KR20210143383A - Volatile Anti-Bacterial Pack manufacturing method which has Anti-Bacterial and Sterilization with Deodorizing function - Google Patents

Volatile Anti-Bacterial Pack manufacturing method which has Anti-Bacterial and Sterilization with Deodorizing function Download PDF

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KR20210143383A
KR20210143383A KR1020200060039A KR20200060039A KR20210143383A KR 20210143383 A KR20210143383 A KR 20210143383A KR 1020200060039 A KR1020200060039 A KR 1020200060039A KR 20200060039 A KR20200060039 A KR 20200060039A KR 20210143383 A KR20210143383 A KR 20210143383A
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백현선
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    • AHUMAN NECESSITIES
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/12Powders or granules
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
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    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
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    • AHUMAN NECESSITIES
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    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/015Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone
    • A61L9/04Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air without heating
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    • A61L2209/10Apparatus features
    • A61L2209/13Dispensing or storing means for active compounds
    • A61L2209/135Vaporisers for active components
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
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    • A61L2209/21Use of chemical compounds for treating air or the like

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Abstract

The present invention relates to a method for producing an evaporative antibacterial agent having antibacterial, sterilizing, and deodorizing functions, in which the agent is produced by using a natural deodorant and a natural antibacterial agent made of food additives or food extracts, thereby being safe to the human body and being implemented without causing environmental pollution. In particular, vaporization power of each component is promoted by using octanoic acid components of a coconut oil extract, and thus can be produced to maintain antibacterial and deodorizing power of indoor air for a long time without spraying or application. In particular, the present invention can be packaged in a unit by means of breathable non-woven fabric such that the range of use thereof is expanded and thus, use of the present invention in a place where antibacterial and deodorizing functions are required is conveniently achieved. The method comprises: a grinding and mixing step (S10) of grinding a hardened resin into a size of 50-70 mesh, wherein zeolite and ground resin powder are mixed in a mixing ratio of 70:30 to prevent the ground resin powder from being agglomerated; a mixing and stirring step (S20) of adding pine bark powder and cinnamon powder to the mixture thereof so as to improve sterilization and antibacterial action; a high-speed mixing step (S30) of mixing the mixture thereof with components of a coconut oil extract so as to improve vaporization power of the mixture; and a packaging step (S40) of packaging the mixture thereof in breathable non-woven fabric.

Description

항균 및 살균, 탈취 기능이 있는 기화성 항균팩 제조방법{Volatile Anti-Bacterial Pack manufacturing method which has Anti-Bacterial and Sterilization with Deodorizing function} Volatile Anti-Bacterial Pack manufacturing method which has Anti-Bacterial and Sterilization with Deodorizing function}

본 발명은 항균 및 살균, 탈취 기능이 있는 기화성 항균팩 제조방법에 관한 것으로, 특히 천연 식물류나 식품 추출물들로 구성된 기화력 및 항균, 탈취, 살균 효능 등이 있는 물질을 사용하여 인체에 안전하고, 환경오염을 유발하지 않고 지속적으로 실내 공기 중의 부유 세균, 곰팡이류, 유해 박테리아 및 각종 병원성 세균류를 제거하며, 탈취제를 첨가하여 실내 및 가구, 신발 등의 각종 냄새를 제거할 수 있는 기화성 항균팩 제조방법에 관한 것이다. The present invention relates to a method for manufacturing a vaporizable antibacterial pack having antibacterial, sterilizing, and deodorizing functions, and in particular, it is safe to the human body by using a substance having vaporization power and antibacterial, deodorizing, sterilizing effect, etc. composed of natural plant or food extracts, It is a vaporizable antibacterial pack manufacturing method that continuously removes airborne bacteria, mold, harmful bacteria and various pathogenic bacteria in the indoor air without causing environmental pollution, and removes various odors from indoors, furniture, and shoes by adding a deodorant. it's about

공기 오염도가 증가하고 생활의 질이 높아짐에 따라 가정이나 사무실 등의 실내 공기 오염도는 날이 갈수록 심해짐과 동시에 공기 중의 각종 부유 세균, 곰팡이류, 유해 박테리아 등의 유해성 병원균도 상대적으로 증가하고 있는 현상이다. As the degree of air pollution increases and the quality of life increases, the degree of indoor air pollution in homes and offices is increasing day by day, and at the same time, harmful pathogens such as various airborne bacteria, fungi, and harmful bacteria in the air are also increasing relatively. .

