CN108403522A - A kind of four seasons series toner based on Plant flawer extracts - Google Patents
A kind of four seasons series toner based on Plant flawer extracts Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses a kind of four seasons series toner based on Plant flawer extracts, the present invention improve the oxidation resistance of toner by adding the plant flowers nutritional ingredient of fermentation, pass through and add low temperature supercritical CO2The plant flowers nutrient solution of extraction utmostly saves the preservation of the trace element such as vitamin in plant flowers, and to improve the nutritional ingredient of toner, the compatibility of the antibiotic property and toner and skin of toner is improved by addition carboxymethyl chitosan and propolis；The present invention is using the extract of pure plant flower as active material, without any toxicity and side effects, it does not stimulate mildly, and its active ingredient can be absorbed by the skin by the distinctive aquation of keratin, it prevents the moisture evaporation in cuticula from reducing, has the advantages that excellent replenishing water and preserving moisture, moisturize the skin, prevent skin aging.
Description
Technical field
The invention belongs to the technical fields of cosmetics, and in particular to a kind of four seasons series makeup based on Plant flawer extracts
Water.
Background technology
With the continuous progress of free radical life science, oxidativestress damage and anti-oxidation protection effect research by
The growing interest of people is arrived.Under serious oxidative stress status, when the concentration of active oxygen is more than cytophylaxis ability, oxidation
The structure and function of cell just can be changed in damage, influences body health.With the development of nutrition and biotechnology, it has been found that
Peptides between protein and amino acid, due to its special design feature, edible safety higher, antioxidant activity is more
Significantly, antioxidant can be also belonged to, as the substance source for removing free radical in human body.
Toner, be a kind of low viscosity, good fluidity liquid skin protection cosmetics.In numerous cosmetics, makeup
Water is convenient to use and is taken the course of its own with its unique effect.Such product has cleaning, moistens, is soft, convergent effect.
Currently, various brands, the toner of different efficacies is constantly developed, but these toners are mostly expensive, is used
Effect is general, and What is more there are more side effect, is not suitable for long-term use.Contain day in the toner of plant flowers and plants class
Right herbal medicine essence, while to the Small side effects of face, the skin of people can be nourished, for a long time using the skin that can moisten people
And the immunity of skin can be adjusted, there is preferable practicability.
The main reason for as skin aging, can enumerate sunlight and active oxygen.Active oxygen be to play such a work
Substance, that is, foreign matter is decomposed during being removed into internal foreign matter to remove foreign matter.Although playing positive work
With, but if generating excessive active oxygen due to various reasons, not only encroach on the cell tissue of itself, but also with it is internal not
Saturated fatty acid in conjunction with and form lipid peroxide.In particular, in skin with protein, lipid binding and generate oxide, from
And promote skin aging, and play the role of stronger, initiation pigmentation to the oxidation process of melanin.Therefore skin aging
The problem of it is urgently to be resolved hurrily.
Invention content
The purpose of the present invention is to provide a kind of four seasons series toner based on Plant flawer extracts, according to quality percentage
Include plant flowers extractive from fermentative than calculating：0.05%-1.2%；Supercritical CO2The plant flowers extraction solution of extraction：0.03-
2%；Niacinamide：0.05-0.1%；Allantoin：0.05%；Carboxymethyl chitosan：0.03-0.1%；Propolis extract：0.08-
0.25%；Glycerine：4%；Sodium Hyaluronate：0.01%-0.03%；Pure water：85%-95%；The present invention is by adding fermentation
Plant flowers nutritional ingredient improves the oxidation resistance of toner, by adding low temperature supercritical CO2The plant flowers nutrition of extraction
Liquid utmostly saves the preservation of the trace element such as vitamin in plant flowers, is carried by adding carboxymethyl chitosan and propolis
The high compatibility of the antibiotic property and toner and skin of toner；The present invention is faced by adding plant flowers extractive from fermentative and surpassing
Boundary CO2The plant flowers extraction solution of extraction improves the compatibility and synergistic effect of nutriment in the plant flowers in toner,
To improve the nutritional ingredient of toner；The present invention is using the extract of pure plant flower as active material, nontoxic no pair
Effect does not stimulate mildly, and its active ingredient can be absorbed by the skin by the distinctive aquation of keratin, be prevented in cuticula
Moisture evaporation reduce, have the advantages that excellent replenishing water and preserving moisture, moisturize the skin, prevent skin aging.
