CN105616319A - Toothpaste and preparation method thereof - Google Patents
Toothpaste and preparation method thereof Download PDFInfo
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- CN105616319A CN105616319A CN201610004599.5A CN201610004599A CN105616319A CN 105616319 A CN105616319 A CN 105616319A CN 201610004599 A CN201610004599 A CN 201610004599A CN 105616319 A CN105616319 A CN 105616319A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/618—Molluscs, e.g. fresh-water molluscs, oysters, clams, squids, octopus, cuttlefish, snails or slugs
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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Abstract
The invention belongs to the technical field of daily necessities, and particularly relates to toothpaste and a preparation method thereof. The toothpaste is prepared from the following raw materials in parts by weight: 40 to 50 parts of abrasive agent, 10 to 30parts of humectant, 1.5 to 2.5 parts of foaming agent, 1 to 2 parts of thickening agent, 0.5 to 1.5 parts of fragrance, 0.1-0.5 part of sweetening agent, 0.1-0.5 part of preservative, 15 to 20 parts of deep-sea fishbone meal, 0.4 to 0.5 part of pearl powder, and 20 to 50 parts of water. The toothpaste provided by the invention contains the deep-sea fishbone meal and the pearl powder which are cooperated with other components in the toothpaste, so that the bleeding gums can be effectively inhibited, teeth can be whitened, the dental calculus can be removed effectively, the teeth can be stronger, meanwhile, the generation of dental plaque can be effectively inhibited, and the teeth can be protected better.
Description
Technical field
The invention belongs to article of everyday use technical field, be specifically related to a kind of toothpaste and preparation method thereof.
Background technology
Society, people increasingly pay close attention to oneself oral hygiene with healthy, and the pure white tooth of a bite becomes the target that many people pursue, how tooth-whitening and effectively remove the dental plaque of dental surface and just become the problem that scientific research field is paid close attention to.
Toothpaste is cleaning supplies conventional in daily life, has very long history. Development along with science and technology, updating and perfect of technological equipment, various types of toothpaste are come out one after another, quality and the class of product improve constantly, present toothpaste variety by single clean type toothpaste, develops into great variety of goods, diverse in function, the Mobyneb toothpaste of up to a hundred brands, meets the needs of different levels level of consumption.
Summary of the invention
In order to solve the problems referred to above that prior art exists, the invention provides a kind of toothpaste and preparation method thereof.
The technical solution adopted in the present invention is:
A kind of toothpaste, the raw material including following weight portion is prepared from: 40-50 part abrasivus, 10-30 part wetting agent, 1.5-2.5 part foaming agent, 1-2 part thickening agent, 0.5-1.5 part spice, 0.1-0.5 part sweeting agent, 0.1-0.5 part preservative, 15-20 part deep-sea fish bone meal, 0.4-0.5 part Margarita powder and 20-50 part water.
Further, described toothpaste includes the raw material of following weight portion and is prepared from: 43-49 part abrasivus, 15-28 part wetting agent, 1.8-2.4 part foaming agent, 1.3-1.8 part thickening agent, 0.8-1.2 part spice, 0.2-0.4 part sweeting agent, 0.2-0.4 part preservative, 17-19 part deep-sea fish bone meal, 0.4-0.5 part Margarita powder and 25-40 part water.
Further, described toothpaste includes the raw material of following weight portion and is prepared from: 48 parts of abrasivuss, 27 parts of wetting agents, 2.3 parts of foaming agent, 1.6 parts of thickening agents, 1 part of spice, 0.3 part of sweeting agent, 0.3 portion of preservative, 18 parts of deep-sea fish bone meal, 0.5 part of Margarita powder and 32 parts of water.
Described toothpaste also includes the raw material of following weight portion and is prepared from: 0.1-2 part additive. Described additive includes the combination of a kind of or at least two in water-soluble mill base, DP300, glycyrrhizic acid dipotassium, silicon dioxide, propylene glycol.
