CN106265360B - A kind of facial cleanser of the product containing fermentation of seaweed and preparation method thereof - Google Patents
A kind of facial cleanser of the product containing fermentation of seaweed and preparation method thereof Download PDFInfo
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- CN106265360B CN106265360B CN201610861970.XA CN201610861970A CN106265360B CN 106265360 B CN106265360 B CN 106265360B CN 201610861970 A CN201610861970 A CN 201610861970A CN 106265360 B CN106265360 B CN 106265360B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The present invention relates to daily cosmetics fields, more particularly to a kind of facial cleanser and preparation method thereof of product containing fermentation of seaweed.It includes the fermentation of seaweed product that weight percent is 0.05%-10%.The present invention is using tangleweed tunning as main active, cooperation addition algal oil, hyaluronic acid, niacinamide, tocopherol, Sweet Almond Oil isoreactivity ingredient, product cut size is reduced using simple ultrasonic shear method, obtains the nano-scale multifunctional facial cleanser of deep layer cleaning, nourishing and moisturizing, Whitening, spot.The present invention solves in facial cleanser on the market that chemicals, antiseptic content are big, and neutraceutical active ingredients are low, and skin whitening, moisturizing is poor, irritation is big, with the problems such as rear tight, deep layer cleaning power is small, provide a kind of abundant active constituent, natural no stimulation, skin whitening, moisturizing, nutrition moist seaweed facial cleanser.
Description
Technical field
The present invention relates to daily cosmetics field fields, a kind of facial cleanser more particularly to product containing fermentation of seaweed and its
Preparation method.
Background technique
Facial cleanser is the cleaning supplies for being exclusively used in cleaning face, has both cleaning and nursing function.But washing one's face on the market
Milk is prepared based on chemical component mostly, the ratio very little that natural component accounts for, and most facial cleanser partial sizes are larger, Bu Nengshen
Enter pore and carries out deep layer cleaning.
Facial cleanser on the market at present often excessively adds chemicals, artificial essence, artificial color and preservative etc.,
Although can achieve the purpose that cleaning skin, to skin generate intense stimulus, cause with it is rear tight, moisture retention is poor the problems such as.
In addition, most facial cleanser partial sizes are big, the dirt of skin surface can only be cleared up, the depths dirt inside pore is difficult to thorough
Bottom cleaning.
With the enhancing of people's skin care consciousness and the frequent use of cosmetics, what natural materials were modulated into has both deep layer clean skin
Gradually liked by people with the facial cleanser demand of nourishing effect.Tangleweed polyphenol rich in, polysaccharide, vitamin,
The natural active matters such as unsaturated fatty acid have all multiactions such as anti-inflammatory, anti-oxidant and skin whitening, moisturizing.Although currently, comprising
The cosmetics of marine algae extract have exploitation, but most only using common water extracting mode, the active material molecules of proposition
Amount is big, is not easy to absorb.
The present invention in view of the shortcomings of the prior art, using fermentation method, is released the active constituent of seaweed using microorganism
Come, and the active material for being not easy the macromolecular absorbed is further resolved into the small-molecule active substance for being easier to absorption of human body, obtains
It must be easier to the marine algae extract of absorption, more active materials.The active material of macromolecular is degraded by the present invention is easy to skin suction
The small-molecule active substance of receipts cooperates algal oil, hyaluronic acid, niacinamide, tocopherol, Sweet Almond Oil isoreactivity ingredient, improves
The stimulation of chemicals and preservative reduces partial size using ultrasonication technology, obtains the facial cleanser of Nano Particle,
The effect of reaching deep layer cleaning, Whitening, spot, nourishing and moisturizing.
Summary of the invention
It is an object of the invention to contain a large amount of chemicals, preservative for facial cleanser on the market, functional components are few,
It is big to skin irritation, with it is rear it is tight, moisture retention is poor, and the problems such as most of particle is big, and deep layer cleaning dynamics is small, provide one kind
Deep layer cleaning, Whitening, spot, nourishing and moisturizing seaweed facial cleanser, which enriches, is easy to absorb, and energy
The effect of deep layer dirt is cleaned without damaging skin, reaches whitening, moisturizing, nutrition.
