CN112716867A - Bath lotion containing Chinese herbal medicine components and preparation process thereof - Google Patents
Bath lotion containing Chinese herbal medicine components and preparation process thereof Download PDFInfo
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- CN112716867A CN112716867A CN202110246121.4A CN202110246121A CN112716867A CN 112716867 A CN112716867 A CN 112716867A CN 202110246121 A CN202110246121 A CN 202110246121A CN 112716867 A CN112716867 A CN 112716867A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9767—Pinaceae [Pine family], e.g. pine or cedar
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- A61Q17/02—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings containing insect repellants
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Abstract
The invention relates to the technical field of daily chemical products, and discloses bath foam with Chinese herbal medicine components and a preparation process thereof, wherein the bath foam comprises 66.6% of Chinese herbal medicine extracting solution, 23.4% of surfactant and auxiliary raw materials, and 10% of absolute ethyl alcohol diluent; the method comprises the following steps: A. preparing a Chinese herbal medicine extracting solution: firstly, water extraction, secondly, boiling extraction, secondly, preparing a surfactant and auxiliary raw materials, thirdly, preparing absolute ethyl alcohol diluent, fourthly, synthesizing a finished product, and E, detecting and bottling. The invention adopts 9 kinds of Chinese herbal medicine extract as main material, surfactant and auxiliary material in specific proportion, 3 kinds of Chinese herbal medicine and absolute ethyl alcohol to prepare diluent, and finally synthesizes the three into the finished bath lotion according to a certain sequence and proportion.
Description
Technical Field
The invention relates to the technical field of daily chemical products, in particular to bath foam containing Chinese herbal medicine components and a preparation process thereof.
Background
Bath foam, also called shower cream, is a liquid cleaning agent used during bathing, and is a common cleaning product for modern people. The bath foam is mainly used for replacing the traditional cleaning soap, has the characteristics of convenience and quickness in use, soft touch and the like while having the same or more effects, and is well loved by consumers.
However, in the existing market, although the bath foam has a plurality of varieties, the quality of the bath foam is not uniform. Many bath foam adopts more chemical components, so that the effect is single and short, for example, the bath foam cannot play a role in preventing and treating various skin diseases in daily use, cannot effectively inhibit bacteria and sterilize and the like, and even can cause different degrees of damage to human bodies after long-term use. Therefore, the person skilled in the art provides a bath foam containing Chinese herbal medicine components and a preparation process thereof, so as to solve the problems in the background art.
Disclosure of Invention
The invention aims to provide bath foam containing Chinese herbal medicine components and a preparation process thereof, so as to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a bath lotion containing Chinese herbal materials comprises 66.6% of Chinese herbal extract, 23.4% of surfactant and adjuvant, 10% of absolute ethanol diluent,
the Chinese herbal medicine extracting solution comprises 9 Chinese herbal medicine components in parts by weight:
12-15 parts of a rheum officinale extracting solution, 12-15 parts of a sophora flavescens extracting solution, 10-12 parts of a fructus forsythiae extracting solution, 10-12 parts of a fructus cnidii extracting solution, 6-8 parts of a cortex dictamni extracting solution, 5-7 parts of a polygonum multiflorum extracting solution, 3-4 parts of a cortex phellodendri extracting solution, 2-3 parts of a cortex pseudolaricis extracting solution and 1-2 parts of a fructus psoraleae extracting solution;
the surfactant and the auxiliary raw materials comprise the following components in parts by weight:
10% of AES-NA, 6% of CAB, 5% of 6501%, 2% of nacreous slurry, 0.2% of EDTA, 0.1% of citric acid and 0.1% of cason;
the absolute ethyl alcohol diluent comprises the following components in parts by weight:
4% of absolute ethyl alcohol, 2% of camphor, 2% of menthol and 2% of borneol.
As a still further scheme of the invention: the concentration of the absolute ethyl alcohol is more than or equal to 99.5 percent.
