CN110951553A - Water lily compound essential oil handmade soap with anti-aging effect and preparation method thereof - Google Patents
Water lily compound essential oil handmade soap with anti-aging effect and preparation method thereof Download PDFInfo
- Publication number
- CN110951553A CN110951553A CN201911075491.5A CN201911075491A CN110951553A CN 110951553 A CN110951553 A CN 110951553A CN 201911075491 A CN201911075491 A CN 201911075491A CN 110951553 A CN110951553 A CN 110951553A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- soap
- water lily
- parts
- citrus
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a water lily compound essential oil handmade soap with an anti-aging effect and a preparation method thereof. The invention firstly provides a plant compound essential oil with an anti-aging effect, wherein the plant compound essential oil is composed of water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil; the volume ratio of the water lily essential oil to the citrus essential oil to the lavender essential oil to the cinnamon essential oil is (5-10): (0.5-3): (0.5-3): (0.5 to 3); based on the compound essential oil, the water lily compound essential oil handmade soap with the anti-aging effect is prepared by optimizing the proportioning amount of the components of the compound essential oil and the synergistic effect of the compound essential oil, and the handmade soap is fine in hand feeling, good in soap body stability, free of stimulation to skin, remarkable in antibacterial, moisturizing and antioxidant effects and wide in application prospect.
Description
Technical Field
The invention belongs to the technical field of daily chemical articles. More particularly, relates to a water lily compound essential oil handmade soap with an anti-aging effect and a preparation method thereof.
Background
The toilet soap is an indispensable washing and nursing article in daily life, and in recent years, along with the improvement of living standard of people, the requirement on the toilet soap is higher and higher, and the demand of people on resisting the aging toilet soap is also followed by the increased importance on skin nursing. The common anti-aging ingredients in the skin care product comprise polyphenols, sodium hyaluronate and the like. Through investigation, few handmade soaps with anti-aging efficacy are sold on the market, and are mostly made by hands in a home workshop manner, and the product quality is uneven. Therefore, the demand of people for daily chemical products cannot be met.
Plant essential oil (Plant essential oil) is an aromatic substance obtained by extracting Plant raw materials, and is extracted from flowers, leaves, roots, barks, fruits, seeds, resins, and the like of herbaceous plants by distillation and squeezing. Because the essential oil of the fumigation has high volatility and small molecules, the essential oil is easy to be absorbed by human bodies and can quickly permeate into internal organs of the human bodies to discharge redundant components out of the human bodies, the whole process only needs a few minutes, and the fragrance of the plants directly stimulates the secretion of pituitary gland, the secretion of enzymes, hormones and the like, balances the internal functions of the human bodies, and plays a role in beautifying and protecting the skin. The compound essential oil is prepared by mixing more than two single essential oils and base oil according to a certain proportion, and the essential oils are mutually coordinated and some of the essential oils have the functions of supplementing each other and enhancing the curative effect. Through literature search, the combination of the compound essential oil is various in the aspect of anti-aging, and the effect brought by the combination is divided into four conditions of synergy, addition, irrelevance and antagonism. Therefore, the anti-aging effect can be better achieved by selecting which plant essential oils to compound into the handmade soap, and the respective effects and interaction of the plant essential oils need to be comprehensively considered.
Nymphaea is a perennial aquatic herb of Nymphaeaceae, and is widely planted in temperate and tropical regions; in China, the distribution is only partial in Hainan island. Tropical water lily is a famous ornamental flower in the world, scented tea and food made of flowers and leaves of the tropical water lily are popular with the public, but at present, the related water lily has fewer product types and low development and utilization rate, so that resource waste is caused, and no report about preparing daily chemical products with anti-aging effect by using the water lily is available.
Disclosure of Invention
The invention aims to solve the technical problem of overcoming the blank of preparing daily chemical products with anti-aging effect by using water lily in the prior art, and provides the water lily compound essential oil handmade soap with anti-aging effect and the preparation method thereof. The invention provides the plant compound essential oil with the anti-aging effect by taking the water lily essential oil which is characterized in Hainan area as the main component and compounding other plant essential oils, the plant compound essential oil is used as an effective additive and a natural perfume in the soap, the synergistic effect is achieved by optimizing the proportion of compounding each plant essential oil, and the prepared handmade soap has remarkable anti-aging effect, moisturizing performance and bacteriostatic effect.
The invention aims to provide a plant compound essential oil with an anti-aging effect.
The invention also aims to provide application of the plant compound essential oil in preparing daily chemical products with anti-aging effect.
The invention also aims to provide the water lily compound essential oil handmade soap with the anti-aging effect.
Still another object of the present invention is to provide a method for preparing said handmade soap.