The technical solution adopted by the invention is as follows: a kind of facial cleanser of product containing fermentation of seaweed, including following weight percent
The composition of ratio is made: fermentation of seaweed product 0.05%-10%.
Further, the preparation method of above-mentioned fermentation of seaweed product include the following:
(1) after rinsing seaweed well, drying crushes to obtain algae powder;
(2) 1g algae powder is uniformly mixed, inoculating lactic acid bacterium, saccharomycete with the water of 10mL, is placed in fermentor, in 20-40
At DEG C, ferment 24-48h, and fermentation of seaweed product is finally obtained by filtration;
(3) seaweed described in refers to the combination of one or more of brown alga, red algae, green alga.
Further, the present invention also provides the preparation methods of above-mentioned seaweed facial cleanser, including following preparation step:
(1) successively by 5%-30% glycerol, 2%-20% butanediol, 2-20% propylene glycol, 10%-18% stearic acid,
5%-15% myristic acid, 3%-10% lauric acid are uniformly mixed, and 80 DEG C are heated under stirring condition, is allowed to be completely dissolved, obtain
To A phase;
(2) 4%-10% potassium hydroxide is dissolved in the deionized water of 8%-20%, obtains B phase;
(3) by 0.5%-3% single stearic acid glycerine lipoprotein, 0.5%-3% polysorbas20,0.1%-5% sodium lauroyl sarcosine,
0.1%-5% cocounut oil acyl glycine potassium, 0.1%-5% Cocoamidopropyl betaine are uniformly mixed, and obtain C phase;
(4) by 0.1%-3% citric acid, 0.1%-1% sodium alginate, 0.01%-1% niacinamide, 0.05%-0.5%
Hyaluronic acid, 0.5%-2% algal oil, 0.05%-3% tocopherol, 0.01%-5% Sweet Almond Oil, 0.05%-10% seaweed
Tunning, which is dissolved in 5%-20% deionized water, obtains D phase.
(5) B is added in A phase, after being heated to 85 DEG C, agitating and heating 10min adds C phase and stirs 10min, drop
Temperature is placed in supersonic generator and is ultrasonically treated after stirring 10min to 40 DEG C of addition D phases, in power 200W, ultrasound
Continue to be ultrasonically treated after mixing evenly after 10min, total sonication treatment time is 10-60min, is finally cooled to room temperature;
(6) it is filling to obtain product after facial cleanser stands 2 days at room temperature.
Fermentation of seaweed product of the invention is the mixture that a variety of tangleweeds are obtained through saccharomycete and lactobacillus-fermented, energy
Enough make the nutrition in facial cleanser more comprehensive, Large molecule active mass degradation is easier to absorb.The present invention also contains natural antibacterial
Agent, nutritional agents, moisturizer have the characteristics that deep layer cleaning, nourishing and moisturizing, mild non-stimulated, fit without adding chemical preservative
Crowd for various skin quality.Facial cleanser of the present invention auxiliary addition a variety of active ingredients, as algal oil, hyaluronic acid, niacinamide,
Tocopherol, Sweet Almond Oil isoreactivity ingredient, cooperation fermentation of seaweed product moisten the facial cleanser more nutrition of preparation.The present invention washes
Face milk uses ultrasonication, keeps the partial size of facial cleanser smaller, and deep layer cleaning dynamics is bigger, conducive to the dirt for removing deep skin
Dirt.Preparation method science of the present invention, simple for process, production cost is low, is suitble to industrialized production.
Specific embodiment
The present invention extracts a variety of biologies in seaweed using microbe fermentation method and lives using natural tangleweed as primary raw material
Property substance, and Large molecule active substance of further degrading, extraction cost is low, and product easily absorbs, nutritive value height, A wide selection of colours and designs.
Manufacture craft of the present invention uses ultrasonication mode, so that the entire grain diameter of facial cleanser is reduced to nanoscale, is had
Deep layer cleaning, nourishing and moisturizing, Whitening, spot effect facial cleanser, the crowd suitable for different sexes, age and skin quality.
