CN109512741A - A kind of essential oil is washed one's hands condensation and preparation method thereof - Google Patents
A kind of essential oil is washed one's hands condensation and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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Abstract
It washes one's hands condensation and preparation method thereof the invention discloses a kind of essential oil.Essential oil condensation of washing one's hands is grouped as by each group of following parts by weight: 0.005~0.025 part of bacteria inhibiting composition, 0.003~0.015 part of oil of plant, 60~70 parts of solvent, 7.5~37.5 parts of surfactant, 5.001~15.03 parts of emulsifier, 0.1~0.5 part of moisturizer, 0.25~1.55 part of preservative, 0.1~0.5 part of lauroyl arginine ethyl ester hydrochloride, 0.1~1.0 part of essence, 0.5~1.5 part of pH adjusting agent；The bacteria inhibiting composition is made of Saponaria officinalis extract, Fructus Citri grandis extract, tea tree ethereal oil, grapefruit essential oil and Bergamot.Essential oil obtained by the present invention is washed one's hands condensation, good antimicrobial effect, and cleaning dirt-removing power is strong, non-stimulated to skin, easy to foaming, Yi Chongxi when use, salubrious comfortable after washing, and is had a good application prospect.
Description
Technical field
The present invention relates to daily chemical products technical fields, and in particular, to a kind of essential oil is washed one's hands condensation and preparation method thereof.
Background technique
In recent years, as people's living standard increasingly improves and the reinforcement of health consciousness, people increasingly pay attention to hand
Health problem.It washes one's hands and is related to our health, washing one's hands is thing that everyone will do daily, and frequently washing one's hands is to maintain
The good habit of people's health even more prevents the important intervening measure of transmission.According to health and epidemic prevention department's introduction, blood-shoot-eye illness, skin
Skin disease, hepatitis A, bacillary dysentery etc. are typically all to be infected by the contact of hand.The infections sources such as bacterium and virus are one
A little public places and using being easiest to propagate in frequent article, these places be all infectious disease cross-infection high-incidencely.If
People will contact these things daily, and think little of the health of hand, then the probability being infected will be very high.Cause
This, simple decontamination is also not only satisfied in requirement of the people for wash product, it is also desirable to can reach certain antibacterial anti-
Bacterium effect.
Existing wash product on the market is many kinds of, such as soap, perfumed soap, hand cleanser, condensation of washing one's hands, disposable hand cleanser
Deng.Wherein, condensation is washed one's hands due to environment friendly and pollution-free, mild non-stimulated, easy to use, convenient, the easily stored, foam of carrying
The advantages that enriching and washing rear skin lubrication sense, is liked by people, is widely used in family and public place.
The condensation of washing one's hands of commercial type is although various, but many products are more or less added to some be harmful to the human body
Substance: such as bleaching powder, mercury, detergent, corrosive agent, long-time service have corrosiveness to the skin of people.Accordingly it is desirable to
The condensation of washing one's hands that fungistatic effect is more preferable and does not hurt hands can be developed.The extract (essential oil, medicinal extract, powder etc.) of plant contains natural bacteriostatic
Substance, it is mild and harmless, therefore feasible a kind of selection that condensation of washing one's hands is row is prepared using the extract of plant.
To sum up, a cleaning effect of now urgent need research is good, good antimicrobial effect, has no toxic side effect, mild inirritative condensation of washing one's hands, and reduces
The generation of health event.
Summary of the invention
The purpose of the invention is to overcome the above-mentioned deficiency of the prior art, a kind of essential oil is provided and is washed one's hands condensation, by excellent
The ratio of choosing compounding various plants component and auxiliary material, has reached significant synergy, can be effectively antibacterial and do not stimulate mildly.
It washes one's hands the preparation method of condensation another object of the present invention is to provide above-mentioned essential oil.
To achieve the goals above, the present invention is achieved by following scheme:
A kind of essential oil is washed one's hands condensation, is grouped as by each group of following parts by weight: 0.005~0.025 part of bacteria inhibiting composition,
0.003~0.015 part of oil of plant, 60~70 parts of solvent, 7.5~37.5 parts of surfactant, emulsifier 5.001~15.03
Part, 0.1~0.5 part of moisturizer, 0.25~1.55 part of preservative, 0.1~0.5 part of lauroyl arginine ethyl ester hydrochloride, essence
0.1~1.0 part, 0.5~1.5 part of pH adjusting agent；The bacteria inhibiting composition is by Saponaria officinalis extract, Fructus Citri grandis extract, tea tree essence
Oil, grapefruit essential oil and Bergamot composition.
Saponaria officinalis is pinkwort.Saponaretin rich in Saponaria officinalis extract.Wherein, saponaretin contains
Many ribosome inactivating proteins (RIPs), RIPs have special N- glycosidase activity, can selectively acting in eukaryocyte core
Sugared body and the exposed rRNA of prokaryotic cell make its depurination, thus the effect of inhibiting protein to synthesize, reaching antibacterial.It is used for
In the present invention, fungistatic effect can be improved.
Fructus Citri grandis extract is primarily present in the fruit of Citrus paradisi Macfadyen, and functional components shaddock is contained in Fructus Citri grandis extract
Skin glycosides, aurantiin have antibacterial anti-inflammatory, antiviral, the anti-mutation of anticancer, antiallergy, antiulcer, analgesia, hypotensive activity, can drop
Low cholesterol, the formation for reducing thrombus improve local microcirculation and nutrition supply, can be used for producing prevention and treatment cardiovascular and cerebrovascular disease.
Tea tree ethereal oil, grapefruit essential oil and Bergamot are plants essential oil, and plants essential oil is that extraction plant is distinctive
Aromatic substance is taken from herbal flower, leaf, root, bark, fruit, seed, resin etc. to distill, extract in a manner of squeezing
Come.Since essential oil-fumigation volatility is high, and molecule is small, it is easy to and it is absorbed by the body, and people's intracorporeal organ can be permeated rapidly, it will
Extra ingredient excretes, and whole process only needs a few minutes, and the fragrance of plant itself, also directly stimulates pituitary gland
Secretion, ferment and hormone secretion etc., function in balanced body play the role of beauty and skin care.Contain alcohols, aldehyde in plants essential oil
Class, acids, phenols, acetones, terpenoid substance have the function of to purify air, bactericidal, provide cytotrophy etc..
