CN106265360A - A kind of cleansing milk containing fermentation of seaweed product and preparation method thereof - Google Patents
A kind of cleansing milk containing fermentation of seaweed product and preparation method thereof Download PDFInfo
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- CN106265360A CN106265360A CN201610861970.XA CN201610861970A CN106265360A CN 106265360 A CN106265360 A CN 106265360A CN 201610861970 A CN201610861970 A CN 201610861970A CN 106265360 A CN106265360 A CN 106265360A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The present invention relates to daily cosmetics field, particularly relate to a kind of cleansing milk containing fermentation of seaweed product and preparation method thereof.It includes the fermentation of seaweed product that percentage by weight is 0.05% 10%.The present invention is with tangleweed tunning as main active, coordinate and add algal oil, hyaluronic acid, nicotiamide, tocopherol, Semen pruni armeniacae oil isoreactivity composition, use simple ultrasonic shear method to reduce product cut size, obtain the nano-scale multifunctional cleansing milk of deep layer cleaning, nourishing and moisturizing, Whitening, spot.It is big that the present invention solves chemicals in cleansing milk, antiseptic content on the market, and neutraceutical active ingredients is low, and whitening skin and preserving moisture is poor, zest is big, with rear tight, the problems such as deep layer cleaning power is little, it is provided that the Sargassum cleansing milk that a kind of active component is abundant, natural non-stimulated, whitening skin and preserving moisture, nutrition are moistened.
Description
Technical field
The present invention relates to daily cosmetics FIELD OF THE INVENTIONThe, particularly relate to a kind of cleansing milk containing fermentation of seaweed product and
Preparation method.
Background technology
Cleansing milk is the cleaning supplies being exclusively used in cleaning face, has cleaning and nursing function concurrently.But washing one's face on the market
Milk is main preparation with chemical composition mostly, and the ratio that natural component accounts for is the least, and most cleansing milk particle diameter is bigger, it is impossible to deep
Enter pore and carry out deep layer cleaning.
Cleansing milk the most on the market, the most too much adds chemicals, artificial essence, artificial color and preservative etc.,
Although the purpose of cleaning skin can be reached, but skin is produced intense stimulus, cause by rear tight, the problem such as moisture retention is poor.
It addition, most cleansing milk particle diameters are big, the dirt of skin surface can only be cleared up, the depths dirt within pore is difficult to thorough
The end, is cleaned.
Along with the enhancing of people's skin protection consciousness and frequently using of cosmetics, what natural materials was modulated into has deep layer clean skin concurrently
Gradually liked by people with the cleansing milk demand of nourishing effect.Tangleweed contain abundant polyphenol, polysaccharide, vitamin,
The natural active matters such as unsaturated fatty acid, have all multiactions such as antiinflammatory, antioxidation and whitening skin and preserving moisture.At present, although comprise
The cosmetics of Sargassum extract have been developed, but majority simply uses common water extraction mode, the active material molecules of proposition
Amount is big, is difficult to absorb.
The shortcoming that the present invention is directed to prior art, uses fermentation method, utilizes microorganism to be discharged by the active component of Sargassum
Come, and further the active substance being difficult to the macromole of absorption is resolved into the small-molecule active substance being more easy to absorption of human body, obtain
Absorption, the Sargassum extract of more active substance must be more easy to.The active substance of macromole is degraded into and is prone to skin suction by the present invention
The small-molecule active substance received, coordinates algal oil, hyaluronic acid, nicotiamide, tocopherol, Semen pruni armeniacae oil isoreactivity composition, improves
Chemicals and the stimulation of preservative, use ultrasonic Treatment technology to reduce particle diameter, it is thus achieved that the cleansing milk of Nano Particle,
Reach effect of deep layer cleaning, Whitening, spot, nourishing and moisturizing.
Summary of the invention
Present invention aims to cleansing milk on the market and contain a large amount of chemicals, preservative, functional components is few,
Big to skin irritation, with rear tight, moisture retention is poor, and major part granule is big, the problems such as deep layer cleaning dynamics is little, it is provided that a kind of
Deep layer cleaning, Whitening, spot, the Sargassum cleansing milk of nourishing and moisturizing, this cleansing milk activity substance content enriches, is prone to absorb, and energy
Clean deep layer dirt and do not damage skin, reach effect of whitening, moisturizing, nutrition.