특히 대기 중의 공기 오염도 및 미세먼지 증가로 인해 환기를 자주 시키지 못하는 현 상황에서의 공기 중의 각종 세균이나 박테리아 등의 유해성 병원균 등에 의한 피해는 날이 갈수록 증가하고 있는 현실이다 통계에 의하면 2015년부터 매년 호흡기 질환자는 계속 증가하고 있으며, 올 1분기 최근 5년 간 호흡기 환자 수는 역대 최고치를 갱신하고 있는 상황이다. In particular, in the current situation where ventilation is not frequent due to the increase in air pollution and fine dust in the air, the damage caused by harmful pathogens such as various bacteria and bacteria in the air is increasing day by day. The number of patients with the disease continues to increase, and the number of respiratory patients in the last five years in the first quarter of this year is renewing a record high.

공기 중의 부유 세균, 유해 박테리아, 곰팡이류 등의 병원성 유해균을 제거하기 위해 종래에는 연무 형식의 살균제를 도포하거나, 각종 살균제를 도포하므로 공기 중의 각종 세균류를 제거해왔다. 그러나 이런 류의 도포 방식은 전문성 업체를 통해 대량 살포 위주의 방식이므로 가정이나 사무실 등의 실내 공기 속의 유해 세균류를 없애기에는 사용상의 한계가 있다. 또한 공기 중의 곰팡이류에 의한 피해는 날이 갈수록 증가하고 있다. 가정용품이나 의류, 신발 등의 곰팡이나 습기에 의한 부수적인 피해 역시 증대되고 있는 현실이다. In order to remove pathogenic harmful bacteria, such as airborne bacteria, harmful bacteria, and molds, conventionally, a mist-type disinfectant is applied or various disinfectants are applied, so that various bacteria in the air have been removed. However, this kind of application method is a method of mass-spraying through a professional company, so there is a limit in use to eliminate harmful bacteria in the indoor air such as home or office. In addition, the damage caused by mold in the air is increasing day by day. Incidental damage caused by mold or moisture on household items, clothes, shoes, etc. is also increasing.

종래의 경우 곰팡이 발생을 방지하기 위해 습기제거제로 주로 실리카겔과 같은 흡습제나 광물성 흡습제, 염화칼슘을 이용한 흡습제를 사용하여 왔다. In the conventional case, a desiccant using a desiccant such as silica gel, a mineral desiccant, or calcium chloride has been mainly used as a dehumidifier to prevent mold growth.

실리카겔은 수분 흡수율이 자기 중량의 20~30% 정도 밖에 되지 못하며 또한 산도가 낮으므로 폐기시 토양의 산성화를 가져오게 되어 각종 환경오염을 유발하거나 생태계에 악영향을 미치는 문제점을 가지고 있다. Silica gel has a problem of causing various environmental pollution or adversely affecting the ecosystem because the water absorption rate of silica gel is only about 20-30% of its own weight and also has a low acidity, which causes acidification of the soil when discarded.

이러한 각종 문제점들을 해소하기 위해 인체에 무해하고 친환경적이고 사용하기 간편한 실내공기용 항균 및 살균, 탈취 기능이 있는 기화성 항균팩을 개발하였다. To solve these various problems, we developed a vaporizable antibacterial pack that is harmless to the human body, eco-friendly and easy to use, with antibacterial, sterilizing and deodorizing functions for indoor air.

기화성 항균팩의 선행기술로는, 대한민국 공개특허등록번호 1014070510000 “부추추출물을 이용한 천연 항균 및 탈취제와 그 제조 방법(등록일자: 2014.06.05)”과, 대한민국 공개특허등록번호 1019912610000 “항균, 살균 및 탈취성이 향상된 항균 탈취제(등록일자: 2019.06.14)”가 개시되어 있다. As prior art of vaporizable antibacterial pack, Republic of Korea Patent Registration No. 1014070510000 “Natural antibacterial and deodorant using leek extract and its manufacturing method (registration date: Jun. 5, 2014)” and Republic of Korea Patent Registration No. 1019912610000 “Antibacterial, sterilizing and An antibacterial deodorant with improved deodorization (registration date: 2019.06.14)” is disclosed.

