CN115212337A - Green persimmon deodorization and bacteriostasis spray and preparation method thereof - Google Patents

Abstract

The invention relates to the technical field of pet care, and particularly discloses a persimmon deodorization and bacteriostasis spray which comprises the following components in parts by weight: 10-30 parts of green persimmon extract, 6-14 parts of motherwort extract, 5-15 parts of lysimachia foenum-graecum extract, 0.2-0.8 part of silver fulvate, 0.3-0.7 part of cetylpyridinium chloride, 0.2-0.4 part of polyaminopropyl biguanide, 0.1-0.3 part of PEG-60 hydrogenated castor oil, 0.1-0.3 part of menthol and 55-65 parts of deionized water. The invention overcomes the defects of the prior art, improves the removal rate of the peculiar smell of pets by the natural extracted green persimmon extract, the motherwort leaching solution and the lysimachia foenum-graecum leaching solution, and simultaneously uses the fulvic acid silver, the cetylpyridinium chloride and the polyaminopropyl biguanide to compound an antiseptic system, and the compound antiseptic system has the advantages of mildness, low irritation and strong bacteriostatic effect.

Description

Green persimmon deodorization and bacteriostasis spray and preparation method thereof

Technical Field

The invention relates to the technical field of pet care, and particularly belongs to a persimmon deodorization and bacteriostasis spray and a preparation method thereof.

Background

The physical life of people is greatly improved at present, the breeding of pets is quite popular at present, the domestic pets can increase much fun of a family in life, and in addition, the breeding of small animals can bring consolation to the solitary old people; patients receiving the visit of the small animals can improve the mood of depression and even relieve the pain; the family for raising the pet has added joy and cohesion; companion animals generally have a family-like relationship with their owners.

At present, peculiar smell is easily generated in the process of raising pets, the individual smell of the pets is wide in source, such as stink smell brought by oil secreted by sweat glands, peculiar smell of excrement, odor generated by accumulated hair, and the like, and the odor is easily generated after the odor comes into contact with bacteria, viruses and parasites through the peculiar smell glands, urine, saliva, excrement, and the like, so that the pets generate the peculiar smell; most of the existing deodorization products are mainly based on physical adsorption, but the effect tends to saturation easily, and the existing bacteria are not inhibited; the biological deodorant has limited use effect, is easily influenced by the activity of biological enzymes, and has poor bacteriostatic effect.

Disclosure of Invention

The invention aims to provide a persimmon deodorization and bacteriostasis spray and a preparation method thereof, which overcome the defects of the prior art, improve the removal rate of pet odor through a naturally extracted persimmon extract, a motherwort leaching solution and a lysimachia foenum-graecum leaching solution, and simultaneously use a silver fulvate, cetylpyridinium chloride and polyaminopropyl biguanide to compound an anticorrosion system, wherein the compound anticorrosion system has the advantages of mildness, low irritation and strong bacteriostasis effect.

In order to solve the problems, the technical scheme adopted by the invention is as follows:

the green persimmon deodorization and bacteriostasis spray comprises the following components in parts by weight: 10-30 parts of green persimmon extract, 6-14 parts of motherwort extract, 5-15 parts of lysimachia foenum-graecum extract, 0.2-0.8 part of silver fulvate, 0.3-0.7 part of cetylpyridinium chloride, 0.2-0.4 part of polyaminopropyl biguanide, 0.1-0.3 part of PEG-60 hydrogenated castor oil, 0.1-0.3 part of menthol and 55-65 parts of deionized water.

Further, the persimmon deodorization and bacteriostasis spray comprises the following components in parts by weight: 20 parts of green persimmon extract, 10 parts of motherwort extract, 10 parts of lysimachia foenum-graecum extract, 0.5 part of silver fulvate, 0.5 part of cetylpyridinium chloride, 0.3 part of polyaminopropyl biguanide, 0.2 part of PEG-60 hydrogenated castor oil, 0.2 part of menthol and 60 parts of deionized water.