The present invention is achieved through the following technical solutions：A kind of four seasons series toner based on Plant flawer extracts,
The pH of the toner is 6.0-7.0, and it includes mainly following component to be calculated according to mass percent：Plant flowers extractive from fermentative：
0.05%-1.2%；Supercritical CO2The plant flowers extraction solution of extraction：0.03-2%；Niacinamide：0.05-0.1%；Allantoin：
0.05%；Carboxymethyl chitosan：0.03-0.1%；Propolis extract：0.08-0.25%；Glycerine：4%；Sodium Hyaluronate：
0.01%-0.03%；Pure water：85%-95%；
Stirring and dissolving, heat preservation at 75-90 DEG C by allantoin, carboxymethyl chitosan, Sodium Hyaluronate, glycerine, pure water
Plant flowers extractive from fermentative, supercritical CO is added when being cooled to 35-40 DEG C in 20min2The plant flowers extraction solution of extraction, nicotinoyl
Amine, propolis extract are uniformly mixed, and the pH for adjusting toner obtains toner later.
The plant flowers are the flowers with skin makeup function, contain abundant trace nutrient in the plant flowers, contain
There is natural herbal medicine essence, while to the Small side effects of face, the skin of people can be nourished, use for a long time can moisten people
Skin and the immunity that can adjust skin have preferable practicability.
A large amount of small molecule amino acid and peptide material are will produce after the plant flowers fermentation, skin can be improved to nutrition
The absorption of substance can also eliminate oxygen radical, reach and exclude the production that cytotoxin eliminates pigementation, slows down wrinkle of skin
Raw, to make, skin is tenderer, smooth, whitening.The plant flowers extractive from fermentative and supercritical CO2The plant flowers of extraction extract
Synergy is will produce after taking solution to mix and improves compatibility, generates effect that is preferable anti-oxidant and moisturizing the skin.
The allantoin is a kind of amphoteric compound, can in conjunction with many kinds of substance formed double salt, have be protected from light, sterilization and anticorrosion,
Analgesic, antioxidation can make skin keep moisture content, moisten and soft, have protective tissue, it is hydrophilic, absorb water and prevent moisture
The effects that distributing；It can make skin emolliency high resilience, and have beautiful gloss.
The hyaluronic acid can help skin to draw a large amount of moisture, can moment deep moisturizing, increase skin elasticity with
Power helps and restores the normal oil-water balance of skin, improves dry and relaxation skin.
The carboxymethyl chitosan is a kind of water-solubility chitosan derivative, and antibiotic property is strong, has preservation, is a kind of
Polyampholyte.The carboxymethyl chitosan has preferably stable property and antibacterial anti-infection, lipid-loweringing and prevention artery
The pharmacological actions such as hardening.
The propolis extract is the prior art, and the preparation method of the propolis extract is as follows：Propolis is removed into impurity
48h is freezed at -5 DEG C of temperature below afterwards, then by the propolis quick crashing after freezing, screening, the propolis after screening is added
Enter ethanol solution and impregnate 5h at a temperature of 25 DEG C, takes out supernatant liquor after then standing 2h, remaining substance adds ethanol solution again
Continue dipping, stand, so repeats at least three times, then to merge the supernatant liquor that each time obtains and cool to 5 DEG C hereinafter, mistake
Filter, carries out heating evaporation at 50 DEG C or less by filtrate, is concentrated into a concentration of 10g/mL to get propolis extract.
Rich in a variety of flavone compounds, terpenoid, minerals, trace element, dimension life in the propolis extract
Element, organic acid, amino acid etc..Flavonoid substances have extremely strong antioxidation, prevent the generation of the free radical in skin, can
Senile plaque, anti-aging, anti-inflammatory, anti-acne are eliminated, also absorbable 200-450nm length ultraviolet lines are effectively prevented and absorbed purple
Injury of the outside line to human body.Galangin in propolis, AVM hereinafter acid, caffeic acid and salicylic acid have stronger antibacterial anti-inflammatory, soft
The effect for changing cutin, can effectively kill and inhibit the pathogenic bacteria such as bacillus acnes, acarid, remove the hair funnel of obstruction, right
Face acnes have significant therapeutic effect.
