KR101407051B1 - A producing method for natural antimicrobial using chives - Google Patents

Abstract

A manufacturing method of natural antimicrobial and deodorant using a chive extract according to the present invention comprising a smashing step (S10) of cleaning and smashing chives; a ripening step (S20) of producing a ripening mixture by mixing the smashed chives with ethanol of purity more than or equal to 95% and ripening the mixture at room temperature for 7 to 8days; a concentration step (S30) of producing a chive extract in a juice state by taking only a supernatant fluid of the ripening mixture and mixing the supernatant fluid with purified water and heating and concentrating the mixture with high temperature steam; a mixing step (S40) of producing a chive extract mixed liquid by mixing a gallnut extract, a myrobalan extract, a dendrobium extract, a Chinese pepper extract, and a persimmon extract to improve antibacterial activity in the chive extract; a homogenization step (S50) of producing natural antimicrobial and deodorant by mixing a natural emulsifying agent with a natural hub to maintain the chive extract mixed liquid as a homogenized liquid and remove a chive smell. The present invention is harmless to humans and animals by manufacturing the natural antimicrobial and deodorant using a natural chive extract. Also, the stability is improved without the generation of environmental pollution and a lot of chives which have a short distribution period and are discarded after a harvest time can be utilized. Therefore, the present invention can obtain an economical effect.

Description

Technical Field [0001] The present invention relates to a natural antimicrobial and deodorant using leek extract,

The present invention relates to a natural antibacterial and deodorant and a method of preparing the same, and more particularly, to a natural antibacterial and deodorant having a strong antibacterial effect and a deodorizing effect by using a leek extract and a preparation method thereof.

In general, when sweat, sebum, and contaminants secreted from the human body are ingested by microorganisms or bacteria, inflammation caused by strong skin irritation is induced, and bacteria such as Staphylococcus aureus and Escherichia coli And the bacteria may reproduce in daily necessities such as clothing, bedclothes, and shoes contaminated with the secretions of the human body as described above, which may cause health hazard.

In the case of an office or a house, various microorganisms such as bacteria, fungi, pathogenic fungi, fungus and the like are breeding because of the abundant nutrients to be consumed by the bacteria in the corner where the humidity and temperature conditions are matched and respiratory diseases, itching, It causes allergic diseases such as rash or it causes odor in the room.

On the other hand, organic or inorganic synthetic antibacterial and deodorizing agents for inhibiting the proliferation of microorganisms and removing odor caused by microorganisms have been variously manufactured. A method for producing an antimicrobial agent by synthesizing such a conventional chemical agent is described in detail in Korean Patent Registration No. 10-1180117.

However, the antimicrobial and deodorant synthesized with the above-mentioned conventional chemicals may cause side effects harmful to human body such as rash, itching and the like when they are applied to everyday articles that come into contact with human body such as clothes, bedding, shoes, There is a problem that by-products are discharged and pollute the environment.

The present invention has been made to solve the above problems of the prior art, and it is an object of the present invention to provide a method and apparatus for processing a leek containing a strong antibacterial component to remove various mycelia and causative bacteria of microorganisms while harmless to the human body, The present invention provides a natural antimicrobial and deodorant using a leek extract and a method for producing the same.

In order to accomplish the above object, the present invention provides a method for producing natural antimicrobial and deodorant using leek extract, comprising: a step of washing and crushing leeks; Aging in which the crushed leek is mixed with ethanol having a purity of 95% or more and aged at room temperature for 7 to 8 days to produce a ripening mixture; Adding a supernatant of the above-mentioned aging mixture, mixing with purified water, and concentrating the mixture with hot steam to produce a juicy leek extract; Mixing the extract of Opuntia ficus-indica, Gadja extract, Cryptomeria japonica extract, Acanthopanax senticosus extract and Sensory extract to produce an extract of Leek extract so as to increase the antibacterial activity of the Leek extract; A homogenizing step of mixing a natural emulsifier and a natural herb to produce a natural antibacterial and deodorizing agent so that the mixture of the leek extract is maintained in a homogeneous liquid state and a leek smell is removed.

The aging step is characterized in that a fermentation alcohol is used as ethanol having a purity of 95% or more.

The leek extract mixture contains 95 to 97.5 wt% of the leek extract, 0.5 to 1 wt% of the rhizome extract, 0.5 to 1 wt% of the Rhizome Extract, 0.5 to 1 wt% of the Rhizome Extract, 0.5 to 1 wt% of the Rhizome Extract, 1 Wt%.

