CN112891292A - A moisturizing facial cleanser containing natural plant effective components for removing speckle, brightening skin and nourishing skin, and its preparation method - Google Patents
A moisturizing facial cleanser containing natural plant effective components for removing speckle, brightening skin and nourishing skin, and its preparation method Download PDFInfo
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- CN112891292A CN112891292A CN202110320014.1A CN202110320014A CN112891292A CN 112891292 A CN112891292 A CN 112891292A CN 202110320014 A CN202110320014 A CN 202110320014A CN 112891292 A CN112891292 A CN 112891292A
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Abstract
The invention provides a spot-removing skin-brightening nourishing moisturizing facial cleanser containing natural plant active ingredients and a preparation method thereof, wherein the spot-removing skin-brightening moisturizing facial cleanser comprises the following components: the feed comprises basil seed extract, peach blossom extract, agar extract, okra extract, chanterelle extract, tribulus terrestris extract, poria cocos extract, green tea extract, cherry juice, motherwort extract, cordyceps flower extract, wolfberry extract, tremella extract, synthetic egg white powder, skimmed milk powder, vitamin C, pistachio nut oil, shea butter, malus micromalus oil, universal emulsifier, olive emulsifier, coconut oil fatty acid potassium glycinate, lauroyl amphoacetate, cocoyl amphoacetate, 1, 2-propylene glycol, sodium carboxymethylcellulose, sodium alginate, potassium hydroxide, essence, distilled water and nipagin ethyl ester. Compared with the prior art, the facial cleanser disclosed by the invention can effectively remove color spots, brighten skin color, comprehensively repair skin injury, deeply nourish and moisturize skin and improve skin resistance.
Description
Technical Field
The invention relates to the field of skin care products, in particular to a spot-removing, skin-brightening and nourishing moisturizing facial cleanser containing natural plant active ingredients and a preparation method thereof.
Background
The color spots are easily generated by the damage of modern living environment and the increase of living pressure, the use of inferior cosmetics and poor living habits. The color spot is contrary to the modern aesthetic feeling of people, and the pursuit of beauty is influenced. However, some of the existing spot removing products in the market can add a large amount of metal or nonmetal chemical components to achieve the effect, and after long-term use, the effect cannot be achieved, and the facial skin injury can be aggravated; even some products can achieve the freckle removing effect, the skin cannot be comprehensively repaired, and the original state of the skin is restored. Therefore, the safe and effective freckle-removing skin care product has wide market demand.
The existing facial cleanser has incomplete functions, on one hand, the skin moisturizing function is reduced due to excessive cleaning after long-term use, and on the other hand, the functions of cleaning, whitening and maintaining cannot be achieved simultaneously. Along with the continuous improvement of the living standard and the pursuit of beauty of people, the requirements of people on washing and protecting products are higher and higher. Because the facial skin care is very important, people can select the facial cleanser more carefully and select mild and non-irritant products.
Disclosure of Invention
The invention aims to provide the spot-removing, skin-brightening and nourishing moisturizing facial cleanser containing the natural plant effective ingredients, and the moisturizing facial cleanser containing the natural plant effective ingredients can remove spots, comprehensively repair and nourish skin and improve the skin color.
The invention also aims to provide a preparation method of the freckle-removing, skin-brightening and nourishing moisturizing facial cleanser containing natural plant active ingredients, wherein the addition sequence and parameters are designed and prepared according to the ingredients and effects of the raw materials, so that the facial cleanser which is suitable in viscosity, fine and uniform in texture, bright and moist in luster, rapid in absorption, good in foamability, fragrant in smell, capable of effectively removing freckles, capable of comprehensively repairing skin injury, deeply nourishing skin, improving skin resistance and playing a good moisturizing role is finally obtained.
The specific technical scheme of the invention is as follows:
a moisturizing facial cleanser containing natural plant effective components and capable of removing freckles, brightening skin and nourishing skin comprises the following raw materials in parts by weight:
the content of the ethylparaben in the moisturizing facial cleanser is 0.2-0.4 wt%.
The universal emulsifier is a universal self-emulsifying compound emulsifier AC-402;
the olive emulsifier is a liquid crystal type olive emulsifier.
Further, the above basil seed extract, peach blossom extract, gelidium amansii extract, okra extract, chanterelle extract, tribulus terrestris extract, poria cocos extract, green tea extract, cherry extract, motherwort extract, cordyceps flower extract, wolfberry fruit extract, tremella extract, coconut oil fatty acid potassium glycinate, lauroyl amphoacetate, sodium cocoyl amphoacetate, 1, 2-propylene glycol, distilled water and essence are correspondingly in parts by volume.
The components of the cream tree fruit oil, the Qiongya crabapple oil, the universal emulsifier, the olive emulsifier, the synthetic egg white powder, the skimmed milk powder, the vitamin C, the pistachio nut oil, the potassium hydroxide, the sodium alginate, the sodium carboxymethylcellulose and the ethylparaben are correspondingly in parts by weight.
When the volume part unit is mL, the corresponding weight part unit is g.
Preferably, the spot-removing, skin-brightening and nourishing moisturizing facial cleanser containing natural plant active ingredients comprises the following components in parts by weight:
the basil seed extracting solution is prepared by the following method:
weighing appropriate amount of basil seed, heating and reflux extracting with water for 3 times: adding water 20-25 times the weight of the cymbidium seed for 1 time, soaking for 0.25-0.75 hr, and extracting for 1.5-2.5 hr; adding 15-18 times of water for 2 times, and extracting for 1.0-1.5 hr; adding water 8-12 times the weight of the basil seeds at the 3 rd time, extracting for 0.5-1.0h, filtering each time, combining filtrates, performing suction filtration, and concentrating the volume of the filtrate to 15-20 times mL/g of the weight of the basil seeds to obtain a basil seed extract for later use; the volume of the basil seed extract obtained per gram of the basil seed is 15-20 ml.
The peach blossom extracting solution is prepared by the following method:
weighing appropriate amount of dried flos persicae, and extracting with water under heating and refluxing for 3 times: adding water 15-20 times the weight of the dried peach blossom for the first time, soaking for 0.5-1.0h, and extracting for 1.0-1.5 h; adding 10-14 times of water of the weight of the dried peach blossom for the 2 nd time, and extracting for 1.0-1.5 h; adding water 5-10 times the weight of the dried peach blossom 3 times, extracting for 0.5-1.5h, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 5-10 times mL/g of the weight of the dried peach blossom to obtain peach blossom extract.
The agar extracting solution is prepared by the following method:
weighing appropriate amount of Eucheuma Gelatinosum, heating and reflux-extracting with water for 3 times: adding 10-15 times of water by mass of Eucheuma Gelatinosum at 1 st time, soaking for 0.2-0.7 hr, and extracting for 1.0-2.5 hr; adding 10-13 times of water by mass of Gelidium amansii for 2 times, and extracting for 0.5-1.5 hr; adding water 8-10 times the weight of Eucheuma Gelatinosum in 3 rd time, extracting for 0.5-1.0 hr, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 3-8 times mL/g of Eucheuma Gelatinosum weight to obtain Eucheuma Gelatinosum extractive solution;
the okra extracting solution is prepared by the following method:
weighing appropriate amount of okra, heating and reflux-extracting with water for 3 times: adding water 8-10 times the weight of okra at the 1 st time, soaking for 0.2-0.7 hr, and extracting for 1.0-1.5 hr; adding water 8-10 times the weight of okra at the 2 nd time, and extracting for 0.5-1.5 h; adding water 6-8 times the weight of okra in the 3 rd time, extracting for 0.5-1.0h, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 2-7 times of weight of okra (mL/g) to obtain okra extractive solution.
The chanterelle extracting solution is prepared by the following method:
weighing appropriate amount of chanterelle, heating and reflux-extracting with water for 3 times: adding water with the amount of 20-25 times of that of the chanterelle at the 1 st time, soaking for 0.5-1.0h, and extracting for 1.5-2.0 h; adding 15-20 times of water of adeps gallus Domesticus for 2 times, and extracting for 1.5-2.0 hr; adding water with the weight 5-10 times of that of the chanterelle at the 3 rd time, extracting for 0.5-1.5h, filtering each time, combining the filtrates, performing suction filtration, and concentrating the volume of the filtrate to 10-13 times of mL/g of the weight of the chanterelle to obtain an chanterelle extracting solution for later use;
the tribulus terrestris extracting solution is prepared by the following method:
weighing appropriate amount of fructus Tribuli coarse powder, and extracting with water under heating and refluxing for 3 times: adding water 15-20 times the weight of fructus Atriplicis Sibiricae at 1 time, soaking for 0.2-0.7 hr, and extracting for 1.0-2.5 hr; adding 12-15 times of water of the weight of the Tribulus terrestris at the 2 nd time, and extracting for 1.0-1.5 h; adding water 8-12 times the weight of fructus Atriplicis Sibiricae at 3 times, extracting for 0.5-1.0 hr, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 8-12 times of the weight of fructus Atriplicis Sibiricae mL/g to obtain fructus Atriplicis Sibiricae extract.
The poria cocos extracting solution is prepared by the following method:
weighing appropriate amount of Poria cocos slice, heating and reflux extracting with water for 3 times: adding water 12-16 times the weight of Poria tablet at 1 st time, soaking for 0.5-1.0 hr, and extracting for 1.0-2.5 hr; adding water 8-12 times the weight of Poria tablet for the 2 nd time, extracting for 1.0-1.5 hr, and filtering to obtain filtrate; adding water 7-9 times the weight of Poria tablet at 3 rd time, extracting for 0.5-1.2 hr, filtering each time, mixing filtrates, filtering, and concentrating the filtrate to 10-20 times mL/g of Poria weight to obtain Poria extract;
the green tea extracting solution is prepared by the following method:
weighing appropriate amount of green tea, heating and reflux extracting with water for 3 times: adding 10-15 times of water by weight of green tea for the first time, soaking for 0.5-0.7 hr, and extracting for 1.0-2.0 hr; adding water 8-12 times the weight of green tea in the 2 nd time, and extracting for 1.0-1.5 hr; adding water 7-10 times the weight of green tea in the 3 rd time, extracting for 0.5-1.0 hr, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to volume of 15-18 times of green tea weight mL/g to obtain green tea extractive solution.
The cherry squeezing liquid is prepared by the following steps:
weighing a proper amount of fresh cherries, putting the fresh cherries into a juicer, adding 10-15 times of water, squeezing for 0.5-2.0min in a juicing mode to obtain filtrate, filtering the filtrate by using four layers of gauze, centrifuging the filtrate, taking supernate, and concentrating the volume of the filtrate to 1-1.5 times of the weight of the cherries (mL/g) to obtain cherry squeezed liquid for later use;
the motherwort herb extracting solution is prepared by the following method:
weighing appropriate amount of herba Leonuri, extracting with water under heating and refluxing for 3 times: adding 18-22 times of water by mass of herba Leonuri at 1 st time, soaking for 0.5-1.0 hr, and extracting for 1.5-2.5 hr; adding 15-18 times of water of herba Leonuri for the 2 nd time, and extracting for 1.5-2.0 h; adding 8-13 times of water by mass of herba Leonuri in 3 rd time, extracting for 0.5-1.0h, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 20-25 times of herba Leonuri weight mL/g to obtain herba Leonuri extractive solution.
The cordyceps flower extracting solution is prepared by the following method:
weighing appropriate amount of Cordyceps flower, and extracting with water under heating and refluxing for 3 times: adding water 20-25 times the mass of Cordyceps flower at 1 st time, soaking for 0.5-1.0 hr, and extracting for 1.5-2.0 hr; adding 18-20 times of water of Cordyceps flower for 2 times, and extracting for 1.0-1.5 hr; adding water 15-18 times the weight of Cordyceps flower in 3 rd time, extracting for 0.5-1.5 hr, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 10-15 times of Cordyceps flower weight (mL/g) to obtain Cordyceps flower extractive solution;
the wolfberry fruit extracting solution is prepared by the following method:
weighing appropriate amount of fructus Lycii, and extracting with water under heating and refluxing for 3 times: adding 16-18 times of water of fructus Lycii at 1 st time, and reflux extracting for 1.0-2.0 hr; adding 12-14 times of water of fructus Lycii for the 2 nd time, reflux extracting for 1.0-1.5 hr; adding 8-10 times of water by weight of fructus Lycii in 3 rd time, reflux extracting for 1.0-1.5 hr, filtering to obtain filtrate, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to volume of 15-20 times of fructus Lycii weight mL/g to obtain fructus Lycii extractive solution.