The niacinamide is one kind of B family vitamin, also known as：Vitamin B3, nicotinic acid are that human body and animal body are constituted
The direct precursor of important Coenzyme I and Coenzyme I I.In field of medicaments, niacinamide is for preventing pellagra and stomatitis and glossitis etc..Institute
It states transfer that niacinamide can inhibit melanin from from melanocyte to albuminous cell, reduced pigment deposition, this function is different
Only focus on inhibiting the generation of black in previous whitening composition, but act on the melanin generated, people are able to from black
Pigment, which is generated to the every link to fall off, improves skin color and luster；The niacinamide can accelerate skin metabolism, promote containing black
The horn cell of pigment falls off, while keeping cell balance horizontal, and younger state is presented；The niacinamide can promote epidermis
The synthesis of protein enhances the aqueous degree of skin, so as to improve skin quality.
In order to preferably realize the present invention, further, it includes mainly following component to be calculated according to mass percent：Peach blossom
Extractive from fermentative：1.2%, supercritical CO2The peach blossom extraction solution of extraction：0.8%, niacinamide：0.1%, allantoin：
0.05%, carboxymethyl chitosan：0.05%, propolis extract：0.13%, glycerine：4%, Sodium Hyaluronate：0.01%, pure water：
85%-90%.
In order to preferably realize the present invention, further, it includes mainly following component to be calculated according to mass percent：Rose
Flower extractive from fermentative：1.2%, the rose extracting solution of SCF-CO 2：0.8%, niacinamide：0.1%, allantoin：
0.05%, carboxymethyl chitosan：0.05%, propolis extract：0.13%, glycerine：4%, Sodium Hyaluronate：0.01%, pure water：
85%-90%.
In order to preferably realize the present invention, further, it includes mainly following component to be calculated according to mass percent：Chrysanthemum
Extractive from fermentative：1.2%, the chrysanthemum extraction solution of SCF-CO 2：0.8%, niacinamide：0.1%, allantoin：
0.05%, carboxymethyl chitosan：0.05%, propolis extract：0.13%, glycerine：4%, Sodium Hyaluronate：0.01%, pure water：
85%-90%.
In order to preferably realize the present invention, further, it includes mainly following component to be calculated according to mass percent：Golden small cup
Flower extractive from fermentative：1.2%, the pot marigold extraction solution of SCF-CO 2：0.8%, niacinamide：0.1%, allantoin：
0.05%, carboxymethyl chitosan：0.05%, propolis extract：0.13%, glycerine：4%, Sodium Hyaluronate：0.01%, pure water：
85%-90%.
Containing Kaempferol, coumarin, trifolin and vitamin A, the ingredients such as B, C in the peach blossom, in the peach blossom
Nutritional ingredient can expand blood vessel, promotion of blood circulation, moist skin, make the yellowish-brown quality and senile plaque of promotion human senility.
Existing is a kind of good natural studies have shown that the rose contains high-efficiency antioxidant ingredient, right
The tissue and cell of lesion of aging rats have significant antioxidation.The rose is containing daucosterol, Quercetin, apiolin, abundant
Vitamin C and carbohydrate content (such as glucose, sucrose, fructose) and organic acid (citric acid, malic acid, quininic acid), and plant
For son containing vitamin E, vitaminF, the wherein unsaturated fatty acid content in the seed oil of rose is more.
The main active of the chrysanthemum is flavonoids and phenolic compound, and chrysanthemum flavones mainly has diosmetin, wood
Rhinoceros grass element, apiolin, Quercetin, diosmetin -7- glucosides, luteolin-7-glucoside, apiolin -7- glucose
Glycosides, acacetin galactoside etc.；Polyphenol compound is mainly chlorogenic acid.
Contain a large amount of lutein, luteole, beta carotene, also mineral phosphor and vitamin C in the pot marigold
Deng；The pot marigold has analgesic, sterilization, anti-inflammatory and oxidation resistant effect, can effective Polyglucan sensitivity skin, can also change
Kind eczema and pruitus.
In order to preferably realize the present invention, further, the preparation method of the plant flowers extractive from fermentative includes mainly
Following steps：Sterilize after plant flowers are cleaned at 120 DEG C 5-12min, then accesses strain seed culture fluid and ferment
To fermented material；The zymophyte in fermented material is sterilized using the method for high-temperature instantaneous sterilization, is centrifugally separating to obtain plant flowers
Extractive from fermentative.
In order to preferably realize the present invention, further, using bacillus subtilis or lactobacillus plantarum to plant flowers
It ferments.
