CN106420466A - Plant bacteriostatic composition and application thereof in daily necessities - Google Patents
Plant bacteriostatic composition and application thereof in daily necessities Download PDFInfo
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- CN106420466A CN106420466A CN201610923943.0A CN201610923943A CN106420466A CN 106420466 A CN106420466 A CN 106420466A CN 201610923943 A CN201610923943 A CN 201610923943A CN 106420466 A CN106420466 A CN 106420466A
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- bacteriostatic composition
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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Abstract
The invention discloses a plant bacteriostatic composition and application thereof in daily necessities. The plant bacteriostatic composition is prepared from the following plants: radix sophorae flavescentis, radix et rhizoma rhei, rhizoma belamcandae, radix scutellariae and rhizoma polygoni cuspidati. The plant bacteriostatic composition is prepared by carrying out high pressure homogeneous extraction, centrifugal separation and membrane concentration, and then carrying out macroreticular resin absorption separation and membrane concentration. The plant bacteriostatic composition does not contain chemosynthetic substances, thus being non-toxic, free from side effects, safe and reliable, and being directly applied to the skin; the plant bacteriostatic composition effectively removes and inhibits microorganisms such as bacteria, fungi and viruses on the skin of a human body, and has the functions of being capable of effectively preventing the human skin from being infected by the microorganisms, resisting allergy, treating eczema, and the like. The plant bacteriostatic composition can be used as a bacteriostatic function material for the daily necessities with a bacteriostasis function, and can be added into the daily necessities such as shampoo, bath foam, liquid soap, cosmetics and soaps so as to be prepared into anti-dandruff shampoo, antibacterial bath foam, antibacterial liquid soap, acne-removing cosmetics and antibacterial soaps.
Description
Technical field
The present invention relates to a kind of plant bacteriostatic composition, the extract of said composition has bacteria resistance function, can apply to
Prepare commodity, belong to commodity technical field.
Background technology
In daily life, particularly spring and summer, ambient humidity increases people, and the temperature rises, various thin
Bacterium, fungi and virus are active, and bacterium and virus always constantly travel to people with the contact between article and other channels
On the skin of body.Bacterium on skin, fungi give people to live and bring very big potential safety hazard, and cause some skin diseases
Disease, such as dandruff, eczema, psoriasis, acne, antibiotic-resistant infectious disease etc..
With growth in the living standard, people grow with each passing day to the consumption figure of commodity, to having the daily of bacteriostasis efficacy
Product also increasingly increase.At present, most bacteriostatic agent is to be formed by synthetics allotment, the bacteriostatic agent price of these chemical syntheses
Cheap, and play antibacterial effect to a certain extent, but Long-Time Service easily makes skin stimulation, allergy, accelerate aging
Etc. phenomenon, even result in potentially carcinogenic, teratogenesis and mutagenesis.People increasingly improve for the Safety Cognition of commodity, sky
So, low irritant enjoys great popularity.
Some Chinese herbal medicine extract have excellent fungistatic effect, and its abundance, safety and low toxicity, excitant
Little, it is added into commodity and can effectively suppress various bacteria and the growth of fungi.Chinese herbal medicine stresses prescription compatibility, multi-flavor medium-height grass
Medicine can significantly increase effect by rational compatibility.
Content of the invention
The invention aims to overcoming the defect of the bacteriostatic agent of chemical synthesis, provide a kind of plant bacteriostatic composition and
Its preparation method.
To achieve the object of the present invention, present invention employs following technical scheme：
A kind of plant bacteriostatic composition is it is characterised in that be made up of the Chinese medicine of following weight portion：Kuh-seng 10-40 part；Rheum officinale 5-
35 parts；Blackberry lily 5-30 part；Root of large-flowered skullcap 5-30 part；Giant knotweed 5-30 part.