Further, the preparation method of the green persimmon extract comprises the following steps:

(1) Selecting the eighty-nine ripe persimmons from late 7 months to late 9 months per year, cleaning and removing stems; the green persimmon is not whitened, yellowed or reddened in color;

(2) Crushing the cleaned green persimmon, juicing, and carrying out rough filtration to remove peel and residues to obtain juice;

(3) Transferring the obtained juice into a fermentation tank, adding deionized water into the fermentation tank according to the mass ratio of 1 (1-3), and continuously fermenting for two years under the condition of stirring;

(4) Filtering the fermented mixed juice, taking the filtrate, and drying to obtain a dehydrated light yellow powdered green persimmon extract;

(5) 2-8 parts of green persimmon extract, 20-40 parts of deionized water, 10-50 parts of butanediol and 20-60 parts of sodium lactate are respectively taken according to the parts by weight, put into a proportioning pot, continuously stirred for 48 hours, then kept stand for 24 hours and filtered to obtain a light yellow liquid green persimmon extract.

Further, the stirring speed of the stirring in the step (3) and the step (5) is 300-400 r/min.

Further, the preparation method of the motherwort leaching solution comprises the following steps:

(1) Selecting motherwort, cleaning in a medicine washing machine, and crushing and grinding the motherwort after cleaning;

(2) Adding deionized water into the herba Leonuri pulverized material, boiling, filtering to obtain a first filtrate, adding equal amount of deionized water, boiling again, filtering to obtain a second filtrate, and mixing the first filtrate and the second filtrate;

(3) And heating and concentrating the combined filtrate to obtain a thick paste motherwort extract with the relative density of 1.2.

Further, the preparation method of the lysimachia foenum-graecum leaching solution comprises the following steps:

(1) Selecting lysimachia foenum-graecum hance, cleaning, and cutting into lysimachia foenum-graecum hance sections of 1-3 cm;

(2) Soaking the lysimachia foenum-graecum hance segments in deionized water for 10-15min, transferring the soaked lysimachia foenum-graecum hance ends to a steam distillation device, and distilling to extract a first extract;

(3) Redistilling the distillate remaining after distillation, adding sodium chloride or potassium chloride into the distillate for salting out, and then adding an organic solvent for extraction to obtain a second extract;

(4) Mixing the first extract and the second extract to obtain the lysimachia foenum-graecum leaching solution.

The invention also provides a preparation method of the persimmon deodorization and bacteriostasis spray, which comprises the following steps:

the method comprises the following steps: putting deionized water into a batching pot according to the volatile amount of 1.03, heating to 80-85 ℃, adding cetylpyridinium chloride under the condition of continuous stirring, continuously stirring for 30min until the solution is dissolved, cooling to 45 ℃, sequentially adding a green persimmon extract, a motherwort extract, a lysimachia foenum-graecum extract and poly aminopropyl biguanide, and fully stirring to obtain a phase A;

step two: adding silver fulvate, PEG-60 hydrogenated castor oil, and menthol into a sterilized container, and stirring for 30min to obtain phase B;

step three: adding the uniformly mixed phase B into the phase A, and continuously stirring for 60min;

step four: taking materials, checking the pH value, and filling after the detection is qualified to obtain the persimmon deodorization and bacteriostasis spray.

Compared with the prior art, the invention has the following implementation effects:

according to the invention, the removal rate of the pet odor is improved by the natural extracted green persimmon extract, the motherwort leaching solution and the lysimachia foenum-graecum leaching solution, and meanwhile, the compound preservative system is compounded by three bacteriostatic agents, namely silver fulvate, cetylpyridinium chloride and polyaminopropyl biguanide, and has the advantages of mildness, low irritation and strong bacteriostatic effect.

Detailed Description

The present invention will be further described with reference to the following examples, but the present invention is not limited to these examples, and any modifications within the scope of the present invention are intended to be included within the spirit of the present invention.

Example 1

The embodiment discloses a preparation method of a persimmon deodorization and bacteriostasis spray, which comprises the following steps:

step one, preparing a green persimmon extract:

(1) Selecting the eight-nine ripe green persimmons from late 7 to late 9 months per year, cleaning and removing pedicels; the color of the green persimmon is not changed into white, yellow or red;

(2) Crushing the cleaned green persimmon, juicing, and carrying out rough filtration to remove peel and residues to obtain juice;

(3) Transferring the obtained juice into a fermentation tank, adding deionized water into the fermentation tank according to the mass ratio of 1:1, and continuously fermenting for two years under the condition of stirring speed of 300-400 r/min;

(4) Filtering the fermented mixed juice, taking the filtrate, and drying to obtain a dehydrated light yellow powdered green persimmon extract;

(5) 2 parts of the green persimmon extract, 20 parts of deionized water, 10 parts of butanediol and 20 parts of sodium lactate are respectively taken according to the parts by weight, put into a proportioning pot, continuously stirred at the stirring speed of 300-400 r/min for 48 hours, then kept stand for 24 hours and filtered to obtain the green persimmon extract liquid in a light yellow liquid state.