The tremella extract is prepared by the following method:
weighing appropriate amount of Tremella, extracting with water under heating and refluxing for 3 times: adding water 20-25 times the weight of Tremella at 1 st time, soaking for 0.5-1.0 hr, and extracting for 1.5-2.0 hr; adding water 15-18 times the weight of Tremella at 2 times, and extracting for 1.0-1.5 hr; adding 10-15 times of water to the tremella in mass for 3 times, extracting for 0.5-1.0h, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 10-15 times of weight of Tremella (mL/g) to obtain Tremella extractive solution.
The essence is selected from one or more of peach blossom essence, strawberry essence, rose essence, osmanthus flower essence, lily essence, milk essence or cucumber essence.
The preparation method of the moisturizing facial cleanser containing natural plant active ingredients and capable of removing freckles, brightening skin and nourishing skin comprises the following steps:
a) weighing sodium alginate according to the formula ratio, adding 30-40 parts of distilled water, placing in a constant temperature water bath kettle at 60-80 deg.C, heating and stirring for 5-15min, standing at room temperature for 2-5h to obtain sodium alginate gel solution for use;
b) weighing sodium carboxymethylcellulose according to the formula ratio, dissolving in 25-30 parts of distilled water, standing for 12-24h, and naturally swelling and dissolving to obtain uniform and transparent sodium carboxymethylcellulose gel solution for later use;
c) weighing the synthetic egg white powder according to the formula ratio, adding 10-20 parts of distilled water, putting into a constant-temperature water bath kettle at 60-80 ℃, stirring for 5-10min, taking out, and standing for 5-6h at normal temperature to obtain a synthetic egg white powder solution for later use;
d) weighing ethylparaben with the formula amount, adding 1, 2-propylene glycol with the formula amount, stirring and dissolving to obtain a preservative solution for later use;
e) weighing pistachio nut oil according to the formula amount, placing the pistachio nut oil in a constant-temperature water bath kettle at 70-90 ℃, and heating to obtain oil A for later use;
f) weighing potassium hydroxide according to the formula ratio, weighing 2-5 parts of distilled water, and adding the distilled water into the potassium hydroxide to completely dissolve the potassium hydroxide;
g) adding the solution obtained in the step f) into the oil A obtained in the step e) in a trickle shape, heating and uniformly stirring in the same direction for reacting for 15-25min to fully react to obtain a soap solution B;
h) weighing the shea butter, the malus sieboldii oil, the universal emulsifier and the olive emulsifier according to the formula ratio respectively, fully mixing the materials, putting the materials into a constant-temperature water bath kettle at 70-90 ℃, and heating while stirring to uniformly mix the materials to obtain an oil phase;
i) weighing 5-20 parts of distilled water, and heating in a constant-temperature water bath kettle at 70-90 ℃ to obtain a water phase;
j) slowly adding the water phase into the oil phase along the wall of the container when the oil phase and the water phase reach the same temperature, heating and stirring at the same direction at constant speed for 15-30min, and emulsifying to obtain O/W emulsion matrix;
k) adding the formed emulsion matrix into soap solution B, placing in 70-90 deg.C water bath, heating while stirring for 10-15min to obtain mixed solution C;
l) respectively measuring the potassium glycinate, the sodium lauroamphoacetate and the sodium cocoamphoacetate with the formula ratio, adding into the mixed solution C, and stirring for 3-10min to uniformly mix to obtain a mixed solution D;
m) weighing the formula amount of the skimmed milk powder and the vitamin C respectively, dissolving the skimmed milk powder and the vitamin C with 2-4 parts of distilled water respectively, and adding the mixture into the mixed solution D;
n) respectively measuring the formula amounts of a basil seed extracting solution, a peach blossom extracting solution, a gelidium amansii extracting solution, an okra extracting solution, a chanterelle extracting solution, a tribulus terrestris extracting solution, a poria cocos extracting solution, a green tea extracting solution, a cherry squeezing solution, a motherwort extracting solution, a cordyceps flower extracting solution, a wolfberry extracting solution and a tremella extracting solution, adding the obtained mixture into the mixed solution D, and uniformly stirring to obtain a mixed solution E;
o) adding the prepared synthetic egg white powder solution, sodium alginate gel solution and sodium carboxymethyl cellulose gel solution into the mixed solution E, stirring to mix uniformly, adding formula amount of essence and preservative solution, stirring and mixing uniformly to obtain the spot-removing, skin-brightening and nourishing moisturizing facial cleanser containing natural plant active ingredients.
The various components of the present invention are described as follows:
the basil seeds can improve the nutritional status of skin, promote the metabolism of the skin, enhance the vitality of the facial skin, repair the skin multiply, reduce the pigmentation of the skin and improve the darkness of the face so as to achieve the effect of brightening the skin. The basil seeds are rich in a plurality of moisturizing components, and form a moisturizing and water-locking barrier on the skin, so that the skin can be kept in a moist and comfortable state. The plant protein and essential fatty acid contained in the basil seed can be fully extracted in water, so that the stability of the chemical property of the basil seed is protected, and the effects of moisturizing and brightening the skin color are better played.
The beauty effect of the peach blossom is mainly caused by that the flower contains nutrient substances such as peach blossom polysaccharide, kaempferol, coumarin, trifolioside, vitamin A, B, C and the like. The substances not only can effectively remove hydroxyl free radicals and delay senility, but also can expand blood vessels, dredge veins, moisten skin, promote blood circulation, promote skin nutrition and oxygen supply, accelerate the excretion of the aged lipofuscin of a human body and prevent melanin from accumulating in the skin, thereby effectively preventing chloasma, black specks and freckles. Peach blossom is also rich in plant protein and free amino acids, is easily absorbed by skin, and has effects of preventing and treating xerosis cutis, pachylosis and wrinkle, and enhancing disease resistance of skin, thereby preventing and treating seborrheic dermatitis, suppurative dermatitis, scurvy, etc. The main component of the peach blossom polysaccharide is a water-soluble substance and is insoluble in an organic solvent, so that the extraction of the effective components is fully ensured by adopting the reflux extraction of distilled water. In addition, the nutrient substances such as kaempferol, coumarins, trifoliosid and vitamin B, C can be fully enriched by heating and refluxing the water, so that the effects of fading color spots and moistening the skin can be well played.
The Eucheuma Gelatinosum contains abundant minerals and vitamins, can absorb water, contains starch sulfate as polysaccharide, and has good effect in protecting skin. The collagen in the cauliflower has the effects of improving wrinkles, fading black spots and the like, has the repairing effect on skin intradermal or subcutaneous tissue damage and deep wrinkles, can repair acne, scars and pimples left by the acne, and has the effects of regulating grease secretion, diminishing inflammation and sterilizing. Because of integrating water retention and tightening, the skin-care liquid can regulate the secretion of dry and oily skin, make the skin slowly tend to neutral skin, and shrink and tighten pores. The agar has good moisturizing effect, and can enhance the moisture retention of skin and improve the moisture of skin, so that the skin becomes more water-tender. It also contains protein, vitamin E, etc., has antioxidant effect, and can inhibit free radical generation, delay skin aging, reduce facial wrinkle generation, remove wrinkle and speckle, whiten skin, relieve inflammation, increase skin nutrition and moisture, and make skin elastic and active. The effective components contained in the extract can be dissolved in distilled water, so that the efficacy of the agar extract is ensured. Moreover, the gelidium amansii expands after absorbing water, and collagen of the gelidium amansii can be extracted under the condition of long-time reflux and micro-boiling, so that the gelidium amansii extracting solution has the effect of caring skin.
The okra is rich in mucilage containing various nutritional ingredients such as glycoprotein, pectin, bovine glycan, gum arabic and the like, and has a certain skin care effect. The okra is rich in protein, free amino acids, vitamin C, A, E, mineral elements such as phosphorus, iron, potassium, calcium, zinc, manganese and the like, and also contains viscous substances such as pectin, polysaccharide and the like, so that the okra can help to improve skin quality. The okra is rich in plant flavone, and the flavone is a good product for female beauty. The okra also contains rich plant flavonoid glycoside, and can promote the self-regulation of a human body in all directions by combining vitamins and trace element nutrient elements, thereby ensuring the effects of endocrine balance, aging resistance, fatigue resistance, blood circulation promotion and the like. The vitamin C has health care effect on skin and can achieve the effects of whitening and beautifying. It also contains vitamin E, has antioxidant effect, and can inhibit free radical generation, delay skin aging, and reduce facial wrinkles. The mucus of okra is the effective component, and the effective components such as pectin and polysaccharide can be fully dissolved by heating and extracting with distilled water, so that the extract has high stability. The pectin is fully extracted under the slightly boiling state, so that the loss of effective components is avoided.
The chanterelle is rich in protein, amino acid, fat, carbohydrate, vitamin, carotene, calcium, iron, phosphorus and other mineral nutrients, and especially rich in vitamin A. The antioxidant function of vitamin A can not only treat redness and swelling caused by sunburn, but also protect skin and prevent aging, can treat rough skin caused by vitamin A deficiency, can eliminate freckles and chloasma on facial parts, can also regulate cell differentiation of epidermal layers and promote cell metabolism, so when acne, spots, pimples or scars appear, the vitamin A is a good skin repairing agent. Vitamin A can also promote the growth of collagen and elastin, thereby enhancing the elasticity of skin and enhancing the water-locking effect. The chanterelle contains volatile ester components, and effective components are retained to the maximum extent by reflux extraction under a heating and micro-boiling state, so that component loss is reduced. In addition, the contained nutritional ingredients such as protein, vitamins and the like have good water solubility, so that the chanterelle extracting solution has rich ingredients and more comprehensive skin care.
Fructus Atriplicis Sibiricae has antiinflammatory and antipruritic effects, and can be used for treating pyocutaneous disease and pruritus due to wind-heat. The contained peroxide decomposing enzyme has obvious functions of resisting aging, removing freckles and softening and lubricating skin. In addition, the tribulus terrestris can effectively remove toxin accumulated in the body, tonify qi and enrich the blood, so that the phenomena of yellow, dark and pale face can be improved, and meanwhile, the tribulus terrestris can also inhibit the breeding of bacteria on the face. The tribulus polysaccharide and the saponin in the tribulus terrestris are easy to dissolve in water, and have good whitening and bacteriostasis effects. Therefore, the reflux extraction of water can keep the activity of the effective components under the premise of ensuring the extraction of the effective components.
Poria has effects in removing speckle, whitening skin, moistening skin, enhancing immunity, and dilating blood vessel. It can not only improve the immunity of the organism, but also make the oxyhemoglobin in the blood release more oxygen to supply to the tissue cells, and can also enhance the activity of the cell tissues, thereby making the skin more moist and achieving the effect of beautifying. Pachyman contained in Poria has effects of inhibiting free radical peroxidation, reducing lipid peroxidation, and reducing lipofuscin formation, thereby delaying organism aging. The poria cocos can effectively inhibit the activity of tyrosinase, prevent the generation of melanin, and effectively remove freckles and whiten the skin. Extracting effective components of Poria, and extracting by heating with water under reflux to avoid gasification of the effective components. Under the condition of ensuring that the effective components are not lost, the effective components are fully extracted and efficiently utilized.
The tea polyphenol in the green tea has the effects of resisting oxidation, removing free radicals and the like, can remove facial greasiness, astringe pores, has the effects of disinfection, antibiosis and skin aging resistance, is beneficial to reducing the damage and aging of ultraviolet rays in sunlight to the skin, can clean the skin, can protect the skin from being damaged, reduces toxins in the skin, and is natural sun cream. The green tea extract has strong antibacterial, enzyme inhibiting and astringent effects. Therefore, it can be used for preventing and treating dermatoses and skin allergy, and reducing skin pigmentation. In addition, theanine contained in green tea has tranquilizing effect, helps relax nerves, relieve body, and protect skin while making user enjoy sense. The green tea contains abundant vitamins, and can effectively inhibit activity of melanocyte and promote blood circulation. For people facing computers for a long time, the anti-radiation function of the green tea can protect cells from being damaged by radiation, is helpful for repairing damaged cells, and can also help to sweep out tarnish of skin, improve dullness and restore the skin to be transparent and white in healthy texture. Green tea helps to soften the skin and even improve skin tone. The distilled water is used for extracting effective components such as tea polyphenol in the green tea, so that the required components are retained, and the harm of other impurities is avoided, thereby ensuring the safety and stability of the green tea extracting solution.
