CN107496345A - A kind of protein chelates mildy wash and preparation method thereof - Google Patents
A kind of protein chelates mildy wash and preparation method thereof Download PDFInfo
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- CN107496345A CN107496345A CN201710779282.3A CN201710779282A CN107496345A CN 107496345 A CN107496345 A CN 107496345A CN 201710779282 A CN201710779282 A CN 201710779282A CN 107496345 A CN107496345 A CN 107496345A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/985—Skin or skin outgrowth, e.g. hair, nails
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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Abstract
The invention discloses a kind of protein chelates mildy wash, and it is made up of the raw material of following weight parts：Sodium alginate 12, ethylmaltol 0.5 1, ethylenediamine tetra-acetic acid 34, sorbitan monostearate 0.1 0.2, magnesium chloride 0.6 1, fermentation protein emulsion 36 40, plants essential oil 24, Cocoamidopropyl betaine 0.7 1, ZPT 0.1 0.2, the present invention is using ethylenediamine tetra-acetic acid as chelating agent, sodium alginate, magnesium chloride is raw material, formed and chelated with fermentation protein emulsion blending, effectively improve stability of the albumen in finished product mildy wash, effectively improve the phenomenon that albumen is easily lost in traditional protein class mildy wash, improve whitening, moisturizing and other effects.
Description
Technical field
The invention belongs to mildy wash field, and in particular to a kind of protein chelates mildy wash and preparation method thereof.
Background technology
Mildy wash is a kind of senior face washing agent, and it is derived from perfumed soap, but is different from perfumed soap.The two all has cleaning skin
The effect of.Different places are that perfumed soap major part raw material is the chemicals of bases, he the effect of be mainly reflected in decontamination, go
On oil.Mildy wash is then that comparison is more, acid, alkaline, neutral to have.Mildy wash is while decontamination, additionally it is possible to has nutrition
The effect of with protection；
But presently commercially available mildy wash easily causes the undue degreasing of epiderm skin due to having used substantial amounts of surfactant,
So that skin is relatively dry, more serious meeting causes the irreversibility infringement to skin, and function is single, can not meet to use
Demand of the person to the multiple efficacies of skin care.
The content of the invention
In view of the defects and deficiencies of the prior art, the present invention intends to provide a kind of protein chelates mildy wash and its system
Preparation Method.
To achieve the above object, the present invention uses following technical scheme：
A kind of protein chelates mildy wash, it is made up of the raw material of following weight parts：
Sodium alginate 1-2, ethylmaltol 0.5-1, ethylenediamine tetra-acetic acid 3-4, sorbitan monostearate 0.1-0.2, chlorination
Magnesium 0.6-1, fermentation protein emulsion 36-40, plants essential oil 2-4, Cocoamidopropyl betaine 0.7-1, ZPT 0.1-
0.2。
Described plants essential oil is made up of one or more of mixing in Rosemary Oil, Rosa Damascana, tea tree ethereal oil
's.
What described fermentation protein emulsion was made up of the raw material of following weight parts：
Fish scale 25-30, pigskin 14-20, folium isatidis 3-5, peppermint 1-2, sorbester p17 0.1-0.2.
The preparation method of described fermentation protein emulsion comprises the following steps：
（1）Folium isatidis, peppermint mixing are taken, is added in the sodium hydroxide solution of 16-20 times of compound weight, at 65-70 DEG C
Insulated and stirred 1-2 hours, filtering, obtain sodium hydroxide filtrate；
（2）Fish scale, pigskin are cleaned up, wear into fine powder, is added in the hydrochloric acid solution of 10-15 times of fine powder weight, at 50-60 DEG C
Lower insulated and stirred 4-5 hours, filtering, filter residue is washed 3-4 times, drying, mixed with above-mentioned sodium hydroxide filtrate, be sent to boiling water
In bath, insulated and stirred 5-7 minutes, discharge, filtering, obtain protein solution；
（3）Above-mentioned protein solution is taken, adds its weight 1-2% lactic acid bacteria, sealing thermal insulation 10-13 hours, go out at 30-35 DEG C
Material, mixes with sorbester p17, stirs, obtain the fermentation protein emulsion.