The preparation method of above-mentioned plant bacteriostatic composition is it is characterised in that follow these steps to be prepared：Chinese medicine is pulverized,
20-100 mesh sieve is used to sieve respectively, mixing, adding water or ethanol water by liquid material mass ratio is 5:1 -25:1 as extraction
Solvent, after soaking 1-5h, extracts in 10-100MPa and carries out normal temperature extraction under pressure with high pressure homogenization method machine, extract through from
After the heart separates, concentrated with film, concentrate macroporous resin adsorption, more repeatedly eluted with the ethanol that volume fraction is 10-95%, receive
Collection eluent, it is 1 that film is concentrated into extract with the mass ratio of Chinese medicine:0.5 -1:5, add butanediol dissolving, filter, be obtained
Plant bacteriostatic composition.
It is another object of the present invention to a kind of above-mentioned plant bacteriostatic composition is applied to prepare commodity.
For realizing this purpose of the present invention, present invention employs following technical scheme：By above-mentioned plant bacteriostatic composition
For preparing commodity it is characterised in that containing above-mentioned plant bacteriostatic composition in commodity, its consumption is calculated as with mass fraction
0.01-35%, preferable amount is calculated as 1-20% with mass fraction.
Beneficial effects of the present invention：A lot of bacterium are had on human body skin, some bacterium can make skin infection, the lighter cause acne,
The symptoms such as eczema, allergy, inflammation, severe one or even threat to life.In order to prevent and treat the infection of skin, the present invention adopts the monarch and his subjects
Help the theory of traditional Chinese medical science that makes to design plant bacteriostatic composition, kuh-seng is monarch drug in a prescription, there is very strong clearing heat and detoxicating, anti-inflammatory, disease-resistant
Malicious effect, modern study result shows shrubby sophora extract to tubercle bacillus, shigella dysenteriae, staphylococcus aureus, Escherichia coli
All there is inhibitory action, also have inhibitory action to multiple dermatophytes；Rheum officinale is ministerial drug, has and attacks stagnant, clearing away damp-heat, purging intense heat, cool
The effects such as blood, dissolving stasis, removing toxic substances, modern study result shows that Chinese rhubarb extract has good anti-infectious function, to multiple grams sun
Property and negative bacteria all have an inhibitory action, wherein most sensitive for staphylococcus and streptococcus, be secondly corynebacterium diphtheriae, typhoid fever and
Paratyphosum Bacterium, Diplococcus pneumopniae, shigella dysenteriae etc.；Infected by influenza also has inhibitory action；Blackberry lily and giant knotweed are adjutant, both
It is respectively provided with clearing heat and detoxicating, dissipating bind anti-inflammatory, swelling and pain relieving effect, modern study result shows, Gentrin Knotweed P.E is to golden yellow grape
Coccus, Pseudomonas aeruginosa, hemolytic streptococcus, typhoid bacillus, shigella dysenteriae, Escherichia coli, proteus and some virus all have
Inhibitory action, belamcanda chinensis extract has stronger inhibitory action to Common Pathogenic fungi；The root of large-flowered skullcap is to make medicine, coordinating the drug actions of a prescription, has
Effect of the effects such as heat-clearing and damp-drying drug, purging intense heat and detonicating, hemostasis, modern study result shows that Baical Skullcap root P.E has broad-spectrum antiseptic effect
Really, all there is good antibacterial action to various bacteria, fungi and virus.
A kind of plant bacteriostatic composition that the present invention obtains, without the material of chemical synthesis, nontoxic, have no side effect, safety
Reliable, can be directly used for skin, effectively remove and suppression human body skin on bacterium, the microorganism such as fungi and virus, can simultaneously
Effectively prevention human body skin is by effects such as microorganism infection, antiallergy and treatment eczemas.The plant bacteriostatic composition of the present invention can
For making the bacteria resistance function material of the commodity with bacteria resistance function, shampoo, bath foam, hand cleanser, cosmetic can be added to
In the commodity such as product, perfumed soap.
Specific embodiment
Below by way of specific embodiment come the present invention is further illustrated, but these embodiments simply to illustrate that,
It is not limitation of the present invention.
A kind of plant bacteriostatic composition of embodiment 1-4
Table 1 is the consumption of each component in a kind of plant bacteriostatic composition of embodiment 1-4.
