CN105616319B - A kind of toothpaste and preparation method thereof - Google Patents
A kind of toothpaste and preparation method thereof Download PDFInfo
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- CN105616319B CN105616319B CN201610004599.5A CN201610004599A CN105616319B CN 105616319 B CN105616319 B CN 105616319B CN 201610004599 A CN201610004599 A CN 201610004599A CN 105616319 B CN105616319 B CN 105616319B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/618—Molluscs, e.g. fresh-water molluscs, oysters, clams, squids, octopus, cuttlefish, snails or slugs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
Abstract
The invention belongs to technical field of daily necessities, and in particular to a kind of toothpaste and preparation method thereof.The toothpaste includes that the raw material of following parts by weight is prepared：40 50 parts of rubbing agents, 10 30 parts of moisturizer, 1.5 2.5 parts of foaming agents, 12 parts of thickeners, 0.5 1.5 parts of fragrance, 0.1 0.5 parts of sweeteners, 0.1 0.5 portions of preservatives, 15 20 parts of deep-sea fish bone meals, 0.4 0.5 parts of pearl powders and 20 50 parts of water.Beneficial effects of the present invention are：Containing the other components synergistic effect in deep-sea fish bone meal and pearl powder, with toothpaste in toothpaste provided by the invention, it can effectively inhibit bleeding gums; tooth-whitening, and potent calculus dentalis can be dispelled, keep tooth firmer; the formation that plaque can effectively be inhibited simultaneously, preferably takes care of one's teeth.
Description
Technical field
The invention belongs to technical field of daily necessities, and in particular to a kind of toothpaste and preparation method thereof.
Background technology
Today's society, people increasingly pay close attention to the oral hygiene of oneself and health, and the pure white tooth of a bite becomes many people
The target of pursuit, how tooth-whitening and effectively remove dental surface plaque just become scientific research field concern project.
Toothpaste is common cleaning supplies in daily life, there is very long history.With the continuous hair of science and technology
Exhibition, technological equipment continuously improve and it is perfect, various types of toothpaste are come out one after another, and the quality and grade of product is continuously improved,
Present toothpaste variety develops into great variety of goods by single clean type toothpaste, vdiverse in function, a brands up to a hundred it is multi-functional
Type toothpaste meets the needs of the different levels level of consumption.
Invention content
In order to solve the above problem of the existing technology, the present invention provides a kind of toothpaste and preparation method thereof.
The technical solution adopted in the present invention is：
A kind of toothpaste, including the raw material of following parts by weight are prepared：40-50 parts of rubbing agents, 10-30 parts of moisturizer,
1.5-2.5 parts of foaming agents, 1-2 parts of thickeners, 0.5-1.5 parts of fragrance, 0.1-0.5 parts of sweeteners, 0.1-0.5 parts of preservatives, 15-
20 parts of deep-sea fish bone meals, 0.4-0.5 parts of pearl powders and 20-50 parts of water.
Further, the toothpaste includes that the raw material of following parts by weight is prepared：43-49 parts of rubbing agents, 15-28 parts of guarantors
Humectant, 1.8-2.4 part foaming agent, 1.3-1.8 parts of thickeners, 0.8-1.2 parts of fragrance, 0.2-0.4 parts of sweeteners, 0.2-0.4 parts
Preservative, 17-19 part deep-sea fish bone meal, 0.4-0.5 parts of pearl powders and 25-40 parts of water.
Further, the toothpaste includes that the raw material of following parts by weight is prepared：48 parts of rubbing agents, 27 parts of moisturizer,
2.3 parts of foaming agents, 1.6 parts of thickeners, 1 part of fragrance, 0.3 part of sweetener, 0.3 portion of preservative, 18 parts of deep-sea fish bone meals, 0.5 part
Pearl powder and 32 parts of water.
The toothpaste further includes that the raw material of following parts by weight is prepared：0.1-2 parts of additives.The additive includes water
One kind in molten mill base, Yu Jiechun, dipotassium glycyrrhizinate, silica, propylene glycol or at least two combination.