상기 종래의 선행 기술은 수지 및 액상 제품으로 주로 도포에 의해 사용하므로 살균 사용 대상물에 한계가 있고, 또한 수지류에 의한 방법은 사용상의 제약이 많은 방법이다. The prior art is a resin and a liquid product, mainly used by application, so there is a limit to the object for sterilization, and the method using the resin is a method with many restrictions on use.

특히 액상 제품의 경우 분사 시 추출물에 의한 의복 변색 및 색상 변화를 일으킬 요소가 많으므로 사용시 주의해야 한다. In particular, in the case of liquid products, there are many factors that can cause discoloration and color change of clothes by the extract when spraying, so be careful when using it.

또한 수지에 의한 방법은 기화력이 미비하기 때문에 접촉 부위에 대한 항균 작용은 있지만, 공기 중의 항균력은 기대하기 힘든 제품이 다수를 차지하고 있다. In addition, since the method using the resin has insufficient vaporization power, there are many products that have antibacterial action on the contact site, but whose antibacterial power in the air is difficult to expect.

대한민국 공개특허등록번호 1014070510000호 “부추추출물을 이용한 천연 항균 및 탈취제와 그 제조 방법”(등록일자: 2014.06.05)Republic of Korea Patent Registration No. 1014070510000 “Natural antibacterial and deodorant using leek extract and manufacturing method thereof” (Registration date: 2014.06.05) 대한민국 공개특허등록번호 1019912610000 “항균, 살균 및 탈취성이 향상된 항균 탈취제”(등록일자: 2019.06.14)Republic of Korea Patent Registration No. 1019912610000 “Antibacterial, antibacterial and deodorizing agent with improved antibacterial, sterilizing and deodorizing properties” (Registration date: 2019.06.14)

본 발명의 목적은 실내 공기 중의 부유 세균류, 곰팡이, 유해성 박테리아 등의 유해성 병원균을 효과적으로 제거하고 탈취력을 첨가하여 각종 공기 중의 냄새를 제거하기 위해 소나무 껍질, 송진, 제올라이트, 계피가루 및 코코넛 오일 추출물 성분 등의 천연 물질을 사용하여 도포나 연무 등의 번거로운 작업 없이 성분들의 기화력을 증대시켜 지속적인 항균, 살균 및 탈취 작용을 장시간 유지시킬 수 있는 안전하고, 환경 오염을 유발하지 않는 탈취 기능 및 항균, 살균 작용이 있는 기화성 항균팩 제조 방법이다. An object of the present invention is to effectively remove harmful pathogens such as airborne bacteria, mold, and harmful bacteria in the indoor air and to remove various odors in the air by adding deodorizing power, such as pine bark, rosin, zeolite, cinnamon powder and coconut oil extract ingredients. Safe and non-polluting deodorizing function and antibacterial and sterilizing action that can maintain continuous antibacterial, sterilizing and deodorizing action for a long time by increasing the vaporization power of ingredients without cumbersome work such as application or misting by using natural materials of This is a vaporizable antibacterial pack manufacturing method.

상기의 목적을 달성하기 위하여 본 발명의 기화성 항균팩 제조 방법은, 굳어진 상태의 송진을 50~70mesh 크기로 분쇄하되, 분쇄된 송진가루가 뭉쳐지지 않도록 제올라이트와 분쇄된 송진가루를 70:30의 중량 비율로 혼합하는 분쇄 및 혼합 단계(S10), 상기 혼합물에 소나무 껍질 가루와 계피가루를 첨가하여 살균 및 항균 작용을 향상시키는 혼합 교반 단계(S20), 상기 혼합물에 코코넛 오일 추출물을 혼합시켜 혼합물의 기화력을 향상시키는 고속 혼합 단계(S30), 상기 혼합물을 통기성 부직포에 포장하는 포장 단계(S40)로 구성되어 있다. In order to achieve the above object, the vaporizable antibacterial pack manufacturing method of the present invention grinds the rosin in the hardened state to a size of 50 to 70 mesh, and mixes the zeolite and the pulverized rosin powder with a weight of 70:30 so that the pulverized rosin powder does not agglomerate. Grinding and mixing step of mixing in a ratio (S10), mixing and stirring step of adding pine bark powder and cinnamon powder to the mixture to improve sterilization and antibacterial action (S20), and mixing coconut oil extract with the mixture It consists of a high-speed mixing step (S30) to improve thermal power, and a packaging step (S40) of packaging the mixture in a breathable nonwoven fabric.

