CN102920638A - Cleansing milk containing plant extractives and preparation method of cleansing milk - Google Patents

Cleansing milk containing plant extractives and preparation method of cleansing milk Download PDF

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Publication number
CN102920638A
CN102920638A CN201210477244XA CN201210477244A CN102920638A CN 102920638 A CN102920638 A CN 102920638A CN 201210477244X A CN201210477244X A CN 201210477244XA CN 201210477244 A CN201210477244 A CN 201210477244A CN 102920638 A CN102920638 A CN 102920638A
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Prior art keywords
sodium
cleansing milk
japanese cypress
material pot
acid sodium
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CN201210477244XA
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Chinese (zh)
Inventor
李竟铭
王立升
刘旭
杨华
蒋敏捷
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GUANGXI BREATHING TECHNOLOGY ENGINEERING Co Ltd
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GUANGXI BREATHING TECHNOLOGY ENGINEERING Co Ltd
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Priority to CN201210477244XA priority Critical patent/CN102920638A/en
Publication of CN102920638A publication Critical patent/CN102920638A/en
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Abstract

The invention relates to cleansing milk and a preparation method thereof. The cleansing milk comprises the following main components in percentage by weight: 30-50% of cypress pythoncidere, 5-10% of cocofatty acylamido propyl betaines, 1-2% of cypress essential oil, 0.1-1% of licorice root extractives, 0.1-1% of cucumber fruit extractives and the like. The preparation method of the cleansing milk comprises the following concrete steps of: putting the cypress pythoncidere, glycerol, methyl hydroxybenzoate and the like into a material pot, continuously stirring all the raw materials to be uniform, slowly heating the mixture to 82 DEG C, and keeping the temperature for 10min; then, putting the cocofatty acylamido propyl betaines and sodium chloride into the material pot to continuously stir, cooling the mixed liquid to 45 DEG C, then, putting the cypress essential oil, the licorice root extractives and the cucumber fruit extractives into the material pot, continuously stirring the mixture to be uniform for 1h, and then, cooling the mixture to the room temperature; and detecting the appearance, the smell and the pH value of a sample, and obtaining a finished product if the appearance, the smell and the pH value of the sample are qualified.

