CN109394597B - Special antibacterial natural deodorant extracted from cypress for pet and preparation method thereof - Google Patents
Special antibacterial natural deodorant extracted from cypress for pet and preparation method thereof Download PDFInfo
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- CN109394597B CN109394597B CN201811171361.7A CN201811171361A CN109394597B CN 109394597 B CN109394597 B CN 109394597B CN 201811171361 A CN201811171361 A CN 201811171361A CN 109394597 B CN109394597 B CN 109394597B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
Abstract
The invention relates to the field of pet supplies, in particular to a natural deodorant extracted from cypress and specially used for bacteriostatic pets and a preparation method thereof. The natural deodorant special for bacteriostatic pets, which is extracted from Chinese juniper, comprises the following components: cypress phytoncidere, cypress essential oil, Arabic gum, antioxidant, essence, and antiseptic. The natural deodorant special for pets, prepared by the invention, can straighten animal hair and maintain hair, so that the pet hair has certain luster, and the product is safe, mild and non-irritant, not only can kill harmful bacteria on pets, but also can achieve the effect of removing peculiar smell.
Description
Technical Field
The invention belongs to the field of pet products, and particularly relates to a natural deodorant extracted from cypress and specially used for bacteriostatic pets and a preparation method thereof.
Background
With the improvement of living standard of people and the change of pet-raising concept, more and more pets gradually become members and partners in families, and bring a lot of companions and joys to people. As such, people inevitably need to spend more time, money, and energy to nurture them and care for them.
However, many parents who raise pets often do not have time to clean and sweep the pets because of busy work, and once the pets are not cleaned in time, the pets can emit odor, which not only affects the health of the pets, but also affects the home environment. In addition, pets generally enjoy running around the outside, and almost everything that is motile attracts their attention, while during play they also come into contact with bacteria and other germs. Some bacteria carried by pets, such as salmonella and staphylococci, can cause infections in humans. Although pets have a low chance of contracting infections, good hygiene practices always reduce the risk and thus protect the health of the entire home. Therefore, the development of a novel pet deodorant has become an urgent need in many households.
Disclosure of Invention
In order to solve the above problems, a first aspect of the present invention provides a bacteriostatic pet-specific natural deodorant extracted from juniper, comprising the following components: cypress phytoncidere, cypress essential oil, Arabic gum, antioxidant, essence, and antiseptic.
As a preferable technical scheme, the natural deodorant special for pets comprises the following components in parts by weight: 90-100 parts of cypress phytoncidere, 1-2 parts of cypress essential oil, 2-5 parts of Arabic gum, 0.5-3 parts of antioxidant, 0.1-1 part of essence and 0.01-0.2 part of preservative.
As a preferable technical scheme, the natural deodorant special for pets comprises the following components in parts by weight: 92-97 parts of cypress phytoncidere, 1.5-1.7 parts of cypress essential oil, 3-4 parts of Arabic gum, 1-2 parts of antioxidant, 0.3-0.8 part of essence and 0.1-0.15 part of preservative.
As a preferable technical scheme, the natural deodorant special for pets comprises the following components in parts by weight: 95 parts of cypress phytoncidere, 1.2 parts of cypress essential oil, 3.5 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
As a preferable technical scheme, the weight ratio of the cypress phytoncide to the arabic gum is 20-45: 1.
As a preferable technical scheme, the weight ratio of the Arabic gum to the Juniperus chinensis essential oil is 2-4: 1.
As a preferable technical scheme, the antioxidant is selected from one or more of dihydric phenol, guaiacol, gallic acid and propyl ester and amyl ester thereof, 2, 6-di-tert-butyl-p-cresol, 2, 5-di-tert-butyl-hydroquinone, guaiac resin, nordihydroguaiaretic acid, ascorbic acid, Ethylene Diamine Tetraacetic Acid (EDTA) and vitamin E.
As a preferred technical scheme, the essence is selected from one or more of lavender essence, milk essence, green apple essence, strawberry essence, papaya essence, hami melon essence, cherry essence, sea horse essence, honey peach essence, aloe essence, honeysuckle essence, rose essence, sweet osmanthus essence, olive essence, lily essence, chamomile essence and tea tree essence.
In a preferred embodiment, the preservative is selected from one or more of bronopol, methylisothiazolinone, iodopropynyl butylcarbamate, and paraben.
