CN108158869A - A kind of antibacterial wet tissue liquid, wet tissue and preparation method thereof - Google Patents
A kind of antibacterial wet tissue liquid, wet tissue and preparation method thereof Download PDFInfo
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- CN108158869A CN108158869A CN201810185916.7A CN201810185916A CN108158869A CN 108158869 A CN108158869 A CN 108158869A CN 201810185916 A CN201810185916 A CN 201810185916A CN 108158869 A CN108158869 A CN 108158869A
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- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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Abstract
The present invention relates to a kind of amenities, and in particular to a kind of antibacterial wet tissue liquid, wet tissue and preparation method thereof.A kind of antibacterial wet tissue liquid, which is characterized in that in parts by weight, including at least following components：0.003~0.02 part of 15~20 parts of deionized water, 70~80 parts of cypress hydrosol, 0.001~0.015 part of Cypress ethereal oil, 2~7 parts of moisturizer, 0.5~3 part of skin conditioning agent and solubilizer.
Description
Technical field
The present invention relates to a kind of amenities, and in particular to a kind of antibacterial wet tissue liquid, wet tissue and preparation method thereof.
Background technology
Wet tissue is a kind of common amenities, it is made of the various wet tissue liquid of flexible sheet carrier impregnation.Existing market
On wet tissue largely add chemical bacteriostatic agent, such as quaternary ammonium salt, including Cetylpyridinium Chloride, benzalkonium chloride etc., some researches show that quaternary ammoniums
Salt cation toxicity and irritation are larger, may be made certain harmful using a kind of cationic germicide for a long time in same system
Microorganism develops immunity to drugs.Such as benzalkonium chloride fungicide, Pseudomonas aeruginosa drug resistance may be caused to improve.Also chemical preservative
It is added in wet tissue liquid, such as formaldehyde, methylchloroisothiazandnone and methylisothiazolinone.Formaldehyde can be by building not
It is suitble to the environment of microbe survival, to reach anti-corrosion effect.Although formaldehyde in cosmetics and daily hygiene articles for use hardly enters
To human body, but when exposure exceeds eubolism amount, formaldehyde can enter in blood of human body, and to kidney, liver and hematopoietic tissue etc.
Toxic effect is generated, leads to the damage to multiple systems.There may be lead to the latent of skin allergy for methylisothiazolinone (MIT)
In danger.Methylchloroisothiazandnone (CMIT) belongs to strong sensibiligen.The use of these wet tissues will not only be brought not
Just, it is also possible to cause strong skin irritatin, in turn result in allergy and more serious skin damage.
For above-mentioned technical problem, the present invention provides a kind of antibacterial wet tissue, using natural plant extracts as bacteriostatic activity
Component, non-stimulated to skin, sensitization rate is low, can more meet in the market the needs of to antibacterial wet tissue.
Invention content
In order to solve the above-mentioned technical problem, the first aspect of the invention provides a kind of antibacterial wet tissue liquid, with parts by weight
Meter, including at least following components：15~20 parts of deionized water, 70~80 parts of cypress hydrosol, 0.001~0.015 part of Cypress ethereal oil,
0.003~0.02 part of 2~7 parts of moisturizer, 0.5~3 part of skin conditioning agent and solubilizer.
As a kind of preferred technical solution of the present invention, the moisturizer is selected from small molecule polyol, plant polyose class
Moisturizer, amino acids moisturizer any one or more of.
As a kind of preferred technical solution of the present invention, the moisturizer is small molecule polyol, selected from 1,3- the third two
Alcohol, glycerine, 1,3 butylene glycol, methyl propanediol, 1,2- pentanediols, 3- methyl-1s, 3- butanediols, 1,2- hexylene glycols, dimerization third
Triol, dipropylene glycol, D-sorbite, 1,2- ethohexadiols, parahydroxyacet-ophenone, D-pantothenyl aleohol any one or more of.
As a kind of preferred technical solution of the present invention, the skin conditioning agent is selected from allantoin, ceramide, β-Portugal
Glycan, -8 esters of Babassu seed oil glycerin polyether, composite plant anti-sensitizer any one or more of.
As a kind of preferred technical solution of the present invention, the skin conditioning agent is allantoin, Babassu seed oil glycerine
The mixing of polyethers -8 esters, composite plant anti-sensitizer, wherein allantoin, -8 esters of Babassu seed oil glycerin polyether, composite plant
The mass ratio of anti-sensitizer is 1~3：5：3.6~5.
As a kind of preferred technical solution of the present invention, the solubilizer is selected from PEG-20 rilanit specials, PEG-40
Rilanit special, PEG-60 rilanit specials, Tween-80 any one or more of.
As a kind of preferred technical solution of the present invention, auxiliary agent, the auxiliary agent are further included in the antibacterial wet tissue liquid
For mass fraction in the antibacterial wet tissue liquid less than 0.3%, the auxiliary agent is selected from thickener, chelating agent, pH adjusting agent
Any one or more of.
The second aspect of the invention provides the preparation method of the antibacterial wet tissue liquid, including at least following steps：
Deionized water, cypress hydrosol, moisturizer are added in configuration pot, are heated to 80 DEG C, 25Hz is stirred evenly；It is cooled to
40 DEG C, skin conditioning agent is added in thereto, and 25Hz is stirred until homogeneous；Surplus stock is added in into configuration pot, 25Hz is stirred to equal
It is even；The antibacterial wet tissue liquid is obtained with 200 mesh filter-cloth filterings.
The third aspect of the invention provides a kind of antibacterial wet tissue, and the antibacterial wet tissue is carried including flexible sheet fiber
Body is full of the antibacterial wet tissue liquid in the flexible sheet fiber carrier.
As a kind of preferred technical solution of the present invention, the flexible sheet fiber carrier is spunlace non-woven cloth, cotton
Or paper handkerchief.
The above-mentioned of the application and other features, aspect and advantage is more readily understood with reference to following detailed description.
