CN104983652A - Manufacturing method of toothpaste and toothpaste - Google Patents
Manufacturing method of toothpaste and toothpaste Download PDFInfo
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- CN104983652A CN104983652A CN201510262767.6A CN201510262767A CN104983652A CN 104983652 A CN104983652 A CN 104983652A CN 201510262767 A CN201510262767 A CN 201510262767A CN 104983652 A CN104983652 A CN 104983652A
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Abstract
The invention discloses toothpaste and a manufacturing method thereof. The toothpaste comprises 30-55 parts of calcium carbonate, 2-3 parts of an activity addition agent, 5-6 parts of a stabilizing agent, 0.01-0.1 part of saccharin, 0.5-1 part of sorbitol, 1-1.5 parts of glycerinum, 1-2 parts of propylene glycol, 1000 parts of deionized water, 1000 parts of purified water, 11 parts of an ionized calcium water solubility preparation, and 0.2-0.3 part of spice. The ionized calcium water solubility preparation is added into the toothpaste, is obtained through special technological processing high-temperature treatment, and is not bonded with acid groups; and after the ionized calcium water solubility preparation is dissolved into water, a complex with calcium as the principal and surrounding hydroxy radicals is formed, so that erosion of acid radicals to enamel is reduced so as to clean and strengthen teeth. Due to the fact that the ionized calcium water solubility preparation does not react with fluorochemicals, the ionized calcium water solubility preparation can be used as base materials of the toothpaste containing fluoride, enamel will not be damaged, the brightness of the toothpaste can be improved, and the toothpaste has the good tooth strengthening and cleaning force.
Description
Technical field
The present invention relates to the manufacture method of a kind of toothpaste and toothpaste.
Background technology
Calcium carbonate is a kind of conventional abrasive in toothpaste, and conventional precipitated calcium carbonate powder makes filler or carrier.Usually also have and limestone calcination is obtained calcium oxide, again calcium oxide is added in toothpaste, conventional superfine little calcium carbonate powder does filler, toothpaste is made up of multiple inorganic matter and Organic substance, and it comprises abrasivus, washing foam agent, binding agent, wetting agent, sweeting agent, aromatic and moisture.
Abrasivus is the main body of toothpaste, and conventional abrasivus has calcium carbonate (CaCO
3), calcium hydrogen phosphate (CaHPO
42H
2o), consumption is between 30% ~ 55%.In order to increase clean effect, the inside also needs to add washing foam agent sodium lauryl sulfate (ROSO
3na), consumption is about 2% ~ 3%.Toothpaste energy functions of whitening teeth is mainly by the effect of these two kinds of compositions.Abrasivus has certain frictional force, and washing foam agent has washing and the effect of foam occurs, and the two combines the effect adding toothbrush, just the dirt of dental surface can be brushed away, make teeth whitening as jade.
But calcium carbonate, calcium oxide, lactic acid can make the inorganic matter decalcification in sclerous tissues's enamel of tooth and cementum, dentin; organic substance decomposing; like this; the enamel on tooth top layer just loses protective effect; make tooth be subject to acidic materials to corrode; tooth itself does not have self-healing ability, in the course of time, just defines dental caries gradually.In recent years, in toothpaste, also add various medicine, make multi-medicament toothpaste.A good toothpaste, one squeezes, the mastic of pure white lubrication of just emerging gently.It should have graceful fragrance, the sweetness of appropriateness, fine and smooth mouthfeel and sufficient foam.
Summary of the invention
For the problems referred to above, the object of the present invention is to provide the manufacture method of a kind of toothpaste and toothpaste.
For achieving the above object, the manufacture method of a kind of toothpaste of the present invention, adds ionized calcium water soluble preparation in a step at least in making toothpaste process.