Water-soluble mill base plays hyperchromic effect in the toothpaste of the present invention.Dipotassium glycyrrhizinate is white or off-white color fine powder
End, purity have a special sweet taste up to 98%, it is water-soluble it is good, mouthfeel is pure.With a variety of work(such as antibacterial, anti-inflammatory, removing toxic substances, antiallergic, deodorization
Effect.
The chemical name of Yu Jiechun is triclosan, is commonly called as triclosan.Belong to antibacterial in toothpaste provided by the invention
Agent has antimicrobial component, is a kind of antibacterial medicines of multiple-effect, can be with fluoride compatibility.
The deep-sea fish bone meal is the powder of natural deep-sea fish bone, is mainly derived from cuttlebone, is black Quarry sections animal needleless crow
The inner casing of Quarry or Golden Crow Quarry, main component are calcium carbonate, have the effect of hemostasis, whitening.
Pearl powder can tooth-whitening, it is tasty and refreshing smelly.
The rubbing agent includes mountain flour, calcium phosphate dibasic dihydrate or combinations thereof.Mountain flour is natural whiting, also known as calcite
Powder is that one kind cleans the teeth the strong abrasive material of power, is used in combination with silica that the power that cleans the teeth is strong and does not damage dentine.Two hypophosphite monohydrate hydrogen
Calcium is white powder, is a kind of abrasive material mild, friction is low, the bright and clean exquisiteness of lotion is made, if being compounded with anhydrous calcium phosphate clean
Tooth forces are stronger.
The moisturizer includes sorbierite, polyethylene glycol or combinations thereof.The full name of sorbierite is D- D-sorbites, is glycerine
Substitute, moisture retention compared with glycerine mitigate, taste is also preferable, is used cooperatively with glycerine, manufactured toothpaste diffusivity and thixotropy
More preferably.Polyethylene glycol have thickening, moisture-keeping functions, be used as toothpaste thicken moisturizer, especially in transparent toothpaste use can increase
Gel toothpaste clarity and stripping.
The foaming agent includes lauryl sodium sulfate.Lauryl sodium sulfate abbreviation K-12 is a kind of anionic surface
Activating agent has good blistering, emulsification, infiltration, detergency performance, mainly makees foaming agent in toothpaste, detergent uses.
The thickener includes carboxymethylcellulose sodium, xanthans, SM gels or combinations thereof.Carboxymethylcellulose sodium is referred to as
CMC is most common thickener in domestic toothpaste, has the function of thickening, stablizes, bonding lotion, with silica, xanthans
Deng compounding, salt resistance, the antienzyme performance of toothpaste of the present invention can be further increased, and keep lotion finer and smoother, bright.Xanthans and SM
Gel plays the role of stablizing and thickening in the toothpaste of the present invention.
The fragrance includes fruit essence and Mint Essence.Fragrance used in the present invention is pure and fresh elegant, and refrigerant tasty and refreshing will be natural
Fragrance and artificial perfume are formulated by proper proportion reconciliation, and the fragrance also can directly be bought, or according to prior art system
It is standby to obtain.
The sweetener includes saccharin sodium, sorbierite or combinations thereof；Saccharin sodium coordinates with essence, can improve the mouth of toothpaste
Taste.
The preservative includes nipagin ethylester.Ethylparaben is white crystals thing, mildly bitter flavor, fiber crops of burning.It is mainly used as
The sterilization antiseptic of food, cosmetics, medicine.
The present invention also provides a kind of preparation methods of above-mentioned toothpaste, include the following steps：
Thickener, moisturizer and foaming agent are dissolved in the water by step 1, are uniformly dissolved, obtain mixed solution；
Step 2 mixes the deep-sea fish bone meal and the pearl powder, is ground, obtains deep-sea fish bone meal and pearl
Powder mixture；
Step 3, be added into step 1 gained mixed solution step 2 gained deep-sea fish bone meal and pearl powder mixture and
Surplus stock finally adds fragrance, obtains raw mixture；
The raw mixture is stirred, mediates, grinds by step 4, vacuumizes simultaneously, obtains lotion；
The lotion is stood 1.5-3 hours by step 5, so that it is naturally cooled to room temperature, tinning, packaging obtain the tooth
Cream.
