CN104815454B - Rosemary natural extract and utilize this extract to prepare antibacterial toilet soap and its preparation method and application - Google Patents
Rosemary natural extract and utilize this extract to prepare antibacterial toilet soap and its preparation method and application Download PDFInfo
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- CN104815454B CN104815454B CN201510148284.3A CN201510148284A CN104815454B CN 104815454 B CN104815454 B CN 104815454B CN 201510148284 A CN201510148284 A CN 201510148284A CN 104815454 B CN104815454 B CN 104815454B
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Abstract
The present invention provides rosemary natural extract and utilizes this extract to prepare antibacterial toilet soap and its preparation method and application, overcomes the defect of chemosynthesis antibacterial.The fancy soap of the present invention is possible not only to deep clean skin, and there is good fungistatic effect, common causative antibacterial is had good and lasting Scavenging activity, and skin is had certain maintenance effect, it is particularly suited for child and women and the crowd that passive protective physical fitness is poor.
Description
Technical field
The present invention relates to a kind of novel toilet soap, be specifically related to rosemary natural extract and utilize this extract to prepare antibacterial toilet soap and its preparation method and application.
Background technology
There is substantial amounts of malignant bacteria and fungus in the environment of our life, accidentally it is possible to infect, and skin is the main portions that these pathogenic bacterium are parasitic, and using the fancy soap with bacteriostasis is one of pre-aseptic good measure.The fancy soap major part sold on market is to utilize the chemical substance such as triclocarban, triclosan antibacterial, and its safety needs to be probed into, and certain chemical substance bacteria growing inhibiting of life-time service can cause that this bacterium produces drug resistance.And some manufacturer makes fancy soap with sodium soap and other surfactants for primary raw material, add quality improver and appearance modifying agents, the product made after machine-shaping, because the content of these pH value is high, skin cannot tolerate for a long time, so can only be used for cleaning medicated clothing.The pH value of plant weak base soap is low, the acceptance that human skin can be long-term, and the various nutrient substance contained in plant also have the effect of skin care.The natural bacteriostatic active substance contained in some plant extracts, will not produce untoward reaction and side effect to human body, without compromising on the health of user.
Summary of the invention
In order to solve the deficiencies in the prior art, the present invention provides rosemary natural extract and utilizes this extract to prepare antibacterial toilet soap and its preparation method and application, overcomes the defect of chemosynthesis antibacterial.
The technical scheme is that a kind of rosemary natural extract, prepare according to following steps: weigh Herba Rosmarini Officinalis dry sample 50 kilograms, by Herba Rosmarini Officinalis dry sample grind into fine powder, soak 24h by 80% ethanol 20 times amount, then with filtered on buchner funnel, collect filtrate；Repeat this operation colourless to soak with ethanol liquid, merging filtrate；Filtrate being distilled with Rotary Evaporators decompression, concentrated filtrate obtains Herba Rosmarini Officinalis crude extract；Crude extract, through absorption with macroporous adsorbent resin, obtains fat-soluble Herba Rosmarini Officinalis extract about 10 kilograms after removing the impurity such as chlorophyll.
Another object of the present invention is to provide a kind of antibacterial toilet soap, bacteriostatic activity and fragrance ingredient in described antibacterial toilet soap are rosemary natural extract described above.
As further improvement opportunity scheme, the composition of described antibacterial toilet soap, include Herba Rosmarini Officinalis extract 5-10 part, Oleum Cocois 10-12 part, soybean oil 20-23 part, Oleum Helianthi 20-35 part, sodium hydroxide 8.5-9 part, water 20-25 part according to mass parts.
And another optimisation technique scheme, described antibacterial toilet soap is according to mass parts by Herba Rosmarini Officinalis extract 5-10 part, Oleum Cocois 10-12 part, soybean oil 20-23 part, and Oleum Helianthi 20-35 part, sodium hydroxide 8.5-9 part, water 20-25 part form.
The preparation method that present invention also offers a kind of antibacterial toilet soap described above, its step includes: the first step: Oleum Cocois, soybean oil, Oleum Helianthi are put into heatproof container by weight to scale, boil molten with water proof mode of heating, make the temperature of oil maintain 35 DEG C～40 DEG C；Second step: by the amount of required water and sodium hydroxide, puts into water in glass container, is then slowly added into sodium hydroxide, and limit edged quickly stirs with alkaline-resisting agitator, and sodium hydroxide is cooled to 35 DEG C～40 DEG C after being dissolved completely in water, obtain aqueous slkali；3rd step: the aqueous slkali of second step is slowly poured in the first step equipped with in the glass container of miscella, add while being stirred continuously about 40 minutes with alkaline-resisting agitator and making both saponifications, until both solution are thoroughly mixed and obtain soap base, and regulate pH to 7.5～8；4th step: amount adds Herba Rosmarini Officinalis extract in proportion while stirring in the soap base of the 3rd step, then stirs, obtains mixing soap lye；5th step: dip in a small amount of olive oil brushing die inside with brush, builds mould with plastic sheeting after then pouring the soap lye of the 4th step mixing into mould, and 35 DEG C of couveuses are placed 2～3 days, obtain fancy soap；6th step: be removed from the molds by the 5th ready-made fancy soap of step, is put in ventilation and allows its natural drying, obtain fancy soap finished product.
Present invention also offers a kind of antibacterial toilet soap described above, this antibacterial toilet soap is suppressing the application of bacillus perfringens, staphylococcus aureus, anthrax bacillus, Salmonella, mycobacterium tuberculosis, alpha streptococcus, streptococcus pneumoniae, shigella or S. sonnei.
Bacillus perfringens, staphylococcus aureus, anthrax bacillus, Salmonella, mycobacterium tuberculosis, alpha streptococcus, streptococcus pneumoniae, shigella, S. sonnei are all had bacteriostasis in various degree by the effective ingredient such as the carnosol that contains in Herba Rosmarini Officinalis extract, rosmarinic acid, rosmanol.
Advantages of the present invention:
Product provided by the invention, its bacteriostatic activity is significantly improved, and can effectively suppress the growth of multiple pathogenetic bacteria.
Production technique of the present invention is simple and safe, and Substance used and soap base raw material are natural product, has advantage safe and nontoxic, that have no side effect.Determine effective ingredient consumption.Because natural bacteriostatic active component content is excessive, the emulsifying effectiveness of fancy soap can be affected, and consumption is too small can not play fungistatic effect.Applicant is through research and substantial amounts of analysis of experimental data for a long time, it is determined that the Optimum of this active constituent content, so as to have good fungistatic effect, does not affect again the molding of fancy soap simultaneously.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is elaborated.
Embodiment 1:
The preparation process of Herba Rosmarini Officinalis extract: weigh Herba Rosmarini Officinalis dry sample 50 kilograms, by Herba Rosmarini Officinalis dry sample grind into fine powder, soaks 24h by 80% ethanol 20 times amount, then with filtered on buchner funnel, collects filtrate.Repeat this to operate to soak with ethanol liquid colourless (3～5 times), merging filtrate.Filtrate being distilled with Rotary Evaporators decompression, concentrated filtrate is sticky shape extremely.Concentrate is shifted out, dries in the drying baker of 50 DEG C, obtain Herba Rosmarini Officinalis crude extract.Crude extract is through absorption with macroporous adsorbent resin, after 40% ethanol elution, can remove the impurity such as chlorophyll and obtain fat-soluble Herba Rosmarini Officinalis extract about 10 kilograms.
Embodiment 2: the preparation one of Herba Rosmarini Officinalis antibacterial toilet soap
The first step: weigh Oleum Cocois 11 kilograms, soybean oil 20 kilograms, Oleum Helianthi 30 kilograms, be sequentially placed in heatproof container, boil molten with water proof mode of heating, make miscella temperature maintain 35 DEG C～40 DEG C.
Second step: weigh 20 kilograms of water, sodium hydroxide 9 kilograms.First putting in glass container by water, be then slowly added into sodium hydroxide, limit edged quickly stirs with alkaline-resisting agitator, and sodium hydroxide solution completely is cooled to 35 DEG C～40 DEG C after water, obtains aqueous slkali.
3rd step: the aqueous slkali of second step is slowly poured into the first step equipped with in the glass container of miscella, predominate while being stirred continuously about 40 minutes with alkaline-resisting agitator and making both saponifications, until both solution are thoroughly mixed and obtain soap base, then regulate pH to 7.5～8.
4th step: add 8 kilograms of Herba Rosmarini Officinalis extracts while stirring in the soap base of the 3rd step, then stir, obtains mixing soap lye.
5th step: dip in an olive oil with brush and brush one times inside mould, then pours the soap lye of the 4th step mixing into mould, then with plastic sheeting, mould is built, and 35 DEG C of couveuses are placed 2～3 days, obtain fancy soap.
6th step: be removed from the molds by the 5th ready-made fancy soap of step, is put in ventilation and allows its natural drying, about about 5 weeks, obtain fancy soap finished product.
Embodiment 3: the preparation two of Herba Rosmarini Officinalis antibacterial toilet soap
The first step: weigh Oleum Cocois 12 kilograms, soybean oil 21 kilograms, Oleum Helianthi 25.5 kilograms, be sequentially placed in heatproof container, boil molten with water proof mode of heating, makes the temperature of oil maintain 35 DEG C～40 DEG C.
Second step: weigh 21 kilograms of water, sodium hydroxide 9 kilograms.First putting in glass container by water, be then slowly added into sodium hydroxide, limit edged quickly stirs with alkaline-resisting agitator, and sodium hydroxide solution completely is cooled to 35 DEG C～40 DEG C after water, obtains aqueous slkali.
3rd step: the aqueous slkali of second step is slowly poured into the first step equipped with in the glass container of miscella, predominate while being stirred continuously about 40 minutes with alkaline-resisting agitator and making both saponifications, until both solution are thoroughly mixed and obtain soap base, then regulate pH to 7.5～8.
4th step: add 9 kilograms of Herba Rosmarini Officinalis extracts while stirring in the soap base of the 3rd step, then stir, obtains mixing soap lye.
5th step: dip in an olive oil with brush and brush one times inside mould, then pours the soap lye of the 4th step mixing into mould, then with plastic sheeting, mould is built, and 35 DEG C of couveuses are placed 2～3 days, obtain fancy soap.
6th step: be removed from the molds by the 5th ready-made fancy soap of step, is put in ventilation and allows its natural drying, about about 5 weeks, obtain fancy soap finished product.
Example 4: the preparation three of Herba Rosmarini Officinalis antibacterial toilet soap
The first step: weigh Oleum Cocois: 10 kilograms, soybean oil 22 kilograms, Oleum Helianthi 23 kilograms, be sequentially placed in heatproof container, boil molten with water proof mode of heating, make oil temperature maintain 35 DEG C～40 DEG C.
Second step: weigh 20 kilograms of water, sodium hydroxide 8.8 kilograms.First putting in glass container by water, be then slowly added into sodium hydroxide, limit edged quickly stirs with alkaline-resisting agitator, and sodium hydroxide solution completely is cooled to 35 DEG C～40 DEG C after water, obtains aqueous slkali.
3rd step: the aqueous slkali of second step is slowly poured into the first step equipped with in the glass container of miscella, predominate while being stirred continuously about 40 minutes with alkaline-resisting agitator and making both saponifications, until both solution are thoroughly mixed and obtain soap base, then regulate pH to 7.5～8.
4th step: add 10 kilograms of Herba Rosmarini Officinalis extracts while stirring in the soap base of the 3rd step, then stir, obtains mixing soap lye.
5th step: dip in an olive oil with brush and brush one times inside mould, then pours the soap lye of the 4th step mixing into mould, then with plastic sheeting, mould is built, and 35 DEG C of couveuses are placed 2～3 days, obtain fancy soap.
6th step: be removed from the molds by the 5th ready-made fancy soap of step, is put in ventilation and allows its natural drying, about about 5 weeks, obtain fancy soap finished product.
Example 5: the preparation four of Herba Rosmarini Officinalis antibacterial toilet soap
The first step: weigh Oleum Cocois: 12 kilograms, soybean oil 23 kilograms, Oleum Helianthi 35 kilograms, be sequentially placed in heatproof container, boil molten with water proof mode of heating, make oil temperature maintain 35 DEG C～40 DEG C.
Second step: weigh 25 kilograms of water, sodium hydroxide 9 kilograms.First putting in glass container by water, be then slowly added into sodium hydroxide, limit edged quickly stirs with alkaline-resisting agitator, and sodium hydroxide solution completely is cooled to 35 DEG C～40 DEG C after water, obtains aqueous slkali.
3rd step: the aqueous slkali of second step is slowly poured into the first step equipped with in the glass container of miscella, predominate while being stirred continuously about 40 minutes with alkaline-resisting agitator and making both saponifications, until both solution are thoroughly mixed and obtain soap base, then regulate pH to 7.5～8.