The above purpose of the invention is realized by the following technical scheme:
the invention firstly provides a plant compound essential oil with an anti-aging effect, wherein the plant compound essential oil is composed of water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil; the volume ratio of the water lily essential oil to the citrus essential oil to the lavender essential oil to the cinnamon essential oil is (5-10): (0.5-3): (0.5-3): (0.5 to 3). The plant compound essential oil obtained in the volume ratio range has obvious bacteriostatic effect, moisturizing effect and antioxidant function.
Preferably, the volume ratio of the water lily essential oil, the citrus essential oil, the lavender essential oil and the cinnamon essential oil is (7-10): (1-2): (1-2): (1-2). The bacteriostatic effect, the moisturizing effect and the antioxidant function of the plant compound essential oil obtained in the volume ratio range are further improved.
More preferably, the volume ratio of the water lily essential oil, the citrus essential oil, the lavender essential oil and the cinnamon essential oil is 7: 1: 1: 1. the plant compound essential oil obtained in the volume ratio has the best antibacterial effect, moisturizing effect and antioxidant function.
Wherein, the water lily is a perennial aquatic herbaceous plant, and is only partially distributed in the Hainan island in China. The water lily essential oil has the functions of whitening and fading spots, diminishing inflammation and resisting acne, moistening and smoothing, nourishing and repairing, calming and resisting allergy, exciting blood circulation, enhancing memory and refreshing. The natural water lily essential oil anti-allergy factor eliminates and discharges stubborn skin allergy factors, can effectively treat various allergens in the skin, thoroughly and harmlessly solves various skin allergy phenomena, strengthens the natural health care toxin expelling function of the skin, keeps the contact balanced hyperplasia and regeneration of cells, and effectively improves abnormal skin and aged skin.
Citrus belongs to Rutaceae, and has delicate sweet taste and little faint flower fragrance besides unique citrus peel taste. The fresh smell of the citrus essential oil has the function of refreshing, and is often used for calming and supporting depression and anxiety.
Lavender is a plant of Lavender of Labiatae, and Lavender essential oil has effects of clearing heat and toxic substances, cleaning skin, controlling oil content, removing speckle, whitening skin, removing wrinkle, caring skin, removing black eye under eye, and promoting regeneration and recovery of damaged tissue. The lavender essential oil also has a calming effect on heart, can reduce hypertension and soothe palpitation, and is helpful for insomnia.
The cinnamon is a middle and large tree in the cinnamomum of Lauraceae, the bark is grey brown, and the cinnamon essential oil can mildly astringe the skin, compact the collapsed skin after losing weight, promote blood circulation and remove wart skin.
According to the invention, the water lily essential oil, the citrus essential oil, the lavender essential oil and the cinnamon essential oil are compounded for use, and long-term experiments show that the proportioning dosage of the components is optimized, so that the aims of effectively inhibiting the growth of bacteria, keeping the skin moist and resisting aging can be achieved, and the water lily essential oil is safe, non-irritant and harmless to the skin of a human body.
Therefore, the application of the plant compound essential oil in preparing daily chemical products with anti-aging efficacy also falls within the protection scope of the invention.
The invention also provides the water lily compound essential oil handmade soap with the anti-aging effect, which comprises the plant compound essential oil.
The handmade soap prepared by the invention has fine hand feeling and good soap body stability, has remarkable antibacterial effect, moisturizing effect and antioxidant function, can effectively promote blood circulation, resist aging and remove skin warts, and has excellent soothing effects of relaxing mood, exhaustion, weakness and depression.
Preferably, the handmade soap consists of the following components in volume fraction: 5-10 parts of water lily essential oil, 0.5-3 parts of citrus essential oil, 0.5-3 parts of lavender essential oil, 0.5-3 parts of cinnamon essential oil, 0.1-1 part of vitamin E and 50-100 parts of soap base.
More preferably, the handmade soap consists of the following components in volume fraction: 7-10 parts of water lily essential oil, 1-2 parts of citrus essential oil, 1-2 parts of lavender essential oil, 1-2 parts of cinnamon essential oil, 0.2-0.6 part of vitamin E and 75-100 parts of soap base.
Still further preferably, the handmade soap consists of the following components in volume fraction: 7 parts of water lily essential oil, 1 part of citrus essential oil, 1 part of lavender essential oil, 1 part of cinnamon essential oil, 0.4 part of vitamin E and 75 parts of soap base.
The invention also provides a preparation method of the handmade soap, which comprises the following steps:
s1, mixing water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil according to the volume ratio, and performing ultrasonic oscillation to obtain composite essential oil;
s2, heating the soap base to be molten, mixing the soap base and the compound essential oil obtained in the step S1 according to the volume ratio, stirring, pouring into a mold, and cooling to obtain the handmade soap.
Preferably, the oscillation frequency of step S1 is 50 to 70 hz.
More preferably, the oscillation frequency of step S1 is 60 hz.
Preferably, the oscillation time in step S1 is 15-30S.
More preferably, the oscillation time in step S1 is 22S.
Preferably, the stirring speed in the step S2 is 10-30 r/min.