In order to preferably realize the present invention, further, the supercritical CO2The preparation of the plant flowers extraction solution of extraction
Method mainly includes the following steps that：Plant flowers after cleaning, freezing sterilizing are placed in extractor and are vacuumized, are then faced super
Boundary CO2Extractant is with plant flowers according to 1:The weight ratio of 1-5 mixes in extractor；Temperature be 20-35 DEG C, pressure 5-
1-2.5h is extracted under conditions of 7.2MPa, is repeated above step and is extracted 2-3 times, then gasify CO2After obtain supercritical CO2Extraction
Plant flowers extraction solution.
Beneficial effects of the present invention：
(1) toner includes plant flowers extractive from fermentative according to mass percent calculating：0.05%-1.2%；It is super to face
Boundary CO2The plant flowers extraction solution of extraction：0.03-2%；Niacinamide：0.05-0.1%；Allantoin：0.05%；Carboxymethyl shell
Glycan：0.03-0.1%；Propolis extract：0.08-0.25%；Glycerine：4%；Sodium Hyaluronate：0.01%-0.03%；It is pure
Water：85%-95%；The present invention improves the oxidation resistance of toner by adding the plant flowers nutritional ingredient of fermentation, passes through
Add low temperature supercritical CO2The plant flowers nutrient solution of extraction utmostly saves the trace element such as vitamin in plant flowers
It preserves, the compatibility of the antibiotic property and toner and skin of toner is improved by addition carboxymethyl chitosan and propolis；This
Invention is by adding plant flowers extractive from fermentative and supercritical CO2The plant flowers extraction solution of extraction improves the plant in toner
Object spends the compatibility and synergistic effect of middle nutriment, to improve the nutritional ingredient of toner.
(2) it includes mainly following component that the toner is calculated according to mass percent：Peach blossom extractive from fermentative：1.2%,
Supercritical CO2The peach blossom extraction solution of extraction：0.8%, niacinamide：0.1%, allantoin：0.05%, carboxymethyl chitosan：
0.05%, propolis extract：0.13%, glycerine：4%, Sodium Hyaluronate：0.01%, pure water：85%-90%；The present invention utilizes
The invigorating blood circulation of peach blossom, oxidation resistant function increase the metabolism of skin, have preferable to realize whitening, the activation to skin
Practicability.
(3) it includes mainly following component to be calculated according to mass percent：Rose extractive from fermentative：1.2%, overcritical
The rose extracting solution of CO2 extractions：0.8%, niacinamide：0.1%, allantoin：0.05%, carboxymethyl chitosan：
0.05%, propolis extract：0.13%, glycerine：4%, Sodium Hyaluronate：0.01%, pure water：85%-90%；The present invention utilizes
The moisturizing freckle removing and whitening to skin is realized in the moisturizing of rose, oxidation resistant function, has preferable practicability.
(4) it includes mainly following component to be calculated according to mass percent：Chrysanthemum extractive from fermentative：1.2%, supercritical CO 2
The chrysanthemum extraction solution of extraction：0.8%, niacinamide：0.1%, allantoin：0.05%, carboxymethyl chitosan：0.05%, propolis
Extracting solution：0.13%, glycerine：4%, Sodium Hyaluronate：0.01%, pure water：85%-90%；The present invention utilizes the highly resistance of chrysanthemum
Oxygen highlights the effect to the Whitening, spot of skin, has preferable practicability.
(5) it includes mainly following component to be calculated according to mass percent：Pot marigold extractive from fermentative：1.2%, overcritical
The pot marigold extraction solution of CO2 extractions：0.8%, niacinamide：0.1%, allantoin：0.05%, carboxymethyl chitosan：
0.05%, propolis extract：0.13%, glycerine：4%, Sodium Hyaluronate：0.01%, pure water：85%-90%；The present invention utilizes
The skin of the effective Polyglucan sensitivity of effect of the antibacterial anti-inflammatory of pot marigold, while being realized using the oxidation resistant function of pot marigold
To skin anti-aging, there is preferable practicability.
(6) use bacillus subtilis or lactobacillus plantarum to planting in the preparation method of the plant flowers extractive from fermentative
Object flower ferments, research shows that the antioxygen substance generated is compared with horn of plenty, the zymophyte is conveniently easy to get, and can pass through market
It is commercially available, there is preferable practicability.