A bath lotion containing Chinese herbal medicine components and its preparation method comprise the following steps:
A. preparing a Chinese herbal medicine extracting solution:
water extraction: firstly, taking 9 extraction tanks, injecting a proper amount of purified water into each extraction tank, then respectively putting the 9 Chinese herbal medicines into each extraction tank according to preset components, and standing for 20-30 min;
boiling and extracting method: setting a proper heating temperature according to the characteristics of each Chinese herbal medicine, heating each extraction tank to separate effective components and ineffective components in the Chinese herbal medicine from each other, fully recovering the effective components in the waste residues by adopting a corresponding organic solvent, and finally respectively obtaining 9 concentrated Chinese herbal medicine extracting solutions;
mixing and stirring 9 kinds of concentrated Chinese herbal medicine extracting solutions according to a certain proportion, adding a proper amount of deionized water, fully and uniformly stirring, and blending to 66.6% of solution amount;
B. preparing a surfactant and auxiliary raw materials: respectively measuring 10% of AES-NA, 6% of CAB, 5% of 6501%, 2% of nacreous slurry, 0.2% of EDTA, 0.1% of citric acid and 0.1% of karson, and the total amount of the solution is 23.4%;
C. preparing an absolute ethyl alcohol diluent: adding 2% of camphor, 2% of menthol and 2% of borneol into 4% of absolute ethyl alcohol, and stirring until the camphor, the menthol and the borneol are completely dissolved to obtain 10% solution;
D. synthesizing a finished product:
firstly, adding a Chinese herbal medicine extracting solution with 66.6 percent of solution amount into a boiler, and heating to 75 ℃;
secondly, sequentially adding 6 percent of CAB, 5 percent of 6501 and 10 percent of AES-NA into the boiler, uniformly stirring, sequentially adding 0.1 percent of citric acid, 0.2 percent of EDTA and 2 percent of pearly luster slurry, uniformly stirring, and naturally cooling to 45 ℃ after completely dissolving;
adding 10% solution of absolute ethyl alcohol diluent into a boiler, fully stirring until the absolute ethyl alcohol diluent is completely dissolved and uniform, standing for 24 hours, and screening to obtain a bath foam finished product;
E. detection and bottling: and (3) testing the bath foam by using pH test paper, wherein the test result is between 5.5 and 6.5, which indicates that the finished product is qualified, and then subpackaging the finished bath foam into packaging bottles to form the product.
As a still further scheme of the invention: and the step A-I and the step A-II are automatically completed by adopting a multifunctional extraction thickener.
As a still further scheme of the invention: the ineffective components in the step A-II comprise starch, gum, pectin, mucilage, pigment and the like.
As a still further scheme of the invention: the relative concentration density of the 9 Chinese herbal medicine extracting solutions obtained in the step A- ② is 1.18-1.22.
As a still further scheme of the invention: the 9 concentrated Chinese herbal medicine extracting solutions obtained in the step A- ② are in accordance with GMP medical standards.
As a still further scheme of the invention: and (C) adopting a screen with the mesh number more than or equal to 500 when screening the bath foam in the step (A-III).
Compared with the prior art, the invention has the beneficial effects that:
the bath foam is prepared by respectively extracting effective components from 9 Chinese herbal medicines of rhubarb, sophora flavescens, forsythia, fructus cnidii, cortex dictamni, polygonum multiflorum, phellodendron, cortex pseudolaricis and fructus psoraleae, adopting AES-NA, CAB, 6501, pearly luster slurry, EDTA, citric acid and kasong as a surfactant and auxiliary raw materials, dissolving 3 Chinese herbal medicines of camphor, menthol and borneol in absolute ethyl alcohol to prepare absolute ethyl alcohol diluent, and finally synthesizing the three into a finished bath foam product according to a certain sequence and proportion.
Detailed Description
In the embodiment of the present invention, the first and second substrates,
a bath lotion containing Chinese herbal medicine components comprises 66.6% of Chinese herbal medicine extractive solution, 23.4% of surfactant and adjuvant materials, and 10% of anhydrous alcohol diluent,
the Chinese herbal medicine extract comprises 9 Chinese herbal medicine components in parts by weight:
12-15 parts of a rheum officinale extracting solution, 12-15 parts of a sophora flavescens extracting solution, 10-12 parts of a fructus forsythiae extracting solution, 10-12 parts of a fructus cnidii extracting solution, 6-8 parts of a cortex dictamni extracting solution, 5-7 parts of a polygonum multiflorum extracting solution, 3-4 parts of a cortex phellodendri extracting solution, 2-3 parts of a cortex pseudolaricis extracting solution and 1-2 parts of a fructus psoraleae extracting solution;
the surfactant and the auxiliary raw materials comprise the following components in parts by weight:
10% of AES-NA, 6% of CAB, 5% of 6501%, 2% of nacreous slurry, 0.2% of EDTA, 0.1% of citric acid and 0.1% of cason;
the anhydrous ethanol diluent comprises the following components in parts by weight:
4 percent of absolute ethyl alcohol (the concentration is more than or equal to 99.5 percent), 2 percent of camphor, 2 percent of menthol and 2 percent of borneol.
A preparation process of bath foam containing Chinese herbal medicine components comprises the following steps:
A. preparing a Chinese herbal medicine extracting solution:
water extraction: firstly, taking 9 extraction tanks, injecting a proper amount of purified water into each extraction tank, then respectively putting the 9 Chinese herbal medicines into each extraction tank according to preset components, and standing for 20-30 min;
boiling and extracting method: setting a proper heating temperature according to the characteristics of each Chinese herbal medicine, heating each extraction tank to separate effective components and ineffective components (including starch, gum, pectin, mucilaginous substances, pigments and the like) in the Chinese herbal medicine from each other, fully recovering the effective components in waste residues by adopting corresponding organic solvents, and finally respectively obtaining 9 concentrated Chinese herbal medicine extracting solutions (the relative concentration density is 1.18-1.22, and the GMP medical standard is met);
(step A-I and step A-II are both automatically finished by adopting a multifunctional extraction thickener.)