Description

A kind of cleansing milk that contains plant extract and preparation method thereof
Technical field
The invention belongs to the daily chemicals technical field, be specifically related to a kind of cleansing milk that contains plant extract and preparation method thereof.Technical background
Cleansing milk is face's cleaning article of everyday use of commonly using.Along with economic development, city environmental quality descends gradually.Dust, acarid, antibacterial and the undesired grade of work and rest are brought a lot of skin problems, such as freckle, skin sore, skin accelerated ageing etc.Clean face is the basis of skin protection, therefore the effect of cleansing milk is very large.But the cleansing milk product that exists on the market mostly adopts the surfactant of chemosynthesis, lacks natural component, is not easy to be absorbed by the skin, and also may bring out allergy, and function singleness can't satisfy user to the requirement of many effects such as cleansing milk washing maintenance simultaneously.
Polyphenol powde in the Japanese Cypress extract and derived essential oil, the sense of the emotion of releiving relieving fatigue, and have stronger antibacterial and acaricide function.Studies show that both at home and abroad the Japanese Cypress extract has fabulous killing and permanent inhibition to being attached to the multiple pathogenic bacterias such as staphylococcus aureus on the skin and acarid.Licorice root extract energy effective antiinflammatory, antiviral, and strengthen immunologic function.The Fructus Cucumidis sativi berry extract is rich in vitamin and cucumber chitinase, the energy skin moistening, and delay skin aging also has the effect of good careful pore.Therefore, with the Japanese Cypress extract, licorice root extract and Fructus Cucumidis sativi berry extract are made cleansing milk as the natural formula composition, to the skin nonirritant, except the effect of cleaning face skin is arranged, can also have antibacterially preferably, acaricide is eliminated the skin sore acne, and the careful pore of energy, have cosmetic result and extensive use and be worth.
Summary of the invention
The object of the present invention is to provide a kind of cleansing milk that contains plant extract, except general cleaning skin function, also can be antibacterial, acaricide is eliminated the skin sore acne, careful facial pore.
Another object of the present invention is to provide the preparation method of this cleansing milk.
For achieving the above object, the present invention adopts following technical scheme:
A kind of cleansing milk that contains plant extract, in weight portion, composed of the following components:
Japanese Cypress Phyntocide: 30-50%, cocoyl N-methyltaurine sodium: 1-7%
Cocos nucifera oil alcohol radical hydroxyethyl sodium sulfonate: 1-7%, cocoyl sodium succinate: 1-7%
Cocamido propyl betaine: 5-10%, lauroyl musculamine acid sodium: 1-3%, myristoyl musculamine acid sodium: 1-3%
Palmityl musculamine acid sodium: 1-3%, glycerol: 1-5%, Japanese Cypress quintessence oil: 1-2%
Sodium chloride: 0.1-1%, distearate: 0.1-1%, licorice root extract: 0.1-1%
Fructus Cucumidis sativi berry extract: 0.1-1%, methyl hydroxybenzoate: 0.1-1%, EDETATE SODIUM: 0.1-1%
Its surplus is distilled water.
Described licorice root extract is that the root and rhizome process of China's Chinese medicine glycyrrhizic legume is extracted gained, contains glycyrrhizin, the potassium of glycyrrhizic acid, calcium salt, and liquiritins etc. are purchased in Shaanxi Rui Kang biological engineering company limited.
Described Fructus Cucumidis sativi berry extract is that the cucumber fruits process is extracted gained, is weak yellow liquid, can make skin surface form smooth hygroscopic mem-brane, has the effect of releiving, and increases the water content of skin, purchases the auspicious enlightening bio tech ltd in Xi'an.
Described Japanese Cypress Phyntocide and Japanese Cypress quintessence oil are to be extracted and the separating-purifying gained by the rhizome process distillation of perennial Japanese Cypress.Japanese Cypress Phyntocide is water white water liquid.The Japanese Cypress quintessence oil is pure faint yellow quintessence oil.Both leaching process are:
(1) Japanese Cypress is cleaned, is removed the impurity such as epidermis sandy soil, then with infrared drier cure to water content below 10%, be cut into mechanical chopper again and be about 7 centimetres, wide approximately 3 centimetres, the fuzz stick of thickness about 0.3 centimetre;
(2) pulverizing Japanese Cypress fuzz stick makes it become particle powder between 10 to 30 orders, the alembic middle part of packing into;
(3) in the steam maker, produce 100 ℃ steam, enter from the bottom steam inlet of alembic, contact with the Japanese Cypress raw material that fills, after 50 seconds, start the negative pressure that the oil pump evacuation produces 40 kPas;
(4) after stable gas pressure, normal-temperature water by the alembic top is sprayed cooling, the blood pressure lowering humidification, under reduced pressure, contact fully with the wood materials such as rhizome of Japanese Cypress, so that the volatile ingredients such as the interior quintessence oil of raw tissue, in the situation that less pyrolysis and hydrolysis, by steam extraction and mixing.