Water-soluble mill base plays hyperchromic effect in the toothpaste of the present invention. Glycyrrhizic acid dipotassium is white or off-white color fine powder, and purity reaches 98%, has a special sweet taste, water-soluble good, mouthfeel is pure. There is the multiple efficacies such as antibacterial, antiinflammatory, removing toxic substances, antiallergic, deodorization.
The chemical name of DP300 is trichlorohydroxyl phenylate, is commonly called as triclosan. Toothpaste provided by the invention belongs to antibacterial, there is antimicrobial component, be the antibacterial medicines of a kind of multiple-effect, it is possible to fluoride compatibility.
Described deep-sea fish bone meal is the powder of natural deep-sea fish bone, mainly takes from Endoconcha Sepiae, the inner shell of Shi Wu section animal needleless crow or the Golden Crow, is mainly composed of calcium carbonate, has the effect of hemostasis, whitening.
Margarita powder can tooth-whitening, tasty and refreshing smelly.
Described abrasivus includes stone powder, calcium phosphate dibasic dihydrate or its combination. Stone powder is natural whiting, also known as calcite in powder, is that one cleans the teeth the strong abrasive material of power, uses with silica bound, and the power that cleans the teeth damages by force and not dentin. The abrasive material that calcium phosphate dibasic dihydrate for white powder, is a kind of gentleness, friction is low, makes the bright and clean exquisiteness of mastic, if higher with the composite power of cleaning the teeth of anhydrous calcium phosphate.
Described wetting agent includes sorbitol, Polyethylene Glycol or its combination. The full name of sorbitol is D-Sorbitol, is sweet oil substitute, and moisture retention relatively glycerol relaxes, and taste is also better, with glycerol with the use of, the toothpaste diffusibility made and thixotropy are better. Polyethylene Glycol has thickening, moisture-keeping functions, as toothpaste thickening wetting agent, especially uses in transparent toothpaste and can increase gel toothpaste clarity and stripping.
Described foaming agent includes sodium lauryl sulphate. Sodium lauryl sulphate is called for short K-12, is a kind of anion surfactant, has good foaming, emulsifying, infiltration, de-sludging performance, mainly makes foaming agent, detergent uses in toothpaste.
Described thickening agent includes Sodium Tvlose, xanthan gum, SM gel or its combination. Sodium Tvlose is called for short CMC, it is thickening agent the most frequently used in domestic toothpaste, there is thickening, stablize, bond the effect of mastic, composite with silicon dioxide, xanthan gum etc., the anti-salt of toothpaste of the present invention, antienzyme performance can be increased further, and make mastic finer and smoother, bright. Xanthan gum and SM gel all play stable and thickening effect in the toothpaste of the present invention.
Described spice includes fruit essence and Mint Essence. Spice used by the present invention is pure and fresh delicately, refrigerant tasty and refreshing, is in harmonious proportion formulated by natural perfume material and artificial perfume by proper proportion, and described spice also can directly be bought, or prepares according to prior art.
Described sweeting agent includes saccharin sodium, sorbitol or its combination; Saccharin sodium coordinates with essence, it is possible to improve the taste of toothpaste.
Described preservative includes ethyl hydroxybenzoate. Ethyl hydroxybenzoate is white crystals thing, mildly bitter flavor, fiber crops of burning. It is mainly used as the sterilization antiseptic of food, cosmetics, medicine.
The preparation method that the present invention also provides for a kind of above-mentioned toothpaste, comprises the steps:
Step 1, thickening agent, wetting agent and foaming agent are dissolved in the water, are uniformly dissolved, obtain mixed solution;
Step 2, described deep-sea fish bone meal and described Margarita powder are mixed, be ground, obtain deep-sea fish bone meal and Margarita powder mixture;
Step 3, in step 1 gained mixed solution, add step 2 gained deep-sea fish bone meal and Margarita powder mixture and surplus stock, finally add spice, obtain raw mixture;
Step 4, described raw mixture being stirred, mediate, ground, evacuation, obtains mastic simultaneously;
Step 5, by described mastic stand 1.5-3 hour so that it is naturally cool to room temperature, tinning, packaging, obtain described toothpaste.