The second aspect of the invention provides a preparation method of a natural deodorant extracted from juniper chinensis and specially used for bacteriostatic pets, which comprises the following steps:
(1) uniformly mixing the Chinese juniper essential oil and the Arabic gum to obtain a mixed solution A;
(2) adding the cypress phytoncidere into a material kettle, sequentially adding the antioxidant, the essence, the preservative and the mixed solution A under stirring, and fully dissolving and uniformly stirring to obtain mixed solution B;
(3) and filtering the mixed solution B by using a 200-mesh nylon screen to obtain the natural deodorant special for the pets.
Has the advantages that: the natural deodorant special for pets, prepared by the invention, can straighten animal hair and maintain hair, so that the pet hair has certain luster, and the product is safe, mild and non-irritant, not only can kill harmful bacteria on pets, but also can achieve the effect of removing peculiar smell.
Detailed Description
The technical features of the technical solutions provided by the present invention are further clearly and completely described below with reference to the specific embodiments, and the scope of protection is not limited thereto.
The words "preferred", "more preferred", and the like, in the present invention refer to embodiments of the invention that may provide certain benefits, under certain circumstances. However, other embodiments may be preferred, under the same or other circumstances. Furthermore, the recitation of one or more preferred embodiments does not imply that other embodiments are not useful, nor is it intended to exclude other embodiments from the scope of the invention.
When a range of values is disclosed herein, the range is considered to be continuous and includes both the minimum and maximum values of the range, as well as each value between such minimum and maximum values. Further, when a range refers to an integer, each integer between the minimum and maximum values of the range is included. Further, when multiple range-describing features or characteristics are provided, the ranges may be combined. In other words, unless otherwise indicated, all ranges disclosed herein are to be understood to encompass any and all subranges subsumed therein. For example, a stated range from "1 to 10" should be considered to include any and all subranges between the minimum value of 1 and the maximum value of 10. Exemplary subranges of the range 1 to 10 include, but are not limited to, 1 to 6.1, 3.5 to 7.8, 5.5 to 10, and the like.
In order to solve the above problems, a first aspect of the present invention provides a bacteriostatic pet-specific natural deodorant extracted from juniper, comprising the following components: cypress phytoncidere, cypress essential oil, Arabic gum, antioxidant, essence, and antiseptic.
In some embodiments, the natural pet-specific deodorant comprises the following components in parts by weight: 90-100 parts of cypress phytoncidere, 1-2 parts of cypress essential oil, 2-5 parts of Arabic gum, 0.5-3 parts of antioxidant, 0.1-1 part of essence and 0.01-0.2 part of preservative.
In a preferred embodiment, the natural deodorant special for pets comprises the following components in parts by weight: 92-97 parts of cypress phytoncidere, 1.5-1.7 parts of cypress essential oil, 3-4 parts of Arabic gum, 1-2 parts of antioxidant, 0.3-0.8 part of essence and 0.1-0.15 part of preservative.
In a more preferred embodiment, the natural pet-specific deodorant comprises the following components in parts by weight: 95 parts of cypress phytoncidere, 1.2 parts of cypress essential oil, 3.5 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
Pfitoncidin
The cypress (cypress) is a perennial conifer, and the extract of the cypress is divided into water-soluble phytoncide and oil-soluble essential oil. Wherein the fendorine is a natural bactericide, mainly terpenes, and has fragrant smell. The phytoncide can expel micro-insects, bacteria and viruses which harm the plant body, and promote the repair of the damaged parts of the plant. The cypress phytoncide is water solution separated during the extraction of cypress essential oil, and is named as pure dew. The rhizome of Chinese juniper, such as fir and cypress, which has a longer survival time, contains more potent and effective phytoncide components. The reason is that some main components of the hinokitiol, such as cedrol, carvacrol, bisabolol and the like, have excellent medicinal activity. The cedrol is a good nerve regulator, and medical researches show that a certain amount of cedrol can relieve tension, slow heartbeat and smooth a nervous system, and recently, the cedrol is also found to have a strong inhibiting effect on lung cancer cells. The carvacrol has good killing effect on colibacillus, staphylococcus aureus and other flora. Bisabolol is a good broad-spectrum natural antibiotic and can kill various germs.