The cherry is cool in nature and sweet in taste, and is one of the superior beauty fruits. The cherry contains a large amount of water and vitamin C, and can keep the skin tender, elastic and glossy after being frequently used, has the efficacy of removing freckles and effectively relieves skin aging. The cherry juice can help the facial skin to be tender, white and ruddy, and remove wrinkles and spots. It also contains vitamin A, and can balance sebum secretion, delay aging, enhance cell activity, and beautify skin. Because the vitamins contained in the cherries can be damaged under the heating state, the effective components are extracted by adopting an extraction method, so that the antioxidation effect of the cherries is fully exerted.
The motherwort contains various nutritional ingredients such as protein, carbohydrate and the like, and can effectively remove freckles, inhibit melanin formation, lighten pigments and relieve skin pigmentation. It contains multiple trace elements, wherein selenium has the function of enhancing the activity of immune cells; manganese can prevent aging. Therefore, the motherwort can benefit the face and beautify and resist aging. The motherwort herb is used as the facial cleanser, has the effects of enriching blood and promoting blood circulation, and can also be used for beautifying and protecting skin. The motherwort herb contains protein and trace elements with good water solubility, and can be kept in the extracting solution in the process of water reflux extraction, so that the motherwort herb extracting solution has various components and obvious effect.
The cordyceps flower contains rich protein, amino acid, mannitol, SOD, polysaccharide and other components, can nourish the skin, and has a good repair function on the skin. The nutrient components such as nucleotide and trace element selenium contained in the pigment can also inhibit pigmentation and inhibit the generation of color spots so as to lighten the color spots, and the pigment not only can moisten and preserve moisture, but also can obviously whiten and brighten the skin color. Because the cordyceps polysaccharide can obviously enhance the activity of superoxide dismutase and has obvious effects of resisting oxidation and removing oxygen free radicals and hydroxyl free radicals, the cordyceps polysaccharide has the effect of delaying senility on skin. The cordyceps flower also has a certain radiation resistance effect, and the radiation resistance of the skin is improved. Because the mass concentration of the cordyceps flower polysaccharide is positively correlated with the OH and DPPH free radical scavenging capacity and reducing capacity of the cordyceps flower polysaccharide, the components of the cordyceps flower polysaccharide can be fully extracted by long-time extraction during water extraction, so that the antioxidant and skin moistening effects of the extracting solution are more obvious.
The medlar contains rich medlar polysaccharide, carotene, vitamin E, selenium, flavonoid and other antioxidant substances, and has better antioxidation. The lycium barbarum polysaccharide can resist free radical peroxidation and relieve free radical peroxidation damage, thereby being beneficial to delaying aging, and also has good radiation resistance and effectively reduces the damage of electron radiation to skin. Because it is rich in multiple vitamins, it can discharge the toxin left by acne and metabolic disturbance, and promote the activity of skin cells, so as to obtain the effects of delaying senility, removing colour spot and whitening skin. In addition, the lycium barbarum polysaccharide has strong solubility in water, and the effective components of the lycium barbarum polysaccharide can be fully extracted by using a water reflux extraction method. Has good protection effect on other effective components such as carotene, vitamins and the like.
Tremella is rich in natural plant colloid, wherein Tremella polysaccharide is often used in various skin care cosmetics to repair skin and increase moisture on skin surface. It can improve the moisture of stratum corneum, and make skin softer and more elastic. It also reduces water evaporation and enhances the skin's self-protective barrier. The skin care product containing the tremella polysaccharide has smooth texture and is not sticky, a layer of protective film can be formed on the surface layer of the skin, the skin is kept tender and smooth and moist, the skin is not dry, tight and skinned, the regrowth of cells can be promoted, the skin regeneration is accelerated, the wrinkles are eliminated, and the young state of the skin is kept. In addition, it can activate skin cells damaged by ultraviolet irradiation, and enhance repairing function. The crude fiber of Tremella is extracted in colloid form during long-term water reflux, and can effectively remove chloasma and freckle on face and nourish skin.
The protein, the vitamin and the mineral elements which are rich in the skimmed milk powder can supplement sufficient nutrition to the skin, help the skin to diminish inflammation, reduce swelling and relieve the skin, and achieve the effects of protecting the skin and beautifying. Because the enzyme is contained in the skin care product, the skin care product can generate a beautifying effect on the skin, and can promote the decomposition of cutin on the surface of the skin, so that the skin becomes smoother and more tender. In addition, the vitamins and minerals also have natural moisturizing effect, are easily absorbed by the skin, can prevent the skin from drying, can repair dry lines and have excellent beautifying effect.
Vitamin C can effectively penetrate through the cuticle, permeate into the collagen tissue which directly stimulates the organism in the skin and produce a large amount of collagen, thereby enabling the surface of the skin to become plump and smooth, promoting the aged keratinocyte to fall off, enabling the pores to recover compact feeling from inside to outside, helping to fade spots, uniformize skin color and stably withdraw facial lines. In addition, vitamin C can resist damage of free radicals to skin, thereby delaying aging.
The synthetic egg white powder has the astringent effect of egg white, so that the synthetic egg white powder can effectively control the oil production condition of the face, can shrink pores, enables the skin to be cleaner and firmer, and is very suitable for people with oily skin. It also has the function of removing cutin of natural egg white, and can keep skin clean. The synthetic egg white powder aqueous solution contains fibrous mucin, has strong adsorption capacity, can easily suck out blackheads, whitens skin, has the functions of thickening, film forming, bacteriostasis and the like, and is lubricating and not sticky. It contains protein and monosaccharide, and can moisten and repair skin.
The pistachio nut oil is fresh and cool in texture, has no greasy feeling, can be quickly absorbed by skin, belongs to a nourishing oil product, is rich in vitamins, mineral substances and antioxidant elements, and has the effect of delaying aging. The vitamins and minerals can effectively supplement the elements required by the skin and care the growth of the skin. The antioxidant element changes the state of the skin by preventing the oxidation of free radicals to the skin. It contains a large amount of unsaturated fatty acids, and has effects in resisting aging, softening skin, and preventing sunburn.
Shea butter is pure natural vegetable oil, is mild and non-irritant, and has super-strong antioxidant effect. The shea butter has very close indexes with the human body secretion grease, contains rich non-saponified components which are easy to be absorbed by the human body, is deep and moist, can prevent the skin from drying and cracking, can form a protective film on the surface layer of the skin, and has remarkable moisturizing, sun-proof and protective effects. The shea butter is not only suitable for the skin of various babies and children with sensitive skin, but also can ensure that adults keep the natural elasticity of the skin. It contains triglyceride, and can form protective layer on skin surface to prevent water evaporation and moisturize skin. Shea butter has antiaging effect, and can promote collagen growth, make skin smooth and fine, and reduce wrinkle.
The malus micromalus oil is an excellent external healing agent, can help to restore skin health, has the functions of resisting inflammation, infection, bacteria and oxidation, can accelerate the growth of skin tissues and promote the formation of new epidermis. The malus johnsonii oil contains pyranocoumarin derivatives, wherein the pyranocoumarin can inhibit elastase, thereby preventing wrinkle generation and skin collapse. The malus micromalus oil can also effectively remove skin bacteria.
The universal emulsifier and the olive emulsifier are good emulsifiers. After the emulsifier is added to the oil-water system, the water and oil can be mixed with each other to form a fully dispersed emulsion. The emulsifier can improve the stability of the emulsion.
Sodium alginate is a natural polysaccharide, has high water solubility, is rich in anions, and has effects of promoting skin metabolism, stimulating fibroblast to generate more colloid, elastic scleroprotein and mucopolysaccharide, promoting epidermal cell growth, promoting metabolism, and preventing skin aging. It can make skin care product soft, smooth, and has effects of keeping moisture and resisting wrinkle, and can increase texture and viscosity of the final product. It can be used as stabilizer, thickener, emulsifier, dispersant, gelatinizer, coating agent, and suspending agent.
The lauroyl amphoacetate is a zwitterionic surfactant, is a foam booster, a surfactant and a cleaning solution, has the risk degree of 1, is safe and can be used safely. The sodium lauroamphoacetate has no acne-causing property, has excellent dirt removal, emulsion, dispersion, foam stabilization, wetting and static prevention, is a soft surfactant, can reduce the irritation and water hardness of other surfactants, and has good collocation.
The cocoyl amphoacetate is a zwitterionic surfactant, can be well mixed with various surfactants, can be compatible with soap base, has low irritation and milder to skin and eyes, can obviously reduce the irritation when being compounded with an anionic surfactant, has good foamability, rich and fine foam, good skin feel, can obviously improve the foam state of a formula system, is easy to biodegrade, has the degradation rate of more than 97 percent, and has good safety.
Potassium cocoate fatty acid glycinate is an anionic surfactant prepared from glycine and coconut oil fatty acid extracted from plant, and has hard water resistance and can obtain smooth and elastic foam. The sodium lauroamphoacetate has excellent emulsifying, dispersing, foaming, foam stabilizing, antistatic, solubilizing, wetting and penetrating performances, is a mild zwitterionic surfactant, can reduce the irritation of other surfactants, resists hard water and has good compatibility. The skin compatibility of the product can be obviously improved by compounding the product with an anionic surfactant.
Sodium carboxymethylcellulose is odorless, tasteless, hygroscopic, and easily dispersible in water to form a transparent colloidal solution. The sodium carboxymethyl cellulose is added into the system as a water-soluble colloidal tackifier, so that the viscosity can be increased, and the stability of the product can be improved.
The 1, 2-propylene glycol belongs to a micromolecule humectant, is almost colorless, odorless and non-greasy, can be completely dissolved in water, has an antiseptic effect, has the effects of mainly playing a role in hydrophilic moisture retention on skin, improving and maintaining the moisture retention and moisturizing degree of the skin, can absorb moisture in the environment, and has certain moisture absorption. In addition, the 1, 2-propylene glycol can be used as slipping agent, has strong permeability, is a common penetration enhancer, and can enhance the absorption of other components by skin.
The potassium soap generated by the saponification reaction of potassium hydroxide and fatty acid is an anionic surfactant and has good wetting, penetrating, dispersing and dirt removing capabilities.
The basil seed reduces the pigmentation of the skin; the peach blossom can accelerate the excretion of the aged lipofuscin of the human body and prevent the accumulation of melanin in the skin, thereby effectively preventing chloasma, black specks and freckles; removing black spots from the cauliflower; the chanterelle can eliminate freckle and chloasma on facial parts; removing speckle from fructus Atriplicis Sibiricae; poria can inhibit melanin production and remove speckle; the green tea can effectively inhibit activity of melanocyte and reduce skin pigmentation; removing spots from cherries; herba Leonuri can relieve skin pigmentation; the cordyceps flower can inhibit pigment deposition and inhibit color spot generation so as to fade color spots; removing color spots by using the wolfberry fruit; the tremella can effectively remove chloasma and freckles on the face; vitamin C helps to lighten spots and even skin color. The components supplement each other to reduce skin pigmentation and achieve the effect of fading spots.
The basil seed improves the darkness of the face so as to achieve the effect of brightening the skin; vitamin C in okra has the effects of whitening and beautifying; the tribulus terrestris can improve the phenomena of yellow, dark and pale face; whitening Poria; the poria cocos can help to sweep out tarnish of skin, improve dull and dull skin and restore the skin to be smooth, white and healthy; the cordyceps sinensis flower is white and the skin color is brightened; the medlar has the function of whitening the skin; the synthetic egg white powder can easily suck out blackheads and whiten the skin. In a word, the components supplement each other to achieve the effects of brightening the skin color and whitening and beautifying.
The basil seeds are rich in a plurality of moisturizing components, so that a moisturizing and water-locking barrier is formed on the skin, and the skin is kept in a moist and comfortable state; the peach blossom is also rich in vegetable protein and free amino acid, is easy to be absorbed by the skin, and is effective in preventing and treating dry skin, pachylosis, wrinkles and the like; the agar has good moisturizing effect; the chanterelle strengthens the water locking effect; the cordyceps flower has obvious moistening and moisturizing effects; tremella can increase moisture on skin surface and reduce moisture evaporation; the vitamins and minerals in the skimmed milk powder also have natural moisturizing effect; the 1, 2-propylene glycol belongs to a micromolecule humectant, not only plays a role in making skin hydrophilic and moisturizing, but also can improve and maintain the moistening feeling and the moisturizing degree of the skin. In a word, the components supplement each other to keep moisture and water, so that the skin is kept in a moist state.