A kind of preparation method of protein chelates mildy wash, comprises the following steps：
（1）Sodium alginate, ethylmaltol, magnesium chloride mixing are taken, is added in the deionized water of 30-40 times of compound weight,
Stir, obtain saline aqueous dispersions；
（2）Fermentation protein emulsion is taken, is added in above-mentioned saline aqueous dispersions, stirs, be sent in 70-75 DEG C of water-bath,
Ethylenediamine tetra-acetic acid is added, insulated and stirred 1-2 hours, discharging, ZPT is added, stirs to normal temperature, it is molten to obtain protein chelates
Liquid；
（3）Above-mentioned protein chelates solution is taken, is mixed with above-mentioned Cocoamidopropyl betaine, is concentrated at 35-45 DEG C relative
Density is 1-1.3 thick liquid, adds remaining each raw material, ultrasonic 2-3 minutes, produces the protein chelates mildy wash.
Advantages of the present invention：
The present invention mixes folium isatidis, peppermint, is extracted using sodium hydroxide solution, then using fish scale, pigskin as raw material, passed through
The mode that acid, alkali extract successively obtains protein solution, then the protein solution is effectively raised into finished product by lactobacillus-fermented
The content of beneficial bacterium in mildy wash, the bin stability of finished product is improved, extend the useful life of finished product；
For the present invention using ethylenediamine tetra-acetic acid as chelating agent, sodium alginate, magnesium chloride are raw material, are formed with fermentation protein emulsion blending
Chelating, effectively improves stability of the albumen in finished product mildy wash, effectively improves egg in traditional protein class mildy wash
The phenomenon that Bai Rongyi is lost in, improves whitening, moisturizing and other effects；
The mildy wash of the present invention can effectively remove face's cutin and the dirt including melanin, skin is recovered transparent
Salubrious state, the Proteins in finished product are quickly penetrating into skin, while promoting skin metabolism, also added for face
One layer of protective barrier, it is therefore prevented that the loss of face's epidermis moisture content and extraneous pollutant largely penetrate into, tender and lovely so as to protect
Skin is not attacked by adverse factor.
Embodiment
Embodiment 1
A kind of protein chelates mildy wash, it is made up of the raw material of following weight parts：
Sodium alginate 2, ethylmaltol 1, ethylenediamine tetra-acetic acid 4, sorbitan monostearate 0.2, magnesium chloride 1, fermentation protein
Emulsion 40, plants essential oil 4, Cocoamidopropyl betaine 1, ZPT 0.2.
Described plants essential oil is tea tree ethereal oil.
What described fermentation protein emulsion was made up of the raw material of following weight parts：
Fish scale 30, pigskin 20, folium isatidis 5, peppermint 2, sorbester p17 0.2.
The preparation method of described fermentation protein emulsion comprises the following steps：
（1）Folium isatidis, peppermint mixing are taken, is added in the sodium hydroxide solution of 20 times of compound weight, is incubated and stirs at 70 DEG C
Mix 2 hours, filter, obtain sodium hydroxide filtrate；
（2）Fish scale, pigskin are cleaned up, wear into fine powder, adds in the hydrochloric acid solution of 15 times of fine powder weight, is incubated at 60 DEG C
Stirring 5 hours, filtering, filter residue is washed 4 times, drying, mix, be sent in boiling water bath with above-mentioned sodium hydroxide filtrate, be incubated
Stirring 7 minutes, discharge, filtering, obtain protein solution；
（3）Above-mentioned protein solution is taken, adds the lactic acid bacteria of its weight 2%, sealing thermal insulation 13 hours at 35 DEG C, discharging, with sapn
80 mixing, stir, obtain the fermentation protein emulsion.