The sabina chinensis phytoncide is prepared by the following method.
Through research, the inventor discovers that the cypress phytoncide is added into the formula, so that the product has strong antibacterial, anti-inflammatory, skin-care, itching-relieving and spasmolytic and pain-relieving effects, and the unique smell of the product enables people to feel quiet and pleasant.
Chinese juniper essential oil
The cypress essential oil is a high-grade natural spice accepted in the world, is clear in oil quality and excellent in quality, contains various components beneficial to human bodies, such as cedrene, thujolene, cedrene, cedrol and the like, and has double functions of health care and medical treatment. Meanwhile, the cypress essential oil also has various good physiological and pharmacological activities. The Chinese juniper essential oil is reported to have obvious effects on the sensory nervous system, cardiovascular system, lung function, thermoregulation and gastrointestinal function of some neuropeptides.
In a preferred embodiment, the hinokitiol and the hinokitiol of the present invention are prepared by:
(1) pretreatment: selecting more than 60 years old roots of Chinese juniper at room temperature, cleaning soil, air drying, mechanically pulverizing into wood shavings, sheet materials, powder materials, drying, and putting into a distillation still;
(2) and (3) distillation: after the distillation kettle cover is covered, introducing steam, wherein the steam is generated by independent steam boiler equipment; the pressure during distillation is 0.06MPa, the distillation time is 20h, and the flow of the steam during distillation is 130 mL/min; the temperature of the steam is increased in a gradient manner during distillation, the initial temperature is 80 ℃, the temperature increasing frequency is 5 ℃/min-3 ℃/min, and the temperature is increased to 160 ℃, and the temperature is kept until the distillation is finished;
(3) cooling and separating: cooling the oil-gas mixture distilled from the distillation tower by a cooler, flowing into a cooling tank, standing for layering, wherein the upper layer is juniper oil containing a small amount of water and is called crude oil, and the lower layer is oil-water mixed liquid; standing and separating the primarily separated crude oil again to obtain Chinese juniper essential oil and Chinese juniper phytoncide; wherein the temperature of the cooler is 25 ℃.
The inventor of the application finds that the cypress essential oil added into the formula can make people feel pleasurable and nice instinctively, can be safely used in pets, has the effects of diminishing inflammation, easing pain, resisting bacteria, resisting viruses, killing insects and the like, and is beneficial to enhancing the immunity of the pets.
Arabic gum
The gum arabic of the present invention is also called gum arabic (scientific name: Acacia senegal, Acacia seyal) and is also called Acacia because it is derived from the stem exudates of Acacia belonging to the family Leguminosae, genus Acacia. Arabic gum contains high molecular polysaccharides and its calcium, magnesium and potassium salts. Mainly comprises arabinose, galactose, glucuronic acid and the like. The acacia gum with good quality is amber, has large and round particles and is mainly produced in Africa.
In a preferred embodiment, the weight ratio of sabinenol to gum arabic in the present invention is 20-45: 1.
In a preferred embodiment, the weight ratio of the acacia gum to the juniper essential oil is 2-4: 1.
The inventor of the application finds that the hinokition and the hinokition cannot exist stably for a long time in the research process, so that the inventor adds Arabic gum into the formula to enable the hinokition and the hinokition to be stable for a long time, and the inventor speculates that the probable reason is that the hinokition and the hinokition contain a large amount of water molecules and terpene compounds, and the Arabic gum contains partial protein substances and rhamnose, so that the hinokition and the hinokition can exist stably to achieve a good degerming and deodorizing effect. In addition, the inventor also found that the addition of gum arabic further improves the deodorizing effect, and the inventor believes that it may be capable of reacting with an amine substance having odor to reduce odor in the environment. Surprisingly, the inventors found that when the weight ratio of hinokitiol to gum arabic is 20-45:1, and the weight ratio of gum arabic to hinokitiol is 2-4:1, not only the efficacy of the deodorant is more durable, but also the pet hair is more fluffy and supple and easy to comb. The inventors speculate that the possible reason is that when gum arabic reacts with an amine species, the interfacial film will be negatively charged, which can further increase emulsion stability and increase repulsion.
The gum arabic of the present invention was purchased from shanghai alading biochemical science and technology, ltd.
