Packing Intact with 2000 revs/min, and centrifugal 30 minutes, without oil-water separation phenomenon.
As can be seen here, the cleansing milk of the embodiment of the present invention 4 preparations has good stability.
Application Example 1
Object of study: oily skin person, 10 examples.
Using method: every day, each used the cleansing milk of once being prepared by embodiment 4 sooner or later, used continuously 4 weeks.
Experimental result: effectively clean facial skin, moistening effect is good.
Application Example 2
Object of study: dry skin person, 10 examples.
Using method: every day, each used the cleansing milk of once being prepared by embodiment 4 sooner or later, used continuously 4 weeks.
Experimental result: sensation moistening effect is good, and skin does not have tight sense.
Application Example 3
Object of study: neutral skin person, 10 examples.
Using method: every day, each used the cleansing milk of once being prepared by embodiment 4 sooner or later, used continuously 4 weeks.
Experimental result: feel to have good moisture retention, slightly effective 8 examples.
Table 2
| ? | Effectively | Generally | Invalid | Effective percentage |
| Oily skin | 8 | 1 | 1 | 80％ |
| Neutral skin | 8 | 2 | 0 | 80％ |
| Dry skin | 9 | 1 | 0 | 90％ |
Claims (9)
1. a black Fructus Lycii whitening skin and preserving moisture cleansing milk, is characterized in that: it is that supplementary material by following weight percentage is prepared from:
2. black Fructus Lycii whitening skin and preserving moisture cleansing milk according to claim 1, is characterized in that: described black Fructus Lycii fruit powder extracting solution is the water extract of black Fructus Lycii fruit powder; Preferably, the preparation method of black Fructus Lycii extracting solution is as follows: precision takes the dried powder of 5g black Fructus Lycii, add 50mL deionized-distilled water, in 50 ℃ of water-baths, extract 2 times, each 15 minutes, after filtration, residue is added to water 100mL extracts 2 times at 75 ℃, each 15 minutes, merge extracted twice liquid, filter, be evaporated to 10g/mL, obtain black Fructus Lycii extracting solution.
3. black Fructus Lycii whitening skin and preserving moisture cleansing milk according to claim 1, it is characterized in that: Flos Matricariae chamomillae extracting solution preparation method is as follows: after Flos Matricariae chamomillae is pulverized, soak 1-3 hour, the addition of water is 10-20 times of Flos Matricariae chamomillae, then ultrasonic extraction 10-15 minute, filters, centrifugal, discard precipitation, supernatant concentration, to concentration 10g/mL, is obtained to Flos Matricariae chamomillae extracting solution.
4. black Fructus Lycii whitening skin and preserving moisture cleansing milk according to claim 1, it is characterized in that: Aloe extraction solution preparation method is as follows: get the clean aloe leaf chopping that 200g is fresh, after grinding 0.5h, put into iodine flask, adding 100mL ether to soak 5h decolours, sucking filtration (recovery ether), adds 300mL volume fraction and is distilling under reduced pressure after 95% soak with ethanol 24h, and residual ether and excessive ethanol low temperature are steamed, be concentrated into 10g/mL, obtain Aloe extraction solution.
5. black Fructus Lycii whitening skin and preserving moisture cleansing milk according to claim 1, is characterized in that: described anion surfactant is selected from one or more in polyoxyethylenated alcohol sodium sulfate, sodium lauryl sulphate, ammonium lauryl sulfate, amide groups polyoxyethylene ether magnesium sulfate, 1-isobutyl-3,5-dimethylhexylphosphoric acid potassium salt, Dodecyl Polyoxyethylene Ether sulfosuccinic acid diesters.
6. black Fructus Lycii whitening skin and preserving moisture cleansing milk according to claim 1, is characterized in that: described amphoteric surfactant is selected from one or more in cocamido propyl betaine, coconut oleoyl amine dipropyl betanin, fatty alcohol-polyoxyethylene ether disodium sulfosuccinate, empgen BB, dodecyldimethylammonium hydroxide inner salt.