Below by way of specific preferred embodiment, invention is further described in detail, but the present invention be not limited in it is following
Embodiment.
Embodiment 1:
1.1. the ingredient of the nanometer facial cleanser of fermentation of seaweed product and its weight percent are:
A phase: stearic acid 10%, myristic acid 9%, lauric acid 6%, glycerol 20%, butanediol 5%, propylene glycol 5% are mixed
It closes uniformly, 80 DEG C is heated under stirring condition, is allowed to be completely dissolved, obtains A phase;
B phase: potassium hydroxide 6% is dissolved in deionized water 10%, B phase is obtained.
C phase: by single stearic acid glycerine lipoprotein 0.5%, polysorbas20 0.5%, sodium lauroyl sarcosine 1%, cocounut oil acyl glycine
Potassium 4%, Cocoamidopropyl betaine 4% are uniformly mixed, and obtain C phase;
D phase: by citric acid 1%, sodium alginate 0.05%, hyaluronic acid 0.05%, algal oil 0.5%, tocopherol
0.05%, niacinamide 0.01%, Sweet Almond Oil 2%, fermentation of seaweed product 5% are dissolved in 10.34% deionized water and obtain D phase.
1.2. technical process:
(1) preparation method of above-mentioned fermentation of seaweed product:
After tawny daylily algae is rinsed well, drying crushes to obtain algae powder, 1g algae powder is uniformly mixed with the water of 10mL, and lactic acid is added
Bacterium, saccharomycete, are put into fermentor, maintain the temperature at 20 DEG C, ferment 48 hours, and fermentation of seaweed product is obtained by filtration in taking-up;
(2) A phase is heated to 80 DEG C under agitation, is allowed to be completely dissolved, B is added in A phase, is heated to 85
After DEG C, agitating and heating 10min adds C phase and stirs 10min, is cooled to 40 DEG C of addition D phases, after stirring 10min, is placed in ultrasound
It being ultrasonically treated in wave producer, power 200W, continues after mixing evenly after the 10min that works, total sonication treatment time is 30min,
It is cooled to room temperature;
(3) filling to obtain product after standing 2 days at room temperature.
Embodiment 2:
The ingredient and its weight percent of the nanometer facial cleanser of 2.1 fermentation of seaweed products are:
A phase: by stearic acid 20%, myristic acid 5%, lauric acid 5%, glycerol 10%, butanediol 10%, propylene glycol 10%
It is uniformly mixed, 80 DEG C is heated under stirring condition, is allowed to be completely dissolved, obtains A phase;
B phase: potassium hydroxide 7% is dissolved in 10% deionized water, B phase is obtained;
C phase: by single stearic acid glycerine lipoprotein 1%, polysorbas20 1%, sodium lauroyl sarcosine 2%, cocounut oil acyl glycine potassium
2%, Cocoamidopropyl betaine 2% is uniformly mixed, and obtains C phase;
D phase: by citric acid 2%, sodium alginate 0.01%, hyaluronic acid 0.1%, niacinamide 1%, algal oil 1%, fertility
Phenol 0.5%, Sweet Almond Oil 2%, fermentation of seaweed product 0.5% are dissolved in 7.89% deionized water and obtain D phase.
2.2 technical process:
(1) after rinsing sea grape and sargassum fusifome well, drying crushes to obtain algae powder, 1g algae powder is mixed with the water of 10mL
Uniformly, lactic acid bacteria, saccharomycete is added, is put into fermentor, maintains the temperature at 25 DEG C, ferments 48 hours, sea is obtained by filtration in taking-up
Algae tunning.
(2) A phase is heated to 80 DEG C under agitation, is allowed to be completely dissolved, B is added in A phase, is heated to 85
After DEG C, agitating and heating 10min adds C phase and stirs 10min, is cooled to 40 DEG C of addition D phases, after stirring 10min, is placed in ultrasound
It being ultrasonically treated in wave producer, power 200W, continues after mixing evenly after the 10min that works, total sonication treatment time is 20min,
It is cooled to room temperature;
(3) filling to obtain product after standing 2 days at room temperature.