The technical solution used in the present invention is as follows: a kind of cleansing milk containing fermentation of seaweed product, including following weight percent
The composition of ratio is made: fermentation of seaweed product 0.05%-10%.
Further, the preparation method of above-mentioned fermentation of seaweed product includes following:
(1), after Sargassum being rinsed well, dry, pulverize to obtain algae powder;
(2) 1g algae powder is mixed homogeneously with the water of 10mL, inoculating lactic acid bacterium, yeast, insert in fermentation tank, at 20-40
At DEG C, ferment 24-48h, is finally filtrated to get fermentation of seaweed product;
(3) Sargassum described in refers to one or more the combination in Brown algae, red algae, chlorella.
Further, present invention also offers the preparation method of above-mentioned Sargassum cleansing milk, including following preparation process:
(1) successively by 5%-30% glycerol, 2%-20% butanediol, 2-20% propylene glycol, 10%-18% stearic acid,
5%-15% myristic acid, 3%-10% lauric acid mix homogeneously, be heated to 80 DEG C, be allowed to be completely dissolved under stirring condition,
To A phase;
(2) 4%-10% potassium hydroxide is dissolved in the deionized water of 8%-20%, obtains B phase;
(3) by 0.5%-3% glyceryl monostearate, 0.5%-3% polysorbas20,0.1%-5% sodium lauroyl sarcosine,
0.1%-5% cocos nucifera oil acyl glycine potassium, 0.1%-5% cocamido propyl betaine mix homogeneously, obtain C phase;
(4) by 0.1%-3% citric acid, 0.1%-1% sodium alginate, 0.01%-1% nicotiamide, 0.05%-0.5%
Hyaluronic acid, 0.5%-2% algal oil, 0.05%-3% tocopherol, 0.01%-5% Semen pruni armeniacae oil, 0.05%-10% Sargassum
Tunning is dissolved in 5%-20% deionized water and obtains D phase.
(5) B is added in A phase, after being heated to 85 DEG C, agitating heating 10min, add C phase and stir 10min, fall
Temperature adds D phases to 40 DEG C, after stirring 10min, is placed in supersonic generator and carries out supersound process, at power 200W, ultrasonic
Continuing supersound process after stirring after 10min, total sonication treatment time is 10-60min, is finally cooled to room temperature;
(6), after cleansing milk at room temperature stands 2 days, fill obtains product.
The fermentation of seaweed product of the present invention is the mixture that multiple tangleweed obtains through yeast and lactic acid bacteria fermentation, energy
Enough make the nutrition in cleansing milk more comprehensive, Large molecule active mass degradation, it is more easy to absorb.The present invention is possibly together with natural antibacterial
Agent, nutrient, wetting agent, it is not necessary to add chemical preservative, have deep layer cleaning, nourishing and moisturizing, gentle non-stimulated feature, suitable
Crowd for various skin quality.Cleansing milk of the present invention auxiliary add various active composition, as algal oil, hyaluronic acid, nicotiamide,
Tocopherol, Semen pruni armeniacae oil isoreactivity composition, coordinate fermentation of seaweed product to make the cleansing milk more Ensure Liquid of preparation moisten.The present invention washes
Face milk uses ultrasonic Treatment, and the particle diameter making cleansing milk is less, and deep layer cleaning dynamics is bigger, is beneficial to remove the dirt of deep skin
Dirt.Preparation method science of the present invention, simple for process, production cost is low, is suitable for industrialized production.
Detailed description of the invention
The present invention is with natural tangleweed as primary raw material, and the multiple biology using microbe fermentation method to extract in Sargassum is lived
Property material, and degraded Large molecule active material further, extraction cost is low, and product easily absorbs, is of high nutritive value, A wide selection of colours and designs.
Processing technology of the present invention uses ultrasonic Treatment mode, makes the whole grain diameter of cleansing milk be reduced to nanoscale, is had
Deep layer cleaning, nourishing and moisturizing, the cleansing milk of Whitening, spot effect, it is adaptable to the crowd of different sexes, age and skin quality.