Further, in step 1, the thickener, moisturizer and foaming agent are dissolved in water in being pre-dissolved pot or premix pot.Step
In rapid 2, the grain size of the deep-sea fish bone meal and pearl powder mixture is 1-20 μm.In step 3, the mixed solution is former with residue
Material mixes in cream pot processed.In step 4, vacuumizing makes vacuum degree reach 0.09-0.1Mpa, time 40-60min.It mediates, grind
Temperature control is at 45 DEG C or less when mill.
Beneficial effects of the present invention are：Containing in deep-sea fish bone meal and pearl powder, with toothpaste in toothpaste provided by the invention
Other components synergistic effect, can effectively inhibit bleeding gums, tooth-whitening, and potent can dispel calculus dentalis, make tooth
It is firmer, while can effectively inhibit the formation of plaque, preferably take care of one's teeth.
Specific implementation mode
Embodiment 1
The present invention provides the raw materials of a kind of toothpaste, including following parts by weight to be prepared：40g rubbing agents, 10g moisturizings
Agent, 2.5g foaming agents, 2g thickeners, 0.5g fragrance, 0.5g sweeteners, 0.1g preservatives, 0.1g additives, 20g deep-sea fish bones
Powder, 0.5g pearl powders and 20g water.
Wherein, the deep-sea fish bone meal is the powder of natural deep-sea fish bone, is mainly derived from cuttlebone；The rubbing agent is stone
Powder；The moisturizer is the combination of sorbierite and polyethylene glycol, quality 1:1；The foaming agent is lauryl sodium sulfate；
The thickener is the combination of CMC, xanthans and SM gels, mass ratio 1:1:1；The fragrance is fruit essence；It is described
Sweetener is sorbierite；The preservative is nipagin ethylester；Additive includes water-soluble mill base, Yu Jiechun and dipotassium glycyrrhizinate,
Its mass ratio is 1:1:1.
Preparation method includes the following steps：
Thickener, moisturizer and foaming agent are dissolved in the water by step 1, are uniformly dissolved in being pre-dissolved pot, obtain mixing molten
Liquid；
Step 2 mixes the deep-sea fish bone meal and the pearl powder, is ground, and obtains the depth that grain size is 1-20 μm
Ocean fish bone meal and pearl powder mixture；
Step 3 pours into step 1 gained mixture solution in cream pot processed, is added obtained by step 2 into the mixed solution
Deep-sea fish bone meal and pearl powder mixture and surplus stock, are first added liquid material, add powder, finally add fragrance, obtain
Raw mixture；
The raw mixture is stirred, mediates, grinds by step 4, vacuumizes simultaneously, vacuum degree is made to reach
0.09Mpa, time 40min, obtains lotion；During cream processed, because kneading, process of lapping can rub heat release, therefore in the summer
Season need to use chuck cooling water control temperature≤45 DEG C.
The lotion is stood 1.5 hours by step 5, so that it is naturally cooled to room temperature, while lotion being made fully to expand to be formed
Homogeneous adherend improves the elasticity of lotion, and tinning later, packaging obtain the toothpaste.
Embodiment 2
The present invention provides the raw materials of a kind of toothpaste, including following parts by weight to be prepared：50g rubbing agents, 30g moisturizings
Agent, 1.5g foaming agents, 1g thickeners, 1.5g fragrance, 0.1g sweeteners, 0.5g preservatives, 2g additives, 15g deep-sea fish bone meals,
0.4g pearl powders and 50g water.
