CN102949310A - Traditional Chinese medicine antibacterial hand washing solution and preparation method thereof - Google Patents

Traditional Chinese medicine antibacterial hand washing solution and preparation method thereof Download PDF

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Publication number
CN102949310A
CN102949310A CN2012104266363A CN201210426636A CN102949310A CN 102949310 A CN102949310 A CN 102949310A CN 2012104266363 A CN2012104266363 A CN 2012104266363A CN 201210426636 A CN201210426636 A CN 201210426636A CN 102949310 A CN102949310 A CN 102949310A
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China
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chinese medicine
preparation
herba
medicine antibacterial
rosmarini officinalis
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CN2012104266363A
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CN102949310B (en
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肖军平
吴永忠
郭峰
李旭
刘立鼎
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JIANGXI POZIN PHARMACEUTICAL Co Ltd
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JIANGXI POZIN PHARMACEUTICAL Co Ltd
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Abstract

The invention relates to a traditional Chinese medicine antibacterial hand washing solution and a preparation method thereof, and belongs to the technical field of daily chemical industry. The traditional Chinese medicine antibacterial hand washing solution comprises hydroxyethyl cellulose, sodium lauryl polyoxyethylene ether sulfate, sodium dodecyl sulfate, coconut diethanolamide, Kathon CG, nature borneol, citric acid, sodium benzoate, flavor, a natural pigment, a groundsel and rosemary extract, and deionized water, and is prepared by adopting the following steps: adopting deionized water to heat and dissolve hydroxyethyl cellulose, heating, sequentially adding prescription amounts of sodium lauryl polyoxyethylene ether sulfate, sodium dodecyl sulfate, coconut diethanolamide, Kathon CG, sodium benzoate, nature borneol and citric acid, uniformly stirring until the materials are completely dissolved to achieve a transparent total liquid, adding a groundsel and rosemary extract to the total liquid, uniformly stirring, adding flavor and a pigment, and carrying out filling to obtain the finished product. According to the present invention, the traditional Chinese medicine extract and other components are subjected to mutual compatibility and optimized combination so as to improve functions of cleaning decontamination, antibacterial disinfection, skin nourishing care and the like of the hand washing solution at a maximum.

Description

A kind of Chinese medicine antibacterial handwashing liquid and preparation method thereof
Technical field
The invention belongs to the daily-use chemical industry technical field, relate in particular to a kind of Chinese medicine antibacterial handwashing liquid and preparation method thereof.
Background technology
At present, handwashing liquid is a kind of daily articles for washing that people welcome that more and more is subject to, handwashing liquid of a great variety.But in existing product, most of handwashing liquid only have cleaning decontamination function, and function singleness all is to realize cleaning action by chemical constituent, and cleaning effect is undesirable, easy chafe also, and feel during washing, skin protection moisture-keeping function are relatively poor.People wish to have a kind of can decontamination, again can antibiotic, nourishes rough skin, skin is had the handwashing liquid of protective effect.
Summary of the invention
The objective of the invention is for top described defective, a kind of existing cleaning dirt-removing functions is provided, have again antibiotic and sterilizing, moisten the Chinese medicine antibacterial handwashing liquid of nursing skin function.
Another object of the present invention provides a kind of preparation method of Chinese medicine antibacterial handwashing liquid.
The objective of the invention is to be achieved by the following technical programs.
A kind of Chinese medicine antibacterial handwashing liquid is comprised of the composition of following weight portion: hydroxyethyl-cellulose 240-480 part; Dodecyl Polyoxyethylene Ether sodium sulfate 200-400 part; Sodium lauryl sulphate 120-240 part; Cortex cocois radicis oleoyl diethanolamine 160-320 part; KF88 CG 15-30 part; Natural Broneolum Syntheticum 5-10 part; Citric acid 6-12 part; Sodium benzoate 2-4 part; Essence 2-4 part; Natural pigment 1-2 part; Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract 5-10 part; Deionized water 1000-2000 part, and adopt the following steps preparation:
⑴ deionized water heating for dissolving hydroxyethyl-cellulose, heating-up temperature is 20-50 ℃, after add successively Dodecyl Polyoxyethylene Ether sodium sulfate, sodium lauryl sulphate, Cortex cocois radicis oleoyl diethanolamine, KF88 CG, sodium benzoate, natural Broneolum Syntheticum and the citric acid of recipe quantity, stir to complete dissolving and make the total liquid of transparence;
⑵ be added to Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract in total liquid, stirs;
⑶ add essence and pigment, fill, and get final product.