(7) supercritical CO2The preparation method of the plant flowers extraction solution of extraction mainly includes the following steps that：It will be clear
It washes, freeze the plant flowers after sterilizing and be placed in extractor and vacuumize, then by supercritical CO2Extractant is with plant flowers according to 1:
The weight ratio of 1-5 mixes in extractor；1-2.5h is extracted under conditions of temperature is 20-35 DEG C, pressure is 5-7.2MPa,
It repeats above step to extract 2-3 times, then gasify CO2After obtain supercritical CO2The plant flowers extraction solution of extraction；The present invention is logical
Cross addition low temperature supercritical CO2The plant flowers nutrient solution of extraction utmostly saves the trace elements such as the vitamin in plant flowers
Preservation, have preferable practicability.
Specific implementation mode
Embodiment 1：
The pH of a kind of four seasons series toner based on Plant flawer extracts, the toner is 6.5, according to quality percentage
Include following component than calculating main：Peach blossom extractive from fermentative：1.2%, supercritical CO2The peach blossom extraction solution of extraction：
0.8%, niacinamide：0.1%, allantoin：0.05%, carboxymethyl chitosan：0.05%, propolis extract：0.13%, glycerine：
4%, Sodium Hyaluronate：0.01%, pure water：90%.
By allantoin, carboxymethyl chitosan, Sodium Hyaluronate, glycerine, pure water at 85 DEG C stirring and dissolving, keep the temperature 20min,
Peach blossom extractive from fermentative, supercritical CO is added when being cooled to 30 DEG C2The peach blossom extraction solution of extraction, niacinamide, propolis extract
It is uniformly mixed, the pH for adjusting toner obtains toner later.The toner pH adjusts solvent and is the prior art and is not this
The improvement of invention, so it will not be repeated.
The preparation method of the peach blossom extractive from fermentative mainly includes the following steps that：After plant flowers are cleaned at 120 DEG C
Sterilize 10min, then accesses strain seed culture fluid and is fermented to obtain fermented material；Using the method for high-temperature instantaneous sterilization
By the zymophyte sterilizing in fermented material, it is centrifugally separating to obtain plant flowers extractive from fermentative；Using bacillus subtilis to plant
Flower ferments.
The supercritical CO2The preparation method of the peach blossom extraction solution of extraction mainly includes the following steps that：It will cleaning, freezing
Plant flowers after sterilizing, which are placed in extractor, to be vacuumized, then by supercritical CO2Extractant is with plant flowers according to 1:2.5 weight
Amount ratio mixes in extractor；2h is extracted under conditions of temperature is 35 DEG C, pressure is 6MPa, repeats above step extraction 2
Secondary, then gasify CO2After obtain supercritical CO2The plant flowers extraction solution of extraction.
Collect 50 volunteers to test the anaphylaxis of toner, the age bracket of the volunteer is 20-40, and will
The skin of hope person is without allergies；It is tested, toner is dropped in spot examination device, external application special adhesive tape using the method for patch
It is covered in the back of volunteer, 24 as a child removed, and waited for observe respectively within 0.5,6,12,24,48 hour, found the skin of volunteer
Skin does not occur adverse reaction, thus illustrates that toner is safe to use.
The stability of toner is tested, toner has the light fragrance taste of peach blossom, concrete property such as following table：
| Experimental project | Test result |
| Appearance | Solution is uniform, vibrates and muddiness does not occur, not stratified after standing |
| Heat-resistance test | It keeps 48h in 48 DEG C of baking oven, restores after room temperature without layering and precipitating phenomenon |
| Freezing test | 48h is kept at -10 DEG C, without layering and precipitating phenomenon after restoring to room temperature |
| Centrifugal test | Without layering and precipitating phenomenon after 4000r/min rotations 0.5h in centrifuge |
The moisture retention of toner is tested, toner moisture retention is weighed using percentage of water loss；If percentage of water loss is excessive, easily
Cause the loss of active ingredient, assimilation effect poor；The percentage of water loss of the toner test result is as follows table：
| Experimental project | 2h percentages of water loss wt% | 4h percentages of water loss wt% | 6h percentages of water loss wt% | 8h percentages of water loss wt% |
| As a result | 5.2 | 3.4 | 2.8 | 2.4 |
The toner being prepared in the present embodiment from the data in the table percentage of water loss in 8h is relatively low, illustrates toner
Active ingredient is largely absorbed by the skin, and has preferable practicability.