Further, in step 1, described thickening agent, wetting agent and foaming agent are dissolved in water in pre-molten pot or premix pot. In step 2, the particle diameter of described deep-sea fish bone meal and Margarita powder mixture is 1-20 ��m. In step 3, described mixed solution mixes in cream pot processed with surplus stock. In step 4, evacuation makes vacuum reach 0.09-0.1Mpa, and the time is 40-60min. When kneading, grinding, temperature controls below 45 DEG C.
The invention have the benefit that in toothpaste provided by the invention containing deep-sea fish bone meal and Margarita powder; with other component synergism in toothpaste; can effectively suppress gingival hemorrhage; tooth-whitening; and potent can dispel dental calculus; make tooth firmer, can effectively suppress the formation of dental plaque simultaneously, better take care of one's teeth.
Detailed description of the invention
Embodiment 1
The invention provides a kind of toothpaste, the raw material including following weight portion is prepared from: 40g abrasivus, 10g wetting agent, 2.5g foaming agent, 2g thickening agent, 0.5g spice, 0.5g sweeting agent, 0.1g preservative, 0.1g additive, 20g deep-sea fish bone meal, 0.5g Margarita powder and 20g water.
Wherein, described deep-sea fish bone meal is the powder of natural deep-sea fish bone, mainly takes from Endoconcha Sepiae; Described abrasivus is stone powder; Described wetting agent is the combination of sorbitol and Polyethylene Glycol, and its quality is 1:1; Described foaming agent is sodium lauryl sulphate; Described thickening agent is the combination of CMC, xanthan gum and SM gel, and its mass ratio is 1:1:1; Described spice is fruit essence; Described sweeting agent is sorbitol; Described preservative is ethyl hydroxybenzoate; Additive includes water-soluble mill base, DP300 and glycyrrhizic acid dipotassium, and its mass ratio is 1:1:1.
Its preparation method, comprises the steps:
Step 1, thickening agent, wetting agent and foaming agent are dissolved in the water, are uniformly dissolved in pre-molten pot, obtain mixed solution;
Step 2, described deep-sea fish bone meal and described Margarita powder are mixed, be ground, obtain deep-sea fish bone meal and Margarita powder mixture that particle diameter is 1-20 ��m;
Step 3, step 1 gained mixture solution is poured in cream pot processed, in described mixed solution, add step 2 gained deep-sea fish bone meal and Margarita powder mixture and surplus stock, be initially charged liquid material, add powder, finally add spice, obtain raw mixture;
Step 4, described raw mixture being stirred, mediate, ground, evacuation, makes vacuum reach 0.09Mpa simultaneously, and the time is 40min, obtains mastic; In cream process processed, because kneading, process of lapping can rub heat release, therefore need to use chuck cooling water control temperature��45 DEG C in summer.
Step 5, described mastic is stood 1.5 hours so that it is naturally cool to room temperature, make mastic fully expand simultaneously and form homogeneous adherend, improve the elasticity of mastic, tinning afterwards, packaging, obtain described toothpaste.
Embodiment 2
The invention provides a kind of toothpaste, the raw material including following weight portion is prepared from: 50g abrasivus, 30g wetting agent, 1.5g foaming agent, 1g thickening agent, 1.5g spice, 0.1g sweeting agent, 0.5g preservative, 2g additive, 15g deep-sea fish bone meal, 0.4g Margarita powder and 50g water.
Wherein, described deep-sea fish bone meal is the powder of natural deep-sea fish bone, mainly takes from Endoconcha Sepiae; Described abrasivus is the combination of stone powder and calcium phosphate dibasic dihydrate, and its mass ratio is 1:1; Described wetting agent is sorbitol; Described foaming agent is sodium lauryl sulphate; Described thickening agent is the combination of CMC and xanthan gum, and its mass ratio is 1:1; Described spice is Mint Essence; Described sweeting agent is saccharin sodium; Described preservative is ethyl hydroxybenzoate; Additive is water-soluble mill base, DP300, glycyrrhizic acid dipotassium, silicon dioxide and propylene glycol, and arbitrary proportion mixes.