The basil seeds can improve the skin nutrition condition; the peach blossom moistens the skin and promotes the supply of skin nutrition; the okra is rich in mucilage containing various nutritional ingredients such as glycoprotein, pectin, bovine glycan, gum arabic and the like, and has a certain skin care effect; the chanterelle is rich in protein, amino acid, fat, carbohydrate, vitamin, carotene, calcium, iron, phosphorus and other mineral nutrients, especially rich in vitamin A, and can nourish and protect skin; the Cordyceps flower is rich in protein, amino acids, mannitol, SOD, polysaccharides, etc., and can nourish skin; tremella can nourish skin; the protein, the vitamin and the mineral elements which are rich in the skimmed milk powder can supplement sufficient nutrition for the skin; the synthetic egg white powder can moisten skin; poria moistens skin. In a word, the components supplement each other and play the effects of nourishing and moistening the skin.
The invention is white emulsion, has proper viscosity, fine and uniform texture, bright and moist luster, good foamability and fragrant smell.
Compared with the prior art, the facial cleanser provided by the invention contains various natural plant active ingredients, is fine and smooth in texture, quick to absorb, good in foamability and aromatic in smell, can effectively fade color spots, can comprehensively repair skin damage, deeply nourish and moisturize skin, and improves the skin resistance.
Drawings
FIG. 1 is a diagram of a product of the present invention;
FIG. 2 is a graph of a foaming test of a product of the present invention;
FIG. 3 is a diagram of the preparation process of the product of the present invention;
FIG. 4 is a graph of a comparative product, layered during placement.
Detailed Description
The present invention will be further described with reference to the following examples.
According to the rules of pharmacopoeia, in the preparation process, the coarse powder can completely pass through a No. two sieve, but is mixed with powder which can pass through a No. four sieve by no more than 40%; all heat extractions were carried out under slightly boiling conditions.
Example 1
A preparation method of a moisturizing facial cleanser with freckle removing, skin brightening and nourishing functions and natural plant active ingredients comprises the following steps:
1.1, preparation of a basil seed extracting solution:
weighing appropriate amount of basil seed, heating and reflux extracting with water for 3 times: adding water 20 times the weight of the cymbidium seed for the 1 st time, soaking for 0.25h, and extracting for 1.5 h; adding 15 times of water of the weight of the cymbidium balsamifera seed for 2 times, and extracting for 1.0 h; adding 8 times of water of the weight of the basil seed in the 3 rd time, extracting for 0.5h, filtering with four layers of gauze each time, combining filtrates, performing suction filtration, and concentrating the volume of the filtrate to 15 times of the weight of the basil seed (mL/g), to obtain the basil seed extract for later use.
1.2 preparing peach blossom extracting solution:
weighing appropriate amount of dried flos persicae, and extracting with water under heating and refluxing for 3 times: adding water 15 times the weight of the dried peach blossom for the first time, soaking for 0.5h, and extracting for 1.0 h; adding 10 times of water of the weight of the dried peach blossom for the 2 nd time, and extracting for 1.0 h; adding water 5 times the weight of the dried peach blossom in the 3 rd time, extracting for 0.5h, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 5 mL/g of the weight of the dried peach blossom to obtain peach blossom extract for use.
1.3, preparation of agar extracting solution:
weighing appropriate amount of Eucheuma Gelatinosum, heating and reflux-extracting with water for 3 times: adding 10 times of water by mass of Gelidium amansii into the mixture at the 1 st time, soaking for 0.2h, and extracting for 1.0 h; adding 10 times of water by mass of Gelidium amansii in the 2 nd extraction for 0.5 h; adding 8 times of water by mass of Eucheuma Gelatinosum in 3 rd time, extracting for 0.5 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 3 times of weight of Eucheuma Gelatinosum (mL/g) to obtain Eucheuma Gelatinosum extractive solution.
1.4 preparation of okra extract:
weighing appropriate amount of okra, heating and reflux-extracting with water for 3 times: adding water with the amount of 8 times of that of okra at the 1 st time, soaking for 0.2h, and extracting for 1.0 h; adding water with the amount of 8 times of that of okra at the 2 nd time, and extracting for 0.5 h; adding 6 times of water by weight of okra in the 3 rd time, extracting for 0.5h, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 2 times of okra weight mL/g to obtain okra extractive solution for use.
1.5 preparation of chanterelle extract:
weighing appropriate amount of chanterelle, heating and reflux-extracting with water for 3 times: adding water with the mass of 20 times of that of the chanterelle at the 1 st time, soaking for 0.5h, and extracting for 1.5 h; adding 15 times of water of the mass of the chanterelle at the 2 nd time, and extracting for 1.5 h; adding 5 times of water by mass of chanterelle at 3 rd time, extracting for 0.5h, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 10 times of weight of chanterelle (mL/g) to obtain chanterelle extractive solution.
1.6 preparation of tribulus terrestris extract:
weighing for 1.0 h; adding 12 times of water of the weight of the tribulus terrestris for 2 times, and extracting for 1.0 h; adding fructus Tribuli coarse powder 8 times of the weight of fructus Tribuli at the 3 rd time, and extracting with water under heating and refluxing for 3 times: adding water 15 times the weight of the tribulus terrestris into the mixture at the 1 st time, soaking for 0.2h, extracting water, extracting for 0.5h, filtering with four layers of gauze each time, combining filtrates, performing suction filtration, and concentrating the volume of the filtrate to 8 mL/g of the weight of the tribulus terrestris to obtain the tribulus terrestris extract for later use.
1.7 preparation of tuckahoe extract:
weighing appropriate amount of Poria cocos slice, heating and reflux extracting with water for 3 times: adding 12 times of water for the first time, soaking for 0.5 hr, and extracting for 1.0 hr; adding 8 times of water for 2 times, extracting for 1.0h, and filtering to obtain filtrate; adding 7 times of water for 3 times, extracting for 0.5 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 10 times of Poria weight mL/g to obtain Poria extract.
1.8 preparation of green tea extract:
weighing appropriate amount of green tea, heating and reflux extracting with water for 3 times: adding 10 times of water by mass of green tea at 1 time, soaking for 0.5 hr, and extracting for 1.0 hr; adding water 8 times the weight of green tea in the 2 nd time, and extracting for 1.0 h; adding water 7 times the weight of green tea in the 3 rd time, extracting for 0.5 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 15 times of green tea weight mL/g to obtain green tea extractive solution.
1.9 preparation of cherry squeezing liquid:
weighing a proper amount of fresh cherries, putting the fresh cherries into a juicer, adding 10 times of water, squeezing for 0.5min in a juicing mode to obtain filtrate, filtering the filtrate by using four layers of gauze, centrifuging the filtrate, taking supernate, and concentrating the volume of the filtrate to be 1 mL/g of the weight of the cherries to obtain cherry squeezed liquid for later use.
1.10 preparation of motherwort extract:
weighing appropriate amount of herba Leonuri, extracting with water under heating and refluxing for 3 times: adding 18 times of water of herba Leonuri at 1 st time, soaking for 0.5 hr, and extracting for 1.5 hr; adding 15 times of water of herba Leonuri for the 2 nd time, and extracting for 1.5 hr; adding 8 times of water by mass of herba Leonuri into the filtrate at 3 rd time, extracting for 0.5 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 20 times of herba Leonuri weight mL/g to obtain herba Leonuri extractive solution.
1.11 preparation of cordyceps flower extract:
weighing appropriate amount of Cordyceps flower, and extracting with water under heating and refluxing for 3 times: adding water 20 times the mass of Cordyceps flower at 1 st time, soaking for 0.5 hr, and extracting for 1.5 hr; adding 18 times of water of the mass of Cordyceps for 2 times, and extracting for 1.0 hr; adding 15 times of water of the mass of the cordyceps flower in the 3 rd time, extracting for 0.5h, filtering with four layers of gauze each time, combining filtrates, performing suction filtration, and concentrating the volume of the filtrate to 10 times mL/g of the weight of the cordyceps flower to obtain cordyceps flower extract for later use.
1.12 preparation of the medlar extracting solution:
weighing appropriate amount of fructus Lycii, and extracting with water under heating and refluxing for 3 times: adding 16 times of water of fructus Lycii at 1 st time, and reflux extracting for 1.0 hr; adding 12 times of water of fructus Lycii for 2 times, and reflux extracting for 1.0 hr; adding 8 times of water of fructus Lycii weight for 3 times, reflux extracting for 1.0 hr, filtering to obtain filtrate, mixing filtrates, vacuum filtering, and concentrating the filtrate to 15 times of the weight of fructus Lycii (mL/g) to obtain fructus Lycii extractive solution.
1.13 preparation of tremella extract:
weighing appropriate amount of Tremella, extracting with water under heating and refluxing for 3 times: adding water 20 times the weight of Tremella 1, soaking for 0.5 hr, and extracting for 1.5 hr; adding water 15 times the weight of Tremella at 2 times, and extracting for 1.0 hr; adding 10 times of water by mass of Tremella for 3 times, extracting for 0.5 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 10 times of Tremella weight (mL/g) to obtain Tremella extractive solution.
1.14 preparation method of moisturizing facial cleanser for removing freckles, brightening skin and nourishing skin comprises the following steps:
a) weighing 0.5g of sodium alginate, adding 30mL of distilled water, placing in a constant-temperature water bath kettle at 60 ℃, heating and stirring for 5min, and standing at normal temperature for 2h to obtain a sodium alginate gel solution for later use;
b) weighing 0.5g of sodium carboxymethylcellulose, dissolving in 25mL of distilled water, standing for 12h, and obtaining uniform and transparent sodium carboxymethylcellulose gel liquid for later use after the sodium carboxymethylcellulose is naturally swelled and dissolved;
c) weighing 0.05g of synthetic egg white powder, adding 10mL of distilled water, placing in a constant-temperature water bath kettle at 60 ℃, stirring for 5min, taking out, and standing for 5h at normal temperature to obtain a synthetic egg white powder solution for later use;
d) weighing 0.3g of ethylparaben, adding 1mL of 1, 2-propylene glycol, stirring and dissolving to obtain a preservative solution for later use;
e) weighing 1.5g pistachio nut oil, placing in a constant temperature water bath kettle at 70 deg.C, and heating to obtain oil A;
f) weighing 0.50g of potassium hydroxide, weighing 2mL of distilled water, and adding the distilled water into the potassium hydroxide to completely dissolve the potassium hydroxide;
g) adding the solution obtained in the step f) into the oil A obtained in the step e) in a trickle shape, heating and uniformly stirring in the same direction for reacting for 15min to fully react to obtain a soap solution B;
h) respectively weighing 3.0g of shea butter, 3.0g of malus micromalus linn oil, 2.5g of universal emulsifier and 2.5g of olive emulsifier, fully mixing, placing in a constant-temperature water bath kettle at 70 ℃, heating while stirring to uniformly mix to obtain an oil phase;
i) measuring 5mL of distilled water, and heating in a constant-temperature water bath kettle at 70 ℃ to obtain a water phase;
j) slowly adding the water phase into the oil phase along the wall of the container when the oil phase and the water phase reach the same temperature, heating and stirring at the same direction at constant speed for 15min, and emulsifying to obtain O/W emulsion matrix;
k) adding the formed emulsion matrix into soap solution B, placing in 70 deg.C water bath, heating while stirring for 10min to obtain mixed solution C;
l) respectively measuring 20mL of coconut oil fatty acid potassium glycinate, 2mL of sodium lauroamphoacetate and 2mL of sodium cocoamphoacetate, adding the mixture into the mixed solution C, and stirring for 3min to uniformly mix the mixture to obtain mixed solution D;
m) respectively weighing 0.1g of skimmed milk powder and 0.1g of vitamin C, dissolving with 2mL of distilled water respectively, and adding into the mixed solution D;
n) respectively measuring 1mL of basil seed extract, 1mL of peach blossom extract, 1mL of agar extract, 1mL of okra extract, 1mL of chanterelle extract, 1mL of tribulus terrestris extract, 1mL of poria cocos extract, 1mL of green tea extract, 1mL of cherry extract, 1mL of motherwort extract, 1mL of cordyceps flower extract, 1mL of wolfberry extract and 1mL of tremella extract, adding the obtained mixture into the mixed solution D, and uniformly stirring to obtain mixed solution E;
o) adding the prepared synthetic egg white powder solution, the sodium alginate gel solution and the sodium carboxymethyl cellulose gel solution into the mixed solution E, stirring to mix the mixed solution E fully and uniformly, then adding 0.05g of strawberry essence and preservative solution, stirring and mixing uniformly to obtain the spot-removing, skin-brightening and nourishing moisturizing facial cleanser containing natural plant active ingredients.