또한, 상기 흡습제는 소나무 껍질 가루 1000 중량부에 대해서 상기 송진을 200 중량부 내지 300 중량부이고, 상기 제올라이트는 400 중량부내지 600 중량부이고 상기 계피가루는 50 중량부 내지 100 중량부이고, 상기 코코넛 오일 추출물은 20 중량부 내지 40 중량부인 것을 특징으로 한다. In addition, the moisture absorbent is 200 parts by weight to 300 parts by weight of the rosin with respect to 1000 parts by weight of pine bark powder, the zeolite is 400 parts by weight to 600 parts by weight, and the cinnamon powder is 50 parts by weight to 100 parts by weight, Coconut oil extract is characterized in that 20 to 40 parts by weight.

또한, 상기 기화성 항균제의 공기 밀도(Vapor Density)는 2 이상인 것을 특징으로 한다. In addition, the air density (Vapor Density) of the vaporizable antibacterial agent is characterized in that 2 or more.

본 발명의 항균 및 탈취 기능이 있는 기화성 항균제 제조 방법은 식품 첨가물이나 식품 추출물들로 이루어진 천연 탈취제, 천연 항균제 등을 사용하여 인체에 안전하고, 환경 오염을 유발하지 않고, 특히 각각의 성분들의 기화력을 코코넛 오일 추출물의 옥탄산 성분을 이용하여 촉진시켜 분무나 도포 없이 장기간 실내 공기의 항균 및 탈취력을 유지할 수 있게 제조하였으며, 특히 통기성 부직포를 사용하여 단위 포장이 가능하게 하였으므로 항균 및 탈취 기능이 필요한 곳에 사용이 편리하게끔 사용 범위를 확대시킨 특징이 있다. The method for producing a vaporizable antibacterial agent having an antibacterial and deodorizing function of the present invention uses a natural deodorant made of food additives or food extracts, a natural antibacterial agent, etc. was manufactured to maintain the antibacterial and deodorizing power of the indoor air for a long time without spraying or application by promoting it using the octanoic acid component of coconut oil extract. It has the feature of expanding the range of use for convenient use.

도1은 본 발명의 탈취 및 항균 기능이 있는 흡습제 제조 방법의 공정 순서도이다. 1 is a process flow chart of a method for manufacturing a desiccant having a deodorizing and antibacterial function of the present invention.

첨부된 도면을 참조하여 본 발명의 항균 및 탈취 기능이 있는 기화성 항균팩 제조 방법을 상세히 설명하고자 한다. With reference to the accompanying drawings, the method of manufacturing a vaporizable antibacterial pack having an antibacterial and deodorizing function of the present invention will be described in detail.

도1에 도시된 바와 같이 본 발명의 기화성 항균팩 제조 방법은 굳어진 상태의 송진을 50~70mesh 크기로 분쇄하되, 분쇄된 송진 가루가 뭉쳐지지 않도록 제올라이트와 분쇄된 송진 가루를 70:30 비율로 혼합하는 분쇄 및 혼합 단계(S10), 상기 혼합물에 소나무 껍질 가루와 계피 가루를 첨가하여 살균 및 항균 작용을 향상시키는 혼합 교반 단계(S20), 상기 혼합물에 코코넛 오일 추출물 중 옥탄산을 혼합시켜 혼합물의 기화력을 향상시키는 고속 혼합 단계(S30), 상기 혼합물을 통기성 부직포에 포장하는 포장 단계(S40)로 구성되어 있다. As shown in Figure 1, the vaporizable antibacterial pack manufacturing method of the present invention pulverizes the solidified rosin to a size of 50 to 70 mesh, but mixes the zeolite and the pulverized rosin powder in a 70:30 ratio so that the pulverized rosin powder does not agglomerate. pulverizing and mixing step (S10), mixing and stirring step (S20) of adding pine bark powder and cinnamon powder to the mixture to improve sterilization and antibacterial action (S20), mixing the octanoic acid in the coconut oil extract with the mixture to form the mixture It consists of a high-speed mixing step (S30) to improve thermal power, and a packaging step (S40) of packaging the mixture in a breathable nonwoven fabric.