The antibacterial wet tissue fluidity matter of the present invention is stablized, and solution is transparent to be not likely to produce muddiness, and anti-inflammatory, good anti-bacterial effect.
Specific embodiment
The detailed description for preferred implementation method of the invention below of participating in the election of and including embodiment this hair can be more easily understood
Bright content.Unless otherwise defined, all technologies used herein and scientific terminology have common with fields of the present invention
The normally understood identical meaning of technical staff.When there is a conflict, the definition in this specification shall prevail.
As used herein term " by ... prepare " it is synonymous with "comprising".Term "comprising" used herein, " comprising ",
" having ", " containing " or its any other deformation, it is intended that cover including for non-exclusionism.For example, the combination comprising listed elements
Object, step, method, product or device are not necessarily limited to those elements, but can include not expressly listed other elements or
Such composition, step, method, product or the intrinsic element of device.
Conjunction " Consists of " excludes any element do not pointed out, step or component.If in claim, this
Phrase will make claim be closed, it be made not include the material in addition to the material of those descriptions, but relative normal
Except rule impurity.When being rather than immediately following after theme in the clause that phrase " Consists of " appears in claim main body,
It is only limited to the element described in the clause；Other elements are not excluded except the claim as a whole.
Equivalent, concentration or other values or parameter are excellent with range, preferred scope or a series of upper limit preferred values and lower limit
During the Range Representation that choosing value limits, this, which should be understood as, specifically discloses by any range limit or preferred value and any range
All ranges that any pairing of lower limit or preferred value is formed, regardless of whether the range separately discloses.For example, when open
During range " 1 to 5 ", described range should be interpreted as including range " 1 to 4 ", " 1 to 3 ", " 1 to 2 ", " 1 to 2 and 4 to
5 ", " 1 to 3 and 5 " etc..When numberical range is described herein, unless otherwise stated, otherwise range intention includes its end
Value and all integers and score in the range.
Singulative includes plural number and object is discussed, unless the context clearly dictates otherwise." optional " or it is " arbitrary
It is a kind of " refer to that the item described thereafter or event may or may not occur, and the description include situation that event occurs and
The situation that event does not occur.
Approximate term in specification and claims is used for modifying quantity, represents specific the present invention is not limited to this
Quantity further includes the modified part of the acceptable change without lead to related basic function close to the quantity.Phase
It answers, modifies a numerical value with " about ", " about " etc., mean that the present invention is not limited to the exact numericals.In some examples, it is approximate
Term likely corresponds to the precision of the instrument of measured value.In present specification and claims, range limits can be with
It combines and/or exchanges, these ranges include all subranges contained therebetween if not stated otherwise.
In addition, indefinite article " one kind " before element of the present invention or component and "one" quantitative requirement to element or component
(i.e. occurrence number) unrestriction.Therefore "one" or " one kind " should be read as including one or at least one, and odd number
The element or component of form also include plural form, unless the apparent purport of the quantity refers to singulative.
" polymer " means through the polymerizable compound prepared by the monomer that polymerize identical or different type.Generic term
" polymer " includes term " homopolymer ", " copolymer ", " terpolymer " and " copolymer ".
" copolymer " means the polymer prepared by polymerizeing at least two different monomers.Generic term " copolymer " includes
(it is general with term " terpolymer " for term " copolymer " (its generally to refer to the polymer prepared by two kinds of different monomers)
To refer to the polymer prepared by three kinds of different monomers).It also includes the polymer manufactured by polymerizeing four or more kind monomers.
" blend " means that two or more polymer mixes the polymer to be formed by physics or chemical method jointly.
In order to solve the above-mentioned technical problem, the first aspect of the invention provides a kind of antibacterial wet tissue liquid, with parts by weight
Meter, including at least following components：15~20 parts of deionized water, 70~80 parts of cypress hydrosol, 0.001~0.015 part of Cypress ethereal oil,
0.003~0.02 part of 2~7 parts of moisturizer, 0.5~3 part of skin conditioning agent and solubilizer.
As a kind of preferred technical solution of the present invention, the antibacterial wet tissue liquid, in parts by weight, including at least following
Component：18.70 parts of deionized water, 75 parts of cypress hydrosol, 0.005 part of Cypress ethereal oil, 4 parts of moisturizer, 1.2 parts of skin conditioning agent and
0.01 part of solubilizer.
Cypress of the present invention refers to cypress Maki, and cypress Maki, that is, Chinese juniper (Sabina chinensis (L.) Ant.) is pine
Plant under China fir mesh, Cupressaceae, Sabina, aiphyllium, tree crown steeple shape or cone, veteran are extensively avette.2 type of leaf, treelet or
Sprouting on Nie branches for base portion excessive growth is mostly that triangular shape bores shape, the life of 3 impellers, and base portion has joint and to downward life；Veteran is mostly squama shape leaf,
To life, closely it is affixed on sprig；Also have from the small plant for being all brill shape leaf always.Flower dioecism, male cone autumn is formed, secondary
Year is open, flower yellow；Female cone shape is small, and cone next year is ripe, and berry shape does not crack, outer by white powder.Intolerant tree species, happiness Wen Liang,
Temperature climate and moistening soil, dense materials are hard, available for pencil, furniture, construction material；Juniper is widely distributed, and originates in interior
Mongolian Wula Shan Mountain, Hebei, Shanxi, Shandong, Jiangsu, Zhejiang, Fujian, Anhui, Jiangxi, Henan, Southern Shaanxi, SOUTH OF GANSU, four
The ground such as river, West of Hubei Province, Hunan, Guizhou, Guangdong, In Northern Guangxi and Yunnan.Also there is cultivation in Tibet.Korea, Japan are also distributed.
Cypress used in the present invention originates from Sichuan.