Example 2
A preparation method of a moisturizing facial cleanser with freckle removing, skin brightening and nourishing functions and natural plant active ingredients comprises the following steps:
2.1, preparation of a basil seed extracting solution:
weighing appropriate amount of basil seed, heating and reflux extracting with water for 3 times: adding 22 times of water by mass of the cymbidium balsamifera seed for 1 time, soaking for 0.5h, and extracting for 2.0 h; adding 16 times of water of the weight of the cymbidium balsamifera seed for 2 times, and extracting for 1.3 h; adding 10 times of water of the weight of the basil seed in the 3 rd time, extracting for 0.75h, filtering with four layers of gauze each time, combining filtrates, performing suction filtration, and concentrating the volume of the filtrate to 18 times of the weight of the basil seed in mL/g to obtain a basil seed extract for later use.
2.2 preparing peach blossom extracting solution:
weighing appropriate amount of dried flos persicae, and extracting with water under heating and refluxing for 3 times: adding water with the amount of 18 times of the weight of the dried peach blossom for the first time, soaking for 0.7h, and extracting for 1.2 h; adding water with the amount of 12 times of the weight of the dried peach blossom for the 2 nd time, and extracting for 1.2 h; adding water 8 times the weight of the dried peach blossom into the peach blossom at the 3 rd time, extracting for 1.0h, filtering with four layers of gauze each time, combining filtrates, filtering, and concentrating the filtrate to 8 mL/g times the weight of the dried peach blossom to obtain peach blossom extract for later use.
2.3 preparation of agar extract:
weighing appropriate amount of Eucheuma Gelatinosum, heating and reflux-extracting with water for 3 times: adding 12 times of water by mass of Gelidium amansii at 1 st time, soaking for 0.5 hr, and extracting for 2.0 hr; adding 12 times of water by mass of Gelidium amansii at the 2 nd time, and extracting for 1.0 h; adding water 9 times the weight of Gelidium amansii into the filtrate at 3 rd time, extracting for 0.8 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 5 mL/g times the weight of Gelidium amansii to obtain Gelidium amansii extractive solution.
2.4 preparation of okra extract:
weighing appropriate amount of okra, heating and reflux-extracting with water for 3 times: adding water 9 times the weight of okra at the 1 st time, soaking for 0.5h, and extracting for 1.3 h; adding water 9 times the weight of okra at the 2 nd time, and extracting for 1.0 h; adding water 7 times the weight of okra in the 3 rd time, extracting for 0.8h, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 5 mL/g of okra weight to obtain okra extractive solution.
2.5 preparation of chanterelle extract:
weighing appropriate amount of chanterelle, heating and reflux-extracting with water for 3 times: adding 23 times of water by mass of chanterelle at 1 st time, soaking for 0.8h, and extracting for 1.8 h; adding 18 times of water of the mass of the chanterelle at the 2 nd time, and extracting for 1.8 h; adding 7 times of water by mass of chanterelle at 3 rd time, extracting for 1.0h, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 11 times of weight of chanterelle (mL/g) to obtain chanterelle extractive solution.
2.6 preparation of the tribulus terrestris extract:
weighing appropriate amount of fructus Tribuli coarse powder, and extracting with water under heating and refluxing for 3 times: adding 18 times of water of the weight of the tribulus terrestris at the 1 st time, soaking for 0.5h, and extracting for 2.0 h; adding 13 times of water of the weight of the tribulus terrestris for 2 times, and extracting for 1.3 h; adding 10 times of water by mass of fructus Atriplicis Sibiricae for 3 times, extracting for 0.8 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 10 times of weight of fructus Atriplicis Sibiricae mL/g to obtain fructus Atriplicis Sibiricae extract.
2.7 preparation of Poria cocos extract:
weighing appropriate amount of Poria cocos slice, heating and reflux extracting with water for 3 times: adding 14 times of water for the first time, soaking for 0.8h, and extracting for 2.0 h; adding 10 times of water for the 2 nd time, extracting for 1.3h, and filtering to obtain filtrate; adding 8 times of water at 3 rd time, extracting for 0.8 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to volume 15 times mL/g of Poria to obtain Poria extract.
2.8 preparation of green tea extract:
weighing appropriate amount of green tea, heating and reflux extracting with water for 3 times: adding water 13 times the weight of green tea at 1 st time, soaking for 0.6 hr, and extracting for 1.5 hr; adding 10 times of water by weight of green tea for 2 times, and extracting for 1.3 hr; adding water 8 times the weight of green tea in the 3 rd time, extracting for 0.8 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 16 times mL/g of green tea weight to obtain green tea extractive solution.
2.9 preparation of cherry squeezing liquid:
weighing a proper amount of fresh cherries, putting the fresh cherries into a juicer, adding 13 times of water, squeezing for 1.0min in a juicing mode to obtain filtrate, filtering the filtrate by using four layers of gauze, centrifuging the filtrate, taking supernate, and concentrating the volume of the filtrate to 1.3 times of the weight of the cherries (mL/g), thus obtaining cherry squeezed liquid for later use.
2.10 preparation of motherwort extract:
weighing appropriate amount of herba Leonuri, extracting with water under heating and refluxing for 3 times: adding 20 times of water of herba Leonuri at 1 st time, soaking for 0.7 hr, and extracting for 2.0 hr; adding 16 times of water of herba Leonuri for the 2 nd time, and extracting for 1.7 hr; adding 10 times of water by mass of herba Leonuri in 3 rd time, extracting for 0.8 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 22 times of herba Leonuri weight mL/g to obtain herba Leonuri extractive solution.
2.11 preparation of cordyceps flower extract:
weighing appropriate amount of Cordyceps flower, and extracting with water under heating and refluxing for 3 times: adding 22 times of water of the mass of the cordyceps flower into the cordyceps flower for 1 time, soaking for 0.8h, and extracting for 1.7 h; adding water 19 times the mass of Cordyceps flower in the 2 nd time, and extracting for 1.2 hr; adding 16 times of water for 3 times of the weight of Cordyceps flower, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 12 times of the weight of Cordyceps flower (mL/g) to obtain Cordyceps flower extractive solution.
2.12 preparation of the medlar extracting solution:
weighing appropriate amount of fructus Lycii, and extracting with water under heating and refluxing for 3 times: adding 17 times of water of fructus Lycii at 1 st time, and reflux extracting for 1.5 hr; adding 13 times of water of fructus Lycii for 2 times, and reflux extracting for 1.3 hr; adding 9 times of water by mass of fructus Lycii in 3 rd time, reflux extracting for 1.3 hr, filtering to obtain filtrate, mixing filtrates, vacuum filtering, and concentrating the filtrate to 18 times of weight of fructus Lycii (mL/g) to obtain fructus Lycii extractive solution.
2.13 preparation of tremella extract:
weighing appropriate amount of Tremella, extracting with water under heating and refluxing for 3 times: adding 22 times of water by mass of Tremella 1, soaking for 0.8 hr, and extracting for 1.8 hr; adding 16 times of water by mass of Tremella at 2 times, and extracting for 1.2 hr; adding 12 times of water by mass of Tremella for 3 times, extracting for 0.7 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 12 times of Tremella weight (mL/g) to obtain Tremella extractive solution.
2.14 preparation method of moisturizing facial cleanser for removing freckles, brightening skin and nourishing skin comprises the following steps:
a) weighing 0.6g of sodium alginate, adding 35mL of distilled water, placing in a constant-temperature water bath kettle at 70 ℃, heating and stirring for 10min, and standing at normal temperature for 3h to obtain a sodium alginate gel solution for later use;
b) weighing 0.6g of sodium carboxymethylcellulose, dissolving in 27mL of distilled water, standing for 18h, and obtaining uniform and transparent sodium carboxymethylcellulose gel liquid for later use after the sodium carboxymethylcellulose is naturally swelled and dissolved;
c) weighing 0.07g of synthetic egg white powder, adding 15mL of distilled water, placing in a constant-temperature water bath kettle at 70 ℃, stirring for 7min, taking out, and standing at normal temperature for 5.5h to obtain a synthetic egg white powder solution for later use;
d) weighing 0.5g of ethylparaben, adding 2mL of 1, 2-propylene glycol, stirring and dissolving to obtain a preservative solution for later use;
e) weighing 1.7g pistachio nut oil, placing in a water bath kettle with constant temperature of 80 deg.C, and heating to obtain oil A;
f) weighing 0.60g of potassium hydroxide, weighing 3mL of distilled water, and adding the distilled water into the potassium hydroxide to completely dissolve the potassium hydroxide;
g) adding the solution obtained in the step f) into the oil A obtained in the step e) in a trickle shape, heating and uniformly stirring in the same direction for reacting for 20min to obtain a soap solution B;
h) weighing 5.0g of shea butter, 5.0g of malus micromalus linn oil, 5.2g of universal emulsifier and 4.0g of olive emulsifier respectively, mixing completely, placing in a 80 ℃ constant temperature water bath kettle, heating while stirring to mix uniformly to obtain an oil phase;
i) measuring 15mL of distilled water, and heating in a water bath kettle with constant temperature of 80 ℃ to obtain a water phase;
j) slowly adding the water phase into the oil phase along the wall of the container when the oil phase and the water phase reach the same temperature, heating and stirring at the same direction at constant speed for 22min, and emulsifying to obtain O/W emulsion matrix;
k) adding the formed emulsion matrix into soap solution B, placing in 80 deg.C water bath, heating while stirring for 13min to obtain mixed solution C;
l) respectively measuring 23mL of coconut oil fatty acid potassium glycinate, 5mL of lauroyl amphoteric sodium acetate and 8mL of cocoyl amphoteric sodium acetate, adding into the mixed solution C, and stirring for 6min to uniformly mix to obtain a mixed solution D;
m) respectively weighing 0.15g of skimmed milk powder and 0.12g of vitamin C, dissolving with 3mL of distilled water respectively, and adding into the mixed solution D;
n) respectively measuring 5mL of basil seed extract, 4mL of peach blossom extract, 3mL of gelidium amansii extract, 3mL of okra extract, 5mL of chanterelle extract, 4mL of tribulus terrestris extract, 5mL of poria cocos extract, 6mL of green tea extract, 3mL of cherry extract, 4mL of motherwort extract, 5mL of cordyceps flower extract, 4mL of wolfberry extract and 6mL of tremella extract, adding the obtained mixture into the mixed solution D, and uniformly stirring to obtain mixed solution E;
o) completely adding the prepared synthetic egg white powder solution, the sodium alginate gel solution and the sodium carboxymethyl cellulose gel solution into the mixed solution E, stirring to fully and uniformly mix the mixed solution, then adding 0.20g of osmanthus essence and the preservative solution, and stirring and uniformly mixing to obtain the freckle-removing, skin-brightening and nourishing moisturizing facial cleanser containing natural plant active ingredients.
Example 3
A preparation method of a moisturizing facial cleanser with freckle removing, skin brightening and nourishing functions and natural plant active ingredients comprises the following steps:
3.1 preparation of the basil seed extract:
weighing appropriate amount of basil seed, heating and reflux extracting with water for 3 times: adding water with the amount of 25 times of the weight of the cymbidium balsamifera seed for 1 time, soaking for 0.75h, and extracting for 2.5 h; adding 18 times of water of the weight of the cymbidium balsamifera seed for 2 times, and extracting for 1.5 h; adding 12 times of water of the weight of the basil seed in the 3 rd time, extracting for 1.0h, filtering with four layers of gauze each time, combining filtrates, performing suction filtration, and concentrating the volume of the filtrate to 20 times of the weight of the basil seed (mL/g), to obtain the basil seed extract for later use.
3.2 preparing peach blossom extracting solution:
weighing appropriate amount of dried flos persicae, and extracting with water under heating and refluxing for 3 times: adding water 20 times the weight of the dried peach blossom for the first time, soaking for 1.0h, and extracting for 1.5 h; adding 14 times of water of the weight of the dried peach blossom for the 2 nd time, and extracting for 1.5 h; adding water with the weight 10 times of that of the dried peach blossom in the 3 rd time, extracting for 1.5h, filtering with four layers of gauze each time, combining filtrates, filtering, and concentrating the filtrate to obtain peach blossom extract with the volume 10 times mL/g of the weight of the dried peach blossom.