After (5) 30 minutes, close oil pump, so that negative pressure gradually becomes normal atmosphere pressure, after 30 minutes, open the steam pipework of alembic top again, connect coil condenser.Behind steam-condensation, the liquid that obtains enters the thermostatical oil water separator, depending on biphase color and luster and turbidity, adding activated carbon decolours, separate profit biphase again, further filter removal impurity with filter screen, can get Japanese Cypress quintessence oil and Japanese Cypress hydrosol is the water solublity Japanese Cypress Phyntocide.
Japanese Cypress quintessence oil of the present invention and Japanese Cypress Phyntocide also can extract prepared by the vapor distillation of routine.
Japanese Cypress quintessence oil involved in the present invention, the water solublity Japanese Cypress Phyntocide is hydrosol, all passes through China Guangzhou Analysis ﹠. Test Center, authoritative institution's repeated detection evaluations such as the little analysis of spectrum in Shanghai test center, its main component such as table 1 and table 2 are listed.
The main effective ingredient of table 1 Japanese Cypress quintessence oil
Figure BSA00000809687100021
Figure 3
Figure BSA00000809687100041
The main effective ingredient of table 2 Japanese Cypress Phyntocide
Figure BSA00000809687100042
Figure 1
A kind of cleansing milk preparation method that contains plant extract comprises that successively step is:
(1) Japanese Cypress Phyntocide, cocoyl N-methyltaurine sodium, cocos nucifera oil alcohol radical hydroxyethyl sodium sulfonate, cocoyl sodium succinate, lauroyl musculamine acid sodium, myristoyl musculamine acid sodium, palmityl musculamine acid sodium, glycerol, distearate, EDETATE SODIUM, methyl hydroxybenzoate are dropped into the material pot; constantly stir; be heated to 82 degrees centigrade, be incubated 10 minutes.
(2) cocamido propyl betaine, sodium chloride are dropped in the above-mentioned material pot, constantly stir, in 82 degrees centigrade of insulations 10 minutes.
(3) mixed liquor is cooled to 45 degrees centigrade, again Japanese Cypress quintessence oil, licorice root extract, Fructus Cucumidis sativi berry extract is dropped into the material pot, constantly stir, be incubated 10 minutes.
(4) stir after 1 hour, be cooled to gradually room temperature.
(5) take a sample to check outward appearance, fragrance, pH value, the qualified finished product that is.
The present invention has following characteristics:
Cleansing milk of the present invention contains special natural component Japanese Cypress extract (being Japanese Cypress Phyntocide and Japanese Cypress quintessence oil), licorice root extract, Fructus Cucumidis sativi berry extract, except clean ability is strong, antibacterial in addition, acaricide, eliminate the skin sore acne, the functions such as careful facial pore.
Most of composition of the present invention is plant pure natural product, and skin is had no stimulation.
Cleansing milk abnormal smells from the patient of the present invention fragrance has certain calming the nerves and the effect of the emotion of releiving.
Use cleansing milk provided by the invention, after 130 people use 50 days continuously, all feed back, use rear face to feel clearly comfortable, without greasy feeling, cleannes are high, and the skin exquisiteness is glossy, the colour of skin obviously bleaches, and skin sore acne etc. are had good therapeutic effect, and non-stimulated, allergic phenomena.
The specific embodiment
The present invention will be further described below in conjunction with specific embodiment.
Example I~V
Figure BSA00000809687100081
Preparation Example I~V:
Cleansing milk provided by the invention can by any known or other effectively be applicable to provide the technology preparation of cleansing milk, preferred following preparation method comprises the steps:
(1) Japanese Cypress Phyntocide, cocoyl N-methyltaurine sodium, cocos nucifera oil alcohol radical hydroxyethyl sodium sulfonate, cocoyl sodium succinate, lauroyl musculamine acid sodium, myristoyl musculamine acid sodium, palmityl musculamine acid sodium, glycerol, distearate, EDETATE SODIUM, methyl hydroxybenzoate are dropped into the material pot; constantly stir; be heated to 82 degrees centigrade, be incubated 10 minutes.
(2) cocamido propyl betaine, sodium chloride are dropped in the above-mentioned material pot, constantly stir, in 82 degrees centigrade of insulations 10 minutes.Mixed liquor is slowly cooled to 45 degrees centigrade, again Japanese Cypress quintessence oil, licorice root extract, Fructus Cucumidis sativi berry extract are dropped into the material pot, constantly stir, be incubated 10 minutes.
(3) mixture stirred after 1 hour, was cooled to gradually room temperature.Take a sample to check outward appearance, fragrance, pH value, the qualified finished product that namely is packaged as.Again shipment after the sampling inspection of after the assay was approved packing, finished product.
Experimental data (from China Guangzhou Analysis ﹠. Test Center, the little analysis of spectrum in Shanghai test center, Guangzhou SGS)
Figure BSA00000809687100082
Figure BSA00000809687100091
Conclusion: in the test experiments of product, common bacterium colony, flora are not all detected, common heavy metal and poisonous metal also do not detect, and color, viscosity and acid-base value are suitable, and preferably heat-resisting and tolerance to cold is arranged.