Cypress hydrosol
Hydrosol is also known as crystal's oil, Hua Shui, refers to essential oil during distillation extraction, one separated when refining essential oil
The distillation stoste of 100% saturation of kind is a kind of by-product of essential oil, and ingredient is naturally pure, and fragrance is light pleasant.In cypress hydrosol
Other than containing a small amount of derived essential oil, also containing in whole cypress plants water soluble ingredient (such as tannic acid, flavonoids,
Determine acid, polyphenol powde, cedrol (cedrol, cedar wood alcohol), cedrene, thujopsene, longifolene, cedrene etc. in Lip river), by depth
Detection reaches 49 kinds of ingredients.The characteristic of its low concentration is easily less readily available for absorption by the skin, complete without essence and alcoholic content, mildly without piercing
Swash.Cypress hydrosol has further the advantage that：1. it improves environmental sanitation, remove peculiar smell, decomposing secondhand smoke and purify air.2. enhancing
Resistance prevents disease and reduces hypertension.3. improving respiratory tract, alleviate the defect such as asthma, sensibility rhinitis.4. except mosquito,
Antibacterial mite-removing.5. balance hormone, prevents aging at activating cell.6. calming down impatience, relieving pressure, insomnia, headache enable mood
It is happy.7. it refreshes the mind, improve inferior health constitution etc..
The cypress hydrosol of the present invention uses 100% cypress Maki tree root, and for raw material, the cypress Maki tree root comes from Sichuan Province,
The tree root that successive dynasties have been cut down in the successive dynasties is as raw material.Production technology：After raw material is crushed, using steam distillation abstraction technique
The saturation distilled water stoste rich in 100% oil generated simultaneously during production extraction Cypress ethereal oil.
Cypress ethereal oil
Essential oil be extraction the distinctive aromatic substance of plant, be taken from herbal flower, leaf, root, bark, fruit, seed,
What resin etc. was extract to distill, in a manner of squeezing.Due to essential oil-fumigation volatility height, and molecule is small, it is easy to be inhaled by human body
It receives, and people's intracorporeal organ can be permeated rapidly, extra ingredient is excreted, whole process only needs a few minutes, and plant sheet
The fragrance of body, also directly stimulates the secretion of pituitary gland, ferment and hormone secretion etc., and function in balanced body plays beauty shield
The effect of skin.Cypress ethereal oil is using 100% cypress Maki tree root as raw material, is given birth to after raw material crushes using steam distillation abstraction technique
Production extraction obtains.The main component of Cypress ethereal oil includes ter penoids 22, and account for total amount 93.54% (including monoterpene 7, accounts for
9.05%；84.49%) sequiterpene 15, accounts for；Aliphatic character 5, accounts for 5.28%；Aromatic component 1, accounts for 1.17%.It is main
Want ingredient have (+)-cedar wood alcohol, thujopsene, eneα-cedar, (+)-cuparene, α-curcumene, i- carypohyllenes, β-cedrene,
(+)-β-cedrene, α-eudesmol, (+)-α-longipinene, (+)-longifolene, (-)-isocaryophyllene, myrcene D, (+)-bar
Human relations West Asia tangerine alkene, p- umbrellas ellagic acid, 1,3,5- trimethyl cyclohexenes, 2,3,4,5- tetramethyl -2- cyclopentenones, humulene, (-) -
α-selinene, cuminyl alcohol, aromadendrene, (1R)-(+)-CIS firpenes, 1,1,3- trimethyl-cyclohexanes, isolongitolanone, α-method
Alkene, O-Anisic Acid methyl esters, cis- β-guaiene, androsterone etc..
Cedar wood alcohol in Cypress ethereal oil is a kind of sesquiterpenoid with higher, and boiling point is 294 DEG C, it has wide
General pharmacological action, such as anti-inflammatory, antibacterial, calmness, spasmolysis are twin, anti-cardiovascular disease, anti-aging and antitumor.Current research
Show that Cypress ethereal oil has extremely sensitive fungistatic effect to salmonella, bacillus subtilis, to Escherichia coli, Huo Shi intestines
Bacillus, Klebsiella, bacillus anthracis also have the fungistatic effect of medium sensitive intensity.Simultaneously Cypress ethereal oil to DPPH,
OH、Stronger elimination effect is respectively provided with, shows stronger inoxidizability.
The cypress hydrosol and the preparation method of Cypress ethereal oil, including at least following steps：
A. cypress Maki tree root is cleaned, the impurity such as removal epidermis sandy soil are then dried to water content less than 10%, use pulverizer
10~30 mesh are crushed to, are loaded into the middle part of alembic；
B. 100 DEG C of vapor is generated in vapor generator, is entered from the lower steam import of alembic, with filling
Cypress Maki raw material contacted, start oil pump after 50s and vacuumize the negative pressure for generating 40kPa；
C. after stable gas pressure, cooled down by room temperature water injection at the top of alembic, decompression humidification, at reduced pressure conditions with
The wood materials such as the root of cypress Maki are adequately contacted so that the volatile ingredients such as essential oil are in less pyrolysis and hydrolysis in raw tissue
In the case of, by steam extraction and mix；
D.30min oil pump is closed afterwards, is forced into, the steam pipe above opening alembic identical with external atmosphere pressure naturally
Coil condenser is connected on road.Condensed steam, obtained liquid enter constant temperature oil water separator, are decolourized with activated carbon, separation
Water-oil phase, filtering removal impurity, obtained oil phase are Cypress ethereal oil, and water phase is cypress hydrosol.
The advantageous effect of cypress can be made further to bring into play using cypress hydrosol and Cypress ethereal oil simultaneously, but cypress is pure
Dew and Cypress ethereal oil easily lead to the antibacterial wet tissue liquid stability and reduce when using simultaneously, at slightly higher or slightly lower temperature easily
There is phenomena such as muddy.The inventors discovered that it is avoided that stability reduces this instead of Cypress ethereal oil using cypress and shaddock peel essential oil
The appearance of one phenomenon, and anti-inflammatory, the antibacterial effect of system can be further enhanced using cypress and shaddock peel essential oil.