7. black Fructus Lycii whitening skin and preserving moisture cleansing milk according to claim 1, is characterized in that: described non-ionic surface active agent is selected from one or more in fatty monoethanol amide, fatty acid distribution of coconut oil diglycollic amide, alkyl polyglucoside.
8. according to the black Fructus Lycii whitening skin and preserving moisture cleansing milk described in claim 1～7 any one, it is characterized in that: it is that supplementary material by following weight percentage is prepared from:
9. the preparation method of black Fructus Lycii whitening skin and preserving moisture cleansing milk described in claim 1～8 any one, is characterized in that: it comprises the steps:
(1) guar gum, disodiumedetate are dissolved in suitable quantity of water, at 70 ℃ ± 5 ℃, fully dissolve, obtain the mixed liquor of clarification;
(2) allantoin, cetostearyl alcohol, Jojoba oil, anion surfactant, amphoteric surfactant, non-ionic surface active agent are joined in above-mentioned mixed liquor, add remaining water, 70 ℃ ± 5 ℃ stirring and dissolving;
(3) glycol distearate is joined to mixed liquor in (2), it is dissolved completely, obtain the mixed liquor of transparent clarification;
(4) get citric acid and be added to mixed liquor in (3);
(5) WSR-205 is added after dissolving with glycerol, then join in the solution in (4);
(6) 10% sodium chloride solution is joined in (5) middle solution, stir;
(7) to be cooled during to 40～50 ℃, add Glydant PLUS and essence, stir;
(8) add again black Fructus Lycii extracting solution, Flos Matricariae chamomillae extracting solution, Aloe extraction solution, cooling standing after stirring, obtain black Fructus Lycii whitening skin and preserving moisture cleansing milk.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213261A (en) * | 2015-10-28 | 2016-01-06 | 青海尤尼克生物技术有限公司 | A kind of black fruit matrimony vine oxidation resistant skin care item |
| CN105232442A (en) * | 2015-11-18 | 2016-01-13 | 中山市艾丽意素生物科技有限公司 | Plant antioxidation amino acid cleanser and preparation method thereof |
| CN105267095A (en) * | 2015-11-17 | 2016-01-27 | 中国科学院西北高原生物研究所 | Facial cleanser containing Nitraria tangutorum polysaccharide |
| CN106265289A (en) * | 2016-08-31 | 2017-01-04 | 青海新泰行生物科技有限公司 | A kind of cosmetic composition containing black Fructus Lycii extract and facial cleaning cream |
| CN106821776A (en) * | 2017-02-22 | 2017-06-13 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of blackhead of graphene-containing derives liquid |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101991709A (en) * | 2010-11-09 | 2011-03-30 | 中国科学院西北高原生物研究所 | Method for preparing antioxidant lycium ruthenicum extract |
-
2013
- 2013-11-06 CN CN201310557908.8A patent/CN103565700B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101991709A (en) * | 2010-11-09 | 2011-03-30 | 中国科学院西北高原生物研究所 | Method for preparing antioxidant lycium ruthenicum extract |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105213261A (en) * | 2015-10-28 | 2016-01-06 | 青海尤尼克生物技术有限公司 | A kind of black fruit matrimony vine oxidation resistant skin care item |
| CN105267095A (en) * | 2015-11-17 | 2016-01-27 | 中国科学院西北高原生物研究所 | Facial cleanser containing Nitraria tangutorum polysaccharide |
| CN105232442A (en) * | 2015-11-18 | 2016-01-13 | 中山市艾丽意素生物科技有限公司 | Plant antioxidation amino acid cleanser and preparation method thereof |
| CN106265289A (en) * | 2016-08-31 | 2017-01-04 | 青海新泰行生物科技有限公司 | A kind of cosmetic composition containing black Fructus Lycii extract and facial cleaning cream |
| CN106821776A (en) * | 2017-02-22 | 2017-06-13 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of blackhead of graphene-containing derives liquid |
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| CN103565700B (en) | 2016-01-20 |
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