More preferably, the stirring speed of step S2 is 20 r/min.
Preferably, the stirring time in the step S2 is 5-15 min.
More preferably, the stirring time of step S2 is 10 min.
Preferably, the water lily essential oil is extracted by a supercritical method.
Specifically, the extraction method of the water lily essential oil comprises the following steps: filling flos Nymphaeae petals in the extraction tank, and supplying liquid CO2Compressed by a pump to make liquid CO2In a supercritical state, the extract liquid flows through an extraction tank from bottom to top for extraction, the extract liquid flows through a first separator after being decompressed, and the solubility of resin, grease and pigment is reduced after being decompressed and is settled at the bottom of the first separator; CO 22And water lily essential oil, depressurizing again, settling at the bottom of the second separator, and CO2Evaporating in gas form to obtain the citrus essential oil.
Preferably, the citrus essential oil is supercritical CO2Extracting by an extraction method.
Specifically, the extraction method of the citrus essential oil comprises the following steps: filling the citrus peel in an extraction tank, and supplying liquid CO2Compressed by a pump to make liquid CO2In a supercritical state, the extract liquid flows through an extraction tank from bottom to top for extraction, the extract liquid flows through a first separator after being decompressed, and the solubility of resin, grease and pigment is reduced after being decompressed and is settled at the bottom of the first separator; CO 22And orange essential oil is decompressed again, settled at the bottom of the second separator, and CO is added2Evaporating in gas form to obtain the citrus essential oil.
Preferably, the lavender essential oil is extracted by a steam distillation method.
Specifically, the extraction method of the lavender essential oil comprises the following steps: weighing lavender, soaking for a proper time, putting into a dry three-neck round-bottom flask, adding a certain amount of distilled water for soaking, connecting a test device, and checking the stability and the air tightness of the test device; and then, heating the flask to boiling by using an electric heating sleeve, keeping the slightly boiling distillation at normal pressure, stopping heating after the time is reached, cooling the system to room temperature, starting a piston at the lower end of an oil-water separator, enabling the liquid to flow into a volumetric flask, extracting by using ethyl acetate, taking the upper layer of liquid, and performing rotary evaporation to obtain the lavender essential oil.
Preferably, the cinnamon essential oil is extracted by an ultrahigh pressure method.
Specifically, the extraction method of the cinnamon essential oil comprises the following steps: adding water into the mixture of cinnamon leaves and branches, cooking, performing ultrahigh pressure extraction to obtain an extracting solution, performing rotary evaporation to obtain a mixture of cinnamon essential oil and water, standing at room temperature, layering, and collecting an essential oil layer to obtain the cinnamon essential oil.
Preferably, the water lily essential oil is tropical red water lily essential oil.
The invention has the following beneficial effects:
the invention provides the plant compound essential oil with the anti-aging effect, the proportion and the dosage of each component of the compound essential oil are optimized, the obvious synergistic interaction effect is achieved, and the plant compound essential oil has stronger antibacterial, moisturizing and anti-aging effects; the water lily compound essential oil handmade soap with the anti-aging effect is prepared based on the compound essential oil, has fine hand feeling, good soap body stability and no stimulation to skin, has remarkable antibacterial effect, moisturizing effect and antioxidant function, can effectively promote blood circulation, resist aging, remove skin warts, is favorable for relaxing mood, has excellent effects of soothing exhaustion, weakness and depression, can be used for a long time, and has wide application prospect.
Detailed Description
The present invention is further illustrated by the following specific examples, which are not intended to limit the invention in any way. Reagents, methods and apparatus used in the present invention are conventional in the art unless otherwise indicated.
Unless otherwise indicated, reagents and materials used in the following examples are commercially available.
Example 1 preparation of Water lily composite essential oil handmade soap with anti-aging effect
The water lily compound essential oil handmade soap with the anti-aging effect comprises the following components in parts by volume: 7 parts of water lily essential oil, 1 part of citrus essential oil, 1 part of lavender essential oil, 1 part of cinnamon essential oil, 0.4 part of vitamin E and 75 parts of soap base.
The preparation method of the handmade soap comprises the following steps:
s1, water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil are mixed according to a volume ratio, and ultrasonic oscillation is carried out for 22s by an ultrasonic oscillator under the condition that the oscillation frequency is 60hz, so as to obtain composite essential oil;
s2, heating the soap base in a water bath kettle at 55 ℃ until the soap base is melted, mixing the soap base and the compound essential oil obtained in the step S1 according to the volume ratio, stirring for 10min under the condition that the stirring speed is 20r/min, pouring into a mould, and cooling to obtain the water lily compound essential oil handmade soap which is named as soap A1.
Example 2 preparation of Water lily composite essential oil handmade soap with anti-aging effect
The water lily compound essential oil handmade soap with the anti-aging effect comprises the following components in parts by volume: 5 parts of water lily essential oil, 0.5 part of citrus essential oil, 0.5 part of lavender essential oil, 0.5 part of cinnamon essential oil, 0.1 part of vitamin E and 50 parts of soap base.