Antioxidant agent
The antioxidant in the present invention refers to some chemical or bioactive organic substance that is used to provide electrons, inhibit oxidation, or absorb free radicals, thereby protecting a target substance from attack, but is itself relatively stable.
In some embodiments, the antioxidant of the present invention is selected from one or more of dihydric phenol, guaiacol, gallic acid and its propyl and pentyl esters, 2, 6-di-tert-butyl-p-cresol, 2, 5-di-tert-butylhydroquinone, guaiac, nordihydroguaiaretic acid, ascorbic acid, ethylenediaminetetraacetic acid (EDTA), vitamin E.
In a preferred embodiment, the antioxidant of the present invention is 2, 6-di-tert-butyl-p-cresol (BHT), available from Shanghai Aladdin Biotech, Inc.
The inventor of the application adds the 2, 6-di-tert-butyl-p-cresol (BHT) into the formula, so that the oily components such as oil and fat, hydrocarbon and the like in the product can be effectively prevented from contacting with oxygen in the air to generate oxidation, and peroxide, aldehyde, acid and the like are generated, so that the product is discolored, rancid and degraded in quality.
Essence
The essence of the invention is a raw material which endows cosmetics with certain fragrance, is one of key raw materials in the manufacturing process, can cover certain unpleasant odor in a product medium, is prepared and mixed by a plurality of spices, and has certain type of fragrance, namely fragrance type.
In some embodiments, the essence of the present invention is selected from one or more of lavender essence, milk essence, green apple essence, strawberry essence, papaya essence, hami melon essence, cherry essence, sea horse essence, honey peach essence, aloe essence, honeysuckle essence, rose essence, sweet osmanthus essence, olive essence, lily essence, chamomile essence, and tea tree essence.
In a preferred embodiment, the flavor of the present invention is a Hami melon flavor, available from Guangzhou Baoshidi flavors & fragrances, Inc.
Preservative
The preservative of the present invention refers to a natural or synthetic chemical ingredient used in foods, medicines, paints, biological specimens, etc. to retard spoilage caused by microbial growth or chemical changes.
In some embodiments, the preservative of the present invention is selected from one or more of the group consisting of bronopol, methylisothiazolinone, iodopropynyl butylcarbamate, and paraben.
In a preferred embodiment, the preservative of the present invention is methylisothiazolinone, available from Shanghai Aladdin Biotechnology Ltd.
The methylisothiazolinone is added into the formula, so that the propagation of polluted microorganisms can be killed or inhibited, the product is prevented from being rotted and deteriorated, and the product polluted by microorganisms is prevented from causing infection in use.
The second aspect of the invention provides a preparation method of a natural deodorant extracted from juniper chinensis and specially used for bacteriostatic pets, which comprises the following steps:
(1) uniformly mixing the Chinese juniper essential oil and the Arabic gum to obtain a mixed solution A;
(2) adding the cypress phytoncidere into a material kettle, sequentially adding the antioxidant, the essence, the preservative and the mixed solution A under stirring, and fully dissolving and uniformly stirring to obtain mixed solution B;
(3) and filtering the mixed solution B by using a 200-mesh nylon screen to obtain the natural deodorant special for the pets.
The present invention will now be described in detail by way of examples, and the starting materials used are commercially available unless otherwise specified.
Examples
Example 1
Embodiment 1 provides a bacteriostatic natural deodorant special for pets, which is extracted from juniper, and comprises the following components in parts by weight: 90 parts of cypress phytoncidere, 1 part of cypress essential oil, 2 parts of Arabic gum, 0.5 part of antioxidant, 0.1 part of essence and 0.01 part of preservative.