Below by way of concrete preferred embodiment, the present invention is described in further detail, but the present invention is not limited in following
Embodiment.
Embodiment 1:
1.1. composition and the percentage by weight thereof of the nanometer cleansing milk of fermentation of seaweed product is:
A phase: stearic acid 10%, myristic acid 9%, lauric acid 6%, glycerol 20%, butanediol 5%, propylene glycol 5% are mixed
Close uniformly, be heated to 80 DEG C under stirring condition, be allowed to be completely dissolved, obtain A phase;
B phase: potassium hydroxide 6% is dissolved in deionized water 10%, obtains B phase.
C phase: by glyceryl monostearate 0.5%, polysorbas20 0.5%, sodium lauroyl sarcosine 1%, cocos nucifera oil acyl glycine
Potassium 4%, cocamido propyl betaine 4% mix homogeneously, obtain C phase;
D phase: by citric acid 1%, sodium alginate 0.05%, hyaluronic acid 0.05%, algal oil 0.5%, tocopherol
0.05%, nicotiamide 0.01%, Semen pruni armeniacae oil 2%, fermentation of seaweed product 5% are dissolved in 10.34% deionized water and obtain D phase.
1.2. technical process:
(1) preparation method of above-mentioned fermentation of seaweed product:
After Scytosiphon lomentarius (Lyngh.)J. Ag. is rinsed well, dry, pulverize to obtain algae powder, 1g algae powder is mixed homogeneously with the water of 10mL, add lactic acid
Bacterium, yeast, put in fermentation tank, maintains the temperature at 20 DEG C, ferments 48 hours, takes out and is filtrated to get fermentation of seaweed product;
(2) A phase is heated to 80 DEG C under agitation, is allowed to be completely dissolved, B is added in A phase, is heated to 85
After DEG C, agitating heating 10min, add C phase and stir 10min, be cooled to 40 DEG C and add D phase, after stirring 10min, be placed in ultrasonic
Supersound process in wave producer, power 200W, continue after stirring after work 10min, total sonication treatment time is 30min,
It is cooled to room temperature;
(3), after at room temperature standing 2 days, fill obtains product.
Embodiment 2:
Composition and the percentage by weight thereof of the nanometer cleansing milk of 2.1 fermentation of seaweed products be:
A phase: by stearic acid 20%, myristic acid 5%, lauric acid 5%, glycerol 10%, butanediol 10%, propylene glycol 10%
Mix homogeneously, is heated to 80 DEG C under stirring condition, be allowed to be completely dissolved, and obtains A phase;
B phase: potassium hydroxide 7% is dissolved in 10% deionized water, obtains B phase;
C phase: by glyceryl monostearate 1%, polysorbas20 1%, sodium lauroyl sarcosine 2%, cocos nucifera oil acyl glycine potassium
2%, cocamido propyl betaine 2% mix homogeneously, obtains C phase;
D phase: by citric acid 2%, sodium alginate 0.01%, hyaluronic acid 0.1%, nicotiamide 1%, algal oil 1%, fertility
Phenol 0.5%, Semen pruni armeniacae oil 2%, fermentation of seaweed product 0.5% are dissolved in 7.89% deionized water and obtain D phase.
2.2 technical processs:
(1), after sea grape and Sargassum fusiforme (Harv.) Setch being rinsed well, dry, pulverize to obtain algae powder, 1g algae powder is mixed with the water of 10mL
Uniformly, add lactic acid bacteria, yeast, put in fermentation tank, maintain the temperature at 25 DEG C, ferment 48 hours, take out and be filtrated to get sea
Algae tunning.
(2) A phase is heated to 80 DEG C under agitation, is allowed to be completely dissolved, B is added in A phase, is heated to 85
After DEG C, agitating heating 10min, add C phase and stir 10min, be cooled to 40 DEG C and add D phase, after stirring 10min, be placed in ultrasonic
Supersound process in wave producer, power 200W, continue after stirring after work 10min, total sonication treatment time is 20min,
It is cooled to room temperature;
(3), after at room temperature standing 2 days, fill obtains product.