Claims (2)

1. cleansing milk is characterized in that being made by following raw material and weight proportion:
Japanese Cypress Phyntocide: 30-50%; cocoyl N-methyltaurine sodium: 1-7%; cocos nucifera oil alcohol radical hydroxyethyl sodium sulfonate: 1-7%; cocoyl sodium succinate: 1-7%; cocamido propyl betaine: 5-10%, lauroyl musculamine acid sodium: 1-3%, myristoyl musculamine acid sodium: 1-3%; palmityl musculamine acid sodium: 1-3%; glycerol: 1-5%, Japanese Cypress quintessence oil: 1-2%, sodium chloride: 0.1-1%; distearate: 0.1-1%; licorice root extract: 0.1-1%, Fructus Cucumidis sativi berry extract: 0.1-1%, methyl hydroxybenzoate: 0.1-1%; EDETATE SODIUM: 0.1-1%, its surplus is distilled water.
2. the preparation method of a kind of cleansing milk according to claim 1 is characterized in that in turn including the following steps:
(1) Japanese Cypress Phyntocide, cocoyl N-methyltaurine sodium, cocos nucifera oil alcohol radical hydroxyethyl sodium sulfonate, cocoyl sodium succinate, lauroyl musculamine acid sodium, myristoyl musculamine acid sodium, palmityl musculamine acid sodium, glycerol, distearate, EDETATE SODIUM, methyl hydroxybenzoate are dropped into the material pot; constantly stir; be heated to 82 degrees centigrade, be incubated 10 minutes.
(2) cocamido propyl betaine, sodium chloride are dropped in the above-mentioned material pot, constantly stir, protect 82 degrees centigrade, be incubated 10 minutes.Mixed liquor is slowly cooled to 45 degrees centigrade, again Japanese Cypress quintessence oil, licorice root extract, Fructus Cucumidis sativi berry extract are dropped into the material pot, constantly stir, be incubated 10 minutes.Behind the mixture restir 1 hour, be cooled to gradually room temperature.Take a sample to check outward appearance, fragrance, pH value, the qualified finished product that namely is packaged as.
CN201210477244XA 2012-11-22 2012-11-22 Cleansing milk containing plant extractives and preparation method of cleansing milk Pending CN102920638A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107496345A (en) * 2017-09-01 2017-12-22 安庆徽云博冠化妆品科技有限公司 A kind of protein chelates mildy wash and preparation method thereof
CN107822949A (en) * 2017-11-20 2018-03-23 南宁科城汇信息科技有限公司 A kind of facial mask containing Chinese juniper wood polyphenol powde and preparation method thereof
CN107890452A (en) * 2017-11-20 2018-04-10 南宁科城汇信息科技有限公司 A kind of mildy wash of the polyphenol powde of wood containing Chinese juniper and preparation method thereof
CN108158869A (en) * 2018-03-07 2018-06-15 四川桧元素生物科技有限公司 A kind of antibacterial wet tissue liquid, wet tissue and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1058531A (en) * 1991-08-28 1992-02-12 上海中华日用化工实验所 Cucumber face washing milk and method for making thereof
TW200806336A (en) * 2006-07-19 2008-02-01 Hinoki Life Shop Co Ltd Falsecypress bath salt and manufacturing method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1058531A (en) * 1991-08-28 1992-02-12 上海中华日用化工实验所 Cucumber face washing milk and method for making thereof
TW200806336A (en) * 2006-07-19 2008-02-01 Hinoki Life Shop Co Ltd Falsecypress bath salt and manufacturing method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
徐良等: "洗面奶及其配方技术概述", 《中国化妆品(行业)》, 15 September 2006 (2006-09-15) *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107496345A (en) * 2017-09-01 2017-12-22 安庆徽云博冠化妆品科技有限公司 A kind of protein chelates mildy wash and preparation method thereof
CN107822949A (en) * 2017-11-20 2018-03-23 南宁科城汇信息科技有限公司 A kind of facial mask containing Chinese juniper wood polyphenol powde and preparation method thereof
CN107890452A (en) * 2017-11-20 2018-04-10 南宁科城汇信息科技有限公司 A kind of mildy wash of the polyphenol powde of wood containing Chinese juniper and preparation method thereof
CN108158869A (en) * 2018-03-07 2018-06-15 四川桧元素生物科技有限公司 A kind of antibacterial wet tissue liquid, wet tissue and preparation method thereof
CN108158869B (en) * 2018-03-07 2021-04-30 四川桧元素生物科技有限公司 Antibacterial wet tissue liquid, wet tissue and preparation method of wet tissue

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Application publication date: 20130213