Wherein, the deep-sea fish bone meal is the powder of natural deep-sea fish bone, is mainly derived from cuttlebone；The rubbing agent is stone
The combination of powder and calcium phosphate dibasic dihydrate, mass ratio 1:1；The moisturizer is sorbierite；The foaming agent is dodecane
Base sodium sulphate；The thickener is the combination of CMC and xanthans, mass ratio 1:1；The fragrance is Mint Essence；It is described
Sweetener is saccharin sodium；The preservative is nipagin ethylester；Additive is water-soluble mill base, Yu Jiechun, dipotassium glycyrrhizinate, dioxy
SiClx and propylene glycol, arbitrary proportion mixing.
Preparation method includes the following steps：
Thickener, moisturizer and foaming agent are dissolved in the water by step 1, are uniformly dissolved in being pre-dissolved pot, obtain mixing molten
Liquid；
Step 2 mixes the deep-sea fish bone meal and the pearl powder, is ground, and obtains the depth that grain size is 1-20 μm
Ocean fish bone meal and pearl powder mixture；
Step 3 pours into step 1 gained mixture solution in cream pot processed, is added obtained by step 2 into the mixed solution
Deep-sea fish bone meal and pearl powder mixture and surplus stock, are first added liquid material, add powder, finally add fragrance, obtain
Raw mixture；
The raw mixture is stirred, mediates, grinds by step 4, vacuumizes simultaneously, vacuum degree is made to reach
0.1Mpa, time 60min, obtains lotion；During cream processed, because kneading, process of lapping can rub heat release, therefore in summer
Chuck cooling water control temperature≤45 DEG C need to be used.
The lotion is stood 3 hours by step 5, it is made to naturally cool to room temperature, while it is equal so that lotion is fully expanded formation
The adherend of phase improves the elasticity of lotion, and tinning later, packaging obtain the toothpaste.
Embodiment 3
The present invention provides the raw materials of a kind of toothpaste, including following parts by weight to be prepared：43g rubbing agents, 15g moisturizings
Agent, 1.8g foaming agents, 1.3g thickeners, 1.2g fragrance, 0.2g sweeteners, 0.2g preservatives, 0.3g additives, 19g deep-sea fish
Bone meal, 0.4g pearl powders and 25g water.
Wherein, the deep-sea fish bone meal is the powder of natural deep-sea fish bone, is mainly derived from cuttlebone；The rubbing agent is two
Hypophosphite monohydrate hydrogen calcium；The moisturizer is polyethylene glycol；The foaming agent is lauryl sodium sulfate；The thickener is solidifying for SM
Glue；The fragrance is Mint Essence；The sweetener is saccharin sodium；The preservative is nipagin ethylester；Additive is Radix Glycyrrhizae
Sour dipotassium.
Preparation method includes the following steps：
Thickener, moisturizer and foaming agent are dissolved in the water by step 1, are uniformly dissolved in being pre-dissolved pot, obtain mixing molten
Liquid；
Step 2 mixes the deep-sea fish bone meal and the pearl powder, is ground, and obtains the depth that grain size is 1-20 μm
Ocean fish bone meal and pearl powder mixture；
Step 3 pours into step 1 gained mixture solution in cream pot processed, is added obtained by step 2 into the mixed solution
Deep-sea fish bone meal and pearl powder mixture and surplus stock, are first added liquid material, add powder, finally add fragrance, obtain
Raw mixture；
The raw mixture is stirred, mediates, grinds by step 4, vacuumizes simultaneously, vacuum degree is made to reach
0.096Mpa, time 50min, obtains lotion；During cream processed, because kneading, process of lapping can rub heat release, therefore in the summer
Season need to use chuck cooling water control temperature≤45 DEG C.
The lotion is stood 2 hours by step 5, it is made to naturally cool to room temperature, while it is equal so that lotion is fully expanded formation
The adherend of phase improves the elasticity of lotion, and tinning later, packaging obtain the toothpaste.