The ripening fruits of shaddock Citrus paradisi Macfadyen originates in the southern areas such as China Fujian, Jiangxi, Guangdong, Guangxi.Shaddock
Faint scent, sour-sweet, bright profit, full of nutrition, medical value is very high, is that one of favorite fruit of people and medical field are generally acknowledged most
Has the fruit of dietotherapy benefit.Shaddock is mostly based on fresh food at present, and small part is processing.It is annual to there is a large amount of pomelo peel to work as
It does rubbish arbitrarily to abandon, not only wastes resource, but also polluted environment.Pomelo peel accounts for the 54~55% of shaddock full weight, containing there are many
Active constituent, such as aurantiin, pectin, essential oil, pigment, vitamin B, C and organic acid and higher alcohol have higher guarantor
Strong and medical value is the good raw material of sterilization, anti-inflammatory and beauty and skin care.
As a kind of preferred technical solution of the present invention, the antibacterial wet tissue liquid, in parts by weight, including at least following
Component：15~20 parts of deionized water, 70~80 parts of cypress hydrosol, cypress and 0.001~0.015 part of shaddock peel essential oil, moisturizer 2
0.003~0.02 part of~7 parts, 0.5~3 part of skin conditioning agent and solubilizer.
As a kind of preferred technical solution of the present invention, the antibacterial wet tissue liquid, in parts by weight, including at least following
Component：0.005 part of 18.70 parts of deionized water, 75 parts of cypress hydrosol, cypress and shaddock peel essential oil, 4 parts of moisturizer, skin condition
0.01 part of 1.2 parts of agent and solubilizer.
As a kind of preferred technical solution of the present invention, the preparation method of the cypress and shaddock peel essential oil includes at least
Following steps：
Cypress and pomelo peel are dried to water content less than 10%, are crushed to 100 mesh respectively hereinafter, according to weight ratio 1：
0.1~0.3 weighs cypress powder and pomelo peel powder, adds in the ethyl alcohol of 5~10 times of amounts, and microwave heating is used after impregnating 2~3h
Extraction 2~3 times, filtering, recycling design obtain cypress and shaddock peel essential oil.
Moisturizer
Moisturizer is a kind of hydrophilic Emollient materials, has the ability with reference to water in relatively low humidity range, to skin
It keeps the skin wet, they can be by controlling exchanging for moisture between product and surrounding air skin to be made to be maintained above normal water contain
The equilibrium state of amount plays the role of mitigating dry skin.Moisturizer, it is specifiable to have：Small molecule polyol, plant polyose class
Moisturizer, amino acids moisturizer etc..
As a kind of preferred technical solution of the present invention, the moisturizer is selected from small molecule polyol, plant polyose class
Moisturizer, amino acids moisturizer any one or more of.
Small molecule polyol refers to the alcohol containing two or more hydroxyls containing 2~9 carbon atoms, described
Small molecule polyol is limited there is no other, specifiable to have：1,3- propylene glycol, glycerine, 1,3 butylene glycol, 2- methyl-1s,
3-propanediol, 1,2- pentanediols, 3- methyl-1s, 3- butanediols, 1,2- hexylene glycols, two polyglycerols, dipropylene glycol, sorbose
Alcohol, 1,2- ethohexadiols, parahydroxyacet-ophenone, D-pantothenyl aleohol etc..
The polysaccharide moisturizer includes hyaluronic acid, chitin and its derivative, plant polyose, heparin etc., can arrange
That lifts has：Hyaluronic acid, Sodium Hyaluronate, chitosan, heparin, tremella polysaccharides, trehalose, cactus polyoses, astragalus polyose, Chinese holly
Qi polysaccharide, sugarcane polysaccharide, Flos Lonicerae polysaccharide, Tea Polysaccharides etc..
The amino acids moisturizer is specifiable glycine betaine etc..
As a kind of preferred technical solution of the present invention, the moisturizer is small molecule polyol, selected from 1,3- the third two
Alcohol, glycerine, 1,3 butylene glycol, methyl propanediol, 1,2- pentanediols, 3- methyl-1s, 3- butanediols, 1,2- hexylene glycols, dimerization third
Triol, dipropylene glycol, D-sorbite, 1,2- ethohexadiols, parahydroxyacet-ophenone, D-pantothenyl aleohol any one or more of.
Methyl propanediol
Methyl propanediol, CAS：2163-42-0, abbreviation MPO, it is a kind of competitive polyalcohol regeneration product,
It derives from plant, stronger than 1,3-BDO, propylene glycol moistening effect, salubriouser than glycerine, provides excellent skin sense and moisturizing effect
Fruit, it is almost non-toxic, to skin and eye irritation, ratified by FDA.Can have good as essence synergist and solubilizer
Good antibacterial characteristics.
The methyl propanediol of the present invention is purchased from Guangzhou Bi Sheng trade Co., Ltds, brand DUBOIS, model DUB DIOL.
As a kind of preferred technical solution of the present invention, the skin conditioning agent is selected from allantoin, ceramide, β-Portugal
Glycan, -8 esters of Babassu seed oil glycerin polyether, composite plant anti-sensitizer any one or more of.
As a kind of preferred technical solution of the present invention, the skin conditioning agent is allantoin, Babassu seed oil glycerine
The mixing of polyethers -8 esters, composite plant anti-sensitizer, wherein allantoin, -8 esters of Babassu seed oil glycerin polyether, composite plant
The mass ratio of anti-sensitizer is 1~3：5：3.6~5.
As a kind of preferred technical solution of the present invention, the skin conditioning agent is allantoin, Babassu seed oil glycerine
The mixing of polyethers -8 esters, composite plant anti-sensitizer, wherein allantoin, -8 esters of Babassu seed oil glycerin polyether, composite plant
The mass ratio of anti-sensitizer is 2：5：5.
Allantoin
Allantoin, molecular formula C4H6O3N4, CAS：97-59-6, alias Allantoin, Allantoin, urea
Base glycolylurea, Allantoin are a kind of hydantoin derivatives.About 50,000 tons of the annual production capacity of current allantoin in the world, needs
It is mainly medicine, cosmetics and agriculture three big fields to ask market.
