CN110870885A - A medicinal liquid with cleaning, sterilizing and moisturizing effects, and its application - Google Patents
A medicinal liquid with cleaning, sterilizing and moisturizing effects, and its application Download PDFInfo
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- A61K36/18—Magnoliophyta (angiosperms)
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K9/70—Web, sheet or filament bases ; Films; Fibres of the matrix type containing drug
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Abstract
The invention relates to the technical field of traditional Chinese medicine and sanitation, and particularly discloses a liquid medicine with cleaning, sterilizing and moisturizing effects and application thereof. The liquid medicine comprises 0.5-5.0% of herba elsholtziae extract by mass percent; the elsholtzia splendens extract contains not less than 0.2 percent of elsholtzia splendens seed extract by mass percent, and the elsholtzia splendens seed extract adopts supercritical CO for elsholtzia splendens seeds2The elsholtzia extract also contains elsholtzia essential oil and/or elsholtzia water extract. The liquid medicine has wide application in preparing sanitary articles, especially wet tissue prepared from the liquid medicine has three-in-one functions of cleaning, sterilizing and moisturizing, has unique Chinese herbal medicine faint scent, is extracted from pure plants without artificially synthesized essence, is more acceptable by wide users, and has better market prospect.
Description
Technical Field
The invention belongs to the technical field of traditional Chinese medicine and sanitation, and particularly relates to a liquid medicine with cleaning, sterilizing and moisturizing effects and application thereof.
Background
The wet tissue is a disposable cleaning sanitary article prepared by selecting a wet-strength soft-fiber high-permeability base material, folding, humidifying and packaging, and becomes an essential cleaning article in daily life of people due to the characteristics of basic functions of cleaning and moisturizing skin, convenience in carrying and the like. The antibacterial wet tissue is prepared by adding metals such as silver, copper and lead sulfite, benzalkonium chloride, benzethonium chloride, triclosan, chlorhexidine, alcohol and other chemical agents for inhibiting bacterial reproduction, but the components are often strong in smell and strong in irritation and can influence the health of human bodies. The addition of traditional Chinese medicine components is the most intensive place of wet tissue products in recent years, and medicines are reasonably designed according to different use objects.
Many ingredients in traditional Chinese medicines have the effects of resisting bacteria and diminishing inflammation, and gradually become the concerned field of adding liquid medicine into wet tissues, a plurality of wet tissues are using the ingredients of the traditional Chinese medicines to replace chemical ingredients or metal ingredients, for example, the application number is CN201410766023.3, the invention name is a private part cleaning and sanitary wet tissue and a preparation method thereof, the invention discloses the wet tissue which is developed and used for private parts by using the water extracts of panax notoginseng, day lily, sophora japonica branch, soya bean, licorice, artemisia rupestris, and the essential oil of geranium, lavender, frankincense, myrrh, chamomile, juniper and the like; also, for example, the application number is CN201510843842.8, the invention name is an antibacterial hand wiping wet tissue, and the invention discloses an antibacterial hand wiping wet tissue prepared by adding green tea essence or jasmine flower essence into extract of chamomile, aloe and calendula; the invention also discloses a tissue for disinhibiting and disinfecting for the small intestine and a preparation method thereof, and the tissue is prepared from magnolia officinalis alcohol extract, cnidium fruit volatile oil, senecio scandens alcohol extract, usnic acid and the like, wherein the application number is CN 201610081987.3; the invention discloses an organic anti-inflammatory and anti-allergy sanitary wet tissue prepared from fresh extract liquid of geranium, chamomile, purslane and aloe and a preparation method thereof, wherein the extract liquid of the fresh geranium, the chamomile, the purslane and the aloe are used for preparing the anti-inflammatory and anti-allergy sanitary wet tissue; however, the added combination of the wet tissues needs the synergy of a plurality of traditional Chinese medicines, the combination of the traditional Chinese medicines has difficult sources and complex process, some of the traditional Chinese medicines need fresh herbs, the difficulty is increased, and the formed liquid medicine has single function and generally mainly has the antibacterial and anti-inflammatory effects, so the application range is narrow and the universality is not realized.
At present, no wet tissue product containing the elsholtzia splendens extract exists in the market.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: aiming at the requirements of people on skin and hair cleaning and moistening at the same time and overcoming the defects of products in the market, the invention provides a medicinal liquid containing a elsholtzia haichowensis extract and an application thereof, wherein the medicinal liquid can improve the disinfection and sterilization performance and the moisture retention performance. The medicinal liquid contains Elsholtzia splendens extract. Can effectively moisturize and moisten skin and smooth and repair dry hair; can effectively clean skin and hair, and keep the skin and the hair clean and dry; can effectively resist and inhibit bacteria and maintain the health state of skin; the plant essence has unique Chinese herbal medicine faint scent, is extracted from pure plants without artificially synthesized essence, is more acceptable by wide users, and has better market application prospect.
The invention uses a traditional Chinese medicine of Jiang Xiang Moslae which can be used as medicine and food as a main medicine, and can obtain the liquid medicine for the wet tissue with three-in-one functions of cleaning, antibiosis, anti-inflammation and moisture retention by combining the seed extract, the water extract of the whole herb of the seed extract and volatile essential oil.
The invention adopts the following technical scheme to achieve the purpose of the invention.
Firstly, the invention discloses a liquid medicine with the functions of cleaning, sterilizing and moisturizing. The liquid medicine has three functions of cleaning, sterilizing and moisturizing.
A liquid medicine with cleaning, sterilizing and moisturizing effects comprises 0.5-5.0% of herba Elsholtziae seu Moslae extract by mass percent; the elsholtzia splendens extract contains not less than 0.2 percent of elsholtzia splendens seed extract by mass percent.