Essential oil provided by the present invention washes one's hands condensation using Saponaria officinalis extract, Fructus Citri grandis extract, tea tree ethereal oil, grape fruit
The natural plant active components such as essential oil and Bergamot, all have bacteriostasis antibiosis effect, excellent by each plant component compatible use
The proportion dosage between each component is selected, can be effectively antibacterial, such as to common Escherichia coli, staphylococcus aureus, Candida albicans
Equal pathogens have obvious inhibiting effect；And it is multiple with other auxiliary materials (surfactant, moisturizer, emulsifier, preservative etc.)
Match, is not added with any chemical component, does not stimulate mildly.
Preferably, essential oil condensation of washing one's hands is grouped as by each group of following parts by weight: bacteria inhibiting composition 0.005~
0.015 part, 0.003~0.009 part of oil of plant, 63~66 parts of solvent, 16~27 parts of surfactant, emulsifier 7.01~
It is 13.03 parts, 0.2~0.4 part of moisturizer, 0.4~0.8 part of preservative, 0.2~0.4 part of lauroyl arginine ethyl ester hydrochloride, fragrant
0.5~0.8 part, 0.7~1.2 part of pH adjusting agent of essence.
It is highly preferred that the essential oil is washed one's hands, condensation is grouped as by each group of following parts by weight: bacteria inhibiting composition 0.005
Part, 0.003 part of oil of plant, 64 parts of solvent, 19.9 parts of surfactant, 8.515 parts of emulsifier, 0.3 part of moisturizer, preservative
0.63 part, 0.25 part of lauroyl arginine ethyl ester hydrochloride, 0.7 part of essence, 0.9 part of pH adjusting agent.
Preferably, Saponaria officinalis extract in the bacteria inhibiting composition, Fructus Citri grandis extract, tea tree ethereal oil, grapefruit essential oil and
The weight ratio of Bergamot is (1~5): (1~5): (1~5): (1~5): (1~5).
It is highly preferred that Saponaria officinalis extract, Fructus Citri grandis extract, tea tree ethereal oil, grapefruit essential oil in the bacteria inhibiting composition
Weight ratio with Bergamot is 1:1:1:1:1.
Preferably, the oil of plant is camellia seed oil, peony seed oil and oil and fat of sacha inchi；The solvent is water；The table
Face activating agent is laureth sodium sulfovinate, sodium lauroyl sarcosine, lauroyl glutamate TEA salt and cocamidopropyl propyl amide sweet tea
Dish alkali；The emulsifier be cocoyl-glucoside tartrate sodium and PPG-26 butylol polyether -26/PEG-40 rilanit special/
Water；The moisturizer is Sensiva SC50；The solvent is water；The preservative is DMDMH and potassium sorbate；The pH tune
Section agent is citric acid.
Specific embodiment as one preferred, the essential oil wash one's hands condensation by following parts by weight each group be grouped
At: 0.001~0.005 part of Saponaria officinalis extract, 0.001~0.005 part of Fructus Citri grandis extract, tea tree ethereal oil 0.001~0.005
Part, 0.001~0.005 part of grapefruit essential oil, 0.001~0.005 part of Bergamot, 0.001~0.005 part of camellia seed oil,
0.001~0.005 part of peony seed oil, 0.001~0.005 part of oil and fat of sacha inchi, 60~70 parts of water, laureth sodium sulfovinate 5
~15 parts, 0.5~2.5 part of sodium lauroyl sarcosine, 1~10 part of lauroyl glutamate TEA salt, Cocoamidopropyl betaine 1
~10 parts, cocoyl -5~15 parts of glucoside tartrate sodium, PPG-26 butylol polyether -26/PEG-40 hydrogenated castor oil/water
0.001~0.03 part, 0.1~0.5 part of Sensiva SC50,0.05~0.25 part of DMDMH, 0.1~0.8 part of potassium sorbate, the moon
0.1~0.5 part of osmanthus acyl arginine ethyl ester hydrochloride, 0.1~1.0 part of essence, 0.5~1.5 part of citric acid.
Preferably, essential oil condensation of washing one's hands is grouped as by each group of following parts by weight: Saponaria officinalis extract 0.001~
0.003 part, 0.001~0.003 part of Fructus Citri grandis extract, 0.001~0.003 part of tea tree ethereal oil, grapefruit essential oil 0.001~
0.003 part, 0.001~0.003 part of Bergamot, 0.001~0.003 part of camellia seed oil, peony seed oil 0.001~0.003
Part, 0.001~0.003 part of oil and fat of sacha inchi, 63~66 parts of water, 8~12 parts of laureth sodium sulfovinate, sodium lauroyl sarcosine
1.0~2.0 parts, 3~7 parts of lauroyl glutamate TEA salt, 4~6 parts of Cocoamidopropyl betaine, cocoyl-glucoside winestone
7~13 parts of acid esters sodium, 0.01~0.02 part of oil/water of PPG-26 butylol polyether -26/PEG-40 hydrogenated castor, Sensiva SC50
0.2~0.4 part, 0.1~0.2 part of DMDMH, 0.3~0.6 part of potassium sorbate, lauroyl arginine ethyl ester hydrochloride 0.2~0.4
Part, 0.5~0.8 part of essence, 0.7~1.2 part of citric acid.