Its preparation method, comprises the steps:
Step 1, thickening agent, wetting agent and foaming agent are dissolved in the water, are uniformly dissolved in pre-molten pot, obtain mixed solution;
Step 2, described deep-sea fish bone meal and described Margarita powder are mixed, be ground, obtain deep-sea fish bone meal and Margarita powder mixture that particle diameter is 1-20 ��m;
Step 3, step 1 gained mixture solution is poured in cream pot processed, in described mixed solution, add step 2 gained deep-sea fish bone meal and Margarita powder mixture and surplus stock, be initially charged liquid material, add powder, finally add spice, obtain raw mixture;
Step 4, described raw mixture being stirred, mediate, ground, evacuation, makes vacuum reach 0.1Mpa simultaneously, and the time is 60min, obtains mastic; In cream process processed, because kneading, process of lapping can rub heat release, therefore need to use chuck cooling water control temperature��45 DEG C in summer.
Step 5, described mastic is stood 3 hours so that it is naturally cool to room temperature, make mastic fully expand simultaneously and form homogeneous adherend, improve the elasticity of mastic, tinning afterwards, packaging, obtain described toothpaste.
Embodiment 3
The invention provides a kind of toothpaste, the raw material including following weight portion is prepared from: 43g abrasivus, 15g wetting agent, 1.8g foaming agent, 1.3g thickening agent, 1.2g spice, 0.2g sweeting agent, 0.2g preservative, 0.3g additive, 19g deep-sea fish bone meal, 0.4g Margarita powder and 25g water.
Wherein, described deep-sea fish bone meal is the powder of natural deep-sea fish bone, mainly takes from Endoconcha Sepiae; Described abrasivus is calcium phosphate dibasic dihydrate; Described wetting agent is Polyethylene Glycol; Described foaming agent is sodium lauryl sulphate; Described thickening agent is SM gel; Described spice is Mint Essence; Described sweeting agent is saccharin sodium; Described preservative is ethyl hydroxybenzoate; Additive is glycyrrhizic acid dipotassium.
Its preparation method, comprises the steps:
Step 1, thickening agent, wetting agent and foaming agent are dissolved in the water, are uniformly dissolved in pre-molten pot, obtain mixed solution;
Step 2, described deep-sea fish bone meal and described Margarita powder are mixed, be ground, obtain deep-sea fish bone meal and Margarita powder mixture that particle diameter is 1-20 ��m;
Step 3, step 1 gained mixture solution is poured in cream pot processed, in described mixed solution, add step 2 gained deep-sea fish bone meal and Margarita powder mixture and surplus stock, be initially charged liquid material, add powder, finally add spice, obtain raw mixture;
Step 4, described raw mixture being stirred, mediate, ground, evacuation, makes vacuum reach 0.096Mpa simultaneously, and the time is 50min, obtains mastic; In cream process processed, because kneading, process of lapping can rub heat release, therefore need to use chuck cooling water control temperature��45 DEG C in summer.
Step 5, described mastic is stood 2 hours so that it is naturally cool to room temperature, make mastic fully expand simultaneously and form homogeneous adherend, improve the elasticity of mastic, tinning afterwards, packaging, obtain described toothpaste.
Embodiment 4
The invention provides a kind of toothpaste, the raw material including following weight portion is prepared from: 49g abrasivus, 28g wetting agent, 2.4g foaming agent, 1.8g thickening agent, 0.8g spice, 0.4g sweeting agent, 0.4g preservative, 1.5g additive, 17g deep-sea fish bone meal, 0.5g Margarita powder and 40g water.
Wherein, described deep-sea fish bone meal is the powder of natural deep-sea fish bone, mainly takes from Endoconcha Sepiae; Described abrasivus is stone powder; Described wetting agent is sorbitol; Described foaming agent is sodium lauryl sulphate; Described thickening agent is xanthan gum; Described spice is Mint Essence; Described sweeting agent is sorbitol; Described preservative is ethyl hydroxybenzoate; Additive is glycyrrhizic acid dipotassium.