The juniper phytoncidere and the juniper essential oil are prepared by the following steps:
(1) pretreatment: selecting more than 60 years old roots of Chinese juniper at room temperature, cleaning soil, air drying, mechanically pulverizing into wood shavings, sheet materials, powder materials, drying, and putting into a distillation still;
(2) and (3) distillation: after the distillation kettle cover is covered, introducing steam, wherein the steam is generated by independent steam boiler equipment; the pressure during distillation is 0.06MPa, the distillation time is 20h, and the flow of the steam during distillation is 130 mL/min; the temperature of the steam is increased in a gradient manner during distillation, the initial temperature is 80 ℃, the temperature increasing frequency is 5 ℃/min-3 ℃/min, and the temperature is increased to 160 ℃, and the temperature is kept until the distillation is finished;
(3) cooling and separating: cooling the oil-gas mixture distilled from the distillation tower by a cooler, flowing into a cooling tank, standing for layering, wherein the upper layer is juniper oil containing a small amount of water and is called crude oil, and the lower layer is oil-water mixed liquid; standing and separating the primarily separated crude oil again to obtain Chinese juniper essential oil and Chinese juniper phytoncide; wherein the temperature of the cooler is 25 ℃.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets comprises the following steps:
(1) uniformly mixing the Chinese juniper essential oil and the Arabic gum to obtain a mixed solution A;
(2) adding the cypress phytoncidere into a material kettle, sequentially adding the antioxidant, the essence, the preservative and the mixed solution A under stirring, and fully dissolving and uniformly stirring to obtain mixed solution B;
(3) and filtering the mixed solution B by using a 200-mesh nylon screen to obtain the natural deodorant special for the pets.
Example 2
Embodiment 2 provides a natural deodorant special for bacteriostatic pets, which is extracted from juniper, and comprises the following components in parts by weight: 100 parts of cypress phytoncidere, 2 parts of cypress essential oil, 5 parts of Arabic gum, 3 parts of antioxidant, 1 part of essence and 0.2 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Example 3
Embodiment 3 provides a natural deodorant special for bacteriostatic pets, which is extracted from juniper, and comprises the following components in parts by weight: 92 parts of cypress phytoncidere, 1.7 parts of cypress essential oil, 4 parts of Arabic gum, 1 part of antioxidant, 0.3 part of essence and 0.1 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Example 4
Embodiment 4 provides a bacteriostatic natural deodorant special for pets, which is extracted from juniper, and comprises the following components in parts by weight: 97 parts of cypress phytoncidere, 1.5 parts of cypress essential oil, 3 parts of Arabic gum, 2 parts of antioxidant, 0.8 part of essence and 0.15 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Example 5
Embodiment 5 provides a bacteriostatic natural deodorant special for pets, which is extracted from juniper, and comprises the following components in parts by weight: 95 parts of cypress phytoncidere, 1.2 parts of cypress essential oil, 3.5 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Comparative example 1
Comparative example 1 provides a bacteriostatic natural deodorant special for pets, which is extracted from sabina chinensis, and comprises the following components in parts by weight: 40 parts of cypress phytoncidere, 1.2 parts of cypress essential oil, 3.5 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Comparative example 2
Comparative example 2 provides a bacteriostatic natural deodorant special for pets, which is extracted from sabina chinensis, and comprises the following components in parts by weight: 200 parts of cypress phytoncidere, 1.2 parts of cypress essential oil, 3.5 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Comparative example 3
Comparative example 3 provides a bacteriostatic natural deodorant special for pets, which is extracted from sabina chinensis, and comprises the following components in parts by weight: 95 parts of cypress phytoncidere, 0.05 part of cypress essential oil, 3.5 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Comparative example 4
Comparative example 4 provides a bacteriostatic natural deodorant special for pets, which is extracted from sabina chinensis, and comprises the following components in parts by weight: 95 parts of cypress phytoncidere, 10 parts of cypress essential oil, 3.5 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Comparative example 5
Comparative example 5 provides a bacteriostatic natural deodorant special for pets, which is extracted from sabina chinensis, and comprises the following components in parts by weight: 95 parts of cypress phytoncidere, 1.2 parts of cypress essential oil, 0.05 part of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Comparative example 6
Comparative example 6 provides a bacteriostatic natural deodorant special for pets, extracted from sabina chinensis, comprising the following components in parts by weight: 95 parts of cypress phytoncidere, 1.2 parts of cypress essential oil, 20 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Comparative example 7
Comparative example 7 provides a bacteriostatic natural deodorant special for pets, extracted from sabina chinensis, comprising the following components in parts by weight: 40 parts of cypress phytoncidere, 10 parts of cypress essential oil, 3.5 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Comparative example 8
Comparative example 8 provides a bacteriostatic natural deodorant special for pets, extracted from sabina chinensis, comprising the following components in parts by weight: 200 parts of cypress phytoncidere, 0.05 part of cypress essential oil, 3.5 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
The preparation methods of the cypress phytoncidere and the cypress essential oil are the same as example 1.