It is highly preferred that the essential oil is washed one's hands, condensation is grouped as by each group of following parts by weight: Saponaria officinalis extract 0.001
Part, 0.001 part of Fructus Citri grandis extract, 0.001 part of tea tree ethereal oil, 0.001 part of grapefruit essential oil, 0.001 part of Bergamot, camellia
0.001 part of seed oil, 0.001 part of peony seed oil, 0.001 part of oil and fat of sacha inchi, 64 parts of water, 9 parts of laureth sodium sulfovinate, laurel
1.4 parts of acylsarcosine sodium, 4 parts of lauroyl glutamate TEA salt, 5.5 parts of Cocoamidopropyl betaine, cocoyl-glucoside wine
8.5 parts of stone acid esters sodium, 0.015 part of oil/water of PPG-26 butylol polyether -26/PEG-40 hydrogenated castor, 0.3 part of Sensiva SC50,
0.13 part of DMDMH, 0.5 part of potassium sorbate, 0.25 part of lauroyl arginine ethyl ester hydrochloride, 0.7 part of essence, citric acid 0.9
Part.
Further, above-mentioned essential oil is washed one's hands the preparation method of condensation, is included the following steps:
S1. by deionized water, laureth sodium sulfovinate, sodium lauroyl sarcosine and lauroyl arginine ethyl ester hydrochloric acid
Salt mixes in proportion, and 10~15min is stirred under the conditions of 50~55 DEG C to being completely dissolved, obtains mixture A；
S2. object A to be mixed is cooled to 40~45 DEG C, and cocoyl-glucoside winestone is successively added into mixture A in proportion
Acid esters sodium, Cocoamidopropyl betaine, lauroyl glutamate TEA salt and Sensiva SC50 stir 10~15min, obtain mixed
Close object B；
S3. first by camellia seed oil, peony seed oil, oil and fat of sacha inchi, PPG-26 butylol polyether -26/PEG-40 rilanit special/
Water mixes in proportion, and obtains mixture C；Mixture C is added in mixture B again, 10~15min of stirring is saturating to Material clarification
It is bright, obtain mixture D；
S4. Saponaria officinalis extract, Fructus Citri grandis extract, DMDMH, potassium sorbate, tea is successively added into mixture D in proportion
Essential oil, grapefruit essential oil, Bergamot and essence are set, is stirred evenly；Citric acid is slowly repeatedly added again, is after mixing evenly
Essential oil is washed one's hands condensation.
Preferably, whipping temp described in step S1 is 50 DEG C, mixing time 10min.
Preferably, after object A to be mixed is cooled to 40 DEG C in step S2, then cocounut oil successively is added into mixture A in proportion
Base-glucoside tartrate sodium, Cocoamidopropyl betaine, lauroyl glutamate TEA salt and Sensiva SC50, stirring
10min obtains mixture B.
Preferably, mixing time is 10min in step S3.
Compared with prior art, the invention has the following advantages:
1, bacteria inhibiting composition provided by the present invention by preferably compounding a variety of natural plant extracts according to a certain percentage
(Saponaria officinalis extract, Fructus Citri grandis extract, tea tree ethereal oil, grapefruit essential oil and Bergamot) has reached significant collaboration and has increased
Imitate effect, have stronger bacteriostasis, to the pathogens such as common Escherichia coli, staphylococcus aureus, Candida albicans have compared with
Apparent inhibiting effect, can effectively inhibit disease fungus or bacterium common in human skin or environment, effective guarantee people
Hygiene and health.
2, the present invention by bacteria inhibiting composition and other auxiliary materials, (surfactant, moisturizer, emulsifier, prevent by such as oil of plant
Rotten agent, pH adjusting agent etc.) it is preferred by a certain percentage compound made of essential oil wash one's hands condensation, cleaning dirt-removing power is strong, to skin without
Stimulation, easy to foaming, Yi Chongxi when use is salubrious comfortable after washing, while can also reach bacteriostasis antibiosis effect.
3, essential oil provided by the invention washes one's hands condensation using natural plant composition, effectively prevents the erosion of chemical component
And harm, bring that convenient, safely effectively bactericidal effect, used raw material are easy to get, preparation side for personal cleanliness's nursing
Method is easy, environmentally protective, is suitble to large-scale production, practical value with higher and good application prospect.
Specific embodiment
The present invention is made combined with specific embodiments below and further being elaborated, the embodiment is served only for explaining this
Invention, is not intended to limit the scope of the present invention.Test method as used in the following examples is normal unless otherwise specified
Rule method；Used material, reagent etc., unless otherwise specified, for the reagent and material commercially obtained.
The camellia seed oil is camellia (CAMELLIA JAPONICA) seed oil；
The peony seed oil is tree peony (PAEONIA SUFFRUTICOSA) seed oil；
The oil and fat of sacha inchi is print plus fruit (PLUKENETIA VOLUBILIS) seed oil；
The Saponaria officinalis extract is Saponaria officinalis (SAPONARIA OFFICINALIS) extract；
The Fructus Citri grandis extract is shaddock (CITRUS GRANDIS) berry extract；
The tea tree ethereal oil is Melaleuca alternifolia (MELALEUCA ALTERNIFOLIA) leaf oil；
The grapefruit essential oil is grape fruit (CITRUS PARADISI) peel oil；
The Bergamot is bergamot (CITRUS AURANTIUM BERGAMIA) fruit oil.
A kind of essential oil of embodiment 1 is washed one's hands condensation and preparation method thereof
(1) it is formulated
A kind of essential oil is washed one's hands condensation, is grouped as by each group of following parts by weight: 0.001 part of Saponaria officinalis extract, shaddock fruit
0.001 part of extract, 0.001 part of tea tree ethereal oil, 0.001 part of grapefruit essential oil, 0.001 part of Bergamot, camellia seed oil
0.001 part, 0.001 part of peony seed oil, 0.001 part of oil and fat of sacha inchi, 64 parts of water, 9 parts of laureth sodium sulfovinate, lauroyl flesh
1.4 parts of propylhomoserin sodium, 4 parts of lauroyl glutamate TEA salt, 5.5 parts of Cocoamidopropyl betaine, cocoyl-glucoside tartaric acid
8.5 parts of ester sodium, 0.015 part of oil/water of PPG-26 butylol polyether -26/PEG-40 hydrogenated castor, 0.3 part of Sensiva SC50,
0.13 part of DMDMH, 0.5 part of potassium sorbate, 0.25 part of lauroyl arginine ethyl ester hydrochloride, 0.7 part of essence, citric acid 0.9
Part.