Described hydroxyethyl-cellulose molecular weight is 2000-4000.
The preparation method of described Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract: Herba Senecionis Scandentis and Herba Rosmarini Officinalis feed intake by 7: 3 ratio, twice of the water supersound extraction that adds ten times of weight, each 2 hours, ultrasonic power is 40-80kw, temperature is room temperature, and the filtrate of extract is condensed into Herba Senecionis Scandentis and the Herba Rosmarini Officinalis extract that relative density is 1.1-1.25.
Described essence is a kind of in Fructus Citri Limoniae essence, muguet compound or the aloe flavour.
The color of described natural pigment is a kind of in viride nitens, the golden yellow or sapphirine.
The present invention has added Herba Senecionis Scandentis and the Chinese medicines such as Herba Rosmarini Officinalis extract and natural Broneolum Syntheticum, wherein, Herba Rosmarini Officinalis has astriction, can clean hair follicle and deep skin, and can allow pore more tiny, thereby allow skin seem finer and smoother more smooth, play the good efficacy of the greasy unclean skin of conditioning; Herba Senecionis Scandentis has the effects such as anti-inflammation, heat-clearing and toxic substances removing, antipruritic, treatment skin eczema furuncle, therefore can make handwashing liquid have the effect of more efficient antibiotic, sterilization; Natural Broneolum Syntheticum also is a kind of efficient germicide and Percutaneous absorption enhancer, can more effectively kill various antibacterials on hand, makes the effect of handwashing liquid more complete.
The invention has the beneficial effects as follows: Chinese medicine extract of the present invention and the mutual compatibility of other composition, optimum organization, the effects such as this hand cleanser products cleaning decontamination, antibiotic and sterilizing, moist nursing skin have been strengthened to greatest extent, and utilize state-of-the-art technology to the preparation of Chinese medicine extract, Chinese material medicine resource and production cost have been saved, improve the effect of medicine, be conducive to increase effect of the present invention.
Specific embodiment
Below the invention will be further described by specific embodiment, it should be understood that these embodiment only are used for explanation the present invention, do not limit the scope of the invention.
Embodiment 1.
Prescription forms: hydroxyethyl-cellulose (2000 molecular weight) 240kg, Dodecyl Polyoxyethylene Ether sodium sulfate 200kg, sodium lauryl sulphate 120kg, Cortex cocois radicis oleoyl diethanolamine 160kg, KF88 CG15kg, natural Broneolum Syntheticum 5kg, citric acid 6kg, sodium benzoate 2kg, Fructus Citri Limoniae essence 2kg, natural pigment 1kg, deionized water 10000L, Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract 5kg, make 20000 bottles (500ml/ bottles) altogether.
Employing following steps preparation: the preparation of (1) Chinese medicine extract: 140kg Herba Senecionis Scandentis and 60kg Herba Rosmarini Officinalis adding 2000L water are at room temperature carried out supersound extraction twice, each 2 hours, ultrasonic power is 60kw, filter, merging filtrate, be condensed into relative density and be 1.2 Chinese medical concrete, for subsequent use; (2) deionized water with formula ratio heats (40 ℃) dissolving hydroxyethyl-cellulose slightly, after add successively Dodecyl Polyoxyethylene Ether sodium sulfate, sodium lauryl sulphate, Cortex cocois radicis oleoyl diethanolamine, KF88 CG, sodium benzoate, natural Broneolum Syntheticum and the citric acid of recipe quantity, stir to complete dissolving and make the total liquid of transparence; (3) the Chinese medical concrete 5kg with (1) is added in total liquid, stirs; (4) at last at middle adding natural pigment and the Fructus Citri Limoniae essence of (3), stir, fill namely gets product.