The natural antimicrobial deodorant comprises 96 to 98% by weight of the leek extract mixture, 1 to 2% by weight of a natural emulsifier, and 1 to 2% by weight of a natural herbal extract.

The concentration step is characterized in that the mixed solution of the aged mixture and the purified water is heated at 95 to 105 ° C for 115 to 125 minutes.

The mixing step is characterized by producing a leach extract mixture at 65 to 70 ° C.

The homogenization step is characterized in that the natural antimicrobial and deodorant is produced at 55 to 60 < 0 > C.

The natural antimicrobial and deodorant using the leek extract is characterized in that it is prepared according to the above-mentioned preparation method.

As described above, the method for producing natural antibacterial and deodorant using the leek extract according to the present invention has the following effects.

First, by producing the natural antimicrobial and deodorant by using the leek extract containing the natural antimicrobial component, it is harmless to the human body and animals in use,

Second, due to the characteristics of leek, the distribution period is short, so there is an economical effect to utilize a large amount of leek to be discarded after the harvest.

1 is a flowchart showing a method for producing natural antibacterial and deodorant using an extract of Leek according to the present invention.

Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings.

As shown in FIG. 1, the natural antibacterial and deodorant preparation method using the leek extract according to the present invention comprises a crushing step (S10) of washing and crushing leeks; Aging (S20) in which the crushed leek is mixed with ethanol having a purity of 95% or more and aged at room temperature for 7 to 8 days to produce a ripening mixture; (S30) in which only a supernatant of the above-mentioned aging mixture is mixed with purified water, and the mixture is concentrated by heating with hot steam to produce a leek extract of succulent state; A mixing step (S40) of producing a leek extract solution mixture by mixing the rhizome extract, Rhizome extract, Cryptomeria japonica extract, Acanthopanax senticosus extract and Safflower extract to increase the antibacterial activity of the leek extract; And a homogenization step (S50) of mixing the natural emulsifier and the natural herb to produce an antibacterial deodorant so that the leek extract mixture is maintained in a homogeneous liquid state and the leek smell is removed.

On the other hand, the leek used in the present invention belongs to the lily family and its scientific name is Allium tuberosum Roth. It is a perennial plant which grows mainly in the mountains and fields of Korea, Japan and China. The leaves are linear and fleshy, , Leaves contain a strong antimicrobial component, and if you take it to warm your back and knees, it is known to strengthen the colon and small intestine.

The leeks also contain carotene, vitamins B1, B2, and C, which are known as "vitamins." It is also rich in minerals such as potassium and calcium.

Accordingly, the present invention is a method for producing a natural antibacterial and deodorant by extracting an antibacterial component of leek, which will be described below in more detail.

1. Shredding step (S10)

First, the leaf and stem of the leek constituting the natural antimicrobial and deodorant composition of the present invention are washed with water to remove impurities such as dust and foreign matter, and dehydrate.

Next, the leek is crushed using a crusher or a crusher, and crushed to such an extent that the leek juice is produced so that the leek crushed in the aging step (S20) and ethanol are sufficiently mixed.

Alternatively, the leek may be cut to about 1 to 5 cm, and the juice may be separated into a juice and a solid component using a juicer. In the aging step (S20), the solid component and juice may be mixed with ethanol.

2. Aging step (S20)

The aging step (S20) is a step of extracting the antibacterial component contained in the leek using ethanol.

At this time, the crushed leek and the ethanol having a purity of 95% or more are mixed with stirring at a weight ratio of 1: 100 (that is, 100 g of ethanol per 1 g of leek).

On the other hand, it is preferable to use ethanol which is usable for edible use. In this embodiment, a fermentation alcohol is used as ethanol having a purity of 95% or more.

Also, it is preferable that the mixture of the crushed leek and ethanol is stored in a tank made of stainless steel and able to be sealed, aged at room temperature for 7 to 8 days, and the room temperature is maintained at 15 to 25 ° C.

On the other hand, during the aging step (S20), a ripening mixture is produced, and the ripening mixture is separated into a supernatant in a liquid state on the upper part and a leek solid component immersed in the lower part.

3. Concentration step (S30)

In the concentration step (S30), alcohol is removed from the supernatant and concentrated extract of leek is produced in a mash state.

At this time, when the upper supernatant is attached to the aging mixture, it is preferable to use a filter paper or a filter so that the lower leach precipitate can not be mixed.

Next, the supernatant is mixed with purified water at a weight ratio of 1: 100, and heated at 95 to 105 ° C for 115 to 125 minutes in a hot water bath with hot steam.

At this time, the ethanol contained in the supernatant is evaporated and removed, and a certain amount of purified water is evaporated to produce a highly concentrated succulent extract.

4. Mixing step (S40)

In the mixing step (S40), the antimicrobial activity of the leek extract is increased and the natural plant extract containing the natural antimicrobial substance is mixed with the leek extract so as to be applicable to various microorganisms.

At this time, the plant extracts are prepared by using liquid extract of Rhus verniciflua, Ghazu extract, Cryptomeria japonica extract, Acanthopanax senticosus extract and Sensai extract, and they are mixed with stirring at 65 to 70 ° C.

On the other hand, it has been reported that the dwarf has strong antimicrobial and disinfecting action, antioxidative effect and anti-inflammatory action against pathogenic food poisoning bacteria. have

In addition, the herbaceous ginseng has been reported to have antipyretic, analgesic, anti-tumor and antitumor activities. In experiments, it shows the ability to inhibit growth of staphylococcus aureus, candida albicans, , Insecticidal activity was reported, and other antioxidative and anti-inflammatory effects were reported.

On the other hand, the tannin contains a tannin component which gives a tangy flavor. The tannin has a property of making the fiber hard and strong, and is also used as a preservative, a cloth, a nets and a tie dye of a rope. It is sometimes used as a detergent.

The leek extract mixture contains 95 to 97.5 wt% of the leek extract, 0.5 to 1 wt% of the rhizome extract, 0.5 to 1 wt% of the Rhizome Extract, 0.5 to 1 wt% of the Rhizome Extract, 0.5 to 1 wt% of the Rhizome Extract, 1 Wt%.

5. Homogenization step (S50)

In the homogenizing step (S50), a natural emulsifier is mixed to maintain the mixture of the leek extract solution in a homogeneous liquid phase, and a natural herb extract is mixed to remove the characteristic smell of the leek to produce a natural antibacterial and deodorant.

At this time, the natural emulsifier and the natural herbal extract are mixed into the leek extract mixture at 55 to 60 ° C in succession to the mixing step (S40), and it is preferable that the natural emulsifier and the natural herbal extract are thoroughly mixed with stirring until they are cooled to room temperature.

Meanwhile, the natural emulsifier is preferably a solubiliser extracted from pajama oil, and the natural herbal extract is preferably a liquid extract extracted from rosemary, lavender, jasmine and clarith.

At this time, the finally produced antibacterial and deodorant comprises 96 to 98 wt% of the leek extract mixture, 1 to 2 wt% of a natural emulsifier, and 1 to 2 wt% of a natural herb.

Hereinafter, results of the sterilizing power, single dose toxicity test, skin irritation test and deodorization test of natural antibacterial and deodorant using leek extract according to the present invention will be described below.

<Examples>

The production method according to the present invention is characterized in that 94.5% by weight of leek extract, 0.7% by weight of gibbus extract, 0.7% by weight of Gadja extract, 0.5% by weight of bark extract, 0.5% , And herbal extracts of 1.3 wt%.

1. Sterility test of natural antimicrobial and deodorant

The sterilization test was commissioned by the Korean Institute of Construction & Living Environment Test on Dec. 8, 2010 and the results are shown in Table 1 below.

Test strain Number of bacteria per 1 ml unit Initial sample Life history (1 minute,%) Escherichia coli CFU / ml 1.2 × 10 ⁵ Less than 10 (99.9%) Staphylococcus aureus CFU / ml 1.2 × 10 ⁵ Less than 10 (99.9%)

As shown in the above Table 1, 99.9% of bactericidal activity against Escherichia coli and Staphylococcus aureus was obtained from a natural antimicrobial agent using the leek extract.

On June 29, 2010, the Korean Chemical Fusion Research Institute was commissioned to investigate the sterilizing power against Salmonella and Pseudomonas aeruginosa, and the bactericidal power of 99.9% as shown in Table 2 below was obtained.

Test strain Number of bacteria per 1 ml unit Initial sample Life span (15 seconds ± 3 seconds) Salmonella Typhiumrium CFU / ml 9.5 × 10 ⁵ Less than 10 (99.9%) Pseudomonas aeruginosa CFU / ml 9.5 × 10 ⁵ Less than 10 (99.9%)

2. Natural antibacterial and deodorant single dose toxicity test

The single-dose toxicity test was conducted on June 29, 2010 by the Korea Institute of Construction & Living Environment Research, and it was judged that the half-life lethal dose was 2,000 mg / kg or more as shown in Table 3 below.

Test Items Single dose toxicity test (oral) Test result LD ₅₀ (half lethal dose) = 2,000 mg / kg or more Test Methods Korea Food and Drug Administration Notice No. 2009-116 Toxicological Test Standard Remarks See Attachment

3. Natural antibacterial and deodorant skin irritation test

The skin irritation test was conducted on June 15, 2010 by the Korea Testing and Research Institute for Chemical Fusion Research, and was applied to skin of NZW rabbits as shown in [Table 4] none irritant "substance.

Test Items unit Sample classification Results Test Methods Skin irritation test This test substance did not cause erythema, scaling, edema, and the like. The index is "0" and is considered to be a non-irritant substance (none irritant). Korea Food and Drug Administration Notice No. 2009-116

4. Natural anti-bacterial and deodorant deodorant test

The deodorizing ability test was conducted on June 15, 2010 by the Korean Institute of Living Environment Test and the deodorizing power against ammonia, trimethylamine, hydrogen sulfide, methyl mercaptan, toluene, formaldehyde, ethyl benzene and benzene was examined. And ammonia and trimethylamine were obtained as deodorizing effect.

At this time, the deodorizing force test was carried out in 5 L of deodorizing container under a sample volume of 20 mL.

Test Items Time (min) BLANK (ppm) Sample concentration (ppm) Deodorization rate (%) Test Methods

ammonia
Deodorant power Early 50 50 0

KS I
2218: 2008




60 50 19 62 120 48 17 65 240 46 15 67 360 44 13 70

Trimethylamine
Deodorant power Early 50 50 0 60 49 21 57 120 47 19 60 240 46 18 61 360 44 16 64

It will be understood by those skilled in the art that various changes and modifications may be made without departing from the spirit and scope of the invention as defined in the appended claims and their equivalents. And such changes are within the scope of the claims.

Description of the Related Art [0002]
S10: crushing step S20: ripening step
S30: Concentration step S40: Mixing step
S50: homogenization step

Claims (8)

A method for producing natural antibacterial and deodorant using leek extract,
A shredding step (S10) of washing and crushing the leeks;
Aging (S20) in which the crushed leek is mixed with ethanol having a purity of 95% or more and aged at room temperature for 7 to 8 days to produce a ripening mixture;
(S30) in which only a supernatant of the above-mentioned aging mixture is mixed with purified water, and the mixture is concentrated by heating with hot steam to produce a leek extract of succulent state;
A mixing step (S40) of producing a leek extract solution mixture by mixing the rhizome extract, Rhizome extract, Cryptomeria japonica extract, Acanthopanax senticosus extract and Safflower extract to increase the antibacterial activity of the leek extract;
(S50) which comprises mixing a natural emulsifier and a natural herb to produce a natural antibacterial and deodorizing agent so that the leek extract mixture is maintained in a homogeneous liquid state and a leek odor is removed. A method for manufacturing a deodorant. The method according to claim 1,
Wherein the aging step (S20) comprises using a fermentation alcohol as the ethanol having a purity of 95% or more, and using the extract of Leek. The method according to claim 1,
The leek extract mixture contains 95 to 97.5 wt% of the leek extract, 0.5 to 1 wt% of the rhizome extract, 0.5 to 1 wt% of the Rhizome Extract, 0.5 to 1 wt% of the Rhizome Extract, 0.5 to 1 wt% of the Rhizome Extract, 1 Wt%. &Lt; RTI ID = 0.0 &gt; 8. &lt; / RTI &gt; The method according to claim 1,
Wherein the natural antibacterial and deodorant comprises 96 to 98 wt% of the leek extract mixture, 1 to 2 wt% of a natural emulsifier, and 1 to 2 wt% of a natural herb extract. The method according to claim 1,
Wherein the concentration step (S30) comprises heating the mixed solution of the aged mixture and the purified water at 95 to 105 DEG C for 115 to 125 minutes. The method according to claim 1,
Wherein the mixing step (S40) comprises producing an extract of Leek extract at 65 to 70 ° C. The method according to claim 1,
Wherein the homogenizing step (S50) comprises the step of producing the natural antimicrobial and deodorizing agent at 55 to 60 占 폚. A natural antimicrobial and deodorant using an extract of leek, which is produced according to the production method of any one of claims 1 to 7.

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