Table 1
A kind of preparation method of the plant bacteriostatic composition described in embodiment 1-4 is as follows：Weigh each component, pulverize, respectively with 60
Mesh sieve is sieved, and mixing, by liquid material mass ratio 15:1 adds volume fraction to be 50% ethanol, after soaking 2h, extracts pressure in 40MPa
Carry out normal temperature extraction with high pressure homogenization method machine under power, after extract is centrifuged, concentrated with film, concentrate AB-8 macropore
Resin adsorption, then with volume fraction be 40%, 70%, 95% ethanol repeatedly elute, collect eluent, film be concentrated into extract with
The mass ratio of plant component is 1:1, add butanediol dissolving, filter, prepared plant bacteriostatic composition.
Comparative example 1-5
Comparative example 1 is to be used alone 100 parts of kuh-seng；
Comparative example 2 is to be used alone 100 parts of rheum officinale；
Comparative example 3 is to be used alone 100 parts of blackberry lily；
Comparative example 4 is to be used alone 100 parts of the root of large-flowered skullcap；
Comparative example 5 is to be used alone 100 parts of giant knotweed；
Preparation method is consistent with embodiment 1-4.
Comparative example 6
By commercially available KF88 water dissolves, making mass fraction is 0.1% KF88 solution.
Experimental example 1 bacteriostatic experiment
Tested bacterial classification is bacterium, aspergillus niger and the Candida albicans such as Escherichia coli, staphylococcus aureus and Pseudomonas aeruginosa.Bring back to life
Above bacterial classification, respectively in following CMC model, bacterium uses lecithin Tween 80-nutrient agar, 30-37 DEG C of culture
36-48 hour；Aspergillus niger uses rose bengal medium, cultivates 120 hours for 20-25 DEG C；Candida albicans use potato Portugal
Grape sugar agar medium, 20-25 DEG C of culture 24-48 hour.Bacterial concentration is all diluted to 1.0 × 109CFU/mL, Candida albicans
Concentration dilution is to 1.0 × 109CFU/mL, aspergillus niger concentration dilution to 1.0 × 107CFU/mL.Pipette the above-mentioned bacterium of 0.1 mL respectively
Dilution, on the flat board filling corresponding solid medium, is smoothened with spreading rod, equidistant in each flat board puts into 4 Oxfords
Cup, adds 0.1 mL embodiment and comparative example thereto in 3 Oxford cups, another one Oxford cup adds 01mL sterilizing life
Reason salt solution is as negative control.The flat board of aspergillus niger and Candida albicans is placed in 20-25 DEG C cultivate 72 hours, the flat board of bacterium
It is placed in 30-37 DEG C to cultivate 72 hours.Diameter using vernier caliper measurement inhibition zone.
Table 2
Bacteriostatic experiment result shows, compared with one-component plant, the plant bacteriostatic composition excellent bacteriostasis efficacy of performance and wider
Antimicrobial spectrum, the diameter of inhibition zone is all higher than 20 mm, more much better than the fungistatic effect of single plant extract, with KF88 effect
Quite.
Experimental example 2 irritation test
Traditional bacteriostatic agent of the plant bacteriostatic composition of embodiment 1 and comparative example 6 is carried out chick chorioallantoic membrane blood vessel test,
Observe the response stimulus of blood vessel, thus reflect the excitant size to skin for the sample.This test is to utilize CAM（Hatch
The fertilization chicken embryo mid-term CAM in 10-14 days embryo ages）Complete, the obvious and transparent feature of blood vessel and carry out.To plant respectively
Thing bacteria inhibiting composition is contacted with 2 CAM with traditional bacteriostatic agent of comparative example 6, effect a period of time, observes CAM injury of blood vessel journey
Degree, scores to excitant, injury of blood vessel is more serious, score value is bigger, excitant is bigger.Criterion is shown in Table 3, and excitant is tied
Fruit is shown in Table 4.