Embodiment 2.
Prescription forms :Hydroxyethyl-cellulose (4000 molecular weight) 480kg, Dodecyl Polyoxyethylene Ether sodium sulfate 400kg, sodium lauryl sulphate 240kg, Cortex cocois radicis oleoyl diethanolamine 320kg, KF88 CG30kg, natural Broneolum Syntheticum 10kg, citric acid 12kg, sodium benzoate 4kg, muguet compound 4kg, natural pigment 2kg, deionized water 20000L, Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract 10kg make 40000 bottles (500ml/ bottles) altogether.
Employing following steps preparation: the preparation of (1) Chinese medicine extract: 280kg Herba Senecionis Scandentis and 120kg Herba Rosmarini Officinalis adding 4000L water are at room temperature carried out supersound extraction twice, each 2 hours, ultrasonic power is 80kw, filter, merging filtrate, be condensed into relative density and be 1.15 Chinese medical concrete, for subsequent use; (2) deionized water with formula ratio heats (40 ℃) dissolving hydroxyethyl-cellulose slightly, after add successively Dodecyl Polyoxyethylene Ether sodium sulfate, sodium lauryl sulphate, Cortex cocois radicis oleoyl diethanolamine, KF88 CG, sodium benzoate, natural Broneolum Syntheticum and the citric acid of recipe quantity, stir to complete dissolving and make the total liquid of transparence; (3) the Chinese medical concrete 10kg with (1) is added in total liquid, stirs; (4) at last at middle adding natural pigment and the muguet compound of (3), stir, fill namely gets product.
Embodiment 3.
Prescription forms: hydroxyethyl-cellulose (3000 molecular weight) 360kg, Dodecyl Polyoxyethylene Ether sodium sulfate 300kg, sodium lauryl sulphate 180kg, Cortex cocois radicis oleoyl diethanolamine 240kg, KF88 CG22.5kg, natural Broneolum Syntheticum 7.5kg, citric acid 9kg, sodium benzoate 3kg, aloe flavour 3kg, natural pigment 1.5kg, deionized water 15000L, Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract 7.5kg, make 30000 bottles (500ml/ bottles) altogether.
Employing following steps preparation: the preparation of (1) Chinese medicine extract: 210kg Herba Senecionis Scandentis and 90kg Herba Rosmarini Officinalis adding 3000L water are at room temperature carried out supersound extraction twice, each 2 hours, ultrasonic power is 60kw, filter, merging filtrate, be condensed into relative density and be 1.18 Chinese medical concrete, for subsequent use; (2) deionized water with formula ratio heats (50 ℃) dissolving hydroxyethyl-cellulose slightly, after add successively Dodecyl Polyoxyethylene Ether sodium sulfate, sodium lauryl sulphate, Cortex cocois radicis oleoyl diethanolamine, KF88 CG, sodium benzoate, natural Broneolum Syntheticum and the citric acid of recipe quantity, stir to complete dissolving and make the total liquid of transparence; (3) the Chinese medical concrete 7.5kg with (1) is added in total liquid, stirs; (4) at last at middle adding natural pigment and the aloe flavour of (3), stir, fill namely gets product.