Furthermore, the elsholtzia extract also contains elsholtzia essential oil and/or elsholtzia water extract.
Preferably, the liquid medicine contains, by mass: 0.5 percent of Jiangxiang elsholtzia seed extract, 0.5 percent of Jiangxiang elsholtzia essential oil and 1 percent of Jiangxiang elsholtzia water extract.
Herba Moslae is Labiatae plant herba MoslaeMoslachinensisMax-imakOr herba MoslaeM.chinensis- jiangxiangru．Dried aerial parts of (1). It is recorded in the Ming Yi Bie Lu (miscellaneous records of famous physicians), listed as a middle-grade food, and has the actions of inducing sweat to relieve exterior syndrome, inducing diuresis to alleviate edema, regulating the middle warmer to resolve dampness, etc., with pungent and mild taste. The elsholtzia splendens extract contains aromatic substances, the aromatic substances can inhibit the activities of bacteria, viruses, anaerobes and acidogenesis, and can play a role in accelerating sweat volatilization, removing oil and sweatThe wet tissue keeps the theory of moist and dry state in the process of cleaning skin and hair and has good skin and hair care effect.
The fatty acid components such as linolenic acid in the elsholtzia seeds have the functions of effectively moisturizing, moistening skin and smoothing and repairing dry hair, so the three-effect liquid medicine for cleaning, sterilizing and moisturizing can be formed by adding the whole grass of the elsholtzia and the extract of the seeds.
Further, the extraction method of the seed extract comprises the following steps: by using supercritical CO2Extracting the oily component.
Further, the supercritical CO2The extraction process specifically comprises the following steps: cleaning mature seeds, drying, pulverizing, sieving with 30-50 mesh sieve, weighing 1 weight part of seed powder, placing in extraction tank capable of accommodating 4-8 weight parts of seed powder, sealing system, and introducing CO2The preparation method comprises the steps of taking the extract as an extractant, starting extraction after the extraction temperature reaches 54-56 ℃, controlling the temperature of a separation I and the temperature of a separation II to be 54-56 ℃ and 49-51 ℃, respectively, controlling the pressure of the separation I to be 6.8-7.2 MPa, controlling the pressure of the separation II to be 4.8-5.2 MPa, and obtaining oily components by the separation I and the separation II after the extraction is finished, namely the elsholtzia splendens seed extract.
Compared with conventional squeezing extraction, the supercritical CO is adopted2The extraction technology for extracting the elsholtzia seed extract can not only obviously improve the yield of the elsholtzia seed fatty oil, the yield of the elsholtzia seed fatty oil can be improved by more than 30 percent, but also can treat various active substances with the functions of cleaning, sterilizing and moisturizing, such as unsaturated fatty acids with rare content in seeds and the like in the elsholtzia seed by supercritical CO2The extract can be more completely introduced into the seed extract of herba Elsholtziae seu Moslae, and can be subjected to supercritical CO extraction2The quality of the elsholtzia splendens seed extract obtained by extraction is far superior to that of elsholtzia splendens seed fatty oil obtained by conventional squeezing extraction, and the elsholtzia splendens seed extract is subjected to supercritical CO treatment2The obtained herba Elsholtziae seu Moslae seed extract has cleaning, sterilizing and moisture keeping effects.
Furthermore, the extraction method of the elsholtzia essential oil comprises the following steps: dried whole grass of elsholtzia splendens is soaked in saline water, heated and cooked, circularly distilled, distilled and cooled to obtain oil phase fraction of elsholtzia splendens essential oil.
Furthermore, the extraction method of the elsholtzia water extract comprises the following steps: taking kilogram-liter or gram-milliliter as a weight-volume unit, soaking, boiling, concentrating and the like 5 parts by weight of dried whole grass of elsholtzia splendens to finally obtain 1 part by volume of elsholtzia splendens fluid extract.
The invention also discloses application of the liquid medicine with the functions of cleaning, sterilizing and moisturizing in preparation of sanitary products.
The sanitary article is a wet tissue. The wet tissue has the three-in-one functions of cleaning, sterilizing and moisturizing. The invention uses a Chinese traditional medicine of Jiang Xiang Moslae which can be used as medicine and food as a main medicine, and can obtain the three-in-one liquid medicine for the wet tissue with the functions of cleaning, antibiosis, anti-inflammation and moisture preservation by combining the seed extract, the water extract of the whole herb of the seed extract and volatile essential oil, thereby having the capability of forming the multi-purpose wet tissue.
A wet towel with three-in-one functions of cleaning, sterilizing and moisturizing comprises wet towel medicinal liquid and base material carrying the medicinal liquid; the wet tissue liquid medicine comprises 0.5-5.0% of elsholtzia extract by mass percent, and the pH value of the liquid medicine is 3.5-8.5; the elsholtzia splendens extract contains not less than 0.2 percent of elsholtzia splendens seed extract by mass percent.
Furthermore, the elsholtzia extract also contains elsholtzia essential oil and/or elsholtzia water extract.
Further, the base material is non-woven fabric; the non-woven fabric is spunlace non-woven fabric or bamboo fiber non-woven fabric.
Furthermore, the wet tissue liquid medicine also comprises 0.01 to 2.0 percent of preservative, 0 to 10.0 percent of humectant, 0 to 5.0 percent of skin care agent, 0 to 0.5 percent of stabilizer, 0.01 to 2.0 percent of surfactant and a proper amount of acidity regulator in percentage by mass.