Allantoin, sterling are a kind of nontoxic, tasteless and nonirritants, have promotion cell life without hypersensitive white crystal
It is long, accelerate the physiological functions such as wound healing, cutin-softening albumen, be the good consolidant and antiulcer agents of skin trauma.It can
As alleviating and treating xerodermia, scaling dermatopathy, skin ulcer, digestive tract ulcer and inflammation, to osteomyelitis, sugar
Urine disease, hepatic sclerosis, acne have good therapeutic effect.Since allantoin is a kind of amphoteric compound, can be formed with reference to many kinds of substance multiple
Salt, have be protected from light, sterilization and anticorrosion, analgesic, antioxidation, skin can be made to keep moisture content, moisten and soft, be cosmetology etc.
The additive of cosmetics is widely used in freckle cream, anti-acne toner, shampoo, perfumed soap, toothpaste, shaving lotion, conditioner, convergence
The additive of agent, anti-sweat deodorization lotion etc..The cosmetics of addition allantoin have protective tissue, it is hydrophilic, absorb water and prevent moisture
The effects that distributing；Add allantoin hair-cream, hair cream, shampoo, have protective effect to hair, can make hair not bifurcated, constantly
Hair；Skin, lip can be made soft for lipstick, the face cream of addition allantoin and high resilience, and has beautiful gloss.Allantoin promotes
Tissue growth, cell metabolism, cutin-softening layer albumen.
The allantoin of the present invention is purchased from dutch royal Royal DSM group.
- 8 esters of Babassu seed oil glycerin polyether
- 8 esters of Babassu seed oil glycerin polyether can significantly improve the vigor of superoxide dismutase in red blood cell (SOD),
To delaying body aging, moisturizing improves skin protective capacities.Babassu seed oil glycerine not only there is lubrication to moisten nutrition skin simultaneously
Fat, adjusting and increase skin elasticity effect can also make to cause the substance white three of allergy dilute and intermediate platelet aggregation activate
The yield of the factor (PAF) significantly reduces, wherein being a kind of fragrant acid compound containing Alecrim acid, there is anticoagulation, antibacterial to disappear
There is scorching, antiviral isoreactivity very strong inoxidizability to inhibit allergic reaction.When -8 esters of Babassu seed oil glycerin polyether also
With emulsifying effectiveness, when its concentration in the solution reaches a certain critical value (i.e. critical micelle concentration CMC) and after more than the value,
Its molecule is associated with the aggregation particle particle of colloid size automatically, in equilibrium state between this colloid particle, forms glue
Shu Shui.Before and after micella water is formed, significant changes occur for the dirt-removing power of -8 esters of Babassu seed oil glycerin polyether, form micella
The performance of its surfactant can be given full play to after water, the grease common to color make-up has good solvability.
- 8 esters of Babassu seed oil glycerin polyether of the present invention are purchased from Shanghai Yi Heng Chemical Co., Ltd.s.
Composite plant anti-sensitizer
Whenever weather conversion, the phenomenon that temperature difference great disparity is big or the season of warmed moist, and skin allergy can often occur for many people,
Doctor trained in Western medicine is referred to as " seasonal skin allergy ".The reason of seasonal skin allergy, essentially consists in lag of the people to environmental suitability
Property.First, the grease (sebum) of skin secretion has collectively constituted the chemistry screen of skin with cytoplasm (especially ceramide)
Barrier, and when these substances are reduced, the function of skin barrier will weaken.In winter, as temperature reduces, sebum secretion is notable
It reduces, the epidermis lipid component including ceramide substantially reduces, this allows the barrier of skin to be in more fragile shape
State, it is weaker to extraneous protective capacities.And during winter to spring converts, season alternation, one side temperature gos up comparatively fast, separately
On the one hand, frequently exchange, solar radiation intensity increase, humidity rise cold and heat air again, and bacterium enlivens frequent, and skin can not be timely
Adjusting is made, therefore a series of unconformable symptoms occurs.
The method that confrontation seasonal allergic is taken has：1) one layer of closing " coat " is added to injured skin, obstructed extraneous dirty
Stimulation of the environment to skin is contaminated, prevents water loss in skin；2) make skin calm, various allergic symptoms of releiving prevent
The appearance of the secondary infringement such as " grabbing ", " scratching " repeatedly；3) it is from solving the problems, such as at all, it is desired nonetheless to the skin barrier of fragility again
It is returned to the skin that the general level of the health becomes normal resilience.The use of composite plant anti-sensitizer is that one kind successfully manages season
The method of section property skin allergy, main component come from natural plants, mild non-stimulated, can inhibit because a variety of causes is (external
Stimulation or gene) inflammatory factor that causes, significantly improve the immunocompetence and antioxidant activity of skin itself, releive and
The effect of repairing skin.
As a kind of preferred technical solution of the present invention, the composite plant anti-sensitizer is commercial product CalmYang.
CalmYang includes seven kinds of plant extracts such as centella, giant knotweed, radix scutellariae, green tea, glycyrrhiza glabra, german chamomile, rosemary
Object.It is had dry skin by screening more than 200 kinds of Chinese herbal medicine to develop dedicated for treatment, severe pruritus, inflammation, scar, affected part
Sepage, the product of abnormal pigmentation can inhibit the inflammatory factor caused by a variety of causes (outside stimulus or gene), show
The immunocompetence and antioxidant activity for improving skin itself are write, the effect of releiving and repair skin.
The composite plant anti-sensitizer CalmYang of the present invention is purchased from upper voyage week Chemical Co., Ltd..
As a kind of preferred technical solution of the present invention, the solubilizer is selected from PEG-20 rilanit specials, PEG-40
Rilanit special, PEG-60 rilanit specials, Tween-80 any one or more of.