Claims (10)

1. Chinese medicine antibacterial handwashing liquid, it is characterized in that: the composition by following weight portion forms: hydroxyethyl-cellulose 240-480 part; Dodecyl Polyoxyethylene Ether sodium sulfate 200-400 part; Sodium lauryl sulphate 120-240 part; Cortex cocois radicis oleoyl diethanolamine 160-320 part; KF88 CG 15-30 part; Natural Broneolum Syntheticum 5-10 part; Citric acid 6-12 part; Sodium benzoate 2-4 part; Essence 2-4 part; Natural pigment 1-2 part; Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract 5-10 part; Deionized water 1000-2000 part, and adopt the following steps preparation:
⑴ deionized water heating for dissolving hydroxyethyl-cellulose, heating-up temperature is 20-50 ℃, after add successively Dodecyl Polyoxyethylene Ether sodium sulfate, sodium lauryl sulphate, Cortex cocois radicis oleoyl diethanolamine, KF88 CG, sodium benzoate, natural Broneolum Syntheticum and the citric acid of recipe quantity, stir to complete dissolving and make the total liquid of transparence;
⑵ be added to Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract in total liquid, stirs;
⑶ add essence and pigment, fill, and get final product.
2. a kind of Chinese medicine antibacterial handwashing liquid according to claim 1, it is characterized in that: described hydroxyethyl-cellulose molecular weight is 2000-4000.
3. a kind of Chinese medicine antibacterial handwashing liquid according to claim 1, it is characterized in that: the preparation method of described Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract: Herba Senecionis Scandentis and Herba Rosmarini Officinalis feed intake by 7: 3 ratio, twice of the water supersound extraction that adds ten times of weight, each 2 hours, ultrasonic power is 40-80kw, temperature is room temperature, and the filtrate of extract is condensed into Herba Senecionis Scandentis and the Herba Rosmarini Officinalis extract that relative density is 1.1-1.25.
4. a kind of Chinese medicine antibacterial handwashing liquid according to claim 1 is characterized in that: described essence is a kind of in Fructus Citri Limoniae essence, muguet compound or the aloe flavour.
5. a kind of Chinese medicine antibacterial handwashing liquid according to claim 1 is characterized in that: the color of described natural pigment is a kind of in viride nitens, the golden yellow or sapphirine.
6. the preparation method of a Chinese medicine antibacterial handwashing liquid is comprised of the composition of following weight portion: hydroxyethyl-cellulose 240-480 part; Dodecyl Polyoxyethylene Ether sodium sulfate 200-400 part; Sodium lauryl sulphate 120-240 part; Cortex cocois radicis oleoyl diethanolamine 160-320 part; KF88 CG 15-30 part; Natural Broneolum Syntheticum 5-10 part; Citric acid 6-12 part; Sodium benzoate 2-4 part; Essence 2-4 part; Natural pigment 1-2 part; Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract 5-10 part; Deionized water 1000-2000 part is characterized in that: and adopt the following steps preparation:
⑴ deionized water heating for dissolving hydroxyethyl-cellulose, heating-up temperature is 20-50 ℃, after add successively Dodecyl Polyoxyethylene Ether sodium sulfate, sodium lauryl sulphate, Cortex cocois radicis oleoyl diethanolamine, KF88 CG, sodium benzoate, natural Broneolum Syntheticum and the citric acid of recipe quantity, stir to complete dissolving and make the total liquid of transparence;
⑵ be added to Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract in total liquid, stirs;
⑶ add essence and pigment, fill, and get final product.
7. the preparation method of a kind of Chinese medicine antibacterial handwashing liquid according to claim 6, it is characterized in that: described hydroxyethyl-cellulose molecular weight is 2000-4000.
8. the preparation method of a kind of Chinese medicine antibacterial handwashing liquid according to claim 6, it is characterized in that: the preparation method of described Herba Senecionis Scandentis and Herba Rosmarini Officinalis extract: Herba Senecionis Scandentis and Herba Rosmarini Officinalis feed intake by 7: 3 ratio, twice of the water supersound extraction that adds ten times of weight, each 2 hours, ultrasonic power is 40-80kw, temperature is room temperature, and the filtrate of extract is condensed into Herba Senecionis Scandentis and the Herba Rosmarini Officinalis extract that relative density is 1.1-1.25.
9. the preparation method of a kind of Chinese medicine antibacterial handwashing liquid according to claim 6 is characterized in that: described essence is a kind of in Fructus Citri Limoniae essence, muguet compound or the aloe flavour.