The scavenging ability of DPPH free radical of peach blossom extractive from fermentative is tested, precision weighs DPPH reagent 8mg, with nothing
Water-ethanol dissolves and is settled to 200ml brown volumetric flasks, obtains the DPPH solution that content is 0.004%, is protected from light holding；Peach blossom is taken to send out
Ferment extract 0.5ml is placed in 10ml centrifuge tubes, and the DPPH solution of 3ml is added, and room temperature is protected from light 30min, while with nothing
Water-ethanol is blank, and absorbance is measured at 517nm wavelength, and to calculate the clearance rate of DPPH, experiment is repeated 3 times and makes even
Mean value.The DPPH free radical scavenging activities that toner is obtained after test are 108.3%, the antioxygen of the peach blossom nutriment after fermenting
The property changed improves, to show that the toner has preferable inoxidizability.
The present invention improves the oxidation resistance of toner by adding the peach blossom nutritional ingredient of fermentation, by adding low temperature
Supercritical CO2The peach blossom nutrient solution of extraction utmostly saves the preservation of the trace element such as vitamin in peach blossom, by adding
Carboxymethyl chitosan and propolis is added to improve the compatibility of the antibiotic property and toner and skin of toner；The present invention passes through addition
Peach blossom extractive from fermentative and supercritical CO2The peach blossom extraction solution of extraction improves the phase of nutriment in the peach blossom in toner
Capacitive and synergistic effect, to improve the nutritional ingredient of toner；The present invention is using the extract of pure natural peach blossom as activity
Substance does not stimulate without any toxicity and side effects, mildly, and its active ingredient can be inhaled by the distinctive aquation of keratin by skin
It receives, prevents the moisture evaporation in cuticula from reducing, have the advantages that excellent replenishing water and preserving moisture, moisturize the skin, prevent skin aging.
Embodiment 2：
The pH of a kind of four seasons series toner based on Plant flawer extracts, the toner is 6.2, according to quality percentage
Include following component than calculating main：Rose extractive from fermentative：1.2%, supercritical CO2The rose extracting solution of extraction：
0.8%, niacinamide：0.1%, allantoin：0.05%, carboxymethyl chitosan：0.05%, propolis extract：0.13%, glycerine：
4%, Sodium Hyaluronate：0.01%, pure water：90%.
By allantoin, carboxymethyl chitosan, Sodium Hyaluronate, glycerine, pure water at 85 DEG C stirring and dissolving, keep the temperature 20min,
Rose extractive from fermentative, supercritical CO is added when being cooled to 30 DEG C2Rose extracting solution, niacinamide, the propolis of extraction carry
Liquid is taken to be uniformly mixed, the pH for adjusting toner obtains toner later.It is the prior art and not that the toner pH, which adjusts solvent,
It is the improvement of the present invention, so it will not be repeated.
The preparation method of the rose extractive from fermentative mainly includes the following steps that：At 120 DEG C after rose is cleaned
Then lower sterilizing 10min accesses strain seed culture fluid and is fermented to obtain fermented material；Using the side of high-temperature instantaneous sterilization
Method sterilizes the zymophyte in fermented material, is centrifugally separating to obtain rose extractive from fermentative；Using lactobacillus plantarum to rose
Flower ferments.
The supercritical CO2The preparation method of the rose extracting solution of extraction mainly includes the following steps that：It will clean, is cold
The rose frozen after sterilizing, which is placed in extractor, to be vacuumized, then by supercritical CO2Extractant is with rose according to 1:3 weight
Amount ratio mixes in extractor；2h is extracted under conditions of temperature is 35 DEG C, pressure is 6MPa, repeats above step extraction 3
Secondary, then gasify CO2After obtain supercritical CO2The rose extracting solution of extraction.
Collecting 50 volunteers to test the anaphylaxis of toner, the age bracket of the volunteer is 20-40 Sui, and
The skin of volunteer is without allergies；It is tested, toner is dropped in spot examination device, external application special glue using the method for patch
Band is covered in the back of volunteer, and 24 as a child removed, and waits for observe respectively within 0.5,6,12,24,48 hour, finds volunteer's
Skin does not occur adverse reaction, thus illustrates that toner is safe to use.