(2) preparation method
S1. by deionized water, laureth sodium sulfovinate, sodium lauroyl sarcosine and lauroyl arginine ethyl ester press than
Example is uniformly mixed, and 10min is stirred under the conditions of 50 DEG C to being completely dissolved, obtains mixture A；
S2. object A to be mixed is cooled to 40 DEG C, and cocoyl-glucoside tartrate is successively added into mixture A in proportion
Sodium, Cocoamidopropyl betaine, lauroyl glutamate TEA salt and Sensiva SC50 stir 10min, obtain mixture B；
S3. first by camellia seed oil, peony seed oil, oil and fat of sacha inchi, PPG-26 butylol polyether -26/PEG-40 rilanit special/
Water mixes in proportion, and obtains mixture C；Mixture C is added in mixture B again, stirring 10min to Material clear,
Obtain mixture D；
S4. Saponaria officinalis extract, Fructus Citri grandis extract, DMDMH, potassium sorbate, tea is successively added into mixture D in proportion
Essential oil, grapefruit essential oil, Bergamot and essence are set, is stirred evenly；Citric acid is slowly repeatedly added again, is after mixing evenly
Essential oil is washed one's hands condensation.
A kind of essential oil of embodiment 2 is washed one's hands condensation and preparation method thereof
(1) it is formulated
A kind of essential oil is washed one's hands condensation, is grouped as by each group of following parts by weight: 0.025 part of Saponaria officinalis extract, shaddock fruit
0.025 part of extract, 0.025 part of tea tree ethereal oil, 0.025 part of grapefruit essential oil, 0.025 part of Bergamot, camellia seed oil
0.025 part, 0.025 part of peony seed oil, 0.025 part of oil and fat of sacha inchi, 60 parts of water, 5 parts of laureth sodium sulfovinate, lauroyl flesh
0.5 part of propylhomoserin sodium, 1 part of lauroyl glutamate TEA salt, 1 part of Cocoamidopropyl betaine, cocoyl-glucoside tartrate
5 parts of sodium, 0.001 part of oil/water of PPG-26 butylol polyether -26/PEG-40 hydrogenated castor, 0.1 part of Sensiva SC50, DMDMH
0.05 part, 0.1 part of potassium sorbate, 0.1 part of lauroyl arginine ethyl ester hydrochloride, 0.1 part of essence, 0.5 part of citric acid.
(2) preparation method
S1. by deionized water, laureth sodium sulfovinate, sodium lauroyl sarcosine and lauroyl arginine ethyl ester press than
Example is uniformly mixed, and 10min is stirred under the conditions of 50 DEG C to being completely dissolved, obtains mixture A；
S2. object A to be mixed is cooled to 40 DEG C, and cocoyl-glucoside tartrate is successively added into mixture A in proportion
Sodium, Cocoamidopropyl betaine, lauroyl glutamate TEA salt and Sensiva SC50 stir 10min, obtain mixture B；
S3. first by camellia seed oil, peony seed oil, oil and fat of sacha inchi, PPG-26 butylol polyether -26/PEG-40 rilanit special/
Water mixes in proportion, and obtains mixture C；Mixture C is added in mixture B again, stirring 10min to Material clear,
Obtain mixture D；
S4. Saponaria officinalis extract, Fructus Citri grandis extract, DMDMH, potassium sorbate, tea is successively added into mixture D in proportion
Essential oil, grapefruit essential oil, Bergamot and essence are set, is stirred evenly；Citric acid is slowly repeatedly added again, is after mixing evenly
Essential oil is washed one's hands condensation.
A kind of essential oil of embodiment 3 is washed one's hands condensation and preparation method thereof
(1) it is formulated
A kind of essential oil is washed one's hands condensation, is grouped as by each group of following parts by weight: 0.005 part of Saponaria officinalis extract, shaddock fruit
0.005 part of extract, 0.005 part of tea tree ethereal oil, 0.005 part of grapefruit essential oil, 0.005 part of Bergamot, camellia seed oil
0.005 part, 0.005 part of peony seed oil, 0.005 part of oil and fat of sacha inchi, 70 parts of water, 15 parts of laureth sodium sulfovinate, lauroyl
2.5 parts of sodium sarcosinate, 10 parts of lauroyl glutamate TEA salt, 10 parts of Cocoamidopropyl betaine, cocoyl-glucoside winestone
15 parts of acid esters sodium, 0.03 part of oil/water of PPG-26 butylol polyether -26/PEG-40 hydrogenated castor, 0.5 part of Sensiva SC50,
0.25 part of DMDMH, 0.8 part of potassium sorbate, 0.5 part of lauroyl arginine ethyl ester hydrochloride, 1.0 parts of essence, 1.5 parts of citric acid.
(2) preparation method
S1. by deionized water, laureth sodium sulfovinate, sodium lauroyl sarcosine and lauroyl arginine ethyl ester press than
Example is uniformly mixed, and 10min is stirred under the conditions of 50 DEG C to being completely dissolved, obtains mixture A；
S2. object A to be mixed is cooled to 40 DEG C, and cocoyl-glucoside tartrate is successively added into mixture A in proportion
Sodium, Cocoamidopropyl betaine, lauroyl glutamate TEA salt and Sensiva SC50 stir 10min, obtain mixture B；
S3. first by camellia seed oil, peony seed oil, oil and fat of sacha inchi, PPG-26 butylol polyether -26/PEG-40 rilanit special/
Water mixes in proportion, and obtains mixture C；Mixture C is added in mixture B again, stirring 10min to Material clear,
Obtain mixture D；
S4. Saponaria officinalis extract, Fructus Citri grandis extract, DMDMH, potassium sorbate, tea is successively added into mixture D in proportion
Essential oil, grapefruit essential oil, Bergamot and essence are set, is stirred evenly；Citric acid is slowly repeatedly added again, is after mixing evenly
Essential oil is washed one's hands condensation.