10. the preparation method of a kind of Chinese medicine antibacterial handwashing liquid according to claim 6 is characterized in that: the color of described natural pigment is a kind of in viride nitens, the golden yellow or sapphirine.
CN201210426636.3A 2012-10-31 2012-10-31 Traditional Chinese medicine antibacterial hand washing solution and preparation method thereof Expired - Fee Related CN102949310B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104666173A (en) * 2015-01-27 2015-06-03 普正药业股份有限公司 Hand sanitizer containing antibacterial skincare active ingredients of male flowers of eucommia ulmoides and preparation method of hand sanitizer
CN106852874A (en) * 2017-01-06 2017-06-16 长沙协浩吉生物工程有限公司 A kind of compound method of biological hand sanitizer
CN111905038A (en) * 2020-08-20 2020-11-10 海口植之素生物资源研究所有限公司 Coconut oil-based antibacterial oil hydrogel and preparation method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH1143442A (en) * 1997-07-25 1999-02-16 Lotte Co Ltd Legionella bacteria resistant composition
JP2001226213A (en) * 1999-12-06 2001-08-21 Shiseido Co Ltd Selective antimicrobial composition
DE20207155U1 (en) * 2002-05-07 2002-09-19 Lange Helmut Skin & care ointment for the treatment of mycoses
CN1670150A (en) * 2005-04-16 2005-09-21 王浩贵 Groundsel cleaning products
CN1965877A (en) * 2006-11-06 2007-05-23 赵因 Chinese medicinal eye drop for treating bacteria and virus infected conjunctivitis
CN101966134A (en) * 2010-09-28 2011-02-09 广东海洋大学 Liquid soap with sterilizing and skin protecting functions and preparation method thereof
CN102440266A (en) * 2011-11-02 2012-05-09 安徽亿人安卫生科技有限公司 Chinese traditional medicine preparation for antibiosis, bactriostasis and sterilization and preparation method thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH1143442A (en) * 1997-07-25 1999-02-16 Lotte Co Ltd Legionella bacteria resistant composition
JP2001226213A (en) * 1999-12-06 2001-08-21 Shiseido Co Ltd Selective antimicrobial composition
DE20207155U1 (en) * 2002-05-07 2002-09-19 Lange Helmut Skin & care ointment for the treatment of mycoses
CN1670150A (en) * 2005-04-16 2005-09-21 王浩贵 Groundsel cleaning products
CN1965877A (en) * 2006-11-06 2007-05-23 赵因 Chinese medicinal eye drop for treating bacteria and virus infected conjunctivitis
CN101966134A (en) * 2010-09-28 2011-02-09 广东海洋大学 Liquid soap with sterilizing and skin protecting functions and preparation method thereof
CN102440266A (en) * 2011-11-02 2012-05-09 安徽亿人安卫生科技有限公司 Chinese traditional medicine preparation for antibiosis, bactriostasis and sterilization and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
张泽生等: "迷迭香抑菌及防腐作用研究", 《食品工业科技》 *
敖弟书等: "千里光属植物水煎剂的抑菌作用比较", 《时珍国医国药》 *
易磊: "《妙用本草良方》", 31 January 2006, 中医古籍出版社 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104666173A (en) * 2015-01-27 2015-06-03 普正药业股份有限公司 Hand sanitizer containing antibacterial skincare active ingredients of male flowers of eucommia ulmoides and preparation method of hand sanitizer
CN106852874A (en) * 2017-01-06 2017-06-16 长沙协浩吉生物工程有限公司 A kind of compound method of biological hand sanitizer
CN111905038A (en) * 2020-08-20 2020-11-10 海口植之素生物资源研究所有限公司 Coconut oil-based antibacterial oil hydrogel and preparation method thereof
CN111905038B (en) * 2020-08-20 2022-04-08 海口植之素生物资源研究所有限公司 Coconut oil-based antibacterial oil hydrogel and preparation method thereof

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