Mixing and stirring 9 kinds of concentrated Chinese herbal medicine extracting solutions according to a certain proportion, adding a proper amount of deionized water, fully and uniformly stirring, and blending to 66.6% of solution amount;
B. preparing a surfactant and auxiliary raw materials: respectively measuring 10% of AES-NA, 6% of CAB, 5% of 6501%, 2% of nacreous slurry, 0.2% of EDTA, 0.1% of citric acid and 0.1% of karson, and the total amount of the solution is 23.4%;
C. preparing an absolute ethyl alcohol diluent: adding 2% of camphor, 2% of menthol and 2% of borneol into 4% of absolute ethyl alcohol, and stirring until the camphor, the menthol and the borneol are completely dissolved to obtain 10% solution;
D. synthesizing a finished product:
firstly, adding a Chinese herbal medicine extracting solution with 66.6 percent of solution amount into a boiler, and heating to 75 ℃;
secondly, sequentially adding 6 percent of CAB, 5 percent of 6501 and 10 percent of AES-NA into the boiler, uniformly stirring, sequentially adding 0.1 percent of citric acid, 0.2 percent of EDTA and 2 percent of pearly luster slurry, uniformly stirring, and naturally cooling to 45 ℃ after completely dissolving;
adding 10% solution of absolute ethyl alcohol diluent into a boiler, fully stirring until the absolute ethyl alcohol diluent is completely dissolved and uniform, standing for 24 hours, and screening (by using a screen with a mesh of more than or equal to 500 meshes) to obtain a bath foam finished product;
E. detection and bottling: and (3) testing the bath foam by using pH test paper, wherein the test result is between 5.5 and 6.5, which indicates that the finished product is qualified, and then subpackaging the finished bath foam into packaging bottles to form the product.
The first embodiment is as follows:
the Chinese herbal medicine extract comprises 9 Chinese herbal medicine components in parts by weight:
12 parts of rhubarb extract, 12 parts of sophora flavescens extract, 12 parts of forsythia extract, 10 parts of fructus cnidii extract, 8 parts of cortex dictamni extract, 7 parts of polygonum multiflorum extract, 3 parts of cortex phellodendri extract, 2 parts of cortex pseudolaricis extract and 2 parts of fructus psoraleae extract.
Example two:
the Chinese herbal medicine extract comprises 9 Chinese herbal medicine components in parts by weight:
12 parts of rhubarb extract, 15 parts of sophora flavescens extract, 10 parts of forsythia extract, 12 parts of fructus cnidii extract, 7 parts of cortex dictamni extract, 6 parts of polygonum multiflorum extract, 4 parts of cortex phellodendri extract, 3 parts of cortex pseudolaricis extract and 2 parts of fructus psoraleae extract.
Example three:
the Chinese herbal medicine extract comprises 9 Chinese herbal medicine components in parts by weight:
15 parts of rhubarb extract, 12 parts of sophora flavescens extract, 10 parts of forsythia extract, 10 parts of fructus cnidii extract, 6 parts of cortex dictamni extract, 6 parts of polygonum multiflorum extract, 3 parts of cortex phellodendri extract, 2 parts of cortex pseudolaricis extract and 1 part of fructus psoraleae extract.
Table one:
example one | Example two | EXAMPLE III | |
pH value | 5.8 | 6.3 | 6.1 |
Rate of inhibition of bacteria | 100% | 100% | 100% |
Rate of sterilization | 99.13% | 99.34% | 99.40% |
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention are equivalent to or changed within the technical scope of the present invention.
Claims (8)
1. A bath lotion containing Chinese herbal medicine components comprises 66.6% of Chinese herbal medicine extract, 23.4% of surfactant and auxiliary materials, and 10% of absolute ethyl alcohol diluent,
the Chinese herbal medicine extracting solution comprises 9 Chinese herbal medicine components in parts by weight:
12-15 parts of a rheum officinale extracting solution, 12-15 parts of a sophora flavescens extracting solution, 10-12 parts of a fructus forsythiae extracting solution, 10-12 parts of a fructus cnidii extracting solution, 6-8 parts of a cortex dictamni extracting solution, 5-7 parts of a polygonum multiflorum extracting solution, 3-4 parts of a cortex phellodendri extracting solution, 2-3 parts of a cortex pseudolaricis extracting solution and 1-2 parts of a fructus psoraleae extracting solution;
the surfactant and the auxiliary raw materials comprise the following components in parts by weight:
10% of AES-NA, 6% of CAB, 5% of 6501%, 2% of nacreous slurry, 0.2% of EDTA, 0.1% of citric acid and 0.1% of cason;
the absolute ethyl alcohol diluent comprises the following components in parts by weight:
4% of absolute ethyl alcohol, 2% of camphor, 2% of menthol and 2% of borneol.