The gum arabic was purchased from shanghai alatin biochemical science ltd.
The antioxidant is 2, 6-di-tert-butyl-p-cresol (BHT) and is purchased from Shanghai Aladdin Biotechnology GmbH.
The essence is Hami melon essence, purchased from Guangzhou Baoshidi essence and spices Co.
The preservative is methylisothiazolinone, purchased from Shanghai Aladdin Biotechnology GmbH.
The preparation method of the natural deodorant special for pets is the same as that of example 1.
Evaluation of Performance
1. Test of bacteriostatic Property
The test method comprises the following steps: the test is carried out according to the experiment method of 2.1.1.7.4 bacteria quantitative killing of the Ministry of health (2002 edition), the bacteria test objects are escherichia coli ATCC 25922, staphylococcus aureus ATCC 6538 and candida albicans ATCC 10231, the three bacteria are respectively marked as A, B, C, and the action time is 2 min.
TABLE 1 antibacterial Property test Table
2. Hair softness and combing ease test
The test method comprises the following steps: selecting 65 pet puppies, dividing the pet puppies into 13 groups, testing five puppies in each group, using the puppies in each group according to examples 1-5 and comparative examples 1-8, applying the product to each puppy by 0.2/kg of the pet puppy by adopting the same experimental method, grading the softness and the combing difficulty of the puppy hair by a tester according to the own feeling, wherein the grading standard is 5 grades, and 1 grade represents very poor; 2 denotes the difference; score 3 indicates general; 4 points are well represented; score 5 indicates very good. The statistical results were averaged and the test results are shown in table 2. By analyzing the test results, it was found that the odor eliminating agent described in example 5 was very satisfactory to the test person, and example 5 showed that pet hair was particularly supple, fluffy and natural, and was combed easily without knots.
3. Odor removal efficacy and duration test
The test method comprises the following steps: selecting 65 pet puppies, dividing the pet puppies into 13 groups, testing five of the pet puppies, using each group of puppies according to examples 1-5 and comparative examples 1-8, enabling the puppies not to have a bath for 30 days before testing, applying 0.05mL/kg of the product to each puppy by using the same experimental method, scoring the odor and the odor removal duration of the puppies according to the feelings of the testers, scoring the odor of the puppies by using a score of 5, and scoring 1 to show very strong odor; score 2 indicates strong odor; score 3 indicates moderate odor; score 4 indicates faint odor; and 5 points represent no foul smell. The duration of the odor removal is measured in days (d) to be able to detect when the pet has a faint odor. The statistical results were averaged and the test results are shown in table 2. By analyzing the test results, it was found that the deodorizing agent described in example 5 was very satisfactory for the deodorizing effect of the testers, and example 5 showed no odor in the pets and remained the same for a long time.
TABLE 2 Hair softness and ease of combing, odor removal effectiveness and duration test charts
| Examples | Softness of hair | Degree of combing ease | Odor removal effect | Duration/d |
| Example 1 | 4.2 | 4.3 | 4.6 | 5 |
| Example 2 | 4.4 | 4.5 | 4.6 | 5.5 |
| Example 3 | 4.5 | 4.6 | 4.7 | 6 |
| Example 4 | 4.5 | 4.7 | 4.8 | 6 |
| Example 5 | 5.0 | 5.0 | 5.0 | 7 |
| Comparative example 1 | 3.7 | 3.8 | 3.7 | 3 |
| Comparative example 2 | 3.9 | 4.0 | 4.2 | 4 |
| Comparative example 3 | 3.8 | 3.8 | 4.3 | 4.5 |
| Comparative example 4 | 3.5 | 3.9 | 4.5 | 4 |
| Comparative example 5 | 3.5 | 3.5 | 4.4 | 3 |
| Comparative example 6 | 3.7 | 3.8 | 4.1 | 3.5 |
| Comparative example 7 | 3.4 | 3.3 | 3.3 | 3.5 |
| Comparative example 8 | 3.8 | 3.6 | 3.5 | 3 |
Claims (7)
1. The natural deodorant extracted from juniper chinensis special for bacteriostatic pets is characterized by comprising the following components: cypress phytoncidere, cypress essential oil, Arabic gum, antioxidant, essence and preservative;
90-100 parts of cypress phytoncidere, 1-2 parts of cypress essential oil, 2-5 parts of Arabic gum, 0.5-3 parts of antioxidant, 0.1-1 part of essence and 0.01-0.2 part of preservative;