Still further, the preservative is selected from: geogard Ultra preservative, benzalkonium chloride, sodium methyl p-hydroxybenzoate and sodium salt thereof, ethyl p-hydroxybenzoate and sodium salt thereof, polyhexamethylene monoguanidine, polyhexamethylene biguanidine hydrochloride, phenoxyethanol, methylisothiazolinone, potassium sorbate, dehydroacetic acid, benzyl alcohol, dichlorobenzene, methanol, ethylhexyl glycerol, octanediol and the like, or a mixture of any one or more of the common preservatives. The antiseptic is added into the wet tissue liquid medicine for antisepsis.
Furthermore, the humectant is a polyhydric alcohol humectant, an amino acid humectant or other humectants; the polyalcohol humectant is any one or mixture of propylene glycol, glycerol and the like; the amino acid humectant is any one or mixture of glycine, sarcosine, alanine, proline, hydroxyproline and mixture thereof; the other moisturizers are any one or a mixture of more of collagen, milk protein, hyaluronic acid, sodium hyaluronate, oat glucan, oat protein, urea and derivatives thereof. The humectant is added into the wet tissue liquid medicine for keeping moisture.
Furthermore, the skin care agent is an oily skin care agent and/or a water-soluble skin care agent; the oily skin care agent is selected from one or more of vitamin E acetate, coenzyme Co-Q10, D-panthenol, wheat germ oil, mineral oil, castor oil, shea butter, sweet almond oil, pear oil, lanolin and derivatives thereof, methyl isostearate, isopropyl isostearate, vaseline and polydimethylsiloxane; the water-soluble skin care agent is selected from one or more of folium Artemisiae Argyi extract, fructus Actinidiae chinensis extract, soybean isoflavone extract, flos Lonicerae extract, grape seed extract, green tea extract, radix Puerariae extract, and flos Nelumbinis extract. The oily skin care agent and/or water-soluble skin care agent is added into the wet tissue liquid medicine for skin care.
Furthermore, the surfactant is selected from one or more of sodium cocoamphoacetate, disodium cocoamphodiacetate, cocobetaine and cocamidopropyl betaine. The surfactant is added into the wet tissue liquid medicine to reduce the surface tension.
Furthermore, the acidity regulator is selected from one or more of citric acid, sodium citrate, malic acid and lactic acid. The organic acid is used as acidity regulator in the wet tissue liquid medicine, so that the pH value is regulated, and irritation is avoided.
Further, the stabilizer is disodium EDTA or tetrasodium EDTA. The stabilizer is added into the wet tissue liquid medicine for stabilizing the product.
Further, the preparation method of the wet tissue comprises the following steps:
s1, preparing solution A and solution B:
solution A: respectively weighing herba Moslae chinensis extract (volatile oil or seed extract), oily skin caring agent, and surfactant according to wet towel liquid medicine ratio, mixing, heating to 50-60 deg.C for dissolving, and stirring for 10-15 min;
and B, liquid B: respectively weighing and mixing the water extract of elsholtzia splendens, the humectant and the preservative according to the proportion of the wet tissue liquid medicine, heating to 40-50 ℃ for dissolution, and uniformly stirring for 10-15 minutes;
s2, preparing wet tissue liquid medicine: according to the proportion of the wet tissue liquid medicine, firstly adding pure water into a stirring kettle, adding the liquid A under the stirring state, and slowly adding the liquid B after the pure water is completely dissolved; respectively adding the water-based skin care agent and the stabilizer under stirring until the skin care agent and the stabilizer are completely dissolved to form wet tissue liquid medicine, and regulating and controlling the pH value of the prepared wet tissue liquid medicine to be between 3.5 and 8.5 by using the acidity regulator;
s3, preparing wet tissues: humidifying the base material by using the wet tissue liquid medicine prepared in the step S2, controlling the liquid content of the wet tissue to be 3-6 times of the mass of the base material, and packaging by quality inspection to obtain the wet tissue containing the elsholtzia splendens.
Has the advantages that:
(1) the invention provides a medicinal liquid with cleaning, sterilizing and moisturizing functions, which contains Elsholtzia splendens seed extract component which adopts supercritical CO2The elsholtzia seed extract has high-percentage linolenic acid component, and can effectively moisturize and moisten skin and smooth and repair dry hair.
(2) By using supercritical CO2Extraction technology for extracting elsholtzia splendensSupercritical CO compared to conventional extraction by pressing2The extraction technology can not only obviously improve the yield of the elsholtzia splendens seed fatty oil, the yield can be improved by more than 30 percent, but also can treat various active substances with the functions of cleaning, sterilizing and moisturizing in the elsholtzia splendens seeds, such as unsaturated fatty acids with rare content in the seeds and the like by supercritical CO2The extract can be more completely introduced into the seed extract of herba Elsholtziae seu Moslae, and can be subjected to supercritical CO extraction2The quality of the elsholtzia splendens seed extract obtained by extraction is far superior to that of elsholtzia splendens seed fatty oil obtained by conventional squeezing extraction, and the elsholtzia splendens seed extract is subjected to supercritical CO treatment2The obtained herba Elsholtziae seu Moslae seed extract has cleaning, sterilizing and moisture keeping effects.
(3) The medicinal liquid with the functions of cleaning, sterilizing and moisturizing provided by the invention can effectively clean skin and hair and keep the skin and the hair in a clean and dry state due to the fact that the contained elsholtzia splendens extract contains water extract components.
(4) The medicinal liquid with the functions of cleaning, sterilizing and moisturizing provided by the invention contains volatile essential oil and water extract components in the elsholtzia haichowensis extract, so that the medicinal liquid can effectively resist and inhibit bacteria and maintain the health state of skin.
(5) The liquid medicine with the functions of cleaning, sterilizing and moisturizing provided by the invention has unique Chinese herbal medicine faint scent, and is extracted from pure plants without artificially synthesized essence, so that the liquid medicine is more acceptable to users.