A kind of essential oil of embodiment 4 is washed one's hands condensation and preparation method thereof
(1) it is formulated
A kind of essential oil is washed one's hands condensation, is grouped as by each group of following parts by weight: 0.002 part of Saponaria officinalis extract, shaddock fruit
0.002 part of extract, 0.003 part of tea tree ethereal oil, 0.003 part of grapefruit essential oil, 0.003 part of Bergamot, camellia seed oil
0.001 part, 0.001 part of peony seed oil, 0.001 part of oil and fat of sacha inchi, 65.83 parts of water, 10 parts of laureth sodium sulfovinate, laurel
1.6 parts of acylsarcosine sodium, 5 parts of lauroyl glutamate TEA salt, 5 parts of Cocoamidopropyl betaine, cocoyl-glucoside winestone
10 parts of acid esters sodium, 0.016 part of oil/water of PPG-26 butylol polyether -26/PEG-40 hydrogenated castor, 0.35 part of Sensiva SC50,
0.15 part of DMDMH, 0.4 part of potassium sorbate, 0.3 part of lauroyl arginine ethyl ester hydrochloride, 0.6 part of essence, citric acid 0.75
Part.
(2) preparation method
S1. by deionized water, laureth sodium sulfovinate, sodium lauroyl sarcosine and lauroyl arginine ethyl ester press than
Example is uniformly mixed, and 10min is stirred under the conditions of 50 DEG C to being completely dissolved, obtains mixture A；
S2. object A to be mixed is cooled to 40 DEG C, and cocoyl-glucoside tartrate is successively added into mixture A in proportion
Sodium, Cocoamidopropyl betaine, lauroyl glutamate TEA salt and Sensiva SC50 stir 10min, obtain mixture B；
S3. first by camellia seed oil, peony seed oil, oil and fat of sacha inchi, PPG-26 butylol polyether -26/PEG-40 rilanit special/
Water mixes in proportion, and obtains mixture C；Mixture C is added in mixture B again, stirring 10min to Material clear,
Obtain mixture D；
S4. Saponaria officinalis extract, Fructus Citri grandis extract, DMDMH, potassium sorbate, tea is successively added into mixture D in proportion
Essential oil, grapefruit essential oil, Bergamot and essence are set, is stirred evenly；Citric acid is slowly repeatedly added again, is after mixing evenly
Essential oil is washed one's hands condensation.
A kind of essential oil of embodiment 5 is washed one's hands condensation and preparation method thereof
(1) it is formulated
A kind of essential oil is washed one's hands condensation, is grouped as by each group of following parts by weight: 0.003 part of Saponaria officinalis extract, shaddock fruit
0.003 part of extract, 0.004 part of tea tree ethereal oil, 0.004 part of grapefruit essential oil, 0.004 part of Bergamot, camellia seed oil
0.001 part, 0.001 part of peony seed oil, 0.001 part of oil and fat of sacha inchi, 65.83 parts of water, 10 parts of laureth sodium sulfovinate, laurel
1.6 parts of acylsarcosine sodium, 5 parts of lauroyl glutamate TEA salt, 5 parts of Cocoamidopropyl betaine, cocoyl-glucoside winestone
10 parts of acid esters sodium, 0.016 part of oil/water of PPG-26 butylol polyether -26/PEG-40 hydrogenated castor, 0.35 part of Sensiva SC50,
0.15 part of DMDMH, 0.4 part of potassium sorbate, 0.3 part of lauroyl arginine ethyl ester hydrochloride, 0.6 part of essence, citric acid 0.75
Part.
(2) preparation method
S1. by deionized water, laureth sodium sulfovinate, sodium lauroyl sarcosine and lauroyl arginine ethyl ester press than
Example is uniformly mixed, and 10min is stirred under the conditions of 50 DEG C to being completely dissolved, obtains mixture A；
S2. object A to be mixed is cooled to 40 DEG C, and cocoyl-glucoside tartrate is successively added into mixture A in proportion
Sodium, Cocoamidopropyl betaine, lauroyl glutamate TEA salt and Sensiva SC50 stir 10min, obtain mixture B；
S3. first by camellia seed oil, peony seed oil, oil and fat of sacha inchi, PPG-26 butylol polyether -26/PEG-40 rilanit special/
Water mixes in proportion, and obtains mixture C；Mixture C is added in mixture B again, stirring 10min to Material clear,
Obtain mixture D；
S4. Saponaria officinalis extract, Fructus Citri grandis extract, DMDMH, potassium sorbate, tea is successively added into mixture D in proportion
Essential oil, grapefruit essential oil, Bergamot and essence are set, is stirred evenly；Citric acid is slowly repeatedly added again, is after mixing evenly
Essential oil is washed one's hands condensation.
1~5 one kind of comparative example is washed one's hands condensation
Comparative example 1 is in addition to, without containing Saponaria officinalis extract, remaining component is same as Example 1 in condensation formula of washing one's hands；
Comparative example 2 is in addition to, without containing Fructus Citri grandis extract, remaining component is same as Example 1 in condensation formula of washing one's hands；
Comparative example 3 is in addition to, without containing tea tree ethereal oil, remaining component is same as Example 1 in condensation formula of washing one's hands；
Comparative example 4 is in addition to, without containing grapefruit essential oil, remaining component is same as Example 1 in condensation formula of washing one's hands；
Comparative example 5 is in addition to, without containing Bergamot, remaining component is same as Example 1 in condensation formula of washing one's hands.
Comparative example 1~5 wash one's hands condensation preparation method it is same as Example 1.
1 quality evaluation of application examples
Referring to " cosmetics safety technical specification " version in 2015, sense organ, steady is carried out to Examples 1 to 5 essential oil condensation of washing one's hands
Qualitative, physicochemical property and microbiological indicator measurement, measurement result are as follows.
1, sense organ
Appearance: Examples 1 to 5 essential oil is washed one's hands, and condensation is not stratified, and transparent, no suspended substance or precipitating are miscellaneous without obvious machinery
Matter is met the requirements of the standard.
Smell: Examples 1 to 5 essential oil is washed one's hands the equal free from extraneous odour of condensation, and regulation odor type is met.