A kind of preparation method of protein chelates mildy wash, comprises the following steps：
（1）Sodium alginate, ethylmaltol, magnesium chloride mixing are taken, is added in the deionized water of 40 times of compound weight, stirs
Uniformly, saline aqueous dispersions are obtained；
（2）Fermentation protein emulsion is taken, is added in above-mentioned saline aqueous dispersions, stirs, is sent in 75 DEG C of water-bath, is added
Ethylenediamine tetra-acetic acid, insulated and stirred 2 hours, discharging, ZPT is added, stirs to normal temperature, obtains protein chelates solution；
（3）Above-mentioned protein chelates solution is taken, is mixed with above-mentioned Cocoamidopropyl betaine, relative density is concentrated at 45 DEG C
For 1.3 thick liquid, remaining each raw material is added, ultrasound 3 minutes, produces the protein chelates mildy wash.
Embodiment 2
A kind of protein chelates mildy wash, it is made up of the raw material of following weight parts：
Sodium alginate 1, ethylmaltol 0.5, ethylenediamine tetra-acetic acid 3, sorbitan monostearate 0.1, magnesium chloride 0.6, fermentation
Protein emulsion 36, plants essential oil 2, Cocoamidopropyl betaine 0.7, ZPT 0.1.
Described plants essential oil is Rosemary Oil.
What described fermentation protein emulsion was made up of the raw material of following weight parts：
Fish scale 25, pigskin 14, folium isatidis 3, peppermint 1, sorbester p17 0.1.
The preparation method of described fermentation protein emulsion comprises the following steps：
（1）Folium isatidis, peppermint mixing are taken, is added in the sodium hydroxide solution of 16 times of compound weight, is incubated and stirs at 65 DEG C
Mix 1 hour, filter, obtain sodium hydroxide filtrate；
（2）Fish scale, pigskin are cleaned up, wear into fine powder, adds in the hydrochloric acid solution of 10 times of fine powder weight, is incubated at 50 DEG C
Stirring 4 hours, filtering, filter residue is washed 3 times, drying, mix, be sent in boiling water bath with above-mentioned sodium hydroxide filtrate, be incubated
Stirring 5 minutes, discharge, filtering, obtain protein solution；
（3）Above-mentioned protein solution is taken, adds the lactic acid bacteria of its weight 1%, sealing thermal insulation 10 hours at 30 DEG C, discharging, with sapn
80 mixing, stir, obtain the fermentation protein emulsion.
A kind of preparation method of protein chelates mildy wash, comprises the following steps：
（1）Sodium alginate, ethylmaltol, magnesium chloride mixing are taken, is added in the deionized water of 30 times of compound weight, stirs
Uniformly, saline aqueous dispersions are obtained；
（2）Fermentation protein emulsion is taken, is added in above-mentioned saline aqueous dispersions, stirs, is sent in 70 DEG C of water-bath, is added
Ethylenediamine tetra-acetic acid, insulated and stirred 1 hour, discharging, ZPT is added, stirs to normal temperature, obtains protein chelates solution；
（3）Above-mentioned protein chelates solution is taken, is mixed with above-mentioned Cocoamidopropyl betaine, relative density is concentrated at 35 DEG C
For 1 thick liquid, remaining each raw material is added, ultrasound 2 minutes, produces the protein chelates mildy wash.