The preparation method of the handmade soap comprises the following steps:
s1, water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil are mixed according to a volume ratio, and ultrasonic vibration is carried out for 15s by using an ultrasonic vibrator under the condition that the vibration frequency is 50hz, so as to obtain composite essential oil;
s2, heating the soap base in a water bath kettle at 50 ℃ until the soap base is melted, mixing the soap base and the compound essential oil obtained in the step S1 according to the volume ratio, stirring for 5min under the condition that the stirring speed is 10r/min, pouring the mixture into a mould, and cooling to obtain the water lily compound essential oil handmade soap which is named as soap A2.
Example 3 preparation of Water lily composite essential oil handmade soap with anti-aging effect
The water lily compound essential oil handmade soap with the anti-aging effect comprises the following components in parts by volume: 10 parts of water lily essential oil, 3 parts of citrus essential oil, 3 parts of lavender essential oil, 3 parts of cinnamon essential oil, 1 parts of vitamin E and 100 parts of soap base.
The preparation method of the handmade soap comprises the following steps:
s1, water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil are mixed according to a volume ratio, and ultrasonic vibration is carried out for 30s by using an ultrasonic vibrator under the condition that the vibration frequency is 70hz, so as to obtain composite essential oil;
s2, heating the soap base in a water bath kettle at 50 ℃ until the soap base is melted, mixing the soap base and the compound essential oil obtained in the step S1 according to the volume ratio, stirring for 15min under the condition that the stirring speed is 30r/min, pouring into a mould, and cooling to obtain the water lily compound essential oil handmade soap which is named as soap A3.
Example 4 preparation of Water lily composite essential oil handmade soap with anti-aging effect
The water lily compound essential oil handmade soap with the anti-aging effect comprises the following components in parts by volume: 7 parts of water lily essential oil, 2 parts of citrus essential oil, 2 parts of lavender essential oil, 2 parts of cinnamon essential oil, 0.2 part of vitamin E and 75 parts of soap base.
The preparation method of the handmade soap comprises the following steps:
s1, water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil are mixed according to a volume ratio, and ultrasonic vibration is carried out for 15s by using an ultrasonic vibrator under the condition that the vibration frequency is 50hz, so as to obtain composite essential oil;
s2, heating the soap base in a water bath kettle at 50 ℃ until the soap base is melted, mixing the soap base and the compound essential oil obtained in the step S1 according to the volume ratio, stirring for 15min under the condition that the stirring speed is 30r/min, pouring into a mould, and cooling to obtain the water lily compound essential oil handmade soap which is named as soap A4.
Example 5 preparation of Water lily composite essential oil handmade soap with anti-aging efficacy
The water lily compound essential oil handmade soap with the anti-aging effect comprises the following components in parts by volume: 10 parts of water lily essential oil, 1 part of citrus essential oil, 1 part of lavender essential oil, 1 part of cinnamon essential oil, 0.6 part of vitamin E and 90 parts of soap base.
The preparation method of the handmade soap comprises the following steps:
s1, water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil are mixed according to a volume ratio, and ultrasonic vibration is carried out for 30s by using an ultrasonic vibrator under the condition that the vibration frequency is 70hz, so as to obtain composite essential oil;
s2, heating the soap base in a water bath kettle at 50 ℃ until the soap base is melted, mixing the soap base and the compound essential oil obtained in the step S1 according to the volume ratio, stirring for 5min under the condition that the stirring speed is 10r/min, pouring the mixture into a mould, and cooling to obtain the water lily compound essential oil handmade soap which is named as soap A4.
Comparative example 1
The handmade soap of this comparative example was obtained, named soap D1, with the same components and volume fractions as in example 1 except that no water lily essential oil was present.
The handmade soap of this comparative example was prepared in the same manner as in example 1.
Comparative example 2
The handmade soap of this comparative example was obtained as the same composition and volume fraction as in example 1 except that there were no citrus essential oil and lavender essential oil, and was named soap D2.
The handmade soap of this comparative example was prepared in the same manner as in example 1.
Comparative example 3
The handmade soap of this comparative example, named soap D3, was obtained by following the same components and volume fractions as in example 1 except that cinnamon essential oil was not present.
The handmade soap of this comparative example was prepared in the same manner as in example 1.
Comparative example 4
The handmade soap of this comparative example was obtained under the name of soap D4, except that 2 parts of water lily essential oil were used, and the other components and volume fractions were the same as those of example 1.
The handmade soap of this comparative example was prepared in the same manner as in example 1.
Comparative example 5
The handmade soap of this comparative example, which had the same composition and volume fraction as in example 1 except that 3 parts of citrus essential oil was used, was named soap D5.
The handmade soap of this comparative example was prepared in the same manner as in example 1.