Preferably, the concrete steps making toothpaste are:
1), to 30-55 part calcium carbonate raw material cross 400-500 mesh sieve, and join in premix pot with 2-3 part active additive, 5-6 part stabilizing agent, 0.01-0.1 part glucide;
2), 0.5-1 part sorbitol, 1-1.5 part glycerol, 1-2 part propylene glycol and 1000 parts of deionized waters are joined in liquid material storage tank, fully stir 60-90 minute;
3), will 1000 parts of temperature of reverse osmosis ion exchanging pure water treating device process be adopted to be that the pure water of 3-4 DEG C and 1 part of ionized calcium water soluble preparation jointly join in the airtight water injection tank of 0.3MPA and fully dissolve 30-60 minute;
4), by step 3) in ionized calcium water soluble preparation water evenly join in cream pot processed with the flow velocity being greater than 500L/min, then by step 2) mixing liquid material in liquid material storage tank joins in cream pot processed, fully stirs 20-30 minute;
5), by step 1) in compound join step 4) in cream pot processed in, 10 parts of ionized calcium water soluble preparation powders are injected in cream pot processed with fluidization, 0.2-0.3 part spice is joined in cream pot processed, carry out quick scraper plate stirring be less than or equal to the environment of 40 DEG C again at maximum temperature under, homogenizing stir, grinding 20-30 minute, and carry out vacuum suction simultaneously and reach-0.095Mpa to vacuum;
6), by step 5) mastic raw material after process loads to store in pot and carries out ageing to room temperature.
For achieving the above object, a kind of toothpaste of the present invention, its composition comprises: 30-55 part calcium carbonate, 2-3 part active additive, 5-6 part stabilizing agent, 0.01-0.1 part glucide, 0.5-1 part sorbitol, 1-1.5 part glycerol, 1-2 part propylene glycol, 1000 parts of deionized waters, 1000 parts of pure water, 11 parts of ionized calcium water soluble preparations, 0.2-0.3 part spice.
Beneficial effect of the present invention is:
The present invention adds ionized calcium water soluble preparation in toothpaste, ionized calcium water soluble preparation obtains through special process processing high-temperature process, be not combined with acid group, the surrounding formed after molten water headed by calcium is all complex hydroxy, reduces acid group and can to clean the teeth teeth consolidating to adamantine erosion.Because its discord fluorochemical reacts, therefore also can be used as the base material of toothpaste with fluoride, can not enamel be damaged, and the brightness of toothpaste can be increased, and there is excellent teeth consolidating to clean the teeth power.When adding ionized calcium water soluble preparation in toothpaste, dispelling abnormal flavor removing halitosis can sterilize, preventing halitosis from also having certain effect.Also can prevent and treat dental caries, residue fermentation in oral cavity can be suppressed, make again the enamel strengthening teeth consolidating of dental surface.Also have good Combination, frictional force is strong, can tobacco dirty remover.
Detailed description of the invention
The present invention will be further described below.
A kind of toothpaste of the present invention, its composition comprises: 30-55 part calcium carbonate, 2-3 part active additive, 5-6 part stabilizing agent, 0.01-0.1 part glucide, 0.5-1 part sorbitol, 1-1.5 part glycerol, 1-2 part propylene glycol, 1000 parts of deionized waters, 1000 parts of pure water, 11 parts of ionized calcium water soluble preparations, 0.2-0.3 part spice.Wherein, the processing method of described ionized calcium water soluble preparation is made by following steps:
1, Concha Ostreae 90 kilograms, Margarita 70 kilograms, corallite 3 kilograms, Stalactitum 50 kilograms, Margarita powder 3-5 kilogram, Os Draconis 30 kilograms, Dens Draconis 5 kilograms, nine hole shellfish 50 kilograms and various eggshell and/or other shells 45-50 kilogram is prepared;
2, the existing technique of above-mentioned shell raw material is polished, grind off the impurity of shell surface, dirt, then carry out cleaning, screening, then crush above-mentioned shell raw material by existing technique; After other non-shell raw materials are cleaned, screening, then pulverize;
3, the raw material that step 2 processes is put into calcining furnace, be airtightly forced into 0.8mpa-1.6mpa, through the high-temperature calcination 30-60 minute of 800 DEG C-900 DEG C;
4, the raw material that step 3 is obtained, utilize plasma to prepare ultrafine nanometer calcium oxide technology to comprise, with Radio-frequency plasma torch, air or oxygen or nitrogen are made plasma at 1000 ~ 3000 DEG C of temperature, then in plasma reactor by raw material at 1000 ~ 3000 DEG C, the time of staying is be decomposed into ultrafine particle calcium oxide and carbon dioxide under the condition of 0.1 ~ 0.5 second, then through supercooling, cyclonic separation, cloth bag is collected and is prepared the ultra-fine grain that granularity is less than 0.3 μm, can obtain water-soluble calcium preparation, and its calcium content, more than 50% (percentage by weight), also contains ferrum, potassium, sodium, zinc, magnesium, phosphorus, the various trace elements such as copper and mineral, product is pure white powder, and fineness of powder, more than 600 orders, is bitterness when the crowd of these water-soluble calcium preparation liver and gall imbalance drinks by operation instruction, spleen, stomach, intestinal, the crowd of lung imbalance is micro-astringent taste when drinking by operation instruction, kidney, the crowd of bladder imbalance is micro-fishy smell when drinking by operation instruction, the heart, blood, the crowd of small intestinal imbalance is acescency when drinking by operation instruction, is slight nausea sense when cerebral nervous system imbalance and Low crowd drink by operation instruction, is sweet sense of taste when healthy population is drunk by operation instruction.