Step two, preparing a motherwort leaching solution:

(1) Selecting motherwort, cleaning in a medicine washing machine, and crushing and grinding the motherwort after cleaning;

(2) Adding deionized water into the herba Leonuri pulverized material, boiling, filtering to obtain a first filtrate, adding equal amount of deionized water, boiling again, filtering to obtain a second filtrate, and mixing the first filtrate and the second filtrate;

(3) And heating and concentrating the combined filtrate to obtain a concentrated motherwort extract with the relative density of 1.2.

Step three, preparing a lysimachia foenum-graecum hance extract:

(1) Selecting lysimachia foenum-graecum hance, cleaning, and cutting into lysimachia foenum-graecum hance sections of 1-3 cm;

(2) Soaking the lysimachia foenum-graecum hance segments in deionized water for 10-15min, transferring the soaked lysimachia foenum-graecum hance ends to a steam distillation device, and distilling to extract a first extract;

(3) Redistilling the distillate remaining after distillation, adding sodium chloride or potassium chloride into the distillate for salting out, and then adding an organic solvent for extraction to obtain a second extract;

(4) Mixing the first extract and the second extract to obtain the lysimachia foenum-graecum leaching solution.

Step four, preparing phase A: putting 55 parts of deionized water into a batching pot according to the volatile amount of 1.03, heating to 80-85 ℃, adding 0.3 part of cetylpyridinium chloride under the condition of continuous stirring, continuously stirring for 30min to dissolve, cooling to 45 ℃, and sequentially adding 10 parts of green persimmon extract, 6 parts of motherwort extract, 5 parts of lysimachia foenum-graecum extract and 0.2 part of polyaminopropyl biguanide, and fully stirring to obtain phase A.

Step five, preparing a phase B: adding 0.2 part of silver fulvate, 0.1 part of PEG-60 hydrogenated castor oil and 0.1 part of menthol into a fully sterilized container, and continuously stirring at 300-400 rpm for 30min to mix uniformly to obtain phase B.

Step six, mixing A, B phases: the uniformly mixed phase B was added to phase A and stirred for 60min.

Step seven, checking: taking materials, checking the pH value, and filling after the detection is qualified to obtain the persimmon deodorization and bacteriostasis spray.

Example 2

The preparation method disclosed in this example is substantially the same as that of example 1, except that: the persimmon deodorization and bacteriostasis spray comprises the following components in parts by weight: 20 parts of green persimmon extract, 10 parts of motherwort extract, 10 parts of lysimachia foenum-graecum extract, 0.5 part of silver fulvate, 0.5 part of cetylpyridinium chloride, 0.3 part of polyaminopropyl biguanide, 0.2 part of PEG-60 hydrogenated castor oil, 0.2 part of menthol and 60 parts of deionized water.

Example 3

The preparation method disclosed in this example is substantially the same as that of example 1, except that: the persimmon deodorization and bacteriostasis spray comprises the following components in parts by weight: 30 parts of green persimmon extract, 14 parts of motherwort extract, 15 parts of lysimachia foenum-graecum extract, 0.8 part of silver fulvate, 0.7 part of cetylpyridinium chloride, 0.4 part of polyaminopropyl biguanide, 0.3 part of PEG-60 hydrogenated castor oil, 0.3 part of menthol and 65 parts of deionized water.

Example 4

The preparation method disclosed in this example is substantially the same as that of example 1, except that: the preparation method of the green persimmon extract comprises the following raw materials: 5 parts of green persimmon extract, 30 parts of deionized water, 30 parts of butanediol and 40 parts of sodium lactate.