2, stability
Cold-resistant situation: placing for 24 hours in -5 DEG C ± 2 DEG C of refrigerator, observe when taking out recovery to room temperature, Examples 1 to 5 essence
Oil washes one's hands condensation without precipitating and without metachromatism, haze-free, meets the requirements of the standard.
Heat-resisting situation: placing for 24 hours in 40 DEG C ± 1 DEG C of refrigerator, observe when taking out recovery to room temperature, Examples 1 to 5 essence
Oil wash one's hands the equal free from extraneous odour of condensation, without layering and without metachromatism, it is haze-free, meet the requirements of the standard.
3, physicochemical property and microbiological indicator measurement
Examples 1 to 5 essential oil wash one's hands condensation physicochemical property and microbiological indicator measurement result it is as shown in table 1.
1 Examples 1 to 5 essential oil of table is washed one's hands the physicochemical property and microbioassay result of condensation
More than 2 intact skin irritant tests of application examples
Referring to " disinfection technology standard " 2002 editions, multiple intact skin stimulation is carried out to Examples 1 to 5 essential oil condensation of washing one's hands
Test.
1, operating procedure
(1) before the test for 24 hours, the hair of rabbit or guinea pig back backbone two sides is removed with depilatory agent or scissors, must not be damaged
Hurt skin.Unhairing range, left and right each about 3cm × 3cm.
(2) tested material (concentration be generally skin degerming application liquid 5 times or stoste 0.5mL (g)) is coated in side by next day
On skin, the other side applies solvent as control, and the 4h after smearing is cleaned with water or non-stimulated suitable solvent, removes residue.
It smears once daily, continuously smears 14d.Observation for 24 hours by table 2 as a result, score after each smear.For the ease of the painting of tested material
It smears and is observed with result, answer cropping when necessary.The same trial zone of the processing method of check plot.
2, evaluation regulation
Daily every animal average integral (stimulus index) is calculated according to the following formula, and skin irritatin intensity is determined with table 3.
Examples 1 to 5 essential oil is washed one's hands, and the results are shown in Table 4 to rabbit skin irritation test for condensation.
The standards of grading of 2 skin wound repair of table
Oedema is formed:
3 skin irritatin strength grading of table
4 Examples 1 to 5 essential oil of table washes one's hands condensation to rabbit skin irritation test result
As seen from the results in Table 4, Examples 1 to 5 essential oil wash one's hands condensation to the scoring of rabbit skin wound repair for 0, belong to stingless
Swash rank, it is mild to skin, it is highly-safe.
3 bacteriostatic test of application examples
Referring to " sterile products Hygienic safety evaluation technical requirements " WS 628-2018 and disinfection technology standard (2002 years
Version), condensation is washed one's hands to Examples 1 to 5 essential oil and the condensation of washing one's hands of comparative example 1~5 carries out extracorporeal bacteria inhibitor test.
1, material and bacteria suspension preparation
(1) test strain
Staphylococcus aureus (ATCC6538), Escherichia coli (8099 or ATCC 11229), Candida albicans
(ATCC10231)。
(2) preparation of bacteria suspension
Strain tube is opened in a manner of sterile working, and adequate nutrition broth bouillon, soft pressure-vaccum number is added with capillary syring
It is secondary, so that strain is melted dispersion.The test tube containing 5.0mL~10.0mL nutrient broth medium is taken, a little bacteria suspension is instilled, sets 37 DEG C
Culture 18h~for 24 hours.The bacteria suspension of 1st generation culture is taken with oese, streak inoculation sets 37 on nutrient agar plate
DEG C culture 18h~for 24 hours.Or be inoculated on plate from a bacterium pearl is taken out in microbank, 37 DEG C of culture 18h~for 24 hours are set, are chosen
Colonies typical in above-mentioned 2nd generation culture is taken, nutrient agar slopes are inoculated in, sets 37 DEG C of culture 18h~for 24 hours, the as the 3rd is commissioned to train
Support object.Repeat several generations.The fresh slant culture for taking the nutrient agar culture 18h in the 3rd~6 generation~for 24 hours, uses 5.0mL
Suction pipe is drawn 3.0mL~5.0mL dilution (generally using TPS, acidifying water physiological saline) and is added in slant tube, blows repeatedly
It inhales, washes lower lawn.Then, washing lotion is moved in another sterile test tube with 5.0mL suction pipe, with electronic vortex mixer mixing 20s, or
Rapping 80 times on palm, so that bacterial suspension is uniform.Bacteria suspension made of preliminary, first with the bigness scale of bacterial concentration nephelometry its
Containing bacteria concentration, then with diluted to required concentration.
2, bacteriostatic test
(1) preparation of bacteria inhibition tablet
Experimental group: taking sterile and dry filter paper, and every Examples 1 to 5 essential oil is added dropwise respectively and washes one's hands about 5 μ L of condensation,
Then filter paper is lain against in clean sterilized petri dishes, uncaps to set in constant incubator (37 DEG C) and dries, or set at room temperature certainly
It is so spare after drying.
Control group: taking sterile and dry filter paper, and every comparative example 1~5 is added dropwise respectively and washes one's hands about 5 μ L of condensation, then
Filter paper is lain against in clean sterilized petri dishes, uncaps to set in constant incubator (37 DEG C) and dry, or is set naturally dry at room temperature
It is spare after dry.
Negative control group: sterile and dry filter paper, every about 5 μ L of dropwise addition sterile distilled water, then by filter paper are taken
Lie against in clean sterilized petri dishes, uncap to set in constant incubator (37 DEG C) and dry, or set at room temperature spontaneously dry after it is spare.
(2) inoculation of test organisms
Dipping concentration with sterile cotton swab is 5 × 105Cfu/mL~5 × 106Cfu/mL tests bacteria suspension, in nutrient agar
It uniformly smears 3 times on culture medium flat plate surface.Every to smear 1 time, plate should rotate 60 °, finally smear cotton swab around plate edge
One week.Plate is covered, drying at room temperature 5min is set.