Described ionized calcium water soluble preparation is the master batch group of one kind of multiple trace element and mineral before bath, after bath, the surrounding formed headed by calcium is all complex hydroxy, it is ionized calcium activated water, easily be absorbed by the body, after bath, pH value is 14, aobvious alkalescence, can regulate the acid-base balance of human body, supplements various trace elements and the mineral of needed by human body.Ionized calcium water soluble preparation of the present invention can toxin expelling, regulate acid-base balance, supplement calcium and various trace elements and mineral.And the acid poison can isolated rapidly in fruit and vegerable food.When the best using state of ionized calcium water soluble preparation of the present invention is water temperature 4 degree, every 0.4 gram of punching 1000 milliliters of dissolved in purified water the bests, it is best that empty stomach drinks effect.The effect that ionized calcium water soluble preparation of the present invention smears wound hemostasis under pulverulence is very good, can also direct powder to smear mosquito bite place antipruritic, and spray at present in pulverulence and have abnormal flavour article to get on the excellent that eliminates the unusual smell; Every 0.4 gram of punching 1200 ml tap water water soaking veterinary antibiotics, raw meat class etc. remove pesticide residues and hormone residues best results in 10-30 minute.When arranging food, it is better to add the food mouthfeel after cooking on a small quantity, can also fresh-keeping foodstuff, the deteriorating time of food and extend.Every 0.4 gram of punching 500 milliliters of pure water are drunk, and can obtain effect of well relieving the effect of alcohol.
Embodiment 1:
A kind of manufacture method of toothpaste described in the present embodiment, adds ionized calcium water soluble preparation in a step at least in making toothpaste process.
Concrete steps are:
1), to 30 parts of calcium carbonate raw materials cross 400 mesh sieves, and join in premix pot with 2 parts of active additives, 5 parts of stabilizing agents, 0.01 part of glucide;
2), 0.5 part of sorbitol, 1 part of glycerol, 1 part of propylene glycol and 1000 parts of deionized waters are joined in liquid material storage tank, fully stir 60 minutes;
3), will 1000 parts of temperature of reverse osmosis ion exchanging pure water treating device process be adopted to be that the pure water of 3 DEG C and 1 part of ionized calcium water soluble preparation jointly join in the airtight water injection tank of 0.3MPA and fully dissolve 30 minutes;
4), by step 3) in ionized calcium water soluble preparation water evenly join in cream pot processed with the flow velocity being greater than 500L/min, then by step 2) mixing liquid material in liquid material storage tank joins in cream pot processed, fully stir 20 minutes;
5), by step 1) in compound join step 4) in cream pot processed in, 10 parts of ionized calcium water soluble preparation powders are injected in cream pot processed with fluidization, 0.2 part of spice is joined in cream pot processed, carry out quick scraper plate stirring be less than or equal to the environment of 40 DEG C again at maximum temperature under, homogenizing stir, grinding 20 minutes, and carry out vacuum suction simultaneously and reach-0.095Mpa to vacuum;
6), by step 5) mastic raw material after process loads to store in pot and carries out ageing to room temperature.