Rilanit special
Rilanit special is a kind of castor oil products easily decomposed, do not have remaining modification.Starting material comes from day
Right plant-rilanit special, can be biodegradable in nature, be suitble to pesticide, coating, daily use chemicals, water-based ink, weaving, printing and dyeing,
The industries such as papermaking, cosmetics.Rilanit special is a kind of excellent non-ionic solubilizer and emulsifier；With wider pH value
Stability, low foam can form clear mixture with aliphatic acid and fatty alcohol at high temperature.Rilanit special is a kind of common
Efficient solubilizing agents, available for carrying out the oily matters such as solubilized essence, essential oil and synthetic perfume in water or alcoholic solution, when in use may be used
By it with solubilized substance is needed to press 1：1~3 ratio is mixed and stirred for uniformly until transparent.Pharmaceutical grade solubilizer can be used as.PEG-
20 rilanit specials, Cremophor RH40, PEG-60 rilanit specials are three kinds of common solubilizer, and property is close, can
To be selected according to actual production.
PEG-20 rilanit specials, Cremophor RH40, the PEG-60 rilanit specials of the present invention is purchased from Guangzhou poem
Tender tea leaves chemical industry.
As a kind of preferred technical solution of the present invention, auxiliary agent, the auxiliary agent are further included in the antibacterial wet tissue liquid
For mass fraction in the antibacterial wet tissue liquid less than 0.3%, the auxiliary agent is selected from thickener, chelating agent, pH adjusting agent
Any one or more of.
As a kind of preferred technical solution of the present invention, the thickener is selected from carbomer, xanthans, natto gum, fiber
Element, Sodium Polyacrylate, polysorbate any one or more of.
As a kind of preferred technical solution of the present invention, the chelating agent is selected from disodium ethylene diamine tetraacetate, decoyl hydroxyl
Oxime acid, sodium phytate, hydroxy phenylpropionyl amine benzoic acid any one or more of.
As a kind of preferred technical solution of the present invention, the pH adjusting agent is selected from edetic acid(EDTA), natrium adetate, lemon
Acid, sodium citrate, sodium hydroxide, potassium hydroxide, triethanolamine any one or more of.
The second aspect of the invention provides the preparation method of the antibacterial wet tissue liquid, including at least following steps：
Deionized water, cypress hydrosol, moisturizer are added in configuration pot, are heated to 80 DEG C, 25Hz is stirred evenly；It is cooled to
40 DEG C, skin conditioning agent is added in thereto, and 25Hz is stirred until homogeneous；Surplus stock is added in into configuration pot, 25Hz is stirred to equal
It is even；The antibacterial wet tissue liquid is obtained with 200 mesh filter-cloth filterings.
The third aspect of the invention provides a kind of antibacterial wet tissue, and the antibacterial wet tissue is carried including flexible sheet fiber
Body is full of the antibacterial wet tissue liquid in the flexible sheet fiber carrier.
As a kind of preferred technical solution of the present invention, the flexible sheet fiber carrier is spunlace non-woven cloth, cotton
Or paper handkerchief.
The present invention is specifically described below by embodiment.It is necessarily pointed out that following embodiment is only used
In the invention will be further described, it is impossible to be interpreted as limiting the scope of the invention, professional and technical personnel in the field
Some the nonessential modifications and adaptations made according to the content of the invention described above, still fall within protection scope of the present invention.
It is if raw materials used to be all commercially available in addition, without other explanations.
Embodiment 1：
Embodiment 1 provides a kind of antibacterial wet tissue liquid, in parts by weight, including at least following components：15 parts of deionized water,
0.003 part of 70 parts of cypress hydrosol, 0.001 part of Cypress ethereal oil, 2 parts of moisturizer, 0.5 part of skin conditioning agent and solubilizer.Described
Moisturizer is glycerine.Glycerine also known as glycerine, CAS：56-81-5, glycerine used in the present invention are Thailand's lotus flower board glycerine,
Purchased from Shanghai Wei Gu Chemical Co., Ltd.s.The skin conditioning agent is allantoin, -8 esters of Babassu seed oil glycerin polyether, is answered
Close the mass ratio of the mixing, wherein allantoin, -8 esters of Babassu seed oil glycerin polyether, composite plant anti-sensitizer of plant desensitizer
It is 1：5：3.6.The solubilizer is PEG-20 rilanit specials.
The cypress hydrosol and the preparation method of Cypress ethereal oil, including at least following steps：
A. cypress Maki is cleaned, the impurity such as removal epidermis sandy soil are then dried to water content less than 10%, crushed with pulverizer
To 30 mesh hereinafter, being loaded into the middle part of alembic；
B. 100 DEG C of vapor is generated in vapor generator, is entered from the lower steam import of alembic, with filling
Cypress Maki raw material contacted, start oil pump after 50s and vacuumize the negative pressure for generating 40kPa；
C. after stable gas pressure, cooled down by room temperature water injection at the top of alembic, decompression humidification, at reduced pressure conditions with
The wood materials such as the rhizome of cypress Maki are adequately contacted so that the volatile ingredients such as essential oil are in less pyrolysis and water in raw tissue
In the case of solution, by steam extraction and mix；
D.30min oil pump is closed afterwards, is forced into, the steam pipe above opening alembic identical with external atmosphere pressure naturally
Coil condenser is connected on road.Condensed steam, obtained liquid enter constant temperature oil water separator, are decolourized with activated carbon, separation
Water-oil phase, filtering removal impurity, obtained oil phase are Cypress ethereal oil, and water phase is cypress hydrosol.
The preparation method of the antibacterial wet tissue liquid, including at least following steps：
Deionized water, cypress hydrosol, moisturizer are added in configuration pot, are heated to 80 DEG C, 25Hz is stirred evenly；It is cooled to
40 DEG C, skin conditioning agent is added in thereto, and 25Hz is stirred until homogeneous；Surplus stock is added in into configuration pot, 25Hz is stirred to equal
It is even；The antibacterial wet tissue liquid is obtained with 200 mesh filter-cloth filterings.