Embodiment 3:
3.1. composition and the percentage by weight thereof of the nanometer cleansing milk of fermentation of seaweed product is:
A phase: by stearic acid 10%, myristic acid 9%, lauric acid 11%, glycerol 5%, butanediol 5%, propylene glycol 10%
Mix homogeneously, is heated to 80 DEG C under stirring condition, be allowed to be completely dissolved, and obtains A phase;
B phase: potassium hydroxide 5% is dissolved in 10% deionized water, obtains B phase;
C phase: by glyceryl monostearate 2%, polysorbas20 0.5%, sodium lauroyl sarcosine 4%, cocos nucifera oil acyl glycine potassium
3%, cocamido propyl betaine 2% mix homogeneously, obtains C phase;
D phase: by citric acid 0.5%, sodium alginate 0.5%, hyaluronic acid 0.5%, nicotiamide 1%, algal oil 0.5%,
Tocopherol 0.05%, Semen pruni armeniacae oil 3%, fermentation of seaweed product 1% are dissolved in 16.45% deionized water and obtain D phase.
3.2. technical process:
(1), after Eucheuma muricatum (Gmel.) Web.Van Bos., Yi Guzao and Thallus Porphyrae being rinsed well, dry, pulverize to obtain algae powder, by the water of 1g algae powder Yu 10mL
Mix homogeneously, adds lactic acid bacteria, yeast, puts in fermentation tank, maintain the temperature at 30 DEG C, ferment 24 hours, takes out and filters
To fermentation of seaweed product.
(2) A phase is heated to 80 DEG C under agitation, is allowed to be completely dissolved, B is added in A phase, is heated to 85
After DEG C, agitating heating 10min, add C phase and stir 10min, be cooled to 40 DEG C and add D phase, after stirring 10min, be placed in ultrasonic
Supersound process in wave producer, power 200W, continue after stirring after work 10min, total sonication treatment time is 60min,
It is cooled to room temperature;
(3), after at room temperature standing 2 days, fill obtains product.
Embodiment 4
Above-described embodiment is carried out experimental evaluation
4.1. the detection method of cleaning force: with reference to the detection side in " Yi Rou whitening cleansing milk quality control and efficacy assessments "
Method, inside left arm in the range of 4cm × 5cm, smears oiliness lipstick and the eyebrow pencil of 3cm × 1cm respectively.Weigh sample cleansing milk
0.5g, is applied to spot respectively and gently rubs 1min, clean with water.Observe and clean effect, and shoot record analysis with digital camera.Aobvious
Effect is substantially removed for skin greasepaint, effectively removes more than 1/2 for skin greasepaint, invalid for skin greasepaint without obvious change.
4.2. product moisture-keeping efficacy: reference " cosmetic formulations design and production technology " (Dong Yinmao. cosmetic formulations designs
And production technology. Beijing: China Textiles Press, 2007:298-300) experimental technique detection cleansing milk moisture-keeping efficacy.
4.3 product hydroscopicity tests: weighing cleansing milk sample 4.0g, be placed in weighing botle, 25 DEG C are positioned over relative humidity
It is 4h in the environment of 75%, calculates the hydroscopicity after 4h.Wherein, hydroscopicity=(mEventually-mBegin)/mBegin× 100%, wherein, m begins as putting
Put the quality of front testing sample, g;M is eventually for the quality of sample, g after placement 4h.
4.4 product sensory physicochemical property tests: " GB/T 296802013 washes one's face with reference to National Standard of the People's Republic of China
Milk, cleansing cream " in experimental technique to the sense organ of cleansing milk, physical and chemical index detection.
4.5. foaming power and foam stability test: with reference in " preparation of gentle foam facial milk cleanser and performance study thereof "
Experimental technique, preparation weight/mass percentage composition is each product solution 3mL of 10%, is placed in 50mL tool plug graduated cylinder, adds distilled water dilute
Releasing to 15mL, add a cover, acutely concussion 10 times, immediate record foam volume (mL), record foam volume again after 10min.Repeat
Measure 3 times, average.