Example 5

The preparation method disclosed in this example is substantially the same as that of example 1, except that: the preparation method of the green persimmon extract comprises the following raw materials: 8 parts of green persimmon extract, 40 parts of deionized water, 50 parts of butanediol and 60 parts of sodium lactate.

Example 6

The preparation method disclosed in this example is substantially the same as that of example 1, except that: the mass ratio of the juice in the fermentation tank to the deionized water in the extraction process of the green persimmon extract is 1:3.

And (3) detection:

the analytical detection standard, the detection method and the data of the deodorization and bacteriostasis spray of the green persimmon are as follows:

1. detection standard: the removal rate of the product on methyl mercaptan, hydrogen sulfide and ammonia is determined by referring to GB/T11742-89, QB/T2761-2006 and GB/T18883-2002.

2. The detection method comprises the following steps:

2.1 conditions: six air test chambers (A is a blank chamber, and B is a sample chamber) are used for testing the concentration of the decontamination product for removing gas pollutants. The experimental conditions were normal temperature and normal pressure.

2.2 pretreatment of the test chamber:

2.2.1 the air test chamber is kept clean, the air quality in the chamber is purified to the maximum extent, and no pollutant is ensured.

2.2.2 release profiles of the sources were made separately for the two compartments before the test, and after being essentially parallel, the routine test was performed.

Preparation of the Release Source:

5 layers of 17cm by 40cm medical absorbent gauze are rolled on 2 glass rods with the diameter of 5mm and the length of 30cm, fixed by cotton threads, and are respectively vertically taken and placed in 500ml reagent bottles, 6 bottles are counted, 200ml of pollutants with the concentration of 0.2 percent of hydrogen sulfide, 0.2 percent of methyl mercaptan and 1 percent of ammonia are filled, containers are marked as A1, B1, A2, B2, A3 and B3, and each release source comprises two bottles. The reagents are analytically pure, and after the gauze is completely soaked. The product can be used.

4, experimental steps:

4.1 suspending untreated base paper in three blank test chambers A respectively, and suspending base paper sprayed with the deodorizing and bacteriostatic spray of the green persimmon in three test chambers B respectively.

4.2 containers with the prepared pollutant release sources A1, B1, A2, B2, A3, B3 are placed in the blank test chamber A and the sample test chamber B respectively, and the chamber door is closed immediately.

4.3 turn on all fans of the blank test chamber and the sample test chamber, and stir for 1min. The air in the cabin and the pollutants released by the releasing source are mixed uniformly. And simultaneously, the fan is turned off, air sampling is carried out in the blank cabin, and the concentration values of pollutants in the air in the blank cabin are measured as initial concentrations which are respectively marked as C0I, C0 II and C0 III.

4.4 And after 24h, sampling the concentration of the air pollutants in 6 cabins, and analyzing and testing. Namely, the concentration values in 6 chambers in a certain time period are marked as CA1, CB1, CA2, CB2, CA3 and CB3.

5, calculating the removal rate:

the persimmon deodorization and bacteriostasis sprays prepared in examples 1 to 6 were counted according to the above detection methods and standards, and the statistical results are shown in table 1:

TABLE 1 statistical table of test results

The results in table 1 show that the persimmon deodorizing and bacteriostatic spray disclosed by the application has a good removal rate for various odors, and the natural extract enables the prepared spray to have no strong fragrance, so that the smell of animals cannot be damaged, and the spray is deodorized from the source of the odor, so that the using effect is better.

The foregoing is merely exemplary and illustrative of the present inventive concept and various modifications, additions and substitutions of similar embodiments may be made to the specific embodiments described by those skilled in the art without departing from the inventive concept or exceeding the scope of the claims as defined in the accompanying claims.

Claims (7)

1. A green persimmon deodorization and bacteriostasis spray is characterized in that: the composition comprises the following components in parts by weight: 10-30 parts of green persimmon extract, 6-14 parts of motherwort extract, 5-15 parts of lysimachia foenum-graecum extract, 0.2-0.8 part of silver fulvate, 0.3-0.7 part of cetylpyridinium chloride, 0.2-0.4 part of polyaminopropyl biguanide, 0.1-0.3 part of PEG-60 hydrogenated castor oil, 0.1-0.3 part of menthol and 55-65 parts of deionized water.