2. The bath foam containing herbal ingredients of claim 1, wherein the concentration of said absolute alcohol is not less than 99.5%.
3. A process for preparing a bath foam containing herbal ingredients according to any one of claims 1 to 2, comprising the steps of:
A. preparing a Chinese herbal medicine extracting solution:
water extraction: firstly, taking 9 extraction tanks, injecting a proper amount of purified water into each extraction tank, then respectively putting the 9 Chinese herbal medicines into each extraction tank according to preset components, and standing for 20-30 min;
boiling and extracting method: setting a proper heating temperature according to the characteristics of each Chinese herbal medicine, heating each extraction tank to separate effective components and ineffective components in the Chinese herbal medicine from each other, fully recovering the effective components in the waste residues by adopting a corresponding organic solvent, and finally respectively obtaining 9 concentrated Chinese herbal medicine extracting solutions;
mixing and stirring 9 kinds of concentrated Chinese herbal medicine extracting solutions according to a certain proportion, adding a proper amount of deionized water, fully and uniformly stirring, and blending to 66.6% of solution amount;
B. preparing a surfactant and auxiliary raw materials: respectively measuring 10% of AES-NA, 6% of CAB, 5% of 6501%, 2% of nacreous slurry, 0.2% of EDTA, 0.1% of citric acid and 0.1% of karson, and the total amount of the solution is 23.4%;
C. preparing an absolute ethyl alcohol diluent: adding 2% of camphor, 2% of menthol and 2% of borneol into 4% of absolute ethyl alcohol, and stirring until the camphor, the menthol and the borneol are completely dissolved to obtain 10% solution;
D. synthesizing a finished product:
firstly, adding a Chinese herbal medicine extracting solution with 66.6 percent of solution amount into a boiler, and heating to 75 ℃;
secondly, sequentially adding 6 percent of CAB, 5 percent of 6501 and 10 percent of AES-NA into the boiler, uniformly stirring, sequentially adding 0.1 percent of citric acid, 0.2 percent of EDTA and 2 percent of pearly luster slurry, uniformly stirring, and naturally cooling to 45 ℃ after completely dissolving;
adding 10% solution of absolute ethyl alcohol diluent into a boiler, fully stirring until the absolute ethyl alcohol diluent is completely dissolved and uniform, standing for 24 hours, and screening to obtain a bath foam finished product;
E. detection and bottling: and (3) testing the bath foam by using pH test paper, wherein the test result is between 5.5 and 6.5, which indicates that the finished product is qualified, and then subpackaging the finished bath foam into packaging bottles to form the product.
4. The process for preparing a bath foam containing herbal ingredients as defined in claim 3, wherein said steps A-r and A-r are performed automatically by using a multifunctional extraction thickener.
5. The process of claim 3, wherein the ineffective ingredients of step A- ② include starch, gum, pectin, mucilage, pigment, etc.
6. The preparation process of the bath foam with Chinese herbal medicine components as claimed in claim 3, wherein the relative concentration density of the 9 Chinese herbal medicine extracting solutions obtained in the step A- ② is 1.18-1.22.
7. The process for preparing a bath foam containing herbal ingredients as claimed in claim 3, wherein the 9 concentrated herbal extracts obtained in step A-C are in compliance with GMP standards.
8. The preparation process of the bath foam containing Chinese herbal medicine components according to claim 3, wherein a screen with a mesh size of 500 meshes or more is adopted when the bath foam is screened in the step A-III.
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CN104922310A (en) * | 2015-05-21 | 2015-09-23 | 广东轻工职业技术学院 | Traditional Chinese medicine composition with bacteriostasis function and application of traditional Chinese medicine composition to daily necessities |
CN109718170A (en) * | 2017-10-27 | 2019-05-07 | 位书奎 | A kind of Traditional Chinese medicine bacteriostatic maintenance bath foam and preparation method thereof |
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Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1478464A (en) * | 2002-08-29 | 2004-03-03 | 沈国群 | Chinese medicinal bathing lotion |
CN104042525A (en) * | 2014-07-08 | 2014-09-17 | 福州绿野生化技术有限公司 | Anitbacterial bath foam and preparation method thereof |
CN104922310A (en) * | 2015-05-21 | 2015-09-23 | 广东轻工职业技术学院 | Traditional Chinese medicine composition with bacteriostasis function and application of traditional Chinese medicine composition to daily necessities |
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