3.3 preparation of Eucheuma Gelatinosum extract:
weighing appropriate amount of Eucheuma Gelatinosum, heating and reflux-extracting with water for 3 times: adding water 15 times the weight of Gelidium amansii at 1 st time, soaking for 0.7 hr, and extracting for 2.5 hr; adding 13 times of water by mass of Gelidium amansii at the 2 nd time, and extracting for 1.5 hr; adding 10 times of water by mass of Eucheuma Gelatinosum in 3 rd time, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 8 times of weight of Eucheuma Gelatinosum (mL/g) to obtain Eucheuma Gelatinosum extractive solution.
3.4 preparation of okra extract:
weighing appropriate amount of okra, heating and reflux-extracting with water for 3 times: adding water with the amount of 10 times of that of okra at the 1 st time, soaking for 0.7h, and extracting for 1.5 h; adding water 10 times the weight of okra at the 2 nd time, and extracting for 1.5 h; adding water 8 times the weight of okra in the 3 rd time, extracting for 1.0h, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 7 mL/g of okra weight to obtain okra extractive solution.
3.5 preparation of chanterelle extract:
weighing appropriate amount of chanterelle, heating and reflux-extracting with water for 3 times: adding water with the weight of 25 times of that of the chanterelle at the 1 st time, soaking for 1.0h, and extracting for 2.0 h; adding water with the mass of 20 times of that of the chanterelle for 2 times, and extracting for 2.0 h; adding 8 times of water by mass of chanterelle at 3 rd time, extracting for 1.5h, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 13 times of weight of chanterelle (mL/g) to obtain chanterelle extractive solution.
3.6 preparation of the tribulus terrestris extract:
weighing appropriate amount of fructus Tribuli coarse powder, and extracting with water under heating and refluxing for 3 times: adding water with the amount of 20 times of the weight of the tribulus terrestris into the mixture at the 1 st time, soaking for 0.7h, and extracting for 2.5 h; adding water 15 times the weight of fructus Atriplicis Sibiricae at the 2 nd time, and extracting for 1.5 hr; adding 12 times of water by mass of fructus Atriplicis Sibiricae for 3 times, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 12 times of weight of fructus Atriplicis Sibiricae (mL/g) to obtain fructus Atriplicis Sibiricae extract.
3.7 preparation of Poria cocos extractive solution:
weighing appropriate amount of Poria cocos slice, heating and reflux extracting with water for 3 times: adding 16 times of water for the first time, soaking for 1.0 hr, and extracting for 2.5 hr; adding 12 times of water for the 2 nd time, extracting for 1.5h, and filtering to obtain filtrate; adding 9 times of water at 3 rd time, extracting for 1.2 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 20 times of Poria weight (mL/g) to obtain Poria extract.
3.8 preparation of Green tea extract:
weighing appropriate amount of green tea, heating and reflux extracting with water for 3 times: adding water 15 times the weight of green tea at 1 st time, soaking for 0.7 hr, and extracting for 2.0 hr; adding water 12 times the weight of green tea in the 2 nd time, and extracting for 1.5 hr; adding 10 times of water by weight of green tea in the 3 rd time, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 18 times of green tea weight mL/g to obtain green tea extractive solution.
3.9 preparation of cherry squeezing liquid:
weighing a proper amount of fresh cherries, putting the fresh cherries into a juicer, adding 15 times of water, squeezing for 2.0min in a juicing mode to obtain filtrate, filtering the filtrate by using four layers of gauze, centrifuging the filtrate, taking supernate, and concentrating the volume of the filtrate to 1.5 times mL/g of the weight of the cherries to obtain cherry squeezed liquid for later use.
3.10 preparation of motherwort extract:
weighing appropriate amount of herba Leonuri, extracting with water under heating and refluxing for 3 times: adding 22 times of water by mass of herba Leonuri at 1 st time, soaking for 1.0 hr, and extracting for 2.5 hr; adding 18 times of water of herba Leonuri for 2 times, and extracting for 2.0 hr; adding 13 times of water by mass of herba Leonuri in 3 rd time, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 25 times mL/g of herba Leonuri to obtain herba Leonuri extractive solution.
3.11 preparation of cordyceps flower extract:
weighing appropriate amount of Cordyceps flower, and extracting with water under heating and refluxing for 3 times: adding water with an amount of 25 times of the mass of the cordyceps flower for 1 time, soaking for 1.0h, and extracting for 2.0 h; adding 20 times of water of the mass of Cordyceps for 2 times, and extracting for 1.5 hr; adding 18 times of water of the mass of the cordyceps flower in the 3 rd time, extracting for 1.5h, filtering with four layers of gauze each time, combining filtrates, performing suction filtration, and concentrating the volume of the filtrate to 15 times mL/g of the weight of the cordyceps flower to obtain cordyceps flower extract for later use.
3.12 preparation of the medlar extracting solution:
weighing appropriate amount of fructus Lycii, and extracting with water under heating and refluxing for 3 times: adding 18 times of water of fructus Lycii at 1 st time, and reflux extracting for 2.0 hr; adding 14 times of water of fructus Lycii for 2 times, and reflux extracting for 1.5 hr; adding 10 times of water of fructus Lycii weight for 3 times, reflux extracting for 1.5 hr, filtering to obtain filtrate, mixing filtrates, vacuum filtering, and concentrating the filtrate to 20 times of fructus Lycii weight mL/g to obtain fructus Lycii extractive solution.
3.13 preparation of Tremella extract:
weighing appropriate amount of Tremella, extracting with water under heating and refluxing for 3 times: adding water with an amount of 25 times of the weight of the tremella at 1 st time, soaking for 1.0h, and extracting for 2.0 h; adding 18 times of water by mass of Tremella at 2 times, and extracting for 1.5 hr; adding 15 times of water by mass of Tremella in 3 rd time, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 15 times of Tremella weight (mL/g) to obtain Tremella extractive solution.
3.14 preparation method of moisturizing facial cleanser for removing freckles, brightening skin and nourishing skin comprises the following steps:
a) weighing 0.7g of sodium alginate, adding 40mL of distilled water, placing in a constant-temperature water bath kettle at 80 ℃, heating and stirring for 15min, and standing at normal temperature for 5h to obtain a sodium alginate gel solution for later use;
b) weighing 0.7g of sodium carboxymethylcellulose, dissolving in 30mL of distilled water, standing for 24h, and obtaining uniform and transparent sodium carboxymethylcellulose gel liquid for later use after the sodium carboxymethylcellulose is naturally swelled and dissolved;
c) weighing 0.1g of synthetic egg white powder, adding 20mL of distilled water, placing in a constant temperature water bath kettle at 60-80 deg.C, stirring for 10min, taking out, standing at normal temperature for 6h to obtain synthetic egg white powder solution for use;
d) weighing 0.8g of ethylparaben, adding 3mL of 1, 2-propylene glycol, stirring and dissolving to obtain a preservative solution for later use;
e) weighing 2.0g pistachio nut oil, placing in a water bath kettle with constant temperature of 90 deg.C, and heating to obtain oil A;
f) weighing 0.65g of potassium hydroxide, weighing 5mL of distilled water, and adding the distilled water into the potassium hydroxide to completely dissolve the potassium hydroxide;
g) adding the solution obtained in the step f) into the oil A obtained in the step e) in a trickle shape, heating and uniformly stirring in the same direction for reacting for 25min to fully react to obtain a soap solution B;
h) weighing 7.0g of shea butter, 7.5g of malus micromalus linn oil, 6.5g of universal emulsifier and 6.0g of olive emulsifier respectively, mixing completely, placing in a water bath kettle with constant temperature of 90 ℃, heating while stirring to mix uniformly to obtain an oil phase;
i) measuring 20mL of distilled water, and heating in a 90 ℃ constant-temperature water bath kettle to obtain a water phase;
j) slowly adding the water phase into the oil phase along the wall of the container when the oil phase and the water phase reach the same temperature, heating and stirring at the same direction at constant speed for 30min, and emulsifying to obtain O/W emulsion matrix;
k) adding the formed emulsion matrix into soap solution B, placing in 90 deg.C water bath, heating while stirring for 15min to obtain mixed solution C;
l) respectively measuring 25mL of coconut oil fatty acid potassium glycinate, 10mL of sodium lauroyl amphoacetate and 12mL of sodium cocoyl amphoacetate, adding the mixture into the mixed solution C, and stirring for 10min to uniformly mix the mixture to obtain mixed solution D;
m) respectively weighing 0.2g of skimmed milk powder and 0.15g of vitamin C, dissolving with 4mL of distilled water respectively, and adding into the mixed solution D;
n) respectively measuring 9mL of basil seed extracting solution, 8mL of peach blossom extracting solution, 7mL of gelidium amansii extracting solution, 5mL of okra extracting solution, 10mL of chanterelle extracting solution, 8mL of tribulus terrestris extracting solution, 10mL of poria cocos extracting solution, 11mL of green tea extracting solution, 7mL of cherry squeezing solution, 8mL of motherwort extracting solution, 10mL of cordyceps flower extracting solution, 9mL of medlar extracting solution and 12mL of tremella extracting solution, adding the obtained mixture into the mixed solution D, and uniformly stirring the obtained mixture to obtain mixed solution E;
o) adding the prepared synthetic egg white powder solution, the sodium alginate gel solution and the sodium carboxymethyl cellulose gel solution into the mixed solution E, stirring to mix the mixed solution E fully and uniformly, then adding 0.40g of rose essence and preservative solution, stirring and mixing uniformly to obtain the spot-removing, skin-brightening and nourishing moisturizing facial cleanser containing natural plant active ingredients.
Example 4 (as a comparative example)
4.1 preparation of the basil seed extract:
weighing appropriate amount of basil seed, heating and reflux extracting with water for 3 times: adding water with the amount of 25 times of the weight of the cymbidium balsamifera seed for 1 time, soaking for 0.75h, and extracting for 2.5 h; adding 18 times of water of the weight of the cymbidium balsamifera seed for 2 times, and extracting for 1.5 h; adding 12 times of water of the weight of the basil seed in the 3 rd time, extracting for 1.0h, filtering with four layers of gauze each time, combining filtrates, performing suction filtration, and concentrating the volume of the filtrate to 20 times of the weight of the basil seed (mL/g), to obtain the basil seed extract for later use.
4.2 preparing peach blossom extracting solution:
weighing appropriate amount of dried flos persicae, and extracting with water under heating and refluxing for 3 times: adding water 20 times the weight of the dried peach blossom for the first time, soaking for 1.0h, and extracting for 1.5 h; adding 14 times of water of the weight of the dried peach blossom for the 2 nd time, and extracting for 1.5 h; adding water with the weight 10 times of that of the dried peach blossom in the 3 rd time, extracting for 1.5h, filtering with four layers of gauze each time, combining filtrates, filtering, and concentrating the filtrate to obtain peach blossom extract with the volume 10 times mL/g of the weight of the dried peach blossom.
4.3 preparation of agar extract:
weighing appropriate amount of Eucheuma Gelatinosum, heating and reflux-extracting with water for 3 times: adding water 15 times the weight of Gelidium amansii at 1 st time, soaking for 0.7 hr, and extracting for 2.5 hr; adding 13 times of water by mass of Gelidium amansii at the 2 nd time, and extracting for 1.5 hr; adding 10 times of water by mass of Eucheuma Gelatinosum in 3 rd time, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 8 times of weight of Eucheuma Gelatinosum (mL/g) to obtain Eucheuma Gelatinosum extractive solution.
4.4 preparation of okra extract:
weighing appropriate amount of okra, heating and reflux-extracting with water for 3 times: adding water with the amount of 10 times of that of okra at the 1 st time, soaking for 0.7h, and extracting for 1.5 h; adding water 10 times the weight of okra at the 2 nd time, and extracting for 1.5 h; adding water 8 times the weight of okra in the 3 rd time, extracting for 1.0h, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 7 mL/g of okra weight to obtain okra extractive solution.
4.5 preparation of chanterelle extract:
weighing appropriate amount of chanterelle, heating and reflux-extracting with water for 3 times: adding water with the weight of 25 times of that of the chanterelle at the 1 st time, soaking for 1.0h, and extracting for 2.0 h; adding water with the mass of 20 times of that of the chanterelle for 2 times, and extracting for 2.0 h; adding water with the weight 5-10 times of that of the chanterelle at the 3 rd time, extracting for 1.5h, filtering with four layers of gauze each time, combining filtrates, vacuum-filtering, and concentrating the volume of the filtrate to 13 mL/g of the weight of the chanterelle to obtain chanterelle extract for later use.