4th step: add 10 kilograms of Herba Rosmarini Officinalis extracts while stirring in the soap base of the 3rd step, then stir, obtains mixing soap lye.
5th step: dip in an olive oil with brush and brush one times inside mould, then pours the soap lye of the 4th step mixing into mould, then with plastic sheeting, mould is built, and 35 DEG C of couveuses are placed 2～3 days, obtain fancy soap.
6th step: be removed from the molds by the 5th ready-made fancy soap of step, is put in ventilation and allows its natural drying, about about 5 weeks, obtain fancy soap finished product.
Embodiment 6: the preparation five of Herba Rosmarini Officinalis antibacterial toilet soap
The first step: weigh Oleum Cocois 10 kilograms, soybean oil 20 kilograms, Oleum Helianthi 20 kilograms, be sequentially placed in heatproof container, boil molten with water proof mode of heating, make miscella temperature maintain 35 DEG C～40 DEG C.
Second step: weigh 20 kilograms of water, sodium hydroxide 8.5 kilograms.First putting in glass container by water, be then slowly added into sodium hydroxide, limit edged quickly stirs with alkaline-resisting agitator, and sodium hydroxide solution completely is cooled to 35 DEG C～40 DEG C after water, obtains aqueous slkali.
3rd step: the aqueous slkali of second step is slowly poured into the first step equipped with in the glass container of miscella, predominate while being stirred continuously about 40 minutes with alkaline-resisting agitator and making both saponifications, until both solution are thoroughly mixed and obtain soap base, then regulate pH to 7.5～8.
4th step: add 5 kilograms of Herba Rosmarini Officinalis extracts while stirring in the soap base of the 3rd step, then stir, obtains mixing soap lye.
5th step: dip in an olive oil with brush and brush one times inside mould, then pours the soap lye of the 4th step mixing into mould, then with plastic sheeting, mould is built, and 35 DEG C of couveuses are placed 2～3 days, obtain fancy soap.
6th step: be removed from the molds by the 5th ready-made fancy soap of step, is put in ventilation and allows its natural drying, about about 5 weeks, obtain fancy soap finished product.
Embodiment 7:
Bacteriostatic experiment is carried out with the Herba Rosmarini Officinalis fancy soap of embodiment 4:
(1) preparation of bacteriostatic solution: the Herba Rosmarini Officinalis fancy soap made and conventional fancy soap (non-antimicrobial form fancy soap) are configured to respectively the solution of 1:10.
(2) make into the circular filter paper sheet of diameter 4mm with 102 type middling speed qualitative filter papers, be placed in culture dish 121 DEG C of sterilizing 20min, after cooling, on filter paper, quantitatively drip 20 μ l, 25 DEG C of drying for standby respectively with joined solution in (1).
(3) test strain is: bacillus perfringens, staphylococcus aureus, anthrax bacillus, Salmonella, mycobacterium tuberculosis, alpha streptococcus, streptococcus pneumoniae, shigella, S. sonnei.Being inoculated in MH sausage culture medium by the test organisms after activation, cultivate 24h at 37 DEG C, being diluted to concentration by MH culture medium is 105～108The bacteria suspension of CFU/ml.
(4) adding 15mlMHA culture medium in the culture dish of diameter 9cm, it is 10 that every ware adds 1ml concentration5～108The bacteria suspension of CFU/ml, is uniformly coated in MHA culture medium with spreader, then by being added with the filter paper of bacteriostatic solution, the filter paper of contrast solution is attached to planar surface successively uniformly, every kind of bacterium is cooked 5 parallel tests.Observing after cultivating 24h at 37 DEG C and record inhibition zone (transparent circle) size, inhibition zone size is averaged.Antibacterial result is in Table 1.
Table 1: antibacterial solution is to several Inhibition test results for examination bacterium
Note: measured result is meansigma methods ± standard error
It is shown that the malignant bacteria participating in test is all had a degree of fungistatic effect by Herba Rosmarini Officinalis fancy soap, particularly that anthrax bacillus, Salmonella, S. sonnei and escherichia coli fungistatic effect is better.Compared to conventional fancy soap, the fungistatic effect of Herba Rosmarini Officinalis fancy soap is improved significantly.
The ultimate principle of the present invention and principal character and advantages of the present invention have more than been shown and described.Skilled person will appreciate that of the industry; the present invention is not restricted to the described embodiments; described in above-described embodiment and description is that principles of the invention is described; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements both fall within the claimed scope of the invention.Claimed scope is defined by appending claims and equivalent thereof.
Claims (3)
1. an antibacterial toilet soap, it is characterised in that include Herba Rosmarini Officinalis extract 5-10 part, Oleum Cocois 10-12 part, soybean oil 20-23 part, Oleum Helianthi 20-35 part, sodium hydroxide 8.5-9 part, water 20-25 part according to mass parts；Described Herba Rosmarini Officinalis extract prepares according to following steps: weigh Herba Rosmarini Officinalis dry sample 50 kilograms, by Herba Rosmarini Officinalis dry sample grind into fine powder, soaks 24h by 80% ethanol 20 times amount, then with filtered on buchner funnel, collects filtrate；Repeat this operation colourless to soak with ethanol liquid, merging filtrate；Filtrate being distilled with Rotary Evaporators decompression, concentrated filtrate obtains Herba Rosmarini Officinalis crude extract；Crude extract, through absorption with macroporous adsorbent resin, obtains fat-soluble Herba Rosmarini Officinalis extract 10 kilograms after removing the impurity such as chlorophyll.
2. a kind of antibacterial toilet soap according to claim 1, it is characterised in that according to mass parts by Herba Rosmarini Officinalis extract 5-10 part, Oleum Cocois 10-12 part, soybean oil 20-23 part, Oleum Helianthi 20-35 part, sodium hydroxide 8.5-9 part, water 20-25 part composition.
3. the preparation method of an antibacterial toilet soap as claimed in claim 2, it is characterized in that, its step includes: the first step: Oleum Cocois, soybean oil, Oleum Helianthi are put into heatproof container by weight to scale, boils molten with water proof mode of heating, makes the temperature of oil maintain 35 DEG C～40 DEG C；Second step: by the amount of required water and sodium hydroxide, puts into water in glass container, is then slowly added into sodium hydroxide, and limit edged quickly stirs with alkaline-resisting agitator, and sodium hydroxide is cooled to 35 DEG C～40 DEG C after being dissolved completely in water, obtain aqueous slkali；3rd step: the aqueous slkali of second step is slowly poured in the first step equipped with in the glass container of miscella, add while being stirred continuously 40 minutes with alkaline-resisting agitator and making both saponifications, until both solution are thoroughly mixed and obtain soap base, and regulate pH to 7.5～8；4th step: amount adds Herba Rosmarini Officinalis extract in proportion while stirring in the soap base of the 3rd step, then stirs, obtains mixing soap lye；5th step: dip in a small amount of olive oil brushing die inside with brush, builds mould with plastic sheeting after then pouring the soap lye of the 4th step mixing into mould, and 35 DEG C of couveuses are placed 2～3 days, obtain fancy soap；6th step: be removed from the molds by the 5th ready-made fancy soap of step, is put in ventilation and allows its natural drying, obtain fancy soap finished product.
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| CN105586181A (en) * | 2016-01-15 | 2016-05-18 | 南京科技职业学院 | Natural mung bean soap and preparation method thereof |
| CN110452789A (en) * | 2019-08-29 | 2019-11-15 | 于泽浩 | A kind of ingredient and preparation method thereof of essential oils of herbs handmade soap |
| CN111254024B (en) * | 2020-01-08 | 2021-06-18 | 四川大学 | Compound liquid soap with powerful sterilization effect and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104388215A (en) * | 2014-11-17 | 2015-03-04 | 绵阳原香农业科技有限公司 | Marseille soap |
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| AR054051A1 (en) * | 2006-05-29 | 2007-05-30 | Jose Alejandro Mumoli | COMPOSITION IN SOLID TABLETS OF FAST DISSOLUTION IN WATER OR WATER LIQUIDS FOR BODY OR ORAL HYGIENE, SKIN AND HAIR TREATMENT AND DISINFECTION |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104388215A (en) * | 2014-11-17 | 2015-03-04 | 绵阳原香农业科技有限公司 | Marseille soap |
Non-Patent Citations (2)
| Title |
|---|
| 大孔吸附树脂纯化迷迭香脂溶性总酚酸的研究;杨磊 等;《离子交换与吸附》;20090331;第25卷(第3期);第225-232页 * |
| 迷迭香提取物抑菌作用研究;程伟贤 等;《中国食品卫生杂志》;20060531;第18卷(第5期);第406-408页 * |
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