Embodiment 2:
A kind of manufacture method of toothpaste described in the present embodiment, adds ionized calcium water soluble preparation in a step at least in making toothpaste process.
Concrete steps are:
1), to 55 parts of calcium carbonate raw materials cross 500 mesh sieves, and join in premix pot with 3 parts of active additives, 6 parts of stabilizing agents, 0.1 part of glucide;
2), 1 part of sorbitol, 1.5 parts of glycerol, 2 parts of propylene glycol and 1000 parts of deionized waters are joined in liquid material storage tank, fully stir 90 minutes;
3), will 1000 parts of temperature of reverse osmosis ion exchanging pure water treating device process be adopted to be that the pure water of 4 DEG C and 1 part of ionized calcium water soluble preparation jointly join in the airtight water injection tank of 0.3MPA and fully dissolve 60 minutes;
4), by step 3) in ionized calcium water soluble preparation water evenly join in cream pot processed with the flow velocity being greater than 500L/min, then by step 2) mixing liquid material in liquid material storage tank joins in cream pot processed, fully stir 30 minutes;
5), by step 1) in compound join step 4) in cream pot processed in, 10 parts of ionized calcium water soluble preparation powders are injected in cream pot processed with fluidization, 0.3 part of spice is joined in cream pot processed, carry out quick scraper plate stirring be less than or equal to the environment of 40 DEG C again at maximum temperature under, homogenizing stir, grinding 30 minutes, and carry out vacuum suction simultaneously and reach-0.095Mpa to vacuum;
6), by step 5) mastic raw material after process loads to store in pot and carries out ageing to room temperature.
Embodiment 3:
A kind of manufacture method of toothpaste described in the present embodiment, adds ionized calcium water soluble preparation in a step at least in making toothpaste process.
Concrete steps are:
1), to 40 parts of calcium carbonate raw materials cross 450 mesh sieves, and join in premix pot with 2.5 parts of active additives, 5.5 parts of stabilizing agents, 0.05 part of glucide;
2), 0.75 part of sorbitol, 1.2 parts of glycerol, 1.5 parts of propylene glycol and 1000 parts of deionized waters are joined in liquid material storage tank, fully stir 80 minutes;
3), will 1000 parts of temperature of reverse osmosis ion exchanging pure water treating device process be adopted to be that the pure water of 3.5 DEG C and 1 part of ionized calcium water soluble preparation jointly join in the airtight water injection tank of 0.3MPA and fully dissolve 30-60 minute;
4), by step 3) in ionized calcium water soluble preparation water evenly join in cream pot processed with the flow velocity being greater than 500L/min, then by step 2) mixing liquid material in liquid material storage tank joins in cream pot processed, fully stir 25 minutes;
5), by step 1) in compound join step 4) in cream pot processed in, 10 parts of ionized calcium water soluble preparation powders are injected in cream pot processed with fluidization, 0.25 part of spice is joined in cream pot processed, carry out quick scraper plate stirring be less than or equal to the environment of 40 DEG C again at maximum temperature under, homogenizing stir, grinding 25 minutes, and carry out vacuum suction simultaneously and reach-0.095Mpa to vacuum;
6), by step 5) mastic raw material after process loads to store in pot and carries out ageing to room temperature.
The present invention adds ionized calcium water soluble preparation in toothpaste, ionized calcium water soluble preparation obtains through special process processing high-temperature process, be not combined with acid group, the surrounding formed after molten water headed by calcium is all complex hydroxy, reduces acid group and can to clean the teeth teeth consolidating to adamantine erosion.Because its discord fluorochemical reacts, therefore also can be used as the base material of toothpaste with fluoride, can not enamel be damaged, and the brightness of toothpaste can be increased, and there is excellent teeth consolidating to clean the teeth power.When adding ionized calcium water soluble preparation in toothpaste, dispelling abnormal flavor removing halitosis can sterilize, preventing halitosis from also having certain effect.Also can prevent and treat dental caries, residue fermentation in oral cavity can be suppressed, make again the enamel strengthening teeth consolidating of dental surface.Also have good Combination, frictional force is strong, can tobacco dirty remover.