Its preparation method, comprises the steps:
Step 1, thickening agent, wetting agent and foaming agent are dissolved in the water, are uniformly dissolved in pre-molten pot, obtain mixed solution;
Step 2, described deep-sea fish bone meal and described Margarita powder are mixed, be ground, obtain deep-sea fish bone meal and Margarita powder mixture that particle diameter is 1-20 ��m;
Step 3, step 1 gained mixture solution is poured in cream pot processed, in described mixed solution, add step 2 gained deep-sea fish bone meal and Margarita powder mixture and surplus stock, be initially charged liquid material, add powder, finally add spice, obtain raw mixture;
Step 4, described raw mixture being stirred, mediate, ground, evacuation, makes vacuum reach 0.096Mpa simultaneously, and the time is 50min, obtains mastic; In cream process processed, because kneading, process of lapping can rub heat release, therefore need to use chuck cooling water control temperature��45 DEG C in summer.
Step 5, described mastic is stood 2 hours so that it is naturally cool to room temperature, make mastic fully expand simultaneously and form homogeneous adherend, improve the elasticity of mastic, tinning afterwards, packaging, obtain described toothpaste.
Embodiment 5
The invention provides a kind of toothpaste, the raw material including following weight portion is prepared from: 48g abrasivus, 27g wetting agent, 2.3g foaming agent, 1.6g thickening agent, 1g spice, 0.3g sweeting agent, 0.3g preservative, 1.3g additive, 18g deep-sea fish bone meal, 0.5g Margarita powder and 32g water.
Wherein, described deep-sea fish bone meal is the powder of natural deep-sea fish bone, mainly takes from Endoconcha Sepiae; Described abrasivus is the combination of stone powder and calcium phosphate dibasic dihydrate, and its mass ratio is 1:1; Described wetting agent is sorbitol; Described foaming agent is sodium lauryl sulphate; Described thickening agent is the combination of CMC and xanthan gum, and its mass ratio is 1:1; Described spice is Mint Essence; Described sweeting agent is saccharin sodium; Described preservative is ethyl hydroxybenzoate; Additive is water-soluble mill base, glycyrrhizic acid dipotassium and silicon dioxide, and arbitrary proportion mixes.
Its preparation method, comprises the steps:
Step 1, thickening agent, wetting agent and foaming agent are dissolved in the water, are uniformly dissolved in pre-molten pot, obtain mixed solution;
Step 2, described deep-sea fish bone meal and described Margarita powder are mixed, be ground, obtain deep-sea fish bone meal and Margarita powder mixture that particle diameter is 1-20 ��m;
Step 3, step 1 gained mixture solution is poured in cream pot processed, in described mixed solution, add step 2 gained deep-sea fish bone meal and Margarita powder mixture and surplus stock, be initially charged liquid material, add powder, finally add spice, obtain raw mixture;
Step 4, described raw mixture being stirred, mediate, ground, evacuation, makes vacuum reach 0.096Mpa simultaneously, and the time is 50min, obtains mastic; In cream process processed, because kneading, process of lapping can rub heat release, therefore need to use chuck cooling water control temperature��45 DEG C in summer.
Step 5, described mastic is stood 2 hours so that it is naturally cool to room temperature, make mastic fully expand simultaneously and form homogeneous adherend, improve the elasticity of mastic, tinning afterwards, packaging, obtain described toothpaste.
Randomly selecting 300 examples, every day uses the embodiment of the present invention 1-5 toothpaste provided sooner or later, observes tooth effect, and black tooth tooth, seeing obvious effect once all left and right, continues to use this product to reach January more than, and tooth whitening rate reaches on 95%; Yellow for there being tooth, the crowd of dental calculus, use what this product reached January more than all to reach whitening effect; Toothpaste provided by the invention potent can dispel dental calculus, has good whitening effect, effectively suppresses gingival hemorrhage, makes tooth firmer, can effectively suppress the formation of dental plaque simultaneously, better take care of one's teeth.