Embodiment 4
The present invention provides the raw materials of a kind of toothpaste, including following parts by weight to be prepared：49g rubbing agents, 28g moisturizings
Agent, 2.4g foaming agents, 1.8g thickeners, 0.8g fragrance, 0.4g sweeteners, 0.4g preservatives, 1.5g additives, 17g deep-sea fish
Bone meal, 0.5g pearl powders and 40g water.
Wherein, the deep-sea fish bone meal is the powder of natural deep-sea fish bone, is mainly derived from cuttlebone；The rubbing agent is stone
Powder；The moisturizer is sorbierite；The foaming agent is lauryl sodium sulfate；The thickener is xanthans；The fragrance
For Mint Essence；The sweetener is sorbierite；The preservative is nipagin ethylester；Additive is dipotassium glycyrrhizinate.
Preparation method includes the following steps：
Thickener, moisturizer and foaming agent are dissolved in the water by step 1, are uniformly dissolved in being pre-dissolved pot, obtain mixing molten
Liquid；
Step 2 mixes the deep-sea fish bone meal and the pearl powder, is ground, and obtains the depth that grain size is 1-20 μm
Ocean fish bone meal and pearl powder mixture；
Step 3 pours into step 1 gained mixture solution in cream pot processed, is added obtained by step 2 into the mixed solution
Deep-sea fish bone meal and pearl powder mixture and surplus stock, are first added liquid material, add powder, finally add fragrance, obtain
Raw mixture；
The raw mixture is stirred, mediates, grinds by step 4, vacuumizes simultaneously, vacuum degree is made to reach
0.096Mpa, time 50min, obtains lotion；During cream processed, because kneading, process of lapping can rub heat release, therefore in the summer
Season need to use chuck cooling water control temperature≤45 DEG C.
The lotion is stood 2 hours by step 5, it is made to naturally cool to room temperature, while it is equal so that lotion is fully expanded formation
The adherend of phase improves the elasticity of lotion, and tinning later, packaging obtain the toothpaste.
Embodiment 5
The present invention provides the raw materials of a kind of toothpaste, including following parts by weight to be prepared：48g rubbing agents, 27g moisturizings
Agent, 2.3g foaming agents, 1.6g thickeners, 1g fragrance, 0.3g sweeteners, 0.3g preservatives, 1.3g additives, 18g deep-sea fish bones
Powder, 0.5g pearl powders and 32g water.
Wherein, the deep-sea fish bone meal is the powder of natural deep-sea fish bone, is mainly derived from cuttlebone；The rubbing agent is stone
The combination of powder and calcium phosphate dibasic dihydrate, mass ratio 1:1；The moisturizer is sorbierite；The foaming agent is dodecane
Base sodium sulphate；The thickener is the combination of CMC and xanthans, mass ratio 1:1；The fragrance is Mint Essence；It is described
Sweetener is saccharin sodium；The preservative is nipagin ethylester；Additive be water-soluble mill base, dipotassium glycyrrhizinate and silica,
Arbitrary proportion mixes.
Preparation method includes the following steps：
Thickener, moisturizer and foaming agent are dissolved in the water by step 1, are uniformly dissolved in being pre-dissolved pot, obtain mixing molten
Liquid；
Step 2 mixes the deep-sea fish bone meal and the pearl powder, is ground, and obtains the depth that grain size is 1-20 μm
Ocean fish bone meal and pearl powder mixture；
Step 3 pours into step 1 gained mixture solution in cream pot processed, is added obtained by step 2 into the mixed solution
Deep-sea fish bone meal and pearl powder mixture and surplus stock, are first added liquid material, add powder, finally add fragrance, obtain
Raw mixture；
The raw mixture is stirred, mediates, grinds by step 4, vacuumizes simultaneously, vacuum degree is made to reach
0.096Mpa, time 50min, obtains lotion；During cream processed, because kneading, process of lapping can rub heat release, therefore in the summer
Season need to use chuck cooling water control temperature≤45 DEG C.
The lotion is stood 2 hours by step 5, it is made to naturally cool to room temperature, while it is equal so that lotion is fully expanded formation
The adherend of phase improves the elasticity of lotion, and tinning later, packaging obtain the toothpaste.