(3) bacteriostatic agent print is placed with
Test is placed with 1 microbiological contamination plate every time, and each plate is placed with 4 test prints, 1 negative control print, and totally 5
Piece.It is placed with aseptic nipper coupongs in planar surface.At a distance of 25mm or more between each print center, apart with the periphery of plate
15mm or more.After being placed with, with the light pressure-like piece of aseptic nipper, it is made to be tightly attached to planar surface.Plate is covered, 37 DEG C of constant temperature trainings are set
Case is supported, culture 16h~18h observes result.With the diameter (including patch) of vernier caliper measurement antibacterial ring size and record.Test repeats
3 times, record and calculate average value.
3, evaluation regulation
(1) bacteriostasis judges
Inhibition zone diameter is greater than 7mm person, has been judged to bacteriostasis；Inhibition zone diameter is less than or equal to 7mm person, is judged to no suppression
Bacterium effect.
(2) 3 repetition tests (totally 12 prints), which reach, bacteriostasis result person, is judged to qualification.
(3) negative control group should be generated without antibacterial ring size, and otherwise test is invalid.
4, result
From bacteriostatic test result (table 5 and table 6) as can be seen that 1~5 essential oil of the embodiment of the present invention washes one's hands condensation to golden yellow
Staphylococcus, Escherichia coli and Candida albicans have certain inhibiting effect, and wherein example 1 group is washed one's hands condensation fungistatic effect
It is best；Although comparative example 1~5 is washed one's hands, condensation has inhibiting effect to 3 kinds of bacterium, and effect is not so good as Examples 1 to 5；Negative control group
To 3 kinds of bacteriums without fungistatic effect.
5 Examples 1 to 5 essential oil of table washes one's hands condensation to the bacteriostatic diameter (mm) of different bacterium
6 comparative example 1~5 of table washes one's hands condensation and negative control group to the bacteriostatic diameter (mm) of different bacterium
The evaluation of 4 using effect of application examples
30 testers are equally divided into 5 groups, give test group sample at random by " double blind " test, it is desirable that tester
It washes one's hands (i.e. hand cleanser dosage, Handwashing ways, flushing period is without limitation) by itself daily habit of washing one's hands, successively evaluates hand cleanser
Foaming characteristic, dirt-removing power, irritation when washing one's hands rinse difficulty and salubrious sense of washing one's hands.Tester carries out according to the feeling of oneself
Scoring, standards of grading using 5 points of systems, wherein foaming characteristic, dirt-removing power, wash after salubrious sense it is worst with 1 point, 5 points preferably calculate；Thorn
It is best with 1 point to swash property, flushing difficulty, 5 points of worst calculating record the sensory effects scoring of each embodiment finally with mean values,
It see the table below shown in 7.
Table 7 is washed one's hands the using effect evaluation (unit: point) of condensation hand-washing effect
| Foaming characteristic | Dirt-removing power | Irritation | Rinse difficulty | Salubrious sense after washing | |
| Embodiment 1 | 4.6 | 4.0 | 1.0 | 1.0 | 3.8 |
| Embodiment 2 | 4.5 | 3.9 | 1.1 | 1.2 | 3.9 |
| Embodiment 3 | 4.3 | 3.8 | 1.2 | 1.1 | 3.6 |
| Embodiment 4 | 4.7 | 4.1 | 0.9 | 1.0 | 3.8 |
| Embodiment 5 | 4.6 | 4.2 | 1.0 | 1.3 | 4.0 |
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention
The limitation of shield range can also be made on the basis of above description and thinking for those of ordinary skill in the art
Other various forms of variations or variation, there is no necessity and possibility to exhaust all the enbodiments.It is all of the invention
Made any modifications, equivalent replacements, and improvements etc., should be included in the protection of the claims in the present invention within spirit and principle
Within the scope of.
Claims (10)
- A kind of condensation 1. essential oil is washed one's hands, which is characterized in that be grouped as by each group of following parts by weight: bacteria inhibiting composition 0.005 ~0.025 part, 0.003~0.015 part of oil of plant, 60~70 parts of solvent, 7.5~37.5 parts of surfactant, emulsifier 5.001~15.03 parts, 0.1~0.5 part of moisturizer, 0.25~1.55 part of preservative, lauroyl arginine ethyl ester hydrochloride 0.1 ~0.5 part, 0.1~1.0 part of essence, 0.5~1.5 part of pH adjusting agent；The bacteria inhibiting composition is mentioned by Saponaria officinalis extract, shaddock fruit Take object, tea tree ethereal oil, grapefruit essential oil and Bergamot composition.
- 2. essential oil is washed one's hands condensation according to claim 1, which is characterized in that the essential oil washes one's hands condensation by following parts by weight Each group be grouped as: 0.005~0.015 part of bacteria inhibiting composition, 0.003~0.009 part of oil of plant, 63~66 parts of solvent, table 16~27 parts of face activating agent, 7.01~13.03 parts of emulsifier, 0.2~0.4 part of moisturizer, 0.4~0.8 part of preservative, lauroyl 0.2~0.4 part of arginine ethyl ester hydrochloride, 0.5~0.8 part of essence, 0.7~1.2 part of pH adjusting agent.
- 3. essential oil is washed one's hands condensation according to claim 1, which is characterized in that the essential oil washes one's hands condensation by following parts by weight Each group be grouped as: 0.005 part of bacteria inhibiting composition, 0.003 part of oil of plant, 64 parts of solvent, 19.9 parts of surfactant, emulsification 8.515 parts of agent, 0.3 part of moisturizer, 0.63 part of preservative, 0.25 part of lauroyl arginine ethyl ester hydrochloride, 0.7 part of essence, pH 0.9 part of regulator.
- 4. essential oil is washed one's hands condensation according to claim 1, which is characterized in that Saponaria officinalis extract in the bacteria inhibiting composition, Fructus Citri grandis extract, tea tree ethereal oil, grapefruit essential oil and Bergamot weight ratio be (1~5): (1~5): (1~5): (1~ 5): (1~5).