(6) The wet tissue prepared by the liquid medicine containing the elsholtzia haichowensis extract fills the blank that the traditional Chinese medicine wet tissue product in the market has single function and no three-in-one function, and has better market prospect.
(7) The invention uses a Chinese traditional medicine of Jiang Xiang Moslae which can be used as medicine and food as a main medicine, and the liquid medicine for the wet tissue with three-in-one functions of cleaning, antibiosis, anti-inflammation and moisture retention can be obtained by combining the seed extract, the water extract of the whole herb of the seed extract and volatile essential oil.
(8) The preparation method of the wet tissue with the three-in-one functions of cleaning, sterilizing and moisturizing provided by the invention has the advantages of simple and convenient process method, conventional and universal equipment, stable and reliable product quality, and convenience for industrial, continuous and intelligent production.
Detailed Description
The present invention will be further described with reference to specific examples, but the present invention is not limited to the following examples. The method is a conventional method unless otherwise specified. The starting materials are commercially available from the open literature unless otherwise specified.
Example 1: preparation of elsholtzia seed extract:
by using supercritical CO2Extracting to obtain Elsholtzia splendens seed extract; the supercritical CO2The extraction process flow is as follows: CO 22Steel cylinder-cooling system-high pressure pump-extraction tank-separator I-separator II-cooling system (circulation). Supercritical CO2The extraction process comprises the following steps: cleaning mature seeds, drying, pulverizing, sieving with 40 mesh sieve, weighing 2000 g seed powder, placing in 10L extraction tank, sealing system, and introducing CO2The extraction is carried out when the extraction temperature reaches 55 ℃ as an extracting agent, the temperature of a separation I and the temperature of a separation II are respectively controlled at 55 ℃ and 50 ℃, the pressure of the separation I is controlled at 7.0MPa, the pressure of the separation II is controlled at 5.0MPa, and after the extraction is finished, oily components obtained by the separation I and the separation II are used as the extract of the seeds of the elsholtzia splendens. By using supercritical CO2The extraction technology has the advantages that: supercritical CO compared to conventional squeeze extraction2The extraction technology not only can obviously improve the yield of the elsholtzia splendens seed fatty oil, the yield can be improved by more than 30 percent, but also can treat various active substances with the functions of cleaning, sterilizing and moisturizing in the elsholtzia splendens seeds, such as unsaturated fatty acids with rare content in the seeds and the like by supercritical CO2The extract can be more completely introduced into the seed extract of herba Elsholtziae seu Moslae, and can be subjected to supercritical CO extraction2The quality of the elsholtzia splendens seed extract obtained by extraction is far superior to that of elsholtzia splendens seed fatty oil obtained by conventional squeezing extraction, and the elsholtzia splendens seed extract is subjected to supercritical CO treatment2The seed extract of herba Moslae chinensis obtained by extraction has clear effectCleaning, sterilizing and moisturizing.
Example 2: preparing the elsholtzia essential oil:
5 kg of dry whole grass of elsholtzia splendens and 50 g of salt are soaked in water for 12 hours, and then the oil phase fraction obtained is elsholtzia splendens essential oil through the steps of heating and stewing, circulating distillation, fraction cooling and the like.
Example 3: preparation of a water extract of elsholtzia splendens:
the preparation method comprises the steps of soaking, boiling in water, concentrating and the like 5 kg of dried whole grass of elsholtzia splendens to finally obtain 1L of elsholtzia splendens fluid extract.
Example 4: the herba elsholtziae extract contained in the liquid medicine A:
the embodiment provides a liquid medicine A with the functions of cleaning, sterilizing and moisturizing, which comprises the following components in percentage by weight: 0.5 percent of Jiangxiang elsholtzia seed extract, 0.5 percent of Jiangxiang elsholtzia essential oil and 1 percent of Jiangxiang elsholtzia water extract.
Example 5: the herba elsholtziae extract contained in the liquid medicine B is as follows:
the embodiment provides a liquid medicine B with the functions of cleaning, sterilizing and moisturizing, which comprises the following components in parts by weight: 0.5 percent of Jiangxiang elsholtzia seed extract and 1 percent of Jiangxiang elsholtzia water extract.
Example 6: the herba elsholtziae extract contained in the liquid medicine C is as follows:
the embodiment provides a liquid medicine C with cleaning, sterilizing and moisturizing effects, which comprises the following components in parts by weight: 0.5 percent of elsholtzia seed extract and 0.5 percent of elsholtzia essential oil.
Example 7 (comparative example 1): the herba elsholtziae extract contained in the liquid medicine D:
the present invention provides a medicinal liquid dice containing elsholtzia haichowensis extract, which contains the following components by weight: 0.5 percent of Jiangxiang elsholtzia essential oil.
Example 8 (comparative example 2): the herba elsholtziae extract contained in the liquid medicine amyl:
the present example provides a liquid medicine containing elsholtzia splendens extract, which contains the following components by weight: 1 percent of Jiangxiang elsholtzia aqueous extract.
Example 9 (comparative example 3): the herba elsholtziae extract contained in the liquid medicine is as follows:
the present example provides a liquid medicine containing elsholtzia haichowensis extract, which contains by weight: 0.5 percent of elsholtzia seed extract.