Embodiment 3:
3.1. the ingredient of the nanometer facial cleanser of fermentation of seaweed product and its weight percent are:
A phase: by stearic acid 10%, myristic acid 9%, lauric acid 11%, glycerol 5%, butanediol 5%, propylene glycol 10%
It is uniformly mixed, 80 DEG C is heated under stirring condition, is allowed to be completely dissolved, obtains A phase;
B phase: potassium hydroxide 5% is dissolved in 10% deionized water, B phase is obtained;
C phase: by single stearic acid glycerine lipoprotein 2%, polysorbas20 0.5%, sodium lauroyl sarcosine 4%, cocounut oil acyl glycine potassium
3%, Cocoamidopropyl betaine 2% is uniformly mixed, and obtains C phase;
D phase: by citric acid 0.5%, sodium alginate 0.5%, hyaluronic acid 0.5%, niacinamide 1%, algal oil 0.5%,
Tocopherol 0.05%, Sweet Almond Oil 3%, fermentation of seaweed product 1% are dissolved in 16.45% deionized water and obtain D phase.
3.2. technical process:
(1) after rinsing Eucheuma, Yi Guzao and seaweed well, drying crushes to obtain algae powder, by the water of 1g algae powder and 10mL
It is uniformly mixed, lactic acid bacteria, saccharomycete is added, is put into fermentor, maintain the temperature at 30 DEG C, ferment 24 hours, taking-up is filtered
To fermentation of seaweed product.
(2) A phase is heated to 80 DEG C under agitation, is allowed to be completely dissolved, B is added in A phase, is heated to 85
After DEG C, agitating and heating 10min adds C phase and stirs 10min, is cooled to 40 DEG C of addition D phases, after stirring 10min, is placed in ultrasound
It being ultrasonically treated in wave producer, power 200W, continues after mixing evenly after the 10min that works, total sonication treatment time is 60min,
It is cooled to room temperature;
(3) filling to obtain product after standing 2 days at room temperature.
Embodiment 4
Experimental evaluation is carried out to above-described embodiment
4.1. the detection method of cleaning force: with reference to the detection side in " control of Yi Rou whitening cleansing milk quality and efficacy assessments "
Method on the inside of the left arm within the scope of 4cm × 5cm, smears the oiliness lipstick and eyebrow pencil of 3cm × 1cm respectively.Weigh sample facial cleanser
0.5g is applied to spot respectively and gently rubs 1min, washes with water.It observes and cleans effect, and shot and recorded and analyzed with digital camera.It is aobvious
Effect is that skin greasepaint obviously removes, and is effectively 1/2 or more skin greasepaint removal, is in vain skin greasepaint without substantially changeing.
4.2. product moisture-keeping efficacy: referring to " cosmetic formulations design and producing technique " (Dong Yinmao cosmetic formulations design
With the Beijing production technology: China Textiles Press, 2007:298-300) experimental method detection facial cleanser moisture-keeping efficacy.
The test of 4.3 product hydroscopicities: the milk sample 4.0g that washes one's face is weighed, is placed in weighing bottle, 25 DEG C are placed in relative humidity
Hydroscopicity for 4h in 75% environment, after calculating 4h.Wherein, hydroscopicity=(mEventually-mBegin)/mBegin× 100%, wherein m begins to put
The quality of sample to be tested, g before setting;M is the quality of sample after placing 4h, g eventually.
The test of 4.4 product sensory physicochemical properties: with reference to National Standard of the People's Republic of China, " GB/T 296802013 washes one's face
Milk, cleansing cream " in experimental method the sense organ of facial cleanser, physical and chemical index are detected.
4.5. foaming power and foam stability test: with reference in " preparation of mild foam mildy wash and its performance study "
Experimental method prepares each product solution 3mL that mass percentage is 10%, is placed in 50mL tool plug graduated cylinder, adds distilled water dilute
It releases to 15mL, covers, acutely shake 10 times, immediate record foam volume (mL), record foam volume again after 10min.It repeats
Measurement 3 times, is averaged.