- 5. essential oil is washed one's hands condensation according to claim 4, which is characterized in that Saponaria officinalis extract in the bacteria inhibiting composition, Fructus Citri grandis extract, tea tree ethereal oil, grapefruit essential oil and Bergamot weight ratio be 1:1:1:1:1.
- 6. essential oil is washed one's hands condensation according to claim 1, which is characterized in that the oil of plant is camellia seed oil, peony seeds Oil and oil and fat of sacha inchi；The solvent is water；The surfactant be laureth sodium sulfovinate, sodium lauroyl sarcosine, Lauroyl glutamate TEA salt and Cocoamidopropyl betaine；The emulsifier be cocoyl-glucoside tartrate sodium and PPG-26 butylol polyether -26/PEG-40 hydrogenated castor oil/water；The moisturizer is Sensiva SC50；The solvent is water； The preservative is DMDMH and potassium sorbate；The pH adjusting agent is citric acid.
- 7. essential oil is washed one's hands condensation according to claim 1, which is characterized in that the essential oil washes one's hands condensation by following parts by weight Each group be grouped as: 0.001~0.005 part of Saponaria officinalis extract, 0.001~0.005 part of Fructus Citri grandis extract, tea tree ethereal oil 0.001~0.005 part, 0.001~0.005 part of grapefruit essential oil, 0.001~0.005 part of Bergamot, camellia seed oil 0.001~0.005 part, 0.001~0.005 part of peony seed oil, 0.001~0.005 part of oil and fat of sacha inchi, 60~70 parts of water, laurel 5~15 parts of alcohol polyethers sodium sulfovinate, 0.5~2.5 part of sodium lauroyl sarcosine, 1~10 part of lauroyl glutamate TEA salt, coconut palm 1~10 part of oleamide propyl betaine, cocoyl -5~15 parts of glucoside tartrate sodium, PPG-26 butylol polyether -26/PEG- 40 0.001~0.03 part of hydrogenated castor oil/waters, 0.1~0.5 part of Sensiva SC50,0.05~0.25 part of DMDMH, sorb 0.1~0.8 part of sour potassium, 0.1~0.5 part of lauroyl arginine ethyl ester hydrochloride, 0.1~1.0 part of essence, citric acid 0.5~ 1.5 part.
- 8. essential oil is washed one's hands condensation according to claim 7, which is characterized in that the essential oil washes one's hands condensation by following parts by weight Each group be grouped as: 0.001~0.003 part of Saponaria officinalis extract, 0.001~0.003 part of Fructus Citri grandis extract, tea tree ethereal oil 0.001~0.003 part, 0.001~0.003 part of grapefruit essential oil, 0.001~0.003 part of Bergamot, camellia seed oil 0.001~0.003 part, 0.001~0.003 part of peony seed oil, 0.001~0.003 part of oil and fat of sacha inchi, 63~66 parts of water, laurel 8~12 parts of alcohol polyethers sodium sulfovinate, 1.0~2.0 parts of sodium lauroyl sarcosine, 3~7 parts of lauroyl glutamate TEA salt, cocounut oil 4~6 parts of amido propyl betaine, cocoyl -7~13 parts of glucoside tartrate sodium, PPG-26 butylol polyether -26/PEG-40 0.01~0.02 part of hydrogenated castor oil/water, 0.2~0.4 part of Sensiva SC50,0.1~0.2 part of DMDMH, potassium sorbate 0.3~0.6 part, 0.2~0.4 part of lauroyl arginine ethyl ester hydrochloride, 0.5~0.8 part of essence, 0.7~1.2 part of citric acid.
- 9. essential oil is washed one's hands condensation according to claim 8, which is characterized in that the essential oil washes one's hands condensation by following parts by weight Each group be grouped as: 0.001 part of Saponaria officinalis extract, 0.001 part of Fructus Citri grandis extract, 0.001 part of tea tree ethereal oil, grapefruit essential oil 0.001 part, 0.001 part of Bergamot, 0.001 part of camellia seed oil, 0.001 part of peony seed oil, 0.001 part of oil and fat of sacha inchi, water 64 parts, 9 parts of laureth sodium sulfovinate, 1.4 parts of sodium lauroyl sarcosine, 4 parts of lauroyl glutamate TEA salt, cocounut oil acyl 5.5 parts of amine propyl betaine, cocoyl -8.5 parts of glucoside tartrate sodium, PPG-26 butylol polyether -26/PEG-40 hydrogenates castor 0.015 part of numb oil/water, 0.3 part of Sensiva SC50,0.13 part of DMDMH, 0.5 part of potassium sorbate, lauroyl arginine second 0.25 part of ester hydrochloride, 0.7 part of essence, 0.9 part of citric acid.
- The preparation method of condensation 10. any one of claim 7 to 9 essential oil is washed one's hands, which comprises the steps of:S1. deionized water, laureth sodium sulfovinate, sodium lauroyl sarcosine and lauroyl arginine ethyl ester hydrochloride are pressed Ratio is uniformly mixed, and 10~15min is stirred under the conditions of 50~55 DEG C to being completely dissolved, obtains mixture A；S2. object A to be mixed is cooled to 40~45 DEG C, and cocoyl-glucoside tartrate is successively added into mixture A in proportion Sodium, Cocoamidopropyl betaine, lauroyl glutamate TEA salt and Sensiva SC50 stir 10~15min, must mix Object B；S3. first camellia seed oil, peony seed oil, oil and fat of sacha inchi, PPG-26 butylol polyether -26/PEG-40 hydrogenated castor oil/water are pressed Ratio is uniformly mixed, and obtains mixture C；Mixture C is added in mixture B again, 10~15min of stirring to Material clear, Obtain mixture D；S4. Saponaria officinalis extract, Fructus Citri grandis extract, DMDMH, potassium sorbate, tea tree essence is successively added into mixture D in proportion Oil, grapefruit essential oil, Bergamot and essence, stir evenly；Citric acid is slowly repeatedly added again, after mixing evenly up to essence Oil is washed one's hands condensation.
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