Example 10: a wet towel containing liquid medicine A comprises:
a wet towel A containing Elsholtzia splendens extract comprises wet towel medicinal liquid A and non-woven fabric carrying the medicinal liquid. The wet tissue liquid medicine A is based on the liquid medicine A in the embodiment 4, and other auxiliary components are added, and the specific formula comprises the following components in parts by weight per 100: 2% of elsholtzia extract (0.5% of elsholtzia seed extract, 0.5% of elsholtzia essential oil and 1% of elsholtzia water extract), 2% of vitamin E acetate (oily skin care agent), 1% of cocoampho sodium acetate (surfactant), 5% of glycerin (humectant), 0.01% of sodium methyl p-hydroxybenzoate and sodium salt (preservative), 1.5% of kiwi fruit extract (aqueous skin care agent), 0.2% of EDTA disodium (stabilizer), a proper amount of citric acid (acidity regulator), and the balance of pure water, wherein the pH of the wet tissue liquid medicine is 6.0. The preparation process comprises the following steps:
and S1, preparing a solution A and a solution B. Solution A, according to the proportion of the wet tissue liquid medicine, respectively weighing and mixing elsholtzia extract (volatile oil and seed extract), oily skin care agent and surfactant, heating to 55 ℃ for dissolving, and uniformly stirring for 13 minutes; liquid B, namely weighing and mixing the elsholtzia haichowensis water extract, the humectant and the preservative respectively according to the proportion of the wet tissue liquid medicine, heating to 45 ℃ for dissolution, and uniformly stirring for 13 minutes;
s2, preparing wet tissue liquid medicine: according to the proportion of the wet tissue liquid medicine, firstly adding pure water into a stirring kettle, adding the liquid A under the stirring state, and slowly adding the liquid B after the pure water is completely dissolved; respectively adding the water-based skin care agent and the stabilizer under the stirring state until the skin care agent and the stabilizer are completely dissolved to form wet tissue liquid medicine, and regulating the pH value of the prepared wet tissue liquid medicine to be 6.0 by using the acidity regulator;
s3, preparing wet tissues: humidifying the non-woven fabric base material by using the wet tissue liquid medicine prepared in the step S2, controlling the liquid content of the wet tissue to be 4.5 times of the mass of the non-woven fabric base material, and performing quality inspection and packaging to obtain a wet tissue A containing the elsholtzia haichowensis extract.
Example 11: a wet tissue containing a liquid medicine B comprises:
a wet towel B containing Elsholtzia splendens extract is prepared from wet towel medicinal liquid B and non-woven fabric carrying the medicinal liquid. The wet tissue liquid medicine B is based on the liquid medicine B in the embodiment 5, and other auxiliary components are added, and the specific formula comprises the following components in parts by weight per 100: 1.5 percent of elsholtzia extract (0.5 percent of elsholtzia seed extract and 1 percent of elsholtzia water extract), 2 percent of vitamin E acetate (oily skin care agent), 1 percent of cocoampho sodium acetate (surfactant), 5 percent of glycerin (humectant), 0.01 percent of sodium methyl p-hydroxybenzoate and sodium salt (preservative), 1.5 percent of kiwi fruit extract (aqueous skin care agent), 0.2 percent of EDTA disodium (ethylene diamine tetraacetic acid) (stabilizer), a proper amount of citric acid (acidity regulator), and the balance of pure water, wherein the pH of the wet tissue liquid medicine is 5.0. The preparation process specifically comprises the following steps:
and S1, preparing a solution A and a solution B. Solution A, according to the proportion of the wet tissue liquid medicine, respectively weighing and mixing herba elsholtziae extract (seed extract), oily skin care agent and surfactant, heating to 50 ℃ for dissolution, and uniformly stirring for 15 minutes; liquid B, namely weighing and mixing the elsholtzia haichowensis water extract, the humectant and the preservative respectively according to the proportion of the wet tissue liquid medicine, heating to 40 ℃ for dissolution, and uniformly stirring for 15 minutes;
s2, preparing wet tissue liquid medicine: according to the proportion of the wet tissue liquid medicine, firstly adding pure water into a stirring kettle, adding the liquid A under the stirring state, and slowly adding the liquid B after the pure water is completely dissolved; respectively adding the water-based skin care agent and the stabilizer under the stirring state until the skin care agent and the stabilizer are completely dissolved to form wet tissue liquid medicine, and regulating the pH value of the prepared wet tissue liquid medicine to be 5.0 by using the acidity regulator;
s3, preparing wet tissues: humidifying the non-woven fabric base material by using the wet tissue liquid medicine prepared in the step S2, controlling the liquid content of the wet tissue to be 4.5 times of the mass of the non-woven fabric base material, and performing quality inspection and packaging to obtain a wet tissue B containing the elsholtzia haichowensis extract.
Example 12: a wet tissue containing liquid medicine C:
a wet towel C containing Elsholtzia splendens extract comprises wet towel medicinal liquid C and non-woven fabric carrying the medicinal liquid. The wet tissue liquid medicine C is based on the liquid medicine C in the embodiment 6, and other auxiliary components are added, and the specific formula comprises the following components in parts by weight per 100: 1% of elsholtzia extract (0.5% of elsholtzia seed extract and 0.5% of elsholtzia essential oil), 2% of vitamin E acetate (oily skin care agent), 1% of cocoampho sodium acetate (surfactant), 5% of glycerin (humectant), 0.01% of sodium methyl p-hydroxybenzoate and sodium salt (preservative), 1.5% of kiwi fruit extract (aqueous skin care agent), 0.2% of disodium EDTA (ethylene diamine tetraacetic acid) (stabilizer), a proper amount of citric acid or sodium citrate (acidity regulator), and the balance of pure water, wherein the pH value of the wet tissue liquid medicine is 7.0. The preparation process specifically comprises the following steps:
and S1, preparing a solution A and a solution B. Solution A, namely weighing and mixing herba elsholtziae extract, oily skin care agent and surfactant respectively according to the proportion of the wet tissue liquid medicine, heating to 60 ℃ for dissolving, and uniformly stirring for 10 minutes; b, according to the proportion of the wet tissue liquid medicine, respectively weighing and mixing the humectant and the preservative, heating to 50 ℃ to dissolve, and uniformly stirring for 10 minutes;
s2, preparing wet tissue liquid medicine: according to the proportion of the wet tissue liquid medicine, firstly adding pure water into a stirring kettle, adding the liquid A under the stirring state, and slowly adding the liquid B after the pure water is completely dissolved; respectively adding the water-based skin care agent and the stabilizer under the stirring state until the skin care agent and the stabilizer are completely dissolved to form wet tissue liquid medicine, and regulating the pH value of the prepared wet tissue liquid medicine to be 7.0 by using the acidity regulator;
s3, preparing wet tissues: humidifying the non-woven fabric base material by using the wet tissue liquid medicine prepared in the step S2, controlling the liquid content of the wet tissue to be 4.5 times of the mass of the non-woven fabric base material, and performing quality inspection and packaging to obtain the wet tissue C containing the elsholtzia haichowensis extract.