Table 3
Note：NC value（Normal concentration values）, scoring is made according to the score value of CAM vascular effect, takes one group of data
Mean value, determines excitant size.
Table 4
Table 4 result shows：Plant bacteriostatic composition assumes emergent excitant, and traditional bacteriostatic agent KF88 assumes moderate excitant, says
The plant bacteriostatic composition of the bright present invention shows more low excitant.
The preparation of embodiment 5 antibacterial bath liquor
Table 5 provides the antibacterial bath liquor formula containing plant bacteriostatic composition, and the consumption mass fraction of each material represents.
Table 5
The preparation method of antibacterial bath liquor：Deionized water in component A is heated to 85 DEG C, sequentially adds sodium chloride, EDTA-
2Na, citric acid, after so that raw material is fully dissolved, add sodium sulfate of polyethenoxy ether of fatty alcohol AES, Cocoamidopropyl betaine
CAB-35, alkanolamide 6501, after stirring and dissolving, temperature are adjusted to 75 DEG C, add pearlescent flake, stir, be passed through cooling
Water, progressively cools to 45 DEG C, adds all raw materials of component B, stirs, continue to be cooled to 38 DEG C, you can prepared antibacterial is washed one's hair
Body lotion.
The preparation of embodiment 6 anti-bacterial hand lotion
Table 6 provides the anti-bacterial hand lotion formula containing plant bacteriostatic composition, and the consumption mass fraction of each material represents.
Table 6
The preparation method of anti-bacterial hand lotion：Deionized water in component A is heated to 85 DEG C, sequentially adds sodium chloride, EDTA-
2Na, citric acid, after so that raw material is fully dissolved, add sodium sulfate of polyethenoxy ether of fatty alcohol AES, Cocoamidopropyl betaine
CAB-35, alkanolamide 6501, after stirring and dissolving, are passed through cooling water, progressively cool to 45 DEG C, add all raw materials of component B,
Stir, continue to be cooled to 38 DEG C, you can prepared anti-bacterial hand lotion.
The preparation of embodiment 7 Antibiotic liquid detergent
Table 7 provides the Antibiotic liquid detergent formula containing plant bacteriostatic composition, and the consumption mass fraction of each material represents.
Table 7
The preparation method of Antibiotic liquid detergent：NaOH in component A is dissolved in deionized water, is slowly added to dodecane in batches
There is neutralization reaction with NaOH in base benzene sulfonic acid.After stirring and dissolving, sequentially add all raw materials of component B in order, stirring
It is uniformly dissolved, you can prepared Antibiotic liquid detergent.
The preparation of embodiment 8 antibacterial handmade soap
Table 8 provides the antibacterial handmade soap formula containing plant bacteriostatic composition, and the consumption mass fraction of each material represents.
Table 8
Preparation process：By A heat phase to 70 DEG C then, NaOH and water mix and blend are also heated to 70 DEG C, by hydroxide
Sodium mixed liquor be slowly added to A quite in, then stir half an hour, be allowed to fully saponified, add C phase, be eventually adding white sugar
With modified monocrystal rock sugar slowly stirring and dissolving, it is eventually adding alcohol and plant bacteriostatic composition, after stirring, the fast quickly cooling of discharging
But.
The preparation of embodiment 9 anti-dandruff shampoo
Table 9 provides the anti-dandruff shampoo formula containing plant bacteriostatic composition, and the consumption mass fraction of each material represents.
Table 9
The preparation method of anti-dandruff shampoo：Deionized water in component A is heated to 85 DEG C, sequentially add ammonium chloride, EDTA-2Na,
Citric acid, cation guar gum, maintain the temperature at 80-85 DEG C, after so that raw material is fully dissolved, add AEO sulphur
Sour ammonium AESA, Cocoamidopropyl betaine CAB-35, alkanolamide 6501, stirring and dissolving.Temperature is adjusted to 75 DEG C, adds
Cetostearyl alcohol, pearlescent flake, after fusing, stir, are passed through cooling water, progressively cool to 45 DEG C, add all former of component B
Material, stirs, continues to be cooled to 38 DEG C, you can prepared anti-dandruff shampoo.