4.6 preparation of the tribulus terrestris extract:
weighing appropriate amount of fructus Tribuli coarse powder, and extracting with water under heating and refluxing for 3 times: adding water with the amount of 20 times of the weight of the tribulus terrestris into the mixture at the 1 st time, soaking for 0.7h, and extracting for 2.5 h; adding water 15 times the weight of fructus Atriplicis Sibiricae at the 2 nd time, and extracting for 1.5 hr; adding 12 times of water by mass of fructus Atriplicis Sibiricae for 3 times, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 12 times of weight of fructus Atriplicis Sibiricae (mL/g) to obtain fructus Atriplicis Sibiricae extract.
4.7 preparation of Poria cocos extractive solution:
weighing appropriate amount of Poria cocos slice, heating and reflux extracting with water for 3 times: adding 16 times of water for the first time, soaking for 1.0 hr, and extracting for 2.5 hr; adding 12 times of water for the 2 nd time, extracting for 1.5h, and filtering to obtain filtrate; adding 9 times of water at 3 rd time, extracting for 1.2 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 20 times of Poria weight (mL/g) to obtain Poria extract.
4.8 preparation of Green tea extract:
weighing appropriate amount of green tea, heating and reflux extracting with water for 3 times: adding water 15 times the weight of green tea at 1 st time, soaking for 0.7 hr, and extracting for 2.0 hr; adding water 12 times the weight of green tea in the 2 nd time, and extracting for 1.5 hr; adding 10 times of water by weight of green tea in the 3 rd time, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 18 times of green tea weight mL/g to obtain green tea extractive solution.
4.9 preparation of cherry squeezing liquid:
weighing a proper amount of fresh cherries, putting the fresh cherries into a juicer, adding 15 times of water, squeezing for 2.0min in a juicing mode to obtain filtrate, filtering the filtrate by using four layers of gauze, centrifuging the filtrate, taking supernate, and concentrating the volume of the filtrate to 1.5 times mL/g of the weight of the cherries to obtain cherry squeezed liquid for later use.
4.10 preparation of motherwort extract:
weighing appropriate amount of herba Leonuri, extracting with water under heating and refluxing for 3 times: adding 22 times of water by mass of herba Leonuri at 1 st time, soaking for 1.0 hr, and extracting for 2.5 hr; adding 18 times of water of herba Leonuri for 2 times, and extracting for 2.0 hr; adding 13 times of water by mass of herba Leonuri in 3 rd time, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 25 times mL/g of herba Leonuri to obtain herba Leonuri extractive solution.
4.11 preparation of cordyceps flower extract:
weighing appropriate amount of Cordyceps flower, and extracting with water under heating and refluxing for 3 times: adding water with an amount of 25 times of the mass of the cordyceps flower for 1 time, soaking for 1.0h, and extracting for 2.0 h; adding 20 times of water of the mass of Cordyceps for 2 times, and extracting for 1.5 hr; adding 18 times of water of the mass of the cordyceps flower in the 3 rd time, extracting for 1.5h, filtering with four layers of gauze each time, combining filtrates, performing suction filtration, and concentrating the volume of the filtrate to 15 times mL/g of the weight of the cordyceps flower to obtain cordyceps flower extract for later use.
4.12 preparation of the medlar extracting solution:
weighing appropriate amount of fructus Lycii, and extracting with water under heating and refluxing for 3 times: adding 18 times of water of fructus Lycii at 1 st time, and reflux extracting for 2.0 hr; adding 14 times of water of fructus Lycii for 2 times, and reflux extracting for 1.5 hr; adding 10 times of water of fructus Lycii weight for 3 times, reflux extracting for 1.5 hr, filtering to obtain filtrate, mixing filtrates, vacuum filtering, and concentrating the filtrate to 20 times of fructus Lycii weight mL/g to obtain fructus Lycii extractive solution.
4.13 preparation of Tremella fuciformis extract:
weighing appropriate amount of Tremella, extracting with water under heating and refluxing for 3 times: adding water with an amount of 25 times of the weight of the tremella at 1 st time, soaking for 1.0h, and extracting for 2.0 h; adding 18 times of water by mass of Tremella at 2 times, and extracting for 1.5 hr; adding 15 times of water by mass of Tremella in 3 rd time, extracting for 1.0 hr, filtering with four layers of gauze each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 15 times of Tremella weight (mL/g) to obtain Tremella extractive solution.
4.14 preparation method of moisturizing facial cleanser for removing freckles, brightening skin and nourishing skin comprises the following steps:
a) weighing 1.0g of sodium alginate, adding 40mL of distilled water, placing in a constant-temperature water bath kettle at 80 ℃, heating and stirring for 15min, and standing at normal temperature for 5h to obtain a sodium alginate gel solution for later use;
b) weighing 3.0g of sodium carboxymethylcellulose, dissolving in 40mL of distilled water, standing for 24h, and obtaining uniform and transparent sodium carboxymethylcellulose gel liquid for later use after the sodium carboxymethylcellulose is naturally swelled and dissolved;
c) weighing 2.0g of synthetic egg white powder, adding 30mL of distilled water, placing in a constant-temperature water bath kettle at 60-80 ℃, stirring for 10min, taking out, and standing at normal temperature for 6h to obtain a synthetic egg white powder solution for later use;
d) weighing 0.8g of ethylparaben, adding 3mL of 1, 2-propylene glycol, stirring and dissolving to obtain a preservative solution for later use;
e) weighing 2.0g pistachio nut oil, placing in a water bath kettle with constant temperature of 90 deg.C, and heating to obtain oil A;
f) weighing 0.65g of potassium hydroxide, weighing 5mL of distilled water, and adding the distilled water into the potassium hydroxide to completely dissolve the potassium hydroxide;
g) adding the solution obtained in the step f) into the oil A obtained in the step e) in a trickle shape, heating and uniformly stirring in the same direction for reacting for 25min to fully react to obtain a soap solution B;
h) weighing 7.0g of shea butter, 7.5g of malus micromalus linn oil, 10.0g of universal emulsifier and 10.0g of olive emulsifier respectively, mixing completely, placing in a water bath kettle with constant temperature of 90 ℃, heating while stirring to mix uniformly to obtain an oil phase;
i) measuring 20mL of distilled water, and heating in a 90 ℃ constant-temperature water bath kettle to obtain a water phase;
j) slowly adding the water phase into the oil phase along the wall of the container when the oil phase and the water phase reach the same temperature, heating and stirring at the same direction at constant speed for 30min, and emulsifying to obtain O/W emulsion matrix;
k) adding the formed emulsion matrix into soap solution B, placing in 90 deg.C water bath, heating while stirring for 15min to obtain mixed solution C;
l) respectively measuring 25mL of coconut oil fatty acid potassium glycinate, 10mL of sodium lauroyl amphoacetate and 24mL of sodium cocoyl amphoacetate, adding the mixture into the mixed solution C, and stirring for 10min to uniformly mix the mixture to obtain mixed solution D;
m) respectively weighing 0.2g of skimmed milk powder and 0.15g of vitamin C, dissolving with 4mL of distilled water respectively, and adding into the mixed solution D;
n) respectively measuring 10mL of basil seed extracting solution, 10mL of peach blossom extracting solution, 11mL of gelidium amansii extracting solution, 5mL of okra extracting solution, 10mL of chanterelle extracting solution, 8mL of tribulus terrestris extracting solution, 10mL of poria cocos extracting solution, 11mL of green tea extracting solution, 7mL of cherry squeezing solution, 8mL of motherwort extracting solution, 10mL of cordyceps flower extracting solution, 9mL of medlar extracting solution and 12mL of tremella extracting solution, adding the obtained mixture into the mixed solution D, and uniformly stirring the obtained mixture to obtain mixed solution E;
o) adding the prepared synthetic egg white powder solution, the sodium alginate gel solution and the sodium carboxymethyl cellulose gel solution into the mixed solution E, stirring to mix the mixed solution E fully and uniformly, then adding 0.40g of strawberry essence and preservative solution, stirring and mixing uniformly to obtain the spot-removing, skin-brightening and nourishing moisturizing facial cleanser containing natural plant active ingredients.
After standing for 48h, the prepared facial cleanser showed demixing, as shown in fig. 4: the comparative example has the defect that the layering occurs in the process of sample retention and inspection due to the fact that the dosage proportion is not proper, and other effects are not inspected. Through repeated exploration and experiments, the proper raw material proportion of the invention is finally obtained.
Example 5
The physical and chemical indexes of the examples 1,2 and 3 are as follows:
5.1 Properties
The invention is white emulsion, has proper viscosity, fine and uniform texture, bright and moist luster, good foamability and fragrant smell.
5.2pH check
Taking the product, and measuring by using pH test paper to obtain a pH value of 6-7.
5.3 Cold-Heat test
The facial cleanser is packaged in a transparent cosmetic bottle and refrigerated in a refrigerator at 4 ℃ for one month to observe no layering phenomenon. The emulsion is placed in a constant temperature box at 55 ℃ for 24 hours, and the phenomena of layering, emulsification and odor change of the emulsion are avoided.
5.4 centrifugation test
The facial cleanser is packaged in a test tube with a plug and centrifuged at 3000r/min for 20min, and no layering phenomenon occurs.
5.5 Room temperature standing test
The facial cleanser prepared in the examples 1,2 and 3 was placed in an emulsion bottle and allowed to stand at room temperature for 6 months, and no delamination, no change in quality after use and no change in odor were observed.
5.6 irritation test and allergy test
The back of the mice was shaved, and the cleansers prepared according to examples 1,2 and 3 were applied to the shaved parts, respectively, and compared with the non-applied parts, resulting in no irritation or allergic reaction.
A proper amount of the facial cleanser prepared in examples 1,2 and 3 was applied to the hands of volunteers (20-73 years old, 60 persons), and no redness, rash or blister appeared after 30 minutes.
5.7 examination of the comprehensive effects of facial cleanser
The efficacy of the facial cleansers prepared in examples 1,2 and 3 was evaluated by the test feeling. 60 volunteers of 20-73 years old are selected as trial objects by adopting a civil survey grading method, the trial objects are divided into three groups at will, and the facial cleanser prepared in the embodiment 1, the embodiment 2 and the embodiment 3 is used for daily face cleaning for 2 times a day and two months (10 and 8 days in 2019-12 and 8 days in 2019). The using effects of the ingredients are divided into 5 points: the score of 5 is the highest score, which represents good and very satisfactory; 4, the division is better; 3 is acceptable; when the amount is less than 3 points, the results are not acceptable. The average scores of the respective items are shown below, and the results are shown in Table 1.
Table 1 comprehensive effect investigation
In conclusion, the prepared facial cleanser is fine and uniform in texture, rapid to absorb, good in foamability and aromatic in smell, and can effectively remove color spots, dissolve pore impurities, comprehensively repair skin injury, deeply nourish skin, improve skin resistance and moisturize.
5.8 examination of repair effects of facial cleanser
60 volunteers of 20-73 years old age, wherein 55 volunteers have the effect of relieving acne marks or scars to a certain extent after 2 months of use, which indicates that the facial cleanser has a certain skin repairing effect.
5.9 examination of itch relieving effect of facial cleanser
60 volunteers of 20-73 years old age, wherein 60 volunteers reflect that after 2 months of use, the phenomenon of skin itch is solved, and the situation of skin itch is not generated any more.
5.10 Spot removing effect of facial cleanser
After 60 volunteers of 20-73 years old continuously use the facial cleanser of the invention for half a year, 58 volunteers feed back the effect of fading and removing freckles, and the facial cleanser of the invention can fade and remove freckles with good effect.
Claims (10)
2. the moisturizing facial cleanser according to claim 1, wherein the basil seed extract is prepared by the following method:
weighing appropriate amount of basil seed, heating and reflux extracting with water for 3 times: adding water 20-25 times the weight of the cymbidium seed for 1 time, soaking for 0.25-0.75 hr, and extracting for 1.5-2.5 hr; adding 15-18 times of water for 2 times, and extracting for 1.0-1.5 hr; adding water 8-12 times the weight of the basil seeds at the 3 rd time, extracting for 0.5-1.0h, filtering each time, combining filtrates, performing suction filtration, and concentrating the volume of the filtrate to 15-20 times mL/g of the weight of the basil seeds to obtain a basil seed extract for later use; the volume of the basil seed extracting solution obtained per gram of the basil seed is 15-20 ml;
the peach blossom extracting solution is prepared by the following method:
weighing appropriate amount of dried flos persicae, and extracting with water under heating and refluxing for 3 times: adding water 15-20 times the weight of the dried peach blossom for the first time, soaking for 0.5-1.0h, and extracting for 1.0-1.5 h; adding 10-14 times of water of the weight of the dried peach blossom for the 2 nd time, and extracting for 1.0-1.5 h; adding water 5-10 times the weight of the dried peach blossom 3 times, extracting for 0.5-1.5h, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 5-10 times mL/g of the weight of the dried peach blossom to obtain peach blossom extract.