Example 13 (comparative example 1): a wet tissue containing medicinal liquid D:
a wet towel D containing Elsholtzia splendens extract comprises wet towel medicinal liquid D and non-woven fabric carrying the medicinal liquid. The wet tissue liquid medicine D is based on the liquid medicine D in the embodiment 7, and other auxiliary components are added, and the specific formula comprises the following components in parts by weight per 100: 0.5 percent of elsholtzia essential oil (elsholtzia extract), 2 percent of vitamin E acetate (oily skin care agent), 1 percent of cocoampho sodium acetate (surfactant), 5 percent of glycerin (humectant), 0.01 percent of sodium methyl p-hydroxybenzoate and sodium salt (preservative), 1.5 percent of kiwi fruit extract (aqueous skin care agent), 0.2 percent of EDTA disodium (stabilizer), a proper amount of sodium citrate (acidity regulator), the balance of pure water, and the pH value of the wet tissue liquid medicine is 8.0. The preparation process specifically comprises the following steps:
and S1, preparing a solution A and a solution B. Solution A, namely weighing and mixing herba elsholtziae extract, oily skin care agent and surfactant respectively according to the proportion of the wet tissue liquid medicine, heating to 55 ℃ to dissolve, and uniformly stirring for 13 minutes; b, according to the proportion of the wet tissue liquid medicine, respectively weighing and mixing the humectant and the preservative, heating to 45 ℃ to dissolve, and uniformly stirring for 13 minutes;
s2, preparing wet tissue liquid medicine: according to the proportion of the wet tissue liquid medicine, firstly adding pure water into a stirring kettle, adding the liquid A under the stirring state, and slowly adding the liquid B after the pure water is completely dissolved; respectively adding the water-based skin care agent and the stabilizer under the stirring state until the skin care agent and the stabilizer are completely dissolved to form wet tissue liquid medicine, and regulating the pH value of the prepared wet tissue liquid medicine to be 8.0 by using the acidity regulator;
s3, preparing wet tissues: humidifying the non-woven fabric base material by using the wet tissue liquid medicine prepared in the step S2, controlling the liquid content of the wet tissue to be 4.5 times of the mass of the non-woven fabric base material, and performing quality inspection and packaging to obtain the wet tissue D containing the elsholtzia haichowensis extract.
Example 14 (comparative example 2): a wet tissue containing liquid medicine Wu:
a wet towel penta containing Elsholtzia splendens extract comprises wet towel medicinal liquid penta and non-woven fabric carrying the medicinal liquid. The wet tissue liquid medicine E is based on the liquid medicine E in the embodiment 8, and other auxiliary components are added, and the specific formula comprises the following components in parts by weight per 100: 1 percent of elsholtzia water extract (elsholtzia extract), 2 percent of vitamin E acetate (oily skin care agent), 1 percent of cocoampho sodium acetate (surfactant), 5 percent of glycerin (humectant), 0.01 percent of sodium methyl p-hydroxybenzoate and sodium salt (preservative), 1.5 percent of kiwi fruit extract (aqueous skin care agent), 0.2 percent of EDTA disodium (stabilizer), a proper amount of citric acid (acidity regulator), the balance of pure water, and the pH value of the wet tissue liquid medicine is 4.0. The preparation process specifically comprises the following steps:
and S1, preparing a solution A and a solution B. Liquid A, according to the proportion of the wet tissue liquid medicine, respectively weighing and mixing an oily skin care agent and a surfactant, heating to 55 ℃ for dissolution, and uniformly stirring for 13 minutes; liquid B, namely weighing and mixing the elsholtzia extract, the humectant and the preservative respectively according to the proportion of the wet tissue liquid medicine, heating to 45 ℃ for dissolution, and uniformly stirring for 13 minutes;
s2, preparing wet tissue liquid medicine: according to the proportion of the wet tissue liquid medicine, firstly adding pure water into a stirring kettle, adding the liquid A under the stirring state, and slowly adding the liquid B after the pure water is completely dissolved; respectively adding the water-based skin care agent and the stabilizer under the stirring state until the skin care agent and the stabilizer are completely dissolved to form wet tissue liquid medicine, and regulating the pH value of the prepared wet tissue liquid medicine to be 6.0 by using the acidity regulator;
s3, preparing wet tissues: humidifying the non-woven fabric base material by using the wet tissue liquid medicine prepared in the step S2, controlling the liquid content of the wet tissue to be 4.5 times of the mass of the non-woven fabric base material, and performing quality inspection and packaging to obtain the wet tissue penta containing the elsholtzia haichowensis extract.