4.6 experimental result
1. cleaning force test result:
Sample | Cleaning performance |
Embodiment 1 | Effective |
Embodiment 2 | Effective |
Embodiment 3 | Effective |
2. product performance of keeping humidity:
Sample | Moisturizing rate |
Embodiment 1 | 91.28% |
Embodiment 2 | 93.12% |
Embodiment 3 | 90.87% |
3. hygroscopicity detection:
Sample | Hydroscopicity |
Embodiment 1 | 41.5% |
Embodiment 2 | 40.3% |
Embodiment 3 | 43.1% |
4. product sensory, physicochemical property detection:
Index | Embodiment 1 | Embodiment 2 | Embodiment 3 |
Fragrance | Meet regulation fragrance | Meet regulation fragrance | Meet regulation fragrance |
Outward appearance | Uniform and smooth | Uniform and smooth | Uniform and smooth |
pH | 8.10 | 8.32 | 8.11 |
Cold-resistant | Not stratified | Not stratified | Not stratified |
Heat-resisting | Not stratified | Not stratified | Not stratified |
Centrifugal | Phenomenon without oil-water separation | Phenomenon without oil-water separation | Phenomenon without oil-water separation |
5. foaming power and foam stability test result:
Index | Initial volume (mL) | Volume (mL) after 10min |
Embodiment 1 | 36.67 | 34.12 |
Embodiment 2 | 34.17 | 33.50 |
Embodiment 3 | 38.23 | 36.68 |
Above test result shows, cleansing milk moisture absorption and performance of keeping humidity in the present invention are good, and cleaning force is strong, and foaming abundancy is steady
Fixed, sense organ, physicochemical property are qualified.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited in above-mentioned embodiment
Detail, in the technology concept of the present invention, technical scheme can be carried out multiple simple variant, this
A little simple variant belong to protection scope of the present invention.
Additionally, combination in any can also be carried out between the various different embodiment of the present invention, as long as it is without prejudice to this
The thought of invention, it should be considered as content disclosed in this invention equally.
Claims (3)
1. the cleansing milk containing fermentation of seaweed product, it is characterised in that: include that the composition of following percentage by weight is made: Sargassum
Tunning 0.05%-10%.
A kind of cleansing milk containing fermentation of seaweed product the most according to claim 1, it is characterised in that: fermentation of seaweed product
Preparation method includes following:
(1), after Sargassum being rinsed well, dry, pulverize to obtain algae powder;
(2) 1g algae powder is mixed homogeneously with the water of 10mL, inoculating lactic acid bacterium, yeast, insert in fermentation tank, at 20-40 DEG C,
Fermentation 24-48h, is finally filtrated to get fermentation of seaweed product;
(3) Sargassum described in refers to one or more the combination in Brown algae, red algae, chlorella.
3. according to the preparation method of a kind of cleansing milk containing fermentation of seaweed product described in claim 1 to 2, it is characterised in that:
Including following preparation process:
(1) successively by 5%-30% glycerol, 2%-20% butanediol, 2-20% propylene glycol, 10%-18% stearic acid, 5%-
15% myristic acid, 3%-10% lauric acid mix homogeneously, be heated to 80 DEG C, be allowed to be completely dissolved, obtain A under stirring condition
Phase;
(2) 4%-10% potassium hydroxide is dissolved in the deionized water of 8%-20%, obtains B phase;
(3) by 0.5%-3% glyceryl monostearate, 0.5%-3% polysorbas20,0.1%-5% sodium lauroyl sarcosine,
0.1%-5% cocos nucifera oil acyl glycine potassium, 0.1%-5% cocamido propyl betaine mix homogeneously, obtain C phase;
(4) by transparent to 0.1%-3% citric acid, 0.1%-1% sodium alginate, 0.01%-1% nicotiamide, 0.05%-0.5%
Matter acid, 0.5%-2% algal oil, 0.05%-3% tocopherol, 0.01%-5% Semen pruni armeniacae oil, 0.05%-10% fermentation of seaweed
Product is dissolved in 5%-20% deionized water and obtains D phase.
(5) B is added in A phase, after being heated to 85 DEG C, agitating heating 10min, add C phase and stir 10min, be cooled to
40 DEG C add D phase, after stirring 10min, are placed in supersonic generator and carry out supersound process, after power 200W, ultrasonic 10min
Continuing supersound process after stirring, total sonication treatment time is 10-60min, is finally cooled to room temperature;
(6), after cleansing milk at room temperature stands 2 days, fill obtains product.
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