The scavenging ability of DPPH free radical of rose extractive from fermentative is tested, precision weighs DPPH reagent 8mg, uses
Absolute ethyl alcohol dissolves and is settled to 200ml brown volumetric flasks, obtains the DPPH solution that content is 0.004%, is protected from light holding；Take rose
Flower extractive from fermentative 0.5ml is placed in 10ml centrifuge tubes, the DPPH solution of 3ml is added, room temperature is protected from light 30min, simultaneously
Using absolute ethyl alcohol as blank, absorbance is measured at 517nm wavelength, to calculate the clearance rate of DPPH, experiment is repeated 3 times simultaneously
It is averaged.The DPPH free radical scavenging activities that toner is obtained after test are 113.6%, the peach blossom nutriment after fermenting
Inoxidizability improves, to show that the toner has preferable inoxidizability.
The stability of toner is tested, toner has the light fragrance taste of rose, concrete property such as following table：
| Experimental project | Test result |
| Appearance | Solution is uniform, vibrates and muddiness does not occur, not stratified after standing |
| Heat-resistance test | It keeps 48h in 48 DEG C of baking oven, restores after room temperature without layering and precipitating phenomenon |
| Freezing test | 48h is kept at -10 DEG C, without layering and precipitating phenomenon after restoring to room temperature |
| Centrifugal test | Without layering and precipitating phenomenon after 4000r/min rotations 0.5h in centrifuge |
The moisture retention of toner is tested, toner moisture retention is weighed using percentage of water loss；If percentage of water loss is excessive, easily
Cause the loss of active ingredient, assimilation effect poor；The percentage of water loss of the toner test result is as follows table：
| Experimental project | 2h percentages of water loss wt% | 4h percentages of water loss wt% | 6h percentages of water loss wt% | 8h percentages of water loss wt% |
| As a result | 4.8 | 3 | 2.5 | 2.2 |
The toner being prepared in the present embodiment from the data in the table percentage of water loss in 8h is relatively low, illustrates toner
Active ingredient is largely absorbed by the skin, and has preferable practicability.
The present invention improves the oxidation resistance of toner by adding the rose nutritional ingredient of fermentation, low by adding
Warm supercritical CO2The rose nutrient solution of extraction utmostly saves the preservation of the trace element such as vitamin in rose,
The compatibility of the antibiotic property and toner and skin of toner is improved by addition carboxymethyl chitosan and propolis；The present invention is logical
Cross addition rose extractive from fermentative and supercritical CO2The rose extracting solution of extraction improves in the rose in toner
The compatibility and synergistic effect of nutriment, to improve the nutritional ingredient of toner；The present invention is using pure natural rose
Extract does not stimulate without any toxicity and side effects, mildly, and its active ingredient can pass through the distinctive hydration of keratin as active material
Effect is absorbed by the skin, and prevents the moisture evaporation in cuticula from reducing, and is had excellent replenishing water and preserving moisture, is moisturized the skin, prevents skin
The advantages of skin aging.
The above is only presently preferred embodiments of the present invention, not does limitation in any form to the present invention, it is every according to
According to the technical spirit of the present invention to any simple modification, equivalent variations made by above example, the protection of the present invention is each fallen within
Within the scope of.
Claims (8)
1. a kind of four seasons series toner based on Plant flawer extracts, which is characterized in that the pH of the toner is 6.0-
7.0, it includes mainly following component to be calculated according to mass percent：
Plant flowers extractive from fermentative：0.05%-1.2%；
Supercritical CO2The plant flowers extraction solution of extraction：0.03-2%；
Niacinamide：0.05-0.1%；
Allantoin：0.05%；
Carboxymethyl chitosan：0.03-0.1%；
Propolis extract：0.08-0.25%；
Glycerine：4%；
Sodium Hyaluronate：0.01%-0.03%；
Pure water：85%-95%；
By allantoin, carboxymethyl chitosan, Sodium Hyaluronate, glycerine, pure water at 75-90 DEG C stirring and dissolving, keep the temperature 20min,
Plant flowers extractive from fermentative, supercritical CO is added when being cooled to 35-40 DEG C2The plant flowers extraction solution of extraction, niacinamide, propolis
Extracting solution is uniformly mixed, and the pH for adjusting toner obtains toner later.