또한, 상기 흡습제는 소나무 껍질 가루 1000 중량부에 대해서 상기 송진을 200 중량부 내지 300 중량부이고, 상기 제올라이트는 400 중량부 내지 600 중량부이고, 상기 계피 가루는 50 중량부 내지 100 중량부이고, 상기 코코넛 오일 추출물 중 옥탄산은 20 중량부 내지 40 중량부로 구성된다. In addition, the moisture absorbent is 200 parts by weight to 300 parts by weight of the rosin with respect to 1000 parts by weight of pine bark powder, the zeolite is 400 parts by weight to 600 parts by weight, the cinnamon powder is 50 parts by weight to 100 parts by weight, Octanoic acid in the coconut oil extract is composed of 20 to 40 parts by weight.

또한, 상기 기화성 항균제의 공기 밀도(Vapor Density)는 2 이상을 갖도록 혼합한다. In addition, the air density (Vapor Density) of the vaporizable antibacterial agent is mixed to have 2 or more.

상기의 구성에 따른 본 발명인 기화성 방청 흡습제 제조 방법의 동작은 다음과 같다. The operation of the vaporizable rust preventive desiccant manufacturing method according to the present invention according to the above configuration is as follows.

분쇄 및 혼합 단계(S10)는 살균 및 항균 작용이 있는 송진을 분쇄하여 탈취 및 흡습제로 알려진 제올라이트를 송진과 제올라이트를 70:30 중량 비율로 혼합한다. In the grinding and mixing step (S10), rosin having a sterilizing and antibacterial action is pulverized and a zeolite known as a deodorizing and moisture absorbent is mixed with rosin and zeolite in a weight ratio of 70:30.

이때, 제올라이트 양을 적게 혼합하면 분쇄된 송진 가루가 딱딱하게 굳는 겔화 현상이 발생하여 팩 작업 시 불량률이 높다. 제올라이트의 양을 많이 하면 비경제적이다. At this time, if a small amount of zeolite is mixed, the pulverized rosin powder hardens and gelation occurs, resulting in a high defect rate during pack operation. If the amount of zeolite is large, it is uneconomical.

따라서, 본 발명은 혼합 분쇄 단계(S10)에서 제올라이트와 송진을 70:30 비율로 선택하여 사용한다. Therefore, in the present invention, in the mixing and grinding step (S10), zeolite and rosin are selected and used in a ratio of 70:30.

혼합 교반 단계(S20)는 혼합 분쇄 단계(S10)에서 제조된 혼합물에 소나무 껍질 가루, 계피 가루를 넣고 혼합기를 이용하여 실온에서 750rpm/min.으로 혼합하여 항균력을 증대시킨 혼합물을 제조한다. In the mixing and stirring step (S20), pine bark powder and cinnamon powder are added to the mixture prepared in the mixing and grinding step (S10) and mixed at room temperature at 750 rpm/min. using a mixer to prepare a mixture with increased antibacterial activity.

이때 소나무 껍질 1000 중량부에 계피 가루를 50에서 100 중량부를 혼합한다. At this time, 50 to 100 parts by weight of cinnamon powder is mixed with 1000 parts by weight of pine bark.

계피 가루 양이 많으면 너무 진한 계피향으로 자극적일 수 있다. 송진과의 조화로운 향을 유지하려면 계피가루를 50에서 100 중량부를 사용하는 것이 적절하다. If the amount of cinnamon powder is too much, it can be irritating with too strong cinnamon flavor. It is appropriate to use 50 to 100 parts by weight of cinnamon powder to maintain a harmonious flavor with rosin.