3. The moisturizing facial cleanser according to claim 1, wherein the gelidium amansii extract is prepared by the following method:
weighing appropriate amount of Eucheuma Gelatinosum, heating and reflux-extracting with water for 3 times: adding 10-15 times of water by mass of Eucheuma Gelatinosum at 1 st time, soaking for 0.2-0.7 hr, and extracting for 1.0-2.5 hr; adding 10-13 times of water by mass of Gelidium amansii for 2 times, and extracting for 0.5-1.5 hr; adding water 8-10 times the weight of Eucheuma Gelatinosum in 3 rd time, extracting for 0.5-1.0 hr, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 3-8 times mL/g of Eucheuma Gelatinosum weight to obtain Eucheuma Gelatinosum extractive solution.
4. The moisturizing facial cleanser according to claim 1, wherein the okra extracting solution is prepared by the following method:
weighing appropriate amount of okra, heating and reflux-extracting with water for 3 times: adding water 8-10 times the weight of okra at the 1 st time, soaking for 0.2-0.7 hr, and extracting for 1.0-1.5 hr; adding water 8-10 times the weight of okra at the 2 nd time, and extracting for 0.5-1.5 h; adding water 6-8 times the weight of okra in the 3 rd time, extracting for 0.5-1.0h, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 2-7 times of weight of okra (mL/g) to obtain okra extractive solution.
5. The moisturizing facial cleanser according to claim 1, wherein the okra extracting solution is prepared by the following method:
weighing appropriate amount of okra, heating and reflux-extracting with water for 3 times: adding water 8-10 times the weight of okra at the 1 st time, soaking for 0.2-0.7 hr, and extracting for 1.0-1.5 hr; adding water 8-10 times the weight of okra at the 2 nd time, and extracting for 0.5-1.5 h; adding water 6-8 times the weight of okra in the 3 rd time, extracting for 0.5-1.0h, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 2-7 times of weight of okra (mL/g) to obtain okra extractive solution.
6. The moisturizing facial cleanser according to claim 1, wherein the chanterelle extract is prepared by the following method:
weighing appropriate amount of chanterelle, heating and reflux-extracting with water for 3 times: adding water with the amount of 20-25 times of that of the chanterelle at the 1 st time, soaking for 0.5-1.0h, and extracting for 1.5-2.0 h; adding 15-20 times of water of adeps gallus Domesticus for 2 times, and extracting for 1.5-2.0 hr; adding water with the weight 5-10 times of that of the chanterelle at the 3 rd time, extracting for 0.5-1.5h, filtering each time, combining the filtrates, performing suction filtration, and concentrating the volume of the filtrate to 10-13 times of mL/g of the weight of the chanterelle to obtain an chanterelle extracting solution for later use;
the tribulus terrestris extracting solution is prepared by the following method:
weighing appropriate amount of fructus Tribuli coarse powder, and extracting with water under heating and refluxing for 3 times: adding water 15-20 times the weight of fructus Atriplicis Sibiricae at 1 time, soaking for 0.2-0.7 hr, and extracting for 1.0-2.5 hr; adding 12-15 times of water of the weight of the Tribulus terrestris at the 2 nd time, and extracting for 1.0-1.5 h; adding water 8-12 times the weight of fructus Atriplicis Sibiricae at 3 times, extracting for 0.5-1.0 hr, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 8-12 times of the weight of fructus Atriplicis Sibiricae mL/g to obtain fructus Atriplicis Sibiricae extract.
7. The moisturizing facial cleanser according to claim 1, wherein the poria cocos extract is prepared by the following method:
weighing appropriate amount of Poria cocos slice, heating and reflux extracting with water for 3 times: adding water 12-16 times the weight of Poria tablet at 1 st time, soaking for 0.5-1.0 hr, and extracting for 1.0-2.5 hr; adding water 8-12 times the weight of Poria tablet for the 2 nd time, extracting for 1.0-1.5 hr, and filtering to obtain filtrate; adding water 7-9 times the weight of Poria tablet at 3 rd time, extracting for 0.5-1.2 hr, filtering each time, mixing filtrates, filtering, and concentrating the filtrate to 10-20 times mL/g of Poria weight to obtain Poria extract;
the green tea extracting solution is prepared by the following method:
weighing appropriate amount of green tea, heating and reflux extracting with water for 3 times: adding 10-15 times of water by weight of green tea for the first time, soaking for 0.5-0.7 hr, and extracting for 1.0-2.0 hr; adding water 8-12 times the weight of green tea in the 2 nd time, and extracting for 1.0-1.5 hr; adding water 7-10 times the weight of green tea in the 3 rd time, extracting for 0.5-1.0 hr, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to volume of 15-18 times of green tea weight mL/g to obtain green tea extractive solution.
8. The moisturizing facial cleanser according to claim 1, wherein the motherwort herb extract is prepared by the following method:
weighing appropriate amount of herba Leonuri, extracting with water under heating and refluxing for 3 times: adding 18-22 times of water by mass of herba Leonuri at 1 st time, soaking for 0.5-1.0 hr, and extracting for 1.5-2.5 hr; adding 15-18 times of water of herba Leonuri for the 2 nd time, and extracting for 1.5-2.0 h; adding 8-13 times of water by mass of herba Leonuri in 3 rd time, extracting for 0.5-1.0h, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 20-25 times of herba Leonuri weight mL/g to obtain herba Leonuri extractive solution.
The cordyceps flower extracting solution is prepared by the following method:
weighing appropriate amount of Cordyceps flower, and extracting with water under heating and refluxing for 3 times: adding water 20-25 times the mass of Cordyceps flower at 1 st time, soaking for 0.5-1.0 hr, and extracting for 1.5-2.0 hr; adding 18-20 times of water of Cordyceps flower for 2 times, and extracting for 1.0-1.5 hr; adding 15-18 times of water to the cordyceps flower in the 3 rd time, extracting for 0.5-1.5h, filtering each time, mixing filtrates, vacuum-filtering, and concentrating the filtrate to 10-15 times of the weight of cordyceps flower to obtain cordyceps flower extractive solution.
9. The moisturizing facial cleanser according to claim 1, wherein the wolfberry fruit extracting solution is prepared by the following method:
weighing appropriate amount of fructus Lycii, and extracting with water under heating and refluxing for 3 times: adding 16-18 times of water of fructus Lycii at 1 st time, and reflux extracting for 1.0-2.0 hr; adding 12-14 times of water of fructus Lycii for the 2 nd time, reflux extracting for 1.0-1.5 hr; adding 8-10 times of water by weight of fructus Lycii in 3 rd time, reflux extracting for 1.0-1.5 hr, filtering to obtain filtrate, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to volume of 15-20 times of weight of fructus Lycii (mL/g) to obtain fructus Lycii extractive solution;
the tremella extract is prepared by the following method:
weighing appropriate amount of Tremella, extracting with water under heating and refluxing for 3 times: adding water 20-25 times the weight of Tremella at 1 st time, soaking for 0.5-1.0 hr, and extracting for 1.5-2.0 hr; adding water 15-18 times the weight of Tremella at 2 times, and extracting for 1.0-1.5 hr; adding 10-15 times of water to the tremella in mass for 3 times, extracting for 0.5-1.0h, filtering each time, mixing filtrates, vacuum filtering, and concentrating the filtrate to 10-15 times of weight of Tremella (mL/g) to obtain Tremella extractive solution.
10. A method for preparing the spot-removing, skin-brightening and nourishing moisturizing facial cleanser containing natural plant active ingredients according to any one of claims 1 to 9, which is characterized by comprising the following steps:
a) weighing sodium alginate according to the formula ratio, adding 30-40 parts of distilled water, placing in a constant temperature water bath kettle at 60-80 deg.C, heating and stirring for 5-15min, standing at room temperature for 2-5h to obtain sodium alginate gel solution for use;
b) weighing sodium carboxymethylcellulose according to the formula ratio, dissolving in 25-30 parts of distilled water, standing for 12-24h, and naturally swelling and dissolving to obtain uniform and transparent sodium carboxymethylcellulose gel solution for later use;
c) weighing the synthetic egg white powder according to the formula ratio, adding 10-20 parts of distilled water, putting into a constant-temperature water bath kettle at 60-80 ℃, stirring for 5-10min, taking out, and standing for 5-6h at normal temperature to obtain a synthetic egg white powder solution for later use;
d) weighing ethylparaben with the formula amount, adding 1, 2-propylene glycol with the formula amount, stirring and dissolving to obtain a preservative solution for later use;
e) weighing pistachio nut oil according to the formula amount, placing the pistachio nut oil in a constant-temperature water bath kettle at 70-90 ℃, and heating to obtain oil A for later use;
f) weighing potassium hydroxide according to the formula ratio, weighing 2-5 parts of distilled water, and adding the distilled water into the potassium hydroxide to completely dissolve the potassium hydroxide;
g) adding the solution obtained in the step f) into the oil A obtained in the step e) in a trickle shape, heating and uniformly stirring in the same direction for reacting for 15-25min to fully react to obtain a soap solution B;
h) weighing the shea butter, the malus sieboldii oil, the universal emulsifier and the olive emulsifier according to the formula ratio respectively, fully mixing the materials, putting the materials into a constant-temperature water bath kettle at 70-90 ℃, and heating while stirring to uniformly mix the materials to obtain an oil phase;
i) weighing 5-20 parts of distilled water, and heating in a constant-temperature water bath kettle at 70-90 ℃ to obtain a water phase;
j) slowly adding the water phase into the oil phase along the wall of the container when the oil phase and the water phase reach the same temperature, heating and stirring at the same direction at constant speed for 15-30min, and emulsifying to obtain O/W emulsion matrix;
k) adding the formed emulsion matrix into soap solution B, placing in 70-90 deg.C water bath, heating while stirring for 10-15min to obtain mixed solution C;
l) respectively measuring the potassium glycinate, the sodium lauroamphoacetate and the sodium cocoamphoacetate with the formula ratio, adding into the mixed solution C, and stirring for 3-10min to uniformly mix to obtain a mixed solution D;
m) weighing the formula amount of the skimmed milk powder and the vitamin C respectively, dissolving the skimmed milk powder and the vitamin C with 2-4 parts of distilled water respectively, and adding the mixture into the mixed solution D;
n) respectively measuring the formula amounts of a basil seed extracting solution, a peach blossom extracting solution, a gelidium amansii extracting solution, an okra extracting solution, a chanterelle extracting solution, a tribulus terrestris extracting solution, a poria cocos extracting solution, a green tea extracting solution, a cherry squeezing solution, a motherwort extracting solution, a cordyceps flower extracting solution, a wolfberry extracting solution and a tremella extracting solution, adding the obtained mixture into the mixed solution D, and uniformly stirring to obtain a mixed solution E;
o) adding the prepared synthetic egg white powder solution, sodium alginate gel solution and sodium carboxymethyl cellulose gel solution into the mixed solution E, stirring to mix uniformly, adding formula amount of essence and preservative solution, stirring and mixing uniformly to obtain the spot-removing, skin-brightening and nourishing moisturizing facial cleanser containing natural plant active ingredients.
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CN115414289A (en) * | 2022-08-31 | 2022-12-02 | 浙江理工大学 | Cordyceps flower cosmetics and preparation method thereof |
CN116870061A (en) * | 2023-08-04 | 2023-10-13 | 无限极(中国)有限公司 | Peach blossom extract and preparation method and application thereof |
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CN103565704A (en) * | 2013-11-21 | 2014-02-12 | 广州丹奇日用化工厂有限公司 | Application of basil seed mucopolysaccharides to cosmetics |
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CN115414289A (en) * | 2022-08-31 | 2022-12-02 | 浙江理工大学 | Cordyceps flower cosmetics and preparation method thereof |
CN116870061A (en) * | 2023-08-04 | 2023-10-13 | 无限极(中国)有限公司 | Peach blossom extract and preparation method and application thereof |
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