Comparative example 6
The handmade soap of this comparative example was obtained as soap D6, except that 3 parts of lavender essential oil were used, and the other components and volume fractions were the same as those of example 1.
The handmade soap of this comparative example was prepared in the same manner as in example 1.
Comparative example 7
The handmade soap of this comparative example, which had the same composition and volume fraction as in example 1 except for 3 parts of cinnamon essential oil, was obtained and was named soap D7.
The handmade soap of this comparative example was prepared in the same manner as in example 1.
The anti-aging performance, moisturizing performance and bacteriostatic performance of the water lily compound essential oil handmade soap with the anti-aging effect prepared in the above examples 1-5 and the handmade soaps prepared in the comparative examples 1-7 are tested, and the specific experimental methods and experimental results are as follows:
application example 1 anti-aging Performance test of handmade soap
The method for measuring the free radical scavenging capacity of the handmade soap by adopting the DPPH method comprises the following specific experimental methods and experimental results:
1. experimental methods
Weighing 1mg of DPPH, dissolving in 40mL of absolute ethyl alcohol, and sufficiently shaking to uniformly mix the upper part and the lower part to obtain the DPPH with the concentration of 0.025 mg/mL;
accurately sucking 2mL of DPPH solution with the concentration of 0.025mg/mL, uniformly mixing with 2mL of absolute ethyl alcohol, taking a corresponding solvent (4mL of absolute ethyl alcohol) as a control, and measuring an absorbance value A0 of the solution at 517nm by using a spectrophotometer; accurately sucking 2mL of soap solution to be detected, respectively mixing with 2mL of DPPH solution with the concentration of 0.025mg/mL, shaking uniformly, standing for 30min, adjusting zero by taking a corresponding solvent (absolute ethyl alcohol) as a control, respectively measuring the absorbance values A1 of the solutions at 517nm by using a spectrophotometer, and respectively measuring the A1 values; accurately sucking 2mL of soap solution to be detected, respectively and uniformly mixing with 2mL of absolute ethyl alcohol, taking a corresponding solvent (absolute ethyl alcohol) as a reference for zero adjustment, respectively measuring the absorbance value A2 of each mixed solution at the wavelength of 517nm by using a spectrophotometer, and respectively measuring the A2 value; the above experimental procedure was repeated three times to obtain an average.
The radical clearance was calculated by substituting the above measured data into the following formula:
wherein, A0: 2mL of anhydrous ethanol solvent, and then mixing the solution with 2mL of anhydrous ethanol solvent to obtain an absorbance value at the wavelength of 517 nm; a1: mixing 2mL of soap solution and 2mL of DPPH solution, and then obtaining an absorbance value at the wavelength of 517 nm; a2: absorbance at 517nm after mixing 2mL of soap solution with 2mL of absolute ethanol solvent.
2. Results of the experiment
The results of measuring the free radical scavenging capacity of the handmade soaps prepared in the examples 1-5 and the comparative examples 1-7 are shown in table 1, and it can be seen that the free radical scavenging rate of the handmade soaps prepared in the examples 1-5 is significantly higher than that of the comparative examples 1-7, which indicates that the water lily essential oil, the citrus essential oil, the lavender essential oil and the cinnamon essential oil have a synergistic effect when being compounded, the four essential oils are absent, the free radical scavenging capacity of the handmade soaps prepared is significantly improved, and the anti-oxidation and anti-aging effects are good; the free radical scavenging capacity of the handmade soap prepared in example 1 is obviously higher than that of examples 2-5, and the effect of example 1 is best.
TABLE 1 measurement results of radical scavenging ability of handmade soaps prepared in examples 1 to 5 and comparative examples 1 to 7
| Clearance rate | Soap A1 | Soap A2 | Soap A3 | Soap A4 | Soap A5 | Soap D1 | Soap D2 | Soap D3 | Soap D4 | Soap D5 | Soap D6 | Soap D7 |
| 1 | 96.26％ | 80.6％ | 82.24％ | 92.47％ | 89.16％ | 26.69％ | 19.69％ | 28.02％ | 30.25％ | 27.25％ | 27.68％ | 25.15％ |
| 2 | 70.23％ | 60.14％ | 62.14％ | 65.78％ | 66.18％ | 19.86％ | 26.60％ | 45.36％ | 28.56％ | 23.12％ | 32.15％ | 30.15％ |
| 3 | 88.85％ | 75.45％ | 79.47％ | 83.25％ | 85.29％ | 24.41％ | 31.81％ | 29.58％ | 35.14％ | 28.28％ | 29.46％ | 29.43％ |
| Mean clearance rate | 83.78％ | 72.06％ | 74.61％ | 80.5％ | 80.21％ | 23.65％ | 26.03％ | 34.32％ | 31.32％ | 26.22％ | 29.76％ | 28.24％ |
Application example 2 antibacterial Performance test of handmade soap
Paper sheet diffusion method
1. Experimental methods
Respectively culturing Staphylococcus aureus (bacterium A), Escherichia coli (bacterium B), Bacillus subtilis (bacterium C) and Pseudomonas aeruginosa (bacterium D) with beef extract peptone liquid culture medium, and diluting each bacterium solution to 1 × 10 with turbidimeter before use8CFU·mL。
Sterilizing beef extract peptone agarThe culture medium is injected into a culture dish with the diameter of 9cm, after the culture medium is solidified, 100 mu L of bacterial liquid is respectively sucked by a pipette gun and evenly smeared on a flat plate, and then filter paper with the diameter of 6mm after dry heat sterilization is flatly attached to the center of a paper board by using tweezers. 4 single essential oils of water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil, and the compound essential oils of examples 1 to 5 and comparative examples 1 to 7 were passed through a 0.45 μm microporous filter membrane, and 10 μ L of the compound essential oil was pipetted and dropped onto a filter paper sheet, and each treatment was repeated three times. Tween 80 was set as a control group, and a positive control (antibiotic) was selected for the four bacteria as penicillin (10 mg. mL)-1). After the essential oil is fully absorbed, the mixture is subjected to inverted culture at 37 ℃ for 24 hours, the diameter of the inhibition zone is measured, and the average value of three measurements is taken. It was judged which of the handmade soaps of examples 1 to 5 and comparative examples 1 to 7 had the best bacteriostatic properties and whether or not a synergistic effect was achieved.