2. a kind of four seasons series toner based on Plant flawer extracts according to claim 1, which is characterized in that according to
It includes mainly following component that mass percent, which calculates,：Peach blossom extractive from fermentative：1.2%, supercritical CO2The peach blossom extraction of extraction is molten
Liquid：0.8%, niacinamide：0.1%, allantoin：0.05%, carboxymethyl chitosan：0.05%, propolis extract：0.13%, glycerine：4%、
Sodium Hyaluronate：0.01%, pure water：85%-90%.
3. a kind of four seasons series toner based on Plant flawer extracts according to claim 1, which is characterized in that according to
It includes mainly following component that mass percent, which calculates,：Rose extractive from fermentative：1.2%, supercritical CO2The rose of extraction extracts
Take solution：0.8%, niacinamide：0.1%, allantoin：0.05%, carboxymethyl chitosan：0.05%, propolis extract：0.13%, sweet
Oil：4%, Sodium Hyaluronate：0.01%, pure water：85%-90%.
4. a kind of four seasons series toner based on Plant flawer extracts according to claim 1, which is characterized in that according to
It includes mainly following component that mass percent, which calculates,：Chrysanthemum extractive from fermentative：1.2%, supercritical CO2The chrysanthemum extraction of extraction is molten
Liquid：0.8%, niacinamide：0.1%, allantoin：0.05%, carboxymethyl chitosan：0.05%, propolis extract：0.13%, glycerine：4%、
Sodium Hyaluronate：0.01%, pure water：85%-90%.
5. a kind of four seasons series toner based on Plant flawer extracts according to claim 1, which is characterized in that according to
It includes mainly following component that mass percent, which calculates,：Pot marigold extractive from fermentative：1.2%, supercritical CO2The pot marigold of extraction extracts
Take solution：0.8%, niacinamide：0.1%, allantoin：0.05%, carboxymethyl chitosan：0.05%, propolis extract：0.13%, sweet
Oil：4%, Sodium Hyaluronate：0.01%, pure water：85%-90%.
6. according to a kind of four seasons series toner based on Plant flawer extracts of claim 1-5 any one of them, feature
It is, the preparation method of the plant flowers extractive from fermentative mainly includes the following steps that：It goes out at 120 DEG C after plant flowers are cleaned
Then bacterium 5-12min accesses strain seed culture fluid and is fermented to obtain fermented material；It will using the method for high-temperature instantaneous sterilization
Zymophyte sterilizing in fermented material, is centrifugally separating to obtain plant flowers extractive from fermentative.
7. a kind of four seasons series toner based on Plant flawer extracts according to claim 6, which is characterized in that use
Bacillus subtilis or lactobacillus plantarum ferment to plant flowers.
8. a kind of four seasons series toner based on Plant flawer extracts according to claim 1, which is characterized in that described
Supercritical CO2The preparation method of the plant flowers extraction solution of extraction mainly includes the following steps that：By the plant after cleaning, freezing sterilizing
Object flower, which is placed in extractor, to be vacuumized, then by supercritical CO2Extractant is with plant flowers according to 1:The weight ratio of 1-5 is extracting
It is mixed in tank；1-2.5h is extracted under conditions of temperature is 20-35 DEG C, pressure is 5-7.2MPa, is repeated above step and is extracted 2-3
Secondary, then gasify CO2After obtain supercritical CO2The plant flowers extraction solution of extraction.
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| CN109806201A (en) * | 2019-03-29 | 2019-05-28 | 山东花物堂生物科技有限公司 | A kind of preparation method and application of rose fermentation liquid |
| CN111544371A (en) * | 2020-06-12 | 2020-08-18 | 洋浦吉商生物科技有限公司 | Whitening and repairing mask containing probiotic active extracting solution and nicotinamide |
| CN113384510A (en) * | 2021-06-25 | 2021-09-14 | 科丝美诗(中国)化妆品有限公司 | Fermented composition with anti-photoaging, relieving and cooling effects and preparation method and application thereof |
| CN114288233A (en) * | 2021-12-02 | 2022-04-08 | 科丝美诗(中国)化妆品有限公司 | Composition for promoting metabolism of aged skin and preparation method and application thereof |
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| CN114288233A (en) * | 2021-12-02 | 2022-04-08 | 科丝美诗(中国)化妆品有限公司 | Composition for promoting metabolism of aged skin and preparation method and application thereof |
| CN114288233B (en) * | 2021-12-02 | 2023-09-01 | 科丝美诗(中国)化妆品有限公司 | Composition for promoting metabolism of aged skin and preparation method and application thereof |
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