Above; be only preferred embodiment of the present invention, but protection scope of the present invention is not limited thereto, is anyly familiar with those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed within protection scope of the present invention.Therefore, the protection domain that protection scope of the present invention should define with claim is as the criterion.
Claims (3)
1. a manufacture method for toothpaste, is characterized in that, adds ionized calcium water soluble preparation in a step at least in making toothpaste process.
2. the manufacture method of toothpaste according to claim 1, is characterized in that, the concrete steps making toothpaste are:
1), to 30-55 part calcium carbonate raw material cross 400-500 mesh sieve, and join in premix pot with 2-3 part active additive, 5-6 part stabilizing agent, 0.01-0.1 part glucide;
2), 0.5-1 part sorbitol, 1-1.5 part glycerol, 1-2 part propylene glycol and 1000 parts of deionized waters are joined in liquid material storage tank, fully stir 60-90 minute;
3), will 1000 parts of temperature of reverse osmosis ion exchanging pure water treating device process be adopted to be that the pure water of 3-4 DEG C and 1 part of ionized calcium water soluble preparation jointly join in the airtight water injection tank of 0.3MPA and fully dissolve 30-60 minute;
4), by step 3) in ionized calcium water soluble preparation water evenly join in cream pot processed with the flow velocity being greater than 500L/min, then by step 2) mixing liquid material in liquid material storage tank joins in cream pot processed, fully stirs 20-30 minute;
5), by step 1) in compound join step 4) in cream pot processed in, 10 parts of ionized calcium water soluble preparation powders are injected in cream pot processed with fluidization, 0.2-0.3 part spice is joined in cream pot processed, carry out quick scraper plate stirring be less than or equal to the environment of 40 DEG C again at maximum temperature under, homogenizing stir, grinding 20-30 minute, and carry out vacuum suction simultaneously and reach-0.095Mpa to vacuum;
6), by step 5) mastic raw material after process loads to store in pot and carries out ageing to room temperature.
3. a toothpaste, it is characterized in that, its composition comprises: 30-55 part calcium carbonate, 2-3 part active additive, 5-6 part stabilizing agent, 0.01-0.1 part glucide, 0.5-1 part sorbitol, 1-1.5 part glycerol, 1-2 part propylene glycol, 1000 parts of deionized waters, 1000 parts of pure water, 11 parts of ionized calcium water soluble preparations, 0.2-0.3 part spice.
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| CN201510262767.6A CN104983652A (en) | 2015-05-22 | 2015-05-22 | Manufacturing method of toothpaste and toothpaste |
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|---|---|---|---|
| CN201510262767.6A CN104983652A (en) | 2015-05-22 | 2015-05-22 | Manufacturing method of toothpaste and toothpaste |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106726968A (en) * | 2016-12-27 | 2017-05-31 | 郑州游爱网络技术有限公司 | A kind of function toothpaste for carcinoma of mouth rehabilitation |
| CN111494289A (en) * | 2020-04-26 | 2020-08-07 | 广西医科大学 | Compound oyster tooth-protecting toothpaste and preparation method thereof |
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| CN102716154A (en) * | 2012-06-28 | 2012-10-10 | 舒文一 | Processing method and product of ionized calcium water-solubility preparation |
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2015
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102716154A (en) * | 2012-06-28 | 2012-10-10 | 舒文一 | Processing method and product of ionized calcium water-solubility preparation |
Non-Patent Citations (3)
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106726968A (en) * | 2016-12-27 | 2017-05-31 | 郑州游爱网络技术有限公司 | A kind of function toothpaste for carcinoma of mouth rehabilitation |
| CN111494289A (en) * | 2020-04-26 | 2020-08-07 | 广西医科大学 | Compound oyster tooth-protecting toothpaste and preparation method thereof |
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Application publication date: 20151021 |
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| RJ01 | Rejection of invention patent application after publication |