Performance test：
Subject totally 100 people, wherein male 25 people, the people of female 75, one full year of life at age 20-50, application method is：Subject directly uses
Tested protein chelates mildy wash of the invention, it is daily sooner or later respectively using once, use one month；
Use the effect of the protein chelates mildy wash of embodiment 1：
Subject totally 50 people, wherein male 12 people, the people of female 38.After one month, subject represents to use the albumen chela of embodiment 1
Close the salubrious non-greasy of face after mildy wash, can effectively clean dirt, and skin keep for a long time moistening, salubrious compact and it is rich
Elasticity, face mask lines ratio use preceding apparent clearly demarcated；Subject does not occur local skin adverse reaction, also without apocleisis,
The systemic adverse reactions such as diarrhoea, weak, endocrine disturbance；
Use the effect of the protein chelates mildy wash of embodiment 2：
Subject totally 50 people, wherein male 13 people, the people of female 37.After one month, subject represents to use the albumen chela of embodiment 1
Close the salubrious non-greasy of face after mildy wash, can effectively clean dirt, and skin keep for a long time moistening, salubrious compact and it is rich
Elasticity, face mask lines ratio use preceding apparent clearly demarcated；Subject does not occur local skin adverse reaction, also without apocleisis,
The systemic adverse reactions such as diarrhoea, weak, endocrine disturbance.
Claims (5)
1. a kind of protein chelates mildy wash, it is characterised in that it is made up of the raw material of following weight parts：
Sodium alginate 1-2, ethylmaltol 0.5-1, ethylenediamine tetra-acetic acid 3-4, sorbitan monostearate 0.1-0.2, chlorination
Magnesium 0.6-1, fermentation protein emulsion 36-40, plants essential oil 2-4, Cocoamidopropyl betaine 0.7-1, ZPT 0.1-
0.2。
2. a kind of protein chelates mildy wash according to claim 1, it is characterised in that described plants essential oil is changed by fan
What one or more of mixing in essential oil, Rosa Damascana, tea tree ethereal oil formed.
A kind of 3. protein chelates mildy wash according to claim 1, it is characterised in that described fermentation protein emulsion be by
The raw material composition of following weight parts：
Fish scale 25-30, pigskin 14-20, folium isatidis 3-5, peppermint 1-2, sorbester p17 0.1-0.2.
A kind of 4. protein chelates mildy wash according to claim 3, it is characterised in that the system of described fermentation protein emulsion
Preparation Method comprises the following steps：
（1）Folium isatidis, peppermint mixing are taken, is added in the sodium hydroxide solution of 16-20 times of compound weight, at 65-70 DEG C
Insulated and stirred 1-2 hours, filtering, obtain sodium hydroxide filtrate；
（2）Fish scale, pigskin are cleaned up, wear into fine powder, is added in the hydrochloric acid solution of 10-15 times of fine powder weight, at 50-60 DEG C
Lower insulated and stirred 4-5 hours, filtering, filter residue is washed 3-4 times, drying, mixed with above-mentioned sodium hydroxide filtrate, be sent to boiling water
In bath, insulated and stirred 5-7 minutes, discharge, filtering, obtain protein solution；
（3）Above-mentioned protein solution is taken, adds its weight 1-2% lactic acid bacteria, sealing thermal insulation 10-13 hours, go out at 30-35 DEG C
Material, mixes with sorbester p17, stirs, obtain the fermentation protein emulsion.
5. a kind of preparation method of protein chelates mildy wash as claimed in claim 1, it is characterised in that comprise the following steps：
（1）Sodium alginate, ethylmaltol, magnesium chloride mixing are taken, is added in the deionized water of 30-40 times of compound weight,
Stir, obtain saline aqueous dispersions；
（2）Fermentation protein emulsion is taken, is added in above-mentioned saline aqueous dispersions, stirs, be sent in 70-75 DEG C of water-bath,
Ethylenediamine tetra-acetic acid is added, insulated and stirred 1-2 hours, discharging, ZPT is added, stirs to normal temperature, it is molten to obtain protein chelates
Liquid；
（3）Above-mentioned protein chelates solution is taken, is mixed with above-mentioned Cocoamidopropyl betaine, is concentrated at 35-45 DEG C relative
Density is 1-1.3 thick liquid, adds remaining each raw material, ultrasonic 2-3 minutes, produces the protein chelates mildy wash.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022266943A1 (en) * | 2021-06-24 | 2022-12-29 | L'oreal | Composition for cleansing and/or removing makeups from keratin materials |
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