2. The persimmon deodorization and bacteriostasis spray as claimed in claim 1, which is characterized in that: the persimmon deodorization and bacteriostasis spray comprises the following components in parts by weight: 20 parts of green persimmon extract, 10 parts of motherwort extract, 10 parts of lysimachia foenum-graecum extract, 0.5 part of silver fulvate, 0.5 part of cetylpyridinium chloride, 0.3 part of polyaminopropyl biguanide, 0.2 part of PEG-60 hydrogenated castor oil, 0.2 part of menthol and 60 parts of deionized water.

3. The persimmon deodorization and bacteriostasis spray as claimed in claim 1, which is characterized in that: the preparation method of the green persimmon extract liquid comprises the following steps:

(1) Selecting the eight-nine ripe green persimmons from late 7 to late 9 months per year, cleaning and removing pedicels; the color of the green persimmon is not changed into white, yellow or red;

(2) Crushing the cleaned green persimmon, juicing, and carrying out rough filtration to remove peel and residues to obtain juice;

(3) Transferring the obtained juice into a fermentation tank, adding deionized water into the fermentation tank according to the mass ratio of 1 (1-3), and continuously fermenting for two years under the condition of stirring;

(4) Filtering the fermented mixed juice, taking the filtrate, and drying to obtain a dehydrated light yellow powdered green persimmon extract;

(5) 2-8 parts of green persimmon extract, 20-40 parts of deionized water, 10-50 parts of butanediol and 20-60 parts of sodium lactate are respectively taken according to the parts by weight, put into a proportioning pot, continuously stirred for 48 hours, then kept stand for 24 hours and filtered to obtain a light yellow liquid green persimmon extract.

4. The persimmon deodorization and bacteriostasis spray as claimed in claim 3, which is characterized in that: the stirring speed of the stirring in the step (3) and the step (5) is 300-400 r/min.

5. The persimmon deodorization and bacteriostasis spray as claimed in claim 1, which is characterized in that: the preparation method of the motherwort leaching solution comprises the following steps:

(1) Selecting motherwort, cleaning in a medicine washing machine, and crushing and grinding the motherwort after cleaning;

(2) Adding deionized water into the herba Leonuri pulverized material, boiling, filtering to obtain a first filtrate, adding equal amount of deionized water, boiling again, filtering to obtain a second filtrate, and mixing the first filtrate and the second filtrate;

(3) And heating and concentrating the combined filtrate to obtain a thick paste motherwort extract with the relative density of 1.2.

6. The persimmon deodorization and bacteriostasis spray as claimed in claim 1, which is characterized in that: the preparation method of the lysimachia foenum-graecum hance leaching solution comprises the following steps:

(1) Selecting lysimachia foenum-graecum hance, cleaning, and cutting into lysimachia foenum-graecum hance sections of 1-3 cm;

(2) Soaking the lysimachia foenum-graecum hance segments in deionized water for 10-15min, transferring the soaked lysimachia foenum-graecum hance ends to a steam distillation device, and distilling to extract a first extract;

(3) Redistilling the distillate remaining after distillation, adding sodium chloride or potassium chloride into the distillate for salting out, and then adding an organic solvent for extraction to obtain a second extract;

(4) Mixing the first extract and the second extract to obtain the lysimachia foenum-graecum leaching solution.

7. The preparation method of the persimmon deodorization and bacteriostasis spray as claimed in any one of claims 1 to 6, wherein the preparation method comprises the following steps: the method comprises the following steps:

the method comprises the following steps: putting deionized water into a mixing pot according to the volatile amount of 1.03, heating to 80-85 ℃, adding cetylpyridinium chloride under the condition of continuous stirring, continuously stirring for 30min until the solution is dissolved, cooling to 45 ℃, and sequentially adding a green persimmon extract, a motherwort extract, a lysimachia foenum-graecum extract and poly aminopropyl biguanide to stir fully to prepare a phase A;

step two: adding silver fulvate, PEG-60 hydrogenated castor oil, and menthol into a sterilized container, and stirring for 30min to obtain phase B;

step three: adding the uniformly mixed phase B into the phase A, and continuously stirring for 60min;

step four: taking the materials, checking the pH value of the materials, and filling the materials after the detection is qualified to obtain the deodorizing and bacteriostatic spray for the green persimmon.