2. Results of the experiment
The results of the test on the inhibition zone size of the handmade soaps of examples 1 to 5 and comparative examples 1 to 7 are shown in table 2, and it can be seen that when the essential oil is used alone (single-component essential oil), the inhibition effect of the citrus essential oil and the lavender essential oil on four bacteria is not ideal, while the inhibition effect of the cinnamon essential oil and the water lily essential oil on four bacteria is good, wherein the inhibition effect on bacillus subtilis (bacterium C) is the best; when the essential oil is used in a compounding manner (compound essential oil), the radius of the inhibition zone of the handmade soap in the examples 1-5 is obviously larger than that of the handmade soap in the comparative examples 1-7, and the inhibition zone radius of the handmade soap is larger than that of the single essential oil; the inhibition effect on bacteria is synergistic when the water lily essential oil, the citrus essential oil, the lavender essential oil and the cinnamon essential oil are compounded, and the inhibition performance of the prepared handmade soap is obviously improved; the bacteriostatic effect of the embodiment 1 is obviously better than that of the embodiments 2-5, and the bacteriostatic effect of the embodiment 1 is the best.
TABLE 2 inhibition zone size test results (inhibition zone radius r, mm) of handmade soaps of examples 1 to 5 and comparative examples 1 to 7
| Test object | Bacterium A | Bacterium B | Bacterium C | Bacterium D |
| Water lily essential oil | 10.25 | 10.2 | 10.5 | 10.4 |
| Citrus essential oil | 5.57 | 7.21 | 4.22 | 2.14 |
| Lavender essential oil | 11.12 | 8.7 | 8.0 | 5.57 |
| Cinnamon essential oil | 17.24 | 15.22 | 15.14 | 17.22 |
| Soap A1 | 25.56 | 29.54 | 28.56 | 28.14 |
| Soap A2 | 19.25 | 25.47 | 24.48 | 19.54 |
| Soap A3 | 18.87 | 21.72 | 20.57 | 21.25 |
| Soap A4 | 20.24 | 28.45 | 27.57 | 21.46 |
| Soap A5 | 24.25 | 27.49 | 25.36 | 21.55 |
| Soap D1 | 11.87 | 15.45 | 17.57 | 13.54 |
| Soap D2 | 12.78 | 16.57 | 15.14 | 12.56 |
| Soap D3 | 10.24 | 14.26 | 17.65 | 12.54 |
| Soap D4 | 10.52 | 10.15 | 15.15 | 10.97 |
| Soap D5 | 9.15 | 10.26 | 12.14 | 9.15 |
| Soap D6 | 10.26 | 12.16 | 12.15 | 10.25 |
| Soap D7 | 9.59 | 12.67 | 17.56 | 12.15 |
Second, hand experiment
1. Experimental methods
The test subjects washed the fingers of the left and right hands with clean water, the handmade soaps of examples 1 to 5, the handmade soaps of comparative examples 1 to 7, and commercial bacteriostatic soaps, respectively, after washing with running water, wiped with a nonwoven fabric sterilized at high temperature and high pressure, after wiping, the fingers of the left and right hands were randomly smeared and sampled with the nonwoven fabric within 1h, 2h, 3h, and 4h, respectively, after which the nonwoven fabric was placed in a conical flask containing an MH broth culture medium, after incubation for 18h at constant temperature, the number of bacteria was recorded with a turbidimeter. The bacteriostatic effects of the handmade soaps of examples 1-5, comparative examples 1-7 and commercial bacteriostatic soaps were compared by the concentration of bacteria.