4.6 experimental result
1. cleaning force test result:
Sample | Cleaning effect |
Embodiment 1 | It is effective |
Embodiment 2 | It is effective |
Embodiment 3 | It is effective |
2. product performance of keeping humidity:
Sample | Moisturizing rate |
Embodiment 1 | 91.28% |
Embodiment 2 | 93.12% |
Embodiment 3 | 90.87% |
3. hygroscopicity detects:
Sample | Hydroscopicity |
Embodiment 1 | 41.5% |
Embodiment 2 | 40.3% |
Embodiment 3 | 43.1% |
4. product sensory, physicochemical property detect:
Index | Embodiment 1 | Embodiment 2 | Embodiment 3 |
Fragrance | Meet regulation fragrance | Meet regulation fragrance | Meet regulation fragrance |
Appearance | Uniform and smooth | Uniform and smooth | Uniform and smooth |
pH | 8.10 | 8.32 | 8.11 |
It is cold-resistant | It is not stratified | It is not stratified | It is not stratified |
It is heat-resisting | It is not stratified | It is not stratified | It is not stratified |
Centrifugation | Without water-oil separating phenomenon | Without water-oil separating phenomenon | Without water-oil separating phenomenon |
5. foaming power and foam stability test result:
Index | Initial volume (mL) | Volume (mL) after 10min |
Embodiment 1 | 36.67 | 34.12 |
Embodiment 2 | 34.17 | 33.50 |
Embodiment 3 | 38.23 | 36.68 |
The above test result shows that facial cleanser moisture absorption in the present invention and performance of keeping humidity are good, strong cleaning force, and foaming abundancy is steady
Fixed, sense organ, physicochemical property are qualified.
The preferred embodiment of the present invention has been described above in detail, still, during present invention is not limited to the embodiments described above
Detail within the scope of the technical concept of the present invention can be with various simple variants of the technical solution of the present invention are made, this
A little simple variants all belong to the scope of protection of the present invention.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should also be regarded as the disclosure of the present invention.
Claims (1)
1. a kind of preparation method of the facial cleanser of product containing fermentation of seaweed, it is characterised in that: including following preparation step:
(1) successively by 5%-30% glycerol, 2%-20% butanediol, 2-20% propylene glycol, 10%-18% stearic acid, 5%-
15% myristic acid, 3%-10% lauric acid are uniformly mixed, and 80 DEG C are heated under stirring condition, is allowed to be completely dissolved, obtains A
Phase;
(2) 4%-10% potassium hydroxide is dissolved in the deionized water of 8%-20%, obtains B phase;
(3) by 0.5%-3% single stearic acid glycerine lipoprotein, 0.5%-3% polysorbas20,0.1%-5% sodium lauroyl sarcosine,
0.1%-5% cocounut oil acyl glycine potassium, 0.1%-5% Cocoamidopropyl betaine are uniformly mixed, and obtain C phase;
(4) 0.1%-3% citric acid, 0.1%-1% sodium alginate, 0.01%-1% niacinamide, 0.05%-0.5% is transparent
Matter acid, 0.5%-2% algal oil, 0.05%-3% tocopherol, 0.01%-5% Sweet Almond Oil, 0.05%-10% fermentation of seaweed
Product, which is dissolved in 5%-20% deionized water, obtains D phase;
(5) B is added in A phase, after being heated to 85 DEG C, agitating and heating 10min adds C phase and stirs 10min, is cooled to
40 DEG C of addition D phases are placed in supersonic generator and are ultrasonically treated, after power 200W, ultrasonic 10min after stirring 10min
Continue to be ultrasonically treated after mixing evenly, total sonication treatment time is 10-60min, is finally cooled to room temperature;
(6) it is filling to obtain product after facial cleanser stands 2 days at room temperature.
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CN113413335B (en) * | 2021-07-26 | 2022-08-23 | 广州药妆日用化工有限公司 | Extract containing algae essence, preparation method thereof and prepared moisturizing emulsion |
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CN105816418B (en) * | 2016-05-12 | 2018-11-20 | 吉林敖东大高酵素有限公司 | A kind of plant enzyme nourishing pack and preparation method thereof |
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