300 are randomly selected, the toothpaste provided sooner or later using 1-5 of the embodiment of the present invention daily observes tooth effect, black tooth
Tooth can see apparent effect once or so week, persistently this product be used to reach more than January, tooth whitening rate is sent out up to 95%
On；For thering is tooth Huang, the crowd of calculus dentalis to be reached using this product and more than January reach whitening effect；It is provided by the invention
Toothpaste potent can dispel calculus dentalis, have good whitening effect, effectively inhibit bleeding gums, keep tooth firmer, simultaneously
The formation that plaque can effectively be inhibited, preferably takes care of one's teeth.
Effect example 1
Liu, female, 20 years old, tooth jaundice had calculus dentalis, the toothpaste provided sooner or later using the embodiment of the present invention 1 daily, and one
After a month, teeth whiter, calculus dentalis is reduced, and after three months, calculus dentalis disappears.
Effect example 2
Ren, man, 30 years old, tooth blacked, the toothpaste provided sooner or later using the embodiment of the present invention 2 daily, after one week, tooth
Tooth bleaches.
Effect example 3
Mr. Bao, female, 33 years old, frequent bleeding gums when brushing teeth, the toothpaste provided sooner or later using the embodiment of the present invention 4 daily,
Bleeding gums number is reduced, and after one month, bleeding gums disappear.
Effect example 4
Zhang, man, 38 years old, tooth blacked, and has plaque, the toothpaste provided sooner or later using the embodiment of the present invention 5 daily, and one
After week, teeth whiter, plaque is reduced, and after one month, plaque disappears.
The present invention is not limited to above-mentioned preferred forms, anyone can show that other are various under the inspiration of the present invention
The product of form, however, make any variation on its formula or component, it is every that there is skill identical or similar to the present application
Art scheme, is within the scope of the present invention.
Claims (8)
1. a kind of toothpaste, it is characterised in that：Raw material including following parts by weight is prepared：40-50 parts of rubbing agents, 10-30 parts
Moisturizer, 1.5-2.5 part foaming agent, 1-2 parts of thickeners, 0.5-1.5 parts of fragrance, 0.1-0.5 parts of sweeteners, 0.1-0.5 parts it is anti-
Rotten agent, 15-20 parts of deep-sea fish bone meals, 0.4-0.5 parts of pearl powders and 20-50 parts of water；
The preparation method of the toothpaste, includes the following steps：
Thickener, moisturizer and foaming agent are dissolved in the water by step 1, are uniformly dissolved, obtain mixed solution；
Step 2 mixes the deep-sea fish bone meal and the pearl powder, is ground, and obtains deep-sea fish bone meal and pearl powder is mixed
Close object；The grain size of the deep-sea fish bone meal and pearl powder mixture is 1-20 μm.
2. toothpaste according to claim 1, it is characterised in that：Raw material including following parts by weight is prepared：43-49 parts
Rubbing agent, 15-28 part moisturizer, 1.8-2.4 parts of foaming agents, 1.3-1.8 parts of thickeners, 0.8-1.2 parts of fragrance, 0.2-0.4 parts
Sweetener, 0.2-0.4 portion preservative, 17-19 parts of deep-sea fish bone meals, 0.4-0.5 parts of pearl powders and 25-40 parts of water.
3. toothpaste according to claim 1, it is characterised in that：Raw material including following parts by weight is prepared：48 parts are rubbed
Liniment, 27 parts of moisturizer, 2.3 parts of foaming agents, 1.6 parts of thickeners, 1 part of fragrance, 0.3 part of sweetener, 0.3 portion of preservative, 18 parts
Deep-sea fish bone meal, 0.5 part of pearl powder and 32 parts of water.
4. toothpaste according to claim 1, it is characterised in that：Further include that the raw materials of following parts by weight is prepared：0.1-2
Part additive, the additive are water-soluble mill base and/or dipotassium glycyrrhizinate.