Embodiment 2：
Embodiment 2 provides a kind of antibacterial wet tissue liquid, in parts by weight, including at least following components：20 parts of deionized water,
0.02 part of 80 parts of cypress hydrosol, 0.015 part of Cypress ethereal oil, 7 parts of moisturizer, 3 parts of skin conditioning agent and solubilizer.The moisturizing
Agent is methyl propanediol.Methyl propanediol, CAS：2163-42-0, purchased from ALST CARE.The skin conditioning agent is allantois
The mixing of element, Babassu seed oil glycerin polyether -8 esters, composite plant anti-sensitizer, wherein allantoin, Babassu seed oil glycerine gather
- 8 esters of ether, composite plant anti-sensitizer mass ratio be 3：5：5.The solubilizer is Cremophor RH40.
The preparation method is the same as that of Example 1 for the cypress hydrosol and Cypress ethereal oil.
The preparation method is the same as that of Example 1 for the antibacterial wet tissue liquid.
Embodiment 3：
Embodiment 3 provides a kind of antibacterial wet tissue liquid, in parts by weight, including at least following components：Deionized water 18.70
Part, 75 parts of cypress hydrosol, 0.005 part of Cypress ethereal oil, 4 parts of moisturizer, 1.2 parts of skin conditioning agent and 0.01 part of solubilizer.It is described
Moisturizer be dipropylene glycol.Dipropylene glycol, CAS：246-770-3, purchased from U.S. OXEA.The skin conditioning agent is allantois
The mixing of element, Babassu seed oil glycerin polyether -8 esters, composite plant anti-sensitizer, wherein allantoin, Babassu seed oil glycerine gather
- 8 esters of ether, composite plant anti-sensitizer mass ratio be 2：5：5.The solubilizer is PEG-60 rilanit specials.
The preparation method is the same as that of Example 1 for the cypress hydrosol and Cypress ethereal oil.
The preparation method is the same as that of Example 1 for the antibacterial wet tissue liquid.
Embodiment 4：
Embodiment 4 provides a kind of antibacterial wet tissue liquid, in parts by weight, including at least following components：17 parts of deionized water,
0.015 part of 0.01 part of 75 parts of cypress hydrosol, cypress and shaddock peel essential oil, 5 parts of moisturizer, 1.2 parts of skin conditioning agent and solubilizer.
The moisturizer is methyl propanediol.Methyl propanediol, CAS：2163-42-0, purchased from ALST CARE.The skin tune
Reason agent is the mixing of allantoin, Babassu seed oil glycerin polyether -8 esters, composite plant anti-sensitizer, wherein allantoin, Babassu
- 8 esters of seed oil glycerin polyether, composite plant anti-sensitizer mass ratio be 2：5：5.The solubilizer is Tween-80.Described
Tween-80 is purchased from Guangzhou Sui Ze Environmental Protection Technology Co., Ltd.
The cypress and the preparation method of shaddock peel essential oil, including at least following steps：
Cypress and pomelo peel are dried to water content less than 10%, are crushed to 100 mesh respectively hereinafter, according to weight ratio 1：
0.2 weighs cypress powder and pomelo peel powder, adds in the ethyl alcohol of 8 times of amounts, uses extracting through microwave heating 3 times after impregnating 2.5h, mistake
Filter, recycling design obtain cypress and shaddock peel essential oil.
The preparation method is the same as that of Example 1 for the antibacterial wet tissue liquid.
Embodiment 5：
Embodiment 5 provides the antibacterial wet tissue liquid, in parts by weight, including at least following components：Deionized water
0.005 part of 18.70 parts, 75 parts of cypress hydrosol, cypress and shaddock peel essential oil, 4 parts of moisturizer, 1.2 parts of skin conditioning agent and solubilising
0.01 part of agent.The moisturizer is methyl propanediol.Methyl propanediol, CAS：2163-42-0, purchased from ALST CARE.It is described
Skin conditioning agent be allantoin, Babassu seed oil glycerin polyether -8 esters, composite plant anti-sensitizer mixing, wherein allantois
Element, -8 esters of Babassu seed oil glycerin polyether, composite plant anti-sensitizer mass ratio be 2：5：5.The solubilizer is PEG-
40 rilanit specials.
The cypress and the preparation method of shaddock peel essential oil are the same as embodiment 4.
The preparation method is the same as that of Example 1 for the antibacterial wet tissue liquid.
Embodiment 6：
The specific embodiment of embodiment 6 is with embodiment 5, and the difference lies in the bacteriostatic agent further includes auxiliary agent, institute
Mass fraction of the auxiliary agent stated in antibacterial facial mask liquid is 0.03%, and the auxiliary agent is pH adjusting agent triethanolamine.
Triethanolamine, CAS：102-71-6, purchased from Shanghai Mike's woods biochemical technology Co., Ltd.
Comparative example 1：
The specific embodiment of comparative example 1 is with embodiment 3, difference, and the cypress hydrosol is the quality such as are changed to
Deionized water.
Comparative example 2：
The specific embodiment of comparative example 2 is with embodiment 3, difference, and the Cypress ethereal oil is the quality such as are changed to
Deionized water.
Comparative example 3：
The specific embodiment of comparative example 3 replaces the cypress and shaddock peel essential oil with embodiment 6, difference
For etc. quality deionized water.
Comparative example 4：
The specific embodiment of comparative example 4 replaces the cypress and shaddock peel essential oil with embodiment 6, difference
For etc. quality shaddock peel essential oil.
Comparative example 5：
The specific embodiment of comparative example 5 is with embodiment 6, difference, and cypress and shaddock peel essential oil the matter such as are replaced with
The Cypress ethereal oil of amount and the mixture of shaddock essential oil.
Performance evaluation：
Antibacterial wet tissue liquid is obtained using Examples 1 to 6 and comparative example 1~5 to produce antibacterial wet tissue.Described is antibacterial wet
Towel includes flexible sheet fiber carrier, the flexible sheet fiber carrier is immersed in the antibacterial wet tissue liquid, fully
Wetting post package obtains the antibacterial wet tissue liquid.In the experimentation of the present invention, spunlace non-woven cloth is selected as flexible sheets
Shape fiber carrier.
1. stability
A. antibacterial wet tissue liquid is placed in (45 ± 2) DEG C electro-heating standing-temperature cultivator 30 days, it is observed surely after restoring room temperature
It is qualitative；B. antibacterial wet tissue liquid is placed in the refrigerator of (- 5 ± 2) DEG C 30 days, its stability is observed after restoring room temperature.Observation
Project：The transparency of antibacterial wet tissue liquid, precipitation and smell variation etc., if antibacterial wet tissue liquid keep it is transparent, without precipitation, do not generate
Smell variation is then recorded as stablizing, and is otherwise recorded as unstable.Test result is as shown in table 1.
2. biocidal property
Antibacterial wet tissue made from Examples 1 to 6 and comparative example 1~5 is placed in enclosed environment (25 DEG C, humidity 60%),
Culture of Escherichia coli, the S. aureus culture of open culture are placed in the enclosed environment, after placing 8h, is surveyed
The clump count (CFU/mL) of the amount antibacterial wet tissue, specific measuring method is dispersed in after the antibacterial wet tissue is shredded
In the deionized water of 100mL, 3h is impregnated, filtering takes 1mL samples to cultivate 48h at 37 DEG C, carries out total plate count measure, test
It the results are shown in Table 1.
Table 1
3. skin test
Age, sensibility skin tester (test and determine through irritation) 600 was tested between 18~50 one full year of life,
Six groups are randomly divided into, there was no significant difference between each group.Daily using wet made of the antibacterial wet tissue liquid of an Examples 1 to 6
Towel cleans hand, and experiment carries out 28 days altogether.
Experimental result finds in the test process of 28 days do not have subject that skin allergy and stimulation phenomenon occurs.Pass through
It can be found that the human hand moisture content of skin more than 80% increases, hand skin becomes more to be good for skinanalysis apparatus test result
Health.
As can be seen from Table 1, the antibacterial wet tissue liquid stability in the present invention is good, and biocidal property is good, and is gone back to skin is non-stimulated
With maintenance effect.
Aforementioned example is merely illustrative, for explaining some features of the method for the invention.Appended right will
It asks and is intended to the range as wide as possible that requirement is contemplated that, and embodiments as presented herein is only according to all possible implementation
The explanation of the embodiment of the selection of the combination of example.Therefore, the purpose of applicant is that appended claim is not illustrated this hair
The exemplary selectional restriction of bright feature.Some numberical ranges used also include sub- model in the claims
It encloses, the variation in these ranges should be also construed in the conceived case by appended claim covering.
Claims (10)
1. a kind of antibacterial wet tissue liquid, which is characterized in that in parts by weight, including at least following components：15~20 parts of deionized water,
70~80 parts of cypress hydrosol, 0.001~0.015 part of Cypress ethereal oil, 2~7 parts of moisturizer, 0.5~3 part of skin conditioning agent and solubilising
0.003~0.02 part of agent.
2. antibacterial wet tissue liquid as described in claim 1, which is characterized in that the moisturizer is selected from small molecule polyol, plants
Object polysaccharide moisturizer, amino acids moisturizer any one or more of.
3. antibacterial wet tissue liquid as claimed in claim 2, which is characterized in that the moisturizer is small molecule polyol, is selected from
1,3- propylene glycol, glycerine, 1,3 butylene glycol, methyl propanediol, 1,2- pentanediols, 3- methyl-1s, 3- butanediols, 1,2- oneself two
Any one of alcohol, two polyglycerols, dipropylene glycol, D-sorbite, 1,2- ethohexadiols, parahydroxyacet-ophenone, D-pantothenyl aleohol are more
Kind.
4. antibacterial wet tissue liquid as described in claim 1, which is characterized in that the skin conditioning agent is selected from allantoin, nerve
Amide, beta glucan, -8 esters of Babassu seed oil glycerin polyether, composite plant anti-sensitizer any one or more of.
5. antibacterial wet tissue liquid as claimed in claim 4, which is characterized in that the skin conditioning agent is allantoin, Babassu
The mixing of seed oil glycerin polyether -8 esters, composite plant anti-sensitizer, wherein allantoin, -8 esters of Babassu seed oil glycerin polyether,
The mass ratio of composite plant anti-sensitizer is 1~3：5：3.6~5.
6. antibacterial wet tissue liquid as described in claim 1, which is characterized in that the solubilizer is selected from PEG-20 hydrogenated castors
Oil, Cremophor RH40, PEG-60 rilanit specials, Tween-80 any one or more of.
7. antibacterial wet tissue liquid as described in claim 1, which is characterized in that further include auxiliary agent in the antibacterial wet tissue liquid, institute
Mass fraction of the auxiliary agent stated in the antibacterial wet tissue liquid be less than 0.3%, the auxiliary agent be selected from thickener, chelating agent,
PH adjusting agent any one or more of.
8. such as the preparation method of the antibacterial wet tissue liquid of claim 1~7 any one of them, which is characterized in that including at least following
Step：
Deionized water, cypress hydrosol, moisturizer are added in configuration pot, are heated to 80 DEG C, 25Hz is stirred evenly；It is cooled to 40
DEG C, skin conditioning agent is added in thereto, and 25Hz is stirred until homogeneous；Surplus stock is added in into configuration pot, 25Hz is stirred until homogeneous；
The antibacterial wet tissue liquid is obtained with 200 mesh filter-cloth filterings.
9. a kind of antibacterial wet tissue, which is characterized in that the antibacterial wet tissue includes flexible sheet fiber carrier, the flexible sheet
It is full of in fiber carrier such as the antibacterial wet tissue liquid of claim 1~7 any one of them.
10. antibacterial wet tissue as claimed in claim 9, which is characterized in that the flexible sheet fiber carrier is spun lacing nonwoven
Cloth, cotton or paper handkerchief.
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