Effect example 1
Liu, female, 20 years old, tooth turned to be yellow, and has dental calculus, and every day uses the toothpaste that the embodiment of the present invention 1 provides sooner or later, and after one month, teeth whiter, dental calculus reduces, and after three months, dental calculus disappears.
Effect example 2
Appoint certain, man, 30 years old, tooth turned black, and every day uses the toothpaste that the embodiment of the present invention 2 provides sooner or later, after one week, teeth whiter.
Effect example 3
Bao, female, 33 years old, frequent gingival hemorrhage when brushing teeth, every day used the toothpaste that the embodiment of the present invention 4 provides sooner or later, and gingival hemorrhage number of times reduces, and after one month, gingival hemorrhage disappears.
Effect example 4
Zhang, man, 38 years old, tooth turned black, and has dental plaque, and every day uses the toothpaste that the embodiment of the present invention 5 provides sooner or later, and after one week, teeth whiter, dental plaque reduces, and after one month, dental plaque disappears.
The present invention is not limited to above-mentioned preferred forms; anyone can draw other various forms of products under the enlightenment of the present invention; no matter but on its formula or component, do any change; every have same or like with the application like technical scheme, all fall within protection scope of the present invention.
Claims (10)
1. a toothpaste, it is characterised in that: the raw material including following weight portion is prepared from: 40-50 part abrasivus, 10-30 part wetting agent, 1.5-2.5 part foaming agent, 1-2 part thickening agent, 0.5-1.5 part spice, 0.1-0.5 part sweeting agent, 0.1-0.5 part preservative, 15-20 part deep-sea fish bone meal, 0.4-0.5 part Margarita powder and 20-50 part water.
2. toothpaste according to claim 1, it is characterised in that: the raw material including following weight portion is prepared from: 43-49 part abrasivus, 15-28 part wetting agent, 1.8-2.4 part foaming agent, 1.3-1.8 part thickening agent, 0.8-1.2 part spice, 0.2-0.4 part sweeting agent, 0.2-0.4 part preservative, 17-19 part deep-sea fish bone meal, 0.4-0.5 part Margarita powder and 25-40 part water.
3. toothpaste according to claim 1, it is characterised in that: the raw material including following weight portion is prepared from: 48 parts of abrasivuss, 27 parts of wetting agents, 2.3 parts of foaming agent, 1.6 parts of thickening agents, 1 part of spice, 0.3 part of sweeting agent, 0.3 portion of preservative, 18 parts of deep-sea fish bone meal, 0.5 part of Margarita powder and 32 parts of water.
4. toothpaste according to claim 1, it is characterised in that: the raw material also including following weight portion is prepared from: 0.1-2 part additive.
5. toothpaste according to claim 4, it is characterised in that: described additive includes the combination of a kind of or at least two in water-soluble mill base, DP300, glycyrrhizic acid dipotassium, silicon dioxide, propylene glycol.
6. the preparation method of the arbitrary described toothpaste of claim 1-5, it is characterised in that: comprise the steps:
Step 1, thickening agent, wetting agent and foaming agent are dissolved in the water, are uniformly dissolved, obtain mixed solution;
Step 2, described deep-sea fish bone meal and described Margarita powder are mixed, be ground, obtain deep-sea fish bone meal and Margarita powder mixture;
Step 3, in step 1 gained mixed solution, add step 2 gained deep-sea fish bone meal and Margarita powder mixture and surplus stock, finally add spice, obtain raw mixture;
Step 4, described raw mixture being stirred, mediate, ground, evacuation, obtains mastic simultaneously;
Step 5, by described mastic stand 1.5-3 hour so that it is naturally cool to room temperature, tinning, packaging, obtain described toothpaste.
7. the preparation method of toothpaste according to claim 6, it is characterised in that: in step 1, described thickening agent, wetting agent and foaming agent are dissolved in water in pre-molten pot or premix pot.
8. the preparation method of toothpaste according to claim 6, it is characterised in that: in step 2, the particle diameter of described deep-sea fish bone meal and Margarita powder mixture is 1-20 ��m.
9. the preparation method of toothpaste according to claim 6, it is characterised in that: in step 4, evacuation makes vacuum reach 0.09-0.1Mpa, and the time is 40-60min.
10. the preparation method of toothpaste according to claim 6, it is characterised in that: in step 4, when kneading, grinding, temperature controls below 45 DEG C.
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Cited By (10)
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| CN106176544A (en) * | 2016-08-26 | 2016-12-07 | 吴敬华 | A kind of micro-calcium promoting and tooth-building toothpaste |
| CN106214559A (en) * | 2016-08-25 | 2016-12-14 | 广西慧投互联网金融服务有限公司 | A kind of remove xanthodont toothpaste |
| CN106491493A (en) * | 2016-11-25 | 2017-03-15 | 江苏爱西施科技服务咨询股份有限公司 | One kind brightens antiallergic silk peptide toothpaste and preparation method thereof |
| CN107362088A (en) * | 2017-08-15 | 2017-11-21 | 中国热带农业科学院南亚热带作物研究所 | A kind of toothpaste prepared with macadamia shell micro mist |
| CN107661233A (en) * | 2017-10-23 | 2018-02-06 | 广州市西瑶玉池科技有限公司 | A kind of anhydrous toothpaste of the mineral element containing the tremolite and preparation method thereof |
| CN107854410A (en) * | 2017-11-30 | 2018-03-30 | 浙江海洋大学 | The preparation method of micro-nano fish-bone based toothpastes |
| CN110464694A (en) * | 2018-05-09 | 2019-11-19 | 上海牛樟芝生物技术有限公司 | One white hemostasis toothpaste |
| CN110946772A (en) * | 2019-12-27 | 2020-04-03 | 苏格格 | Toothpaste for preventing dental diseases and preparation method thereof |
| CN111346038A (en) * | 2020-04-09 | 2020-06-30 | 福州帝九生物科技有限公司 | Preparation method of toothpaste with effects of diminishing inflammation, inhibiting bacteria and removing tartar |
| CN111840159A (en) * | 2020-08-03 | 2020-10-30 | 深圳市有用功投资发展有限公司 | Herbal concentrated solution and preparation method thereof and preparation method of toothpaste |
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| CN106214559A (en) * | 2016-08-25 | 2016-12-14 | 广西慧投互联网金融服务有限公司 | A kind of remove xanthodont toothpaste |
| CN106176544A (en) * | 2016-08-26 | 2016-12-07 | 吴敬华 | A kind of micro-calcium promoting and tooth-building toothpaste |
| CN106491493A (en) * | 2016-11-25 | 2017-03-15 | 江苏爱西施科技服务咨询股份有限公司 | One kind brightens antiallergic silk peptide toothpaste and preparation method thereof |
| CN107362088A (en) * | 2017-08-15 | 2017-11-21 | 中国热带农业科学院南亚热带作物研究所 | A kind of toothpaste prepared with macadamia shell micro mist |
| CN107661233A (en) * | 2017-10-23 | 2018-02-06 | 广州市西瑶玉池科技有限公司 | A kind of anhydrous toothpaste of the mineral element containing the tremolite and preparation method thereof |
| CN107854410A (en) * | 2017-11-30 | 2018-03-30 | 浙江海洋大学 | The preparation method of micro-nano fish-bone based toothpastes |
| CN110464694A (en) * | 2018-05-09 | 2019-11-19 | 上海牛樟芝生物技术有限公司 | One white hemostasis toothpaste |
| CN110946772A (en) * | 2019-12-27 | 2020-04-03 | 苏格格 | Toothpaste for preventing dental diseases and preparation method thereof |
| CN111346038A (en) * | 2020-04-09 | 2020-06-30 | 福州帝九生物科技有限公司 | Preparation method of toothpaste with effects of diminishing inflammation, inhibiting bacteria and removing tartar |
| CN111840159A (en) * | 2020-08-03 | 2020-10-30 | 深圳市有用功投资发展有限公司 | Herbal concentrated solution and preparation method thereof and preparation method of toothpaste |
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