the weight ratio of the cypress phytoncide to the Arabic gum is 20-45: 1;
the weight ratio of the Arabic gum to the Chinese juniper essential oil is 2-4: 1;
the juniper phytoncidere and the juniper essential oil are prepared by the following steps:
(1) pretreatment: selecting more than 60 years old roots of Chinese juniper at room temperature, cleaning soil, air drying, mechanically pulverizing into wood shavings, sheet materials, powder materials and drying, and then putting into a distillation still;
(2) and (3) distillation: after the distillation kettle cover is covered, introducing steam, wherein the steam is generated by independent steam boiler equipment; the pressure during distillation is 0.06MPa, the distillation time is 20h, and the flow of the steam during distillation is 130 mL/min; the temperature of the steam is increased in a gradient manner during distillation, the initial temperature is 80 ℃, the temperature increasing frequency is 5 ℃/min-3 ℃/min, and the temperature is increased to 160 ℃, and the temperature is kept until the distillation is finished;
(3) cooling and separating: cooling the oil-gas mixture distilled from the distillation tower by a cooler, flowing into a cooling tank, standing for layering, wherein the upper layer is juniper oil containing a small amount of water and is called crude oil, and the lower layer is oil-water mixed liquid; standing and separating the primarily separated crude oil again to obtain Chinese juniper essential oil and Chinese juniper phytoncide; wherein the temperature of the cooler is 25 ℃.
2. The natural odor eliminating agent for pet use of claim 1, wherein the natural odor eliminating agent for pet use comprises the following components in parts by weight: 92-97 parts of cypress phytoncidere, 1.5-1.7 parts of cypress essential oil, 3-4 parts of Arabic gum, 1-2 parts of antioxidant, 0.3-0.8 part of essence and 0.1-0.15 part of preservative.
3. The natural odor eliminating agent for pet use of claim 1, wherein the natural odor eliminating agent for pet use comprises the following components in parts by weight: 95 parts of cypress phytoncidere, 1.2 parts of cypress essential oil, 3.5 parts of Arabic gum, 1.5 parts of antioxidant, 0.5 part of essence and 0.12 part of preservative.
4. The natural deodorant agent for pets according to claim 1, wherein the antioxidant is selected from one or more of dihydric phenol, guaiacol, gallic acid and propyl and pentyl esters thereof, 2, 6-di-tert-butyl-p-cresol, 2, 5-di-tert-butyl hydroquinone, guaiac, nordihydroguaiaretic acid, ascorbic acid, ethylenediaminetetraacetic acid, vitamin E.
5. The natural deodorant according to claim 1, wherein the essence is selected from one or more of lavender essence, milk essence, green apple essence, strawberry essence, papaya essence, cantaloupe essence, cherry essence, sea horse essence, honey peach essence, aloe essence, honeysuckle essence, rose essence, osmanthus essence, olive essence, lily essence, chamomile essence, and tea tree essence.
6. The natural odor absorber as claimed in claim 1, wherein the preservative is selected from one or more of bronopol, methylisothiazolinone, iodopropynyl butylcarbamate, and paraben.
7. A method for preparing a natural deodorant special for pets according to any one of claims 1 to 6, wherein the method comprises the following steps:
(1) uniformly mixing the Chinese juniper essential oil and the Arabic gum to obtain a mixed solution A;
(2) adding the cypress phytoncidere into a material kettle, sequentially adding the antioxidant, the essence, the preservative and the mixed solution A under stirring, and fully dissolving and uniformly stirring to obtain mixed solution B;
(3) and filtering the mixed solution B by using a 200-mesh nylon screen to obtain the natural deodorant special for the pets.
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| CN115054718A (en) * | 2022-07-25 | 2022-09-16 | 浙江科思达新材科技有限公司 | Plant type long-acting sterilization deodorant and preparation method thereof |
| CN115109422A (en) * | 2022-07-25 | 2022-09-27 | 浙江科思达新材科技有限公司 | Rubber and plastic deodorant and preparation method thereof |
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