5. the preparation method of any toothpaste of claim 1-4, it is characterised in that：Include the following steps：
Thickener, moisturizer and foaming agent are dissolved in the water by step 1, are uniformly dissolved, obtain mixed solution；
Step 2 mixes the deep-sea fish bone meal and the pearl powder, is ground, and obtains deep-sea fish bone meal and pearl powder is mixed
The grain size of conjunction object, the deep-sea fish bone meal and pearl powder mixture is 1-20 μm；
Step 2 gained deep-sea fish bone meal and pearl powder mixture and residue are added into step 1 gained mixed solution for step 3
Raw material finally adds fragrance, obtains raw mixture；
The raw mixture is stirred, mediates, grinds by step 4, vacuumizes simultaneously, obtains lotion；
The lotion is stood 1.5-3 hours by step 5, so that it is naturally cooled to room temperature, tinning, packaging obtain the toothpaste.
6. the preparation method of toothpaste according to claim 5, it is characterised in that：In step 1, the thickener, moisturizer
With foaming agent water is dissolved in being pre-dissolved pot or premix pot.
7. the preparation method of toothpaste according to claim 5, it is characterised in that：In step 4, vacuumizing makes vacuum degree reach
0.09-0.1Mpa, time 40-60min.
8. the preparation method of toothpaste according to claim 5, it is characterised in that：Temperature control when in step 4, mediating, grinding
System is at 45 DEG C or less.
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| CN201610004599.5A CN105616319B (en) | 2016-01-06 | 2016-01-06 | A kind of toothpaste and preparation method thereof |
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| CN201610004599.5A CN105616319B (en) | 2016-01-06 | 2016-01-06 | A kind of toothpaste and preparation method thereof |
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| CN105616319B true CN105616319B (en) | 2018-07-31 |
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| CN106176544A (en) * | 2016-08-26 | 2016-12-07 | 吴敬华 | A kind of micro-calcium promoting and tooth-building toothpaste |
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| CN107362088A (en) * | 2017-08-15 | 2017-11-21 | 中国热带农业科学院南亚热带作物研究所 | A kind of toothpaste prepared with macadamia shell micro mist |
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| CN107854410A (en) * | 2017-11-30 | 2018-03-30 | 浙江海洋大学 | The preparation method of micro-nano fish-bone based toothpastes |
| CN110464694A (en) * | 2018-05-09 | 2019-11-19 | 上海牛樟芝生物技术有限公司 | One white hemostasis toothpaste |
| CN110946772A (en) * | 2019-12-27 | 2020-04-03 | 苏格格 | Toothpaste for preventing dental diseases and preparation method thereof |
| CN111346038A (en) * | 2020-04-09 | 2020-06-30 | 福州帝九生物科技有限公司 | Preparation method of toothpaste with effects of diminishing inflammation, inhibiting bacteria and removing tartar |
| CN111840159A (en) * | 2020-08-03 | 2020-10-30 | 深圳市有用功投资发展有限公司 | Herbal concentrated solution and preparation method thereof and preparation method of toothpaste |
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| CN1079645A (en) * | 1993-05-20 | 1993-12-22 | 程宝义 | Edible toothpaste for children |
| CN104414893A (en) * | 2013-08-23 | 2015-03-18 | 李霞 | Tooth care and whitening toothpaste |
| CN104800139A (en) * | 2015-03-02 | 2015-07-29 | 兰柳生 | Whitening toothpaste |
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| CN1771020A (en) * | 2003-04-04 | 2006-05-10 | 荷兰联合利华有限公司 | Process for the manufacture of an oral composition |
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|---|---|---|---|---|
| CN1079645A (en) * | 1993-05-20 | 1993-12-22 | 程宝义 | Edible toothpaste for children |
| CN104414893A (en) * | 2013-08-23 | 2015-03-18 | 李霞 | Tooth care and whitening toothpaste |
| CN104800139A (en) * | 2015-03-02 | 2015-07-29 | 兰柳生 | Whitening toothpaste |
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