Claims (3)
1. a kind of plant bacteriostatic composition is it is characterised in that be made up of the Chinese medicine of following weight portion：Kuh-seng 10-40 part；Rheum officinale
5-35 part；Blackberry lily 5-30 part；Root of large-flowered skullcap 5-30 part；Giant knotweed 5-30 part.
2. a kind of preparation method of the plant bacteriostatic composition described in claim 1 is it is characterised in that follow these steps to be made
Standby：Chinese medicine is pulverized, uses 20-100 mesh sieve to sieve respectively, mixing, adding water or ethanol water by liquid material mass ratio is 5:1
-25:1 as Extraction solvent, after soaking 1-5h, carries out normal temperature with high pressure homogenization method machine and carry under 10-100MPa extraction pressure
Take, after extract is centrifuged, concentrated with film, concentrate macroporous resin adsorption, then the second being 10-95% with volume fraction
Alcohol repeatedly elutes, and collects eluent, and it is 1 that film is concentrated into extract with the mass ratio of Chinese medicine:0.5 -1:5, add butanediol
Solution, filters, prepared plant bacteriostatic composition.
3. a kind of plant bacteriostatic composition described in claim 1 in the application in commodity it is characterised in that containing in commodity
There is above-mentioned plant bacteriostatic composition, its consumption is calculated as 0.01-35% with mass fraction.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106963676A (en) * | 2017-03-24 | 2017-07-21 | 福建师范大学 | A kind of kiss-me bactericidal composition and preparation method thereof |
| CN109549883A (en) * | 2017-09-26 | 2019-04-02 | 东莞自然衡健康科技有限公司 | A kind of plant antiallergic is releived the preparation method of agent |
| CN109957979A (en) * | 2017-12-26 | 2019-07-02 | 天津胜达瑞泰科技发展有限公司 | A kind of plant bacteriostatic composition, preparation method and its application in leather dye |
| CN110999790A (en) * | 2019-12-26 | 2020-04-14 | 云南师范大学 | Method for simultaneously inhibiting bacteria and prolonging subculture time of potato tissue culture seedlings and subculture method |
| CN112754971A (en) * | 2021-03-24 | 2021-05-07 | 广州环亚化妆品科技有限公司 | Traditional Chinese medicine composition and preparation method and application thereof |
| CN113521164A (en) * | 2021-08-16 | 2021-10-22 | 西藏大学 | Tibetan medicine composition with antibacterial effect and preparation method and application thereof |
| CN115282190A (en) * | 2022-06-06 | 2022-11-04 | 王瑶英 | A skin antibacterial liquid containing plant extract and its preparation method |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106963676A (en) * | 2017-03-24 | 2017-07-21 | 福建师范大学 | A kind of kiss-me bactericidal composition and preparation method thereof |
| CN109549883A (en) * | 2017-09-26 | 2019-04-02 | 东莞自然衡健康科技有限公司 | A kind of plant antiallergic is releived the preparation method of agent |
| CN109957979A (en) * | 2017-12-26 | 2019-07-02 | 天津胜达瑞泰科技发展有限公司 | A kind of plant bacteriostatic composition, preparation method and its application in leather dye |
| CN110999790A (en) * | 2019-12-26 | 2020-04-14 | 云南师范大学 | Method for simultaneously inhibiting bacteria and prolonging subculture time of potato tissue culture seedlings and subculture method |
| CN112754971A (en) * | 2021-03-24 | 2021-05-07 | 广州环亚化妆品科技有限公司 | Traditional Chinese medicine composition and preparation method and application thereof |
| CN113521164A (en) * | 2021-08-16 | 2021-10-22 | 西藏大学 | Tibetan medicine composition with antibacterial effect and preparation method and application thereof |
| CN115282190A (en) * | 2022-06-06 | 2022-11-04 | 王瑶英 | A skin antibacterial liquid containing plant extract and its preparation method |
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Application publication date: 20170222 |