2. Results of the experiment
The results of the effects of the handmade soaps of examples 1 to 5, the handmade soaps of comparative examples 1 to 7, and the commercial bacteriostatic soap on the concentration of bacteria on the hands of the subjects within 4 hours are shown in table 3, and it can be seen that the bacteria on the hands of the subjects are increased significantly in a certain period of time with the increase of time, but the increase degree is different.
In the beginning of the experiment (within 0-1 h), subject 3 had the least number of bacteria on the hands after using the handmade soap of example 1; with the increase of time (within 1-3 h), the number of bacteria on the hands of each subject using the handmade soap of example 1 is lower than that of the handmade soap of clear water, the handmade soaps of comparative examples 1-7 and the commercially available antibacterial soap; at the end of the experiment (within 3-4 h), the number of bacteria on the hands of the subjects using the handmade soap of example 1 was significantly lower than the number of bacteria on the hands after using clear water, the handmade soaps of comparative examples 1-7 and the commercial bacteriostatic soap; the hand soap in the embodiments 1 to 5 has a remarkable continuous bacteriostatic ability, that is, when the water lily essential oil, the citrus essential oil, the lavender essential oil and the cinnamon essential oil are compounded, the hand soap has a synergistic effect on the inhibition effect of bacteria. The bacteria concentration of example 1 was significantly lower than those of examples 2 to 5 at each time period, indicating that the bacteriostatic effect of example 1 was the best.
The above results illustrate that: compared with the commercially available antibacterial soap, the handmade soap prepared in the embodiments 1-5 of the invention has obvious and continuous antibacterial performance.
TABLE 3 results of the effect of the handmade soaps of examples 1 to 5, the handmade soaps of comparative examples 1 to 7, and the commercial bacteriostatic soap on the concentration of bacteria on the hands of the test subjects within 4h (10)8CFU·mL)
Application example 3 moisturizing Performance test of handmade soap
1. Experimental methods
20 healthy skin volunteers were selected and divided into 5 groups. At a position of 5 cm square on the inner side of the right arm, a test area was drawn, 20 volunteers were washed with the handmade soaps prepared in examples 1 to 5 and comparative examples 1 to 7, respectively, skin moisture content of the volunteers before and after 1 hour of washing was measured with a moisture tester, and a percentage of increase in skin moisture content of the volunteers was calculated.
2. Results of the experiment
The results of the percentage influence of the handmade soaps of examples 1-5 and comparative examples 1-7 on the increase of the moisture content of the skin are shown in table 4, and it can be seen that the moisturizing performance of the handmade soaps of examples 1-5 is significantly higher than that of comparative examples 1-7, which shows that when the water lily essential oil, the citrus essential oil, the lavender essential oil and the cinnamon essential oil are compounded, the moisturizing performance of the handmade soaps is significantly improved, and the moisturizing performance of the handmade soaps is significantly improved; volunteers had a problem of decreased skin moisture content after washing with the hand soap of the comparative example; the moisturizing effect of the embodiment 1 is obviously better than that of the embodiments 2-5, and the moisturizing effect of the embodiment 1 is the best.
TABLE 4 The% effect on skin moisture content increase of handmade soaps of examples 1-5 and comparative examples 1-7 on results
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (10)
1. The plant compound essential oil with the anti-aging effect is characterized by comprising water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil; the volume ratio of the water lily essential oil to the citrus essential oil to the lavender essential oil to the cinnamon essential oil is (5-10): (0.5-3): (0.5-3): (0.5 to 3).
2. The plant compound essential oil according to claim 1, wherein the volume ratio of the water lily essential oil, the citrus essential oil, the lavender essential oil and the cinnamon essential oil is (7-10): (1-2): (1-2): (1-2).
3. Use of the plant compound essential oil of claim 1 or 2 in the preparation of daily chemical products with anti-aging effect.
4. The water lily compound essential oil handmade soap with anti-aging effect is characterized by comprising the plant compound essential oil of claim 1 or 2.
5. The handmade soap of claim 4, consisting of the following components in volume fractions: 5-10 parts of water lily essential oil, 0.5-3 parts of citrus essential oil, 0.5-3 parts of lavender essential oil, 0.5-3 parts of cinnamon essential oil, 0.1-1 part of vitamin E and 50-100 parts of soap base.
6. The handmade soap of claim 5, consisting of the following components in volume fractions: 7-10 parts of water lily essential oil, 1-2 parts of citrus essential oil, 1-2 parts of lavender essential oil, 1-2 parts of cinnamon essential oil, 0.2-0.6 part of vitamin E and 75-100 parts of soap base.