고속 혼합 단계(S30)는 상기 (S20)의 혼합물에 코코넛 오일 추출물인 옥탄산을 고속 혼합기에 넣고 실온에서 분당 2,500rpm/min.으로, 고속 혼합 교반시켜 본 발명의 특징인 기화력을 향상시킨 탈취 및 항균 기능이 있는 흡습제를 제조한다. In the high-speed mixing step (S30), octanoic acid, a coconut oil extract, is added to the mixture of (S20) in a high-speed mixer at room temperature at 2,500 rpm/min. and a desiccant having an antibacterial function.

이때, 옥탄산은 제올라이트 1000 중량부에 20에서 40 중량부를 사용하는 것이 적정하다. In this case, it is appropriate to use 20 to 40 parts by weight of octanoic acid in 1000 parts by weight of zeolite.

옥탄산을 많이 사용하면 액상상인 옥탄산이 부직포에 배어 나올 가능성이 있고 냄새 또한 강해 자극적일 수 있다. If you use a lot of octanoic acid, liquid octanoic acid is likely to seep into the nonwoven fabric, and the smell is also strong, which can be irritating.

전체적으로 소나무 껍질 가루 1000 중량부에 대해서 상기 송진을 200 중량부 내지 300 중량부이고, 상기 제올라이트는 400 중량부 내지 600 중량부이고, 상기 계피 가루는 50 중량부 내지 100 중량부이고, 상기 코코넛 오일 추출물 중 옥탄산은 20 중량부 내지 40 중량부로 혼합하는 것이 적정하다. In total, 200 to 300 parts by weight of the rosin with respect to 1000 parts by weight of the pine bark powder, the zeolite is 400 to 600 parts by weight, the cinnamon powder is 50 to 100 parts by weight, and the coconut oil extract It is appropriate to mix 20 to 40 parts by weight of heavy octanoic acid.

특히, 제올라이트는 흡습 기능 및 탈취 기능에 기여하고 송진 및 소나무 껍질 가루, 계피 가루는 항균 및 살균 기능에 기여하고 옥탄산은 살균 및 혼합물의 기화력 증진에 기여한다. 혼합물의 탈취력, 항균력, 살균력을 측정하기 위해 다음과 같이 각각의 샘플들을 제조하였다. In particular, zeolite contributes to moisture absorption and deodorization functions, rosin, pine bark powder, and cinnamon powder contribute to antibacterial and sterilization functions, and octanoic acid contributes to sterilization and enhancement of vaporization power of the mixture. In order to measure the deodorizing power, antibacterial power, and sterilization power of the mixture, each sample was prepared as follows.

샘플1 sample 1

소나무 껍질 1000 중량부에 송진 50 중량부, 제올라이트 200 중량부, 계피 가루 30 중량부를 사용하여 샘플 혼합물을 제조한다. A sample mixture was prepared using 50 parts by weight of pine resin, 200 parts by weight of zeolite, and 30 parts by weight of cinnamon powder in 1000 parts by weight of pine bark.

샘플2 sample 2

소나무 껍질 1000 중량부에 송진 100 중량부, 제올라이트 300 중량부, 계피 가루 50 중량부, 옥탄산 20 중량부를 사용하여 샘플 혼합물을 제조한다. 100 parts by weight of pine resin, 300 parts by weight of zeolite, 50 parts by weight of cinnamon powder, and 20 parts by weight of octanoic acid were used in 1000 parts by weight of pine bark to prepare a sample mixture.

샘플3 sample 3

소나무 껍질 1000 중량부에 송진 150 중량부, 제올라이트 300 중량부, 계피 가루 50 중량부, 옥탄산 30 중량부를 사용하여 샘플 혼합물을 제조한다. A sample mixture was prepared by using 150 parts by weight of rosin, 300 parts by weight of zeolite, 50 parts by weight of cinnamon powder, and 30 parts by weight of octanoic acid in 1000 parts by weight of pine bark.

샘플4 sample 4

소나무 껍질 1000 중량부에 송진 200 중량부, 제올라이트 400 중량부, 계피 가루 50 중량부, 옥탄산 50 중량부를 사용하여 샘플 혼합물을 제조한다. A sample mixture was prepared using 200 parts by weight of pine resin, 400 parts by weight of zeolite, 50 parts by weight of cinnamon powder, and 50 parts by weight of octanoic acid in 1000 parts by weight of pine bark.

샘플5 sample 5

소나무 껍질 1000 중량부에 송진 300 중량부, 제올라이트 600 중량부, 계피 가루 100 중량부, 옥탄산 100 중량부를 사용하여 샘플 혼합물을 제조한다. A sample mixture was prepared by using 300 parts by weight of pine resin, 600 parts by weight of zeolite, 100 parts by weight of cinnamon powder, and 100 parts by weight of octanoic acid in 1000 parts by weight of pine bark.

[표1]은 1000ml Jar에 Methane Gas 5cc를 넣고 루사이트에 상기 샘플1 내지 샘플5 각각에 대해서 10g을 부직포로 포장한 후 열봉합하여 밀봉된 각각의 부직포를 넣고 3시간 후 탈취력을 측정한 것이다(측정기: ShinYei사 Model: OMX-SRM). [Table 1] puts 5cc of Methane Gas in 1000ml jar, 10g of each of the samples 1 to 5 was packaged in a leucite with a non-woven fabric, and then each non-woven fabric sealed by heat sealing was put in, and the deodorization power was measured after 3 hours. (Measuring instrument: ShinYei Model: OMX-SRM).

샘플Sample 1One 22 33 44 55 탈취력deodorizing power 1.831.83 0.360.36 0.370.37 0.360.36 0.340.34

샘플1을 제외한 모든 샘플들의 탈취력이 90% 이상인 것을 확인하였다. It was confirmed that the deodorization power of all samples except for Sample 1 was 90% or more.

샘플1을 제외한 샘플들의 탈취력이 상대적으로 좋은 것을 확인하였다. It was confirmed that the deodorizing power of the samples except for Sample 1 was relatively good.

[표2]는 항균력을 테스트한 결과이다. 신발 속에 각 20g샘플 팩을 넣고 3시간 후의 항균력을 측정하였다(측정기: ATP 측정기 Kikkoman사). [Table 2] shows the results of testing the antibacterial activity. Each 20g sample pack was put in the shoe, and the antibacterial activity was measured after 3 hours (measurement device: ATP measuring device Kikkoman).

샘플팩sample pack 적용전before application 적용후after application 샘플1sample 1 20882088 9292 샘플2sample 2 21192119 1616 샘플3sample 3 23382338 1212 샘플4sample 4 24692469 88 샘플5sample 5 23122312 77

상기 [표2]의 결과 샘플팩 모두 95% 이상의 항균력을 갖춘 것을 확인할 수 있다. As a result of [Table 2], it can be confirmed that all of the sample packs have an antibacterial activity of 95% or more.

[표]은 공기 중의 부유 세균을 측정한 결과이다. [Table] shows the results of measuring airborne bacteria in the air.

0.5CBM 공간에 각각의 샘플팩 20g을 넣고 6시간 후 RCS AIR SAMPLER(Filter: Agar Part No.941100)를 이용하여 공기 중의 부유 세균을 측정하였다(측정단위: CFU/CBM). After putting 20 g of each sample pack in the 0.5 CBM space, the airborne bacteria were measured using RCS AIR SAMPLER (Filter: Agar Part No. 941100) after 6 hours (measurement unit: CFU/CBM).

샘플팩sample pack 적용전before application 적용후after application 샘플1sample 1 8989 2222 샘플2sample 2 104104 1414 샘플3sample 3 9898 1010 샘플4sample 4 100100 1212 샘플5sample 5 8888 55

샘플 실험 결과 공기 중의 부유 세균이 현저히 감소되는 것을 확인하였다. As a result of the sample experiment, it was confirmed that airborne bacteria in the air were significantly reduced.

[표4]는 KS K 0693:2016에 의한 항균성 test 결과이다. 사용한 균은 폐렴균(Klebsiella pneumoniae(ATCC 4352))이다. [Table 4] is the result of the antimicrobial test according to KS K 0693:2016. The bacteria used was Klebsiella pneumoniae (ATCC 4352).

샘플팩sample pack 정균 감소율(%)Bacterial reduction rate (%) 샘플1sample 1 99.499.4 샘플2sample 2 99.999.9 샘플3sample 3 99.999.9 샘플4sample 4 99.999.9 샘플5sample 5 99.999.9

실험 결과, 샘플1을 제외한 샘플 모두가 99.9% 이상의 항균력이 있음을 확인하였다. As a result of the experiment, it was confirmed that all samples except for Sample 1 had an antibacterial activity of 99.9% or more.

[표5]는 암모니아와 초산의 소취성 실험을 JTETC 방법에 의해 실시하였다. 실험 방법은 5L 테트라백에 샘플시료 팩(2g)을 넣고 초기 농도를 조절한 가스 3L를 주입 후 2시간 후 가스 농도를 검지관(암모니아: 3La, 초산: 81)으로 측정한다. [Table 5] shows the deodorization test of ammonia and acetic acid by the JTETC method. The experimental method is to put a sample sample pack (2g) in a 5L tetrabag, inject 3L of gas whose initial concentration is adjusted, and then measure the gas concentration with a detection tube (ammonia: 3La, acetic acid: 81) 2 hours later.

샘플팩sample pack 감소율(%)Decrease rate (%) 암모니아ammonia 초산acetic acid 샘플1sample 1 83.283.2 89.289.2 샘플2sample 2 99.999.9 99.999.9 샘플3sample 3 99.999.9 99.999.9 샘플4sample 4 99.999.9 99.999.9 샘플5sample 5 99.999.9 99.999.9

샘플 측정 결과 샘플1을 제외하고 모두 99.9%의 결과를 확인하였다. As a result of sample measurement, 99.9% of all results were confirmed except for Sample 1.

Claims (4)

소나무 껍질, 계피 가루, 송진, 제올라이트, C8~C12의 카르복실산 중 코코넛 오일 추출물 성분인 옥탄산을 이용하여 기화력을 증진시키고 항균, 탈취성, 살균력이 있는 기화성 항균팩 제조 방법.
A method of manufacturing a vaporizable antibacterial pack that uses pine bark, cinnamon powder, rosin, zeolite, and octanoic acid, which is a component of coconut oil extract among C8~C12 carboxylic acids, and has antibacterial, deodorizing and sterilizing properties.
제1항에 있어서, 상기 분쇄 및 혼합 단계(S10)에서 제올라이트와 송진을 70:30 중량 비율로 혼합하는 것을 특징으로 하는 항균, 탈취성, 살균력이 있는 기화성 항균팩 제조 방법.
The method of claim 1, wherein in the grinding and mixing step (S10), zeolite and rosin are mixed in a weight ratio of 70:30.
제1항에 있어서 소나무 껍질 가루 1000 중량부에 대해서 상기 송진을 200 중량부 내지 300 중량부이고, 상기 제올라이트는 400 중량부 내지 600 중량부이고, 상기 계피 가루는 50 중량부 내지 100 중량부이고, 상기 코코넛 오일 추출물 중 옥탄산은 20 중량부 내지 40 중량부로 구성하는 것을 특징으로 한 기화성 항균팩 제조 방법.
According to claim 1, 200 parts by weight to 300 parts by weight of the rosin with respect to 1000 parts by weight of the pine bark powder, the zeolite is 400 parts by weight to 600 parts by weight, the cinnamon powder is 50 parts by weight to 100 parts by weight, The vaporizable antibacterial pack manufacturing method, characterized in that the octanoic acid in the coconut oil extract is comprised of 20 to 40 parts by weight.
제1항에서 기화성 항균제의 공기 밀도(Vapor Density)는 2 이상을 갖도록 제조하는 것을 특징으로 한 기화성 항균팩 제조 방법.

The method of claim 1, wherein the vaporizable antibacterial pack has an air density of 2 or more.

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101407051B1 (en) 2013-01-14 2014-06-12 양주시 A producing method for natural antimicrobial using chives
KR101991261B1 (en) 2019-02-20 2019-06-20 주식회사 베네거 Antibacterial, sterilization and deodorant improved antimicrobial deodorant

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101407051B1 (en) 2013-01-14 2014-06-12 양주시 A producing method for natural antimicrobial using chives
KR101991261B1 (en) 2019-02-20 2019-06-20 주식회사 베네거 Antibacterial, sterilization and deodorant improved antimicrobial deodorant

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