Example 15 (comparative example 3): a wet tissue containing liquid medicine comprises:
a wet towel bar containing Elsholtzia splendens extract comprises wet towel bar liquid medicine and non-woven fabric carrying the liquid medicine. The wet tissue liquid medicine is based on the liquid medicine of the embodiment 9, and other auxiliary components are added, and the specific formula comprises the following components in parts by weight per 100: 0.5 percent of elsholtzia seed extract, 2 percent of vitamin E acetate (oily skin care agent), 1 percent of cocoampho sodium acetate (surfactant), 5 percent of glycerin (humectant), 0.01 percent of sodium methyl p-hydroxybenzoate and sodium salt (preservative), 1.5 percent of kiwi fruit extract (aqueous skin care agent), 0.2 percent of EDTA disodium (stabilizer), a proper amount of citric acid or sodium citrate (acidity regulator), the balance of pure water, and the pH value of the wet tissue liquid medicine is 7.0. The preparation process specifically comprises the following steps:
and S1, preparing a solution A and a solution B. Liquid A, namely weighing and mixing the elsholtzia seed extract, the oily skin care agent and the surfactant respectively according to the proportion of the wet tissue liquid medicine, heating to 60 ℃ to dissolve, and uniformly stirring for 10 minutes; b, according to the proportion of the wet tissue liquid medicine, respectively weighing and mixing the humectant and the preservative, heating to 50 ℃ to dissolve, and uniformly stirring for 10 minutes;
s2, preparing wet tissue liquid medicine: according to the proportion of the wet tissue liquid medicine, firstly adding pure water into a stirring kettle, adding the liquid A under the stirring state, and slowly adding the liquid B after the pure water is completely dissolved; respectively adding the water-based skin care agent and the stabilizer under the stirring state until the skin care agent and the stabilizer are completely dissolved to form wet tissue liquid medicine, and regulating the pH value of the prepared wet tissue liquid medicine to be 7.0 by using the acidity regulator;
s3, preparing wet tissues: humidifying the non-woven fabric base material by using the wet tissue liquid medicine prepared in the step S2, controlling the liquid content of the wet tissue to be 4.5 times of the mass of the non-woven fabric base material, and performing quality inspection and packaging to obtain the wet tissue containing the elsholtzia haichowensis extract.
Example 16 (comparative example 4): a wet towel heptyl containing liquid medicine A but not containing oily skin care agent, humectant and stabilizer:
a wet towel G containing Elsholtzia splendens extract comprises wet towel medicinal liquid G and non-woven fabric carrying the medicinal liquid. The wet tissue liquid medicine G is obtained by removing the oily skin care agent, the humectant and the stabilizer on the basis of the wet tissue liquid medicine A in the embodiment 11. The specific formula comprises the following components: 2% of Jiang Xiang Ru extract (0.5% of Jiang Xiang Ru seed extract, 0.5% of Jiang Xiang Ru essential oil and 1% of Jiang Xiang Ru water extract), 1% of cocoyl amphoteric sodium acetate (surfactant), 0.01% of sodium methyl p-hydroxybenzoate and sodium salt (preservative), 1.5% of kiwi fruit extract (aqueous skin-care agent), a proper amount of citric acid (acidity regulator), 0% of oily skin-care agent, 0% of humectant, 0% of stabilizer and the balance of pure water, wherein the pH value of the wet tissue liquid medicine is 6.0. The preparation process specifically comprises the following steps:
and S1, preparing a solution A and a solution B. Liquid A, namely weighing and mixing the elsholtzia extract (the elsholtzia seed extract and the elsholtzia volatile oil), the oily skin care agent and the surfactant respectively according to the proportion of the wet tissue liquid medicine, heating to 55 ℃ for dissolving, and uniformly stirring for 13 minutes; liquid B, namely weighing and mixing the elsholtzia haichowensis water extract, the humectant and the preservative respectively according to the proportion of the wet tissue liquid medicine, heating to 45 ℃ for dissolution, and uniformly stirring for 13 minutes;
s2, preparing wet tissue liquid medicine: according to the proportion of the wet tissue liquid medicine, firstly adding pure water into a stirring kettle, adding the liquid A under the stirring state, and slowly adding the liquid B after the pure water is completely dissolved; respectively adding the water-based skin care agent, the acidity regulator and the stabilizer under the stirring state until the water-based skin care agent, the acidity regulator and the stabilizer are completely dissolved to form wet tissue liquid medicine, and regulating the pH value of the prepared wet tissue liquid medicine to be 6.0 by using the acidity regulator;
s3, preparing wet tissues: humidifying the non-woven fabric base material by using the wet tissue liquid medicine prepared in the step S2, controlling the liquid content of the wet tissue to be 4.5 times of the mass of the non-woven fabric base material, and performing quality inspection and packaging to obtain the wet tissue heptyl containing the elsholtzia haichowensis extract.
Example 17: quality detection and comprehensive evaluation
The wet tissues containing the elsholtzia haichowensis extracts prepared in examples 10-16 were subjected to quality inspection, and in addition, the use experience of 100 random persons of different ages, different professions and different sexes was organized, and the comprehensive evaluation was as follows:
the results in the table above show that: the wet towel A containing Elsholtzia splendens prepared by the process formula and process control of the embodiment 10 has the best comprehensive effect. Examples 10, 12, 13, and 16 have strong natural herbal fragrance due to the essential oil component; examples 10 and 16 contain 0.5% of seed extract, 0.5% of essential oil and 1% of water extract, and the fragrance is a natural herbal compound fragrance, and the three have synergistic bactericidal effects, and the bactericidal effect is the best; however, in example 16, the oily skin care agent, humectant and stabilizer were not added, so that the water-retaining effect was inferior to that of example 10.
Although both examples 12 and 13 contained 0.5% of elsholtzia essential oil, example 12 contained 0.5% of seed extract + 0.5% of essential oil, whereas example 13 contained 0.5% of essential oil and no seed extract, so that example 12 had better water retention effect than example 13.
Although the water extract of elsholtzia splendens contained in examples 11 and 14 were both 1%, the sterilization effect of example 11 was better than that of example 14 because example 14 was only 1% of the water extract, and example 11 was 0.5% of the seed extract + 1% of the water extract.
Although both examples 12 and 15 contained 0.5% of the seed extract, example 12 contained 0.5% of the seed extract plus 0.5% of the essential oil, whereas example 15 contained only 0.5% of the seed extract and no essential oil, and therefore the bactericidal effect of example 12 was better than that of example 15.
Example 18: the antibacterial and water retention effects of the wet tissue obtained by the invention are compared with those of a control wet tissue
Test wet tissue: wet wipes containing elsholtzia haichowensis extracts prepared in examples 10 and 11;
control wet tissue: a perpetual motion's group mind-related sterilizing sanitary wet tissue. In the specification of the performance of the wet tissue, it is disclosed that the wet tissue contains honeysuckle, an extract of centella asiatica and Australian tea Tree oil, and the inhibition rate is claimed to be 99.9%, so that the wet tissue is selected as a control group.
The results of observing the bacteriostatic effect of the wet tissue obtained by the invention and the control wet tissue are shown in the following table.
As shown by the results of observing the bacteriostatic effect of the wet tissue obtained by the invention and the control wet tissue, the bacteriostatic effect of the samples in examples 10 and 11 in the early stage of 2 minutes and 10 minutes is better than that of the control. The sample of example 10 was the most effective.
And (4) observing the water retention effect: the wet towel samples obtained in examples 10 and 11 and the control wet towel sample were selected, spread out and put in a porcelain dish by punching 10 pieces each with a punch, and put in an oven at a temperature set at 37 ℃. The results are shown in the following table.
The wet tissue obtained by the invention and the control wet tissue are subjected to water retention effect observation: it can be seen that the water retention of the samples of examples 10 and 11 is superior to the control. Among them, the sample of example 10 was the most effective in retaining water.
In addition, 100 persons of different ages, professions and sexes were randomly selected for use experience, and it was found that none of examples 10 and 11 and the control had hand irritation, and the lubricating and water-retaining feeling was stronger for example 10 than for example 11 and the control.
The embodiments of the present invention have been described in detail, but the embodiments are merely examples, and the present invention is not limited to the above-described embodiments. Any equivalent modifications and substitutions to those skilled in the art are also within the scope of the present invention. Accordingly, equivalent alterations and modifications are intended to be included within the scope of the invention, without departing from the spirit and scope of the invention.
Claims (9)
1. A liquid medicine with cleaning, sterilizing and moisturizing functions is characterized in that: the liquid medicine comprises 0.5-5.0% of herba elsholtziae extract by mass percent; the elsholtzia splendens extract contains not less than 0.2 percent of elsholtzia splendens seed extract by mass percent.
2. The liquid medicine with cleaning, sterilizing and moisturizing functions as claimed in claim 1, wherein the liquid medicine comprises the following components: the elsholtzia extract also contains elsholtzia essential oil and/or elsholtzia water extract.
3. The liquid medicine with cleaning, sterilizing and moisturizing effects as claimed in claim 1, wherein the extraction method of the seed extract comprises: by using supercritical CO2Extracting the oily component.
4. The liquid medicine with cleaning, sterilizing and moisturizing effects as claimed in claim 3, wherein the supercritical CO is2The extraction process specifically comprises the following steps: cleaning mature seeds, drying, pulverizing, sieving with 30-50 mesh sieve, weighing 1 weight part of seed powder, placing in extraction tank capable of accommodating 4-8 weight parts of seed powder, sealing system, and introducing CO2As an extracting agent, opening after the extraction temperature reaches 54-56 DEG CExtracting at 54-56 deg.C and 49-51 deg.C respectively, controlling pressure of separation I at 6.8-7.2 MPa and pressure of separation II at 4.8-5.2 MPa, and separating I and II to obtain oily components, i.e. Elsholtzia splendens seed extract.
5. The liquid medicine with cleaning, sterilizing and moisturizing functions as claimed in claim 2, wherein the extraction method of the elsholtzia essential oil is as follows: dried whole grass of elsholtzia splendens is soaked in saline water, heated and cooked, circularly distilled, distilled and cooled to obtain oil phase fraction of elsholtzia splendens essential oil.
6. The liquid medicine with cleaning, sterilizing and moisturizing functions as claimed in claim 2, wherein the extraction method of the elsholtzia water extract is as follows: taking kilogram-liter or gram-milliliter as a weight-volume unit, soaking, boiling, concentrating and the like 5 parts by weight of dried whole grass of elsholtzia splendens to finally obtain 1 part by volume of elsholtzia splendens fluid extract.
7. The liquid medicine with cleaning, sterilizing and moisturizing functions as claimed in claim 2, wherein the liquid medicine comprises, by mass: 0.5 percent of Jiangxiang elsholtzia seed extract, 0.5 percent of Jiangxiang elsholtzia essential oil and 1 percent of Jiangxiang elsholtzia water extract.
8. Use of a liquid medicine having cleaning, sterilizing and moisturizing effects according to any one of claims 1 to 7 in the preparation of a hygienic article.
9. The use of a liquid medicine having cleaning, sterilizing and moisturizing effects as claimed in claim 8, wherein the sanitary product is a wet wipe.
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