7. A process for the preparation of handmade soap as claimed in any one of claims 4 to 6, characterized in that it comprises the following steps:
s1, mixing water lily essential oil, citrus essential oil, lavender essential oil and cinnamon essential oil according to the volume ratio of claim 5 or 6, and carrying out ultrasonic oscillation to obtain composite essential oil;
s2, heating the soap base to melt, mixing the soap base and the compound essential oil obtained in the step S1 according to the volume ratio of claim 5 or 6, stirring, pouring into a mold, and cooling to obtain the handmade soap.
8. The method according to claim 7, wherein the oscillation frequency of step S1 is 50-70 hz, and the oscillation time is 15-30S.
9. The method according to claim 7, wherein the stirring speed in step S2 is 10-30 r/min, and the stirring time is 5-15 min.
10. The preparation method according to claim 7, wherein the water lily essential oil is extracted by supercritical method; the citrus essential oil adopts supercritical CO2Extracting by an extraction method; extracting the lavender essential oil by adopting a steam distillation method; the cinnamon essential oil is extracted by an ultrahigh pressure method.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911075491.5A CN110951553B (en) | 2019-11-06 | 2019-11-06 | Water lily compound essential oil handmade soap with anti-aging effect and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911075491.5A CN110951553B (en) | 2019-11-06 | 2019-11-06 | Water lily compound essential oil handmade soap with anti-aging effect and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110951553A true CN110951553A (en) | 2020-04-03 |
| CN110951553B CN110951553B (en) | 2021-06-25 |
Family
ID=69976079
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911075491.5A Active CN110951553B (en) | 2019-11-06 | 2019-11-06 | Water lily compound essential oil handmade soap with anti-aging effect and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110951553B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105112180A (en) * | 2015-09-09 | 2015-12-02 | 中国科学院植物研究所 | Natural plant flower fragrance type essential oil soap having bacteriostatic function and producing method thereof |
| CN110042020A (en) * | 2019-05-07 | 2019-07-23 | 海南大学 | A kind of antibacterial handmade soap of essential oil and preparation method thereof |
| KR20200056256A (en) * | 2018-11-14 | 2020-05-22 | 방진영 | Method of processing for rice |
-
2019
- 2019-11-06 CN CN201911075491.5A patent/CN110951553B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105112180A (en) * | 2015-09-09 | 2015-12-02 | 中国科学院植物研究所 | Natural plant flower fragrance type essential oil soap having bacteriostatic function and producing method thereof |
| KR20200056256A (en) * | 2018-11-14 | 2020-05-22 | 방진영 | Method of processing for rice |
| CN110042020A (en) * | 2019-05-07 | 2019-07-23 | 海南大学 | A kind of antibacterial handmade soap of essential oil and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110951553B (en) | 2021-06-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108158869B (en) | Antibacterial wet tissue liquid, wet tissue and preparation method of wet tissue | |
| CN106266685B (en) | A kind of compound essential oil and preparation method thereof | |
| CN106362183A (en) | Deodorant, preparation method and application thereof | |
| CN111714543A (en) | Herbal essential oil with sterilization effect and preparation method and application thereof | |
| CN104127358A (en) | Honeysuckle extract and preparation method thereof as well as floral water and preparation method thereof | |
| KR102227273B1 (en) | Car cleaning composition containing graphene with enhanced cleaning and coating functions | |
| CN113207915B (en) | Essential oil composition and preparation method thereof | |
| CN106318707A (en) | Environment-friendly detergent and preparation method thereof | |
| CN106619373A (en) | Garlicin hand cream | |
| CN101849889A (en) | Fragrance-lasting natural essential oil nanoemulsion used for cosmetology and SPA (essential oil therapy) and preparation method thereof | |
| CN110951553B (en) | Water lily compound essential oil handmade soap with anti-aging effect and preparation method thereof | |
| KR102174199B1 (en) | Manufacturing method for fermented oil of houttuynia cordata comprising wood-cultivated ginseng ingredient and fermented oil of houttuynia cordata manufactured by the same | |
| CN107412038A (en) | A kind of compound essential oil and its preparation method and application | |
| JP2015074757A (en) | Method for producing extract from rush and dementia preventive therapeutic agent utilizing olfactory sense | |
| CN107137316B (en) | Dendrobium lip balm and preparation method thereof | |
| CN105726363A (en) | Plant care composition and preparation method thereof | |
| CN110507572A (en) | A kind of bacteriostasis, and deodorization toothpaste and preparation method thereof | |
| KR20110011257A (en) | Natural detergent composition and preparation method thereof | |
| CN110151627A (en) | A kind of graphene-based clean facial cleanser | |
| CN110699197A (en) | Preparation method and preparation system of pepper degerming soap | |
| CN110402969A (en) | A kind of environmental type plant source thimerosal | |
| CN115212337A (en) | Green persimmon deodorization and bacteriostasis spray and preparation method thereof | |
| Meduri et al. | Formulation and evaluation of fermented rice water herbal shampoo | |
| KR20150141078A (en) | Composition for removing the odor from aged person | |
| KR102267620B1 (en) | Method for Manufacture of Deodorant Sanitary Materials |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |