CN104042525A - Anitbacterial bath foam and preparation method thereof - Google Patents
Anitbacterial bath foam and preparation method thereof Download PDFInfo
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- CN104042525A CN104042525A CN201410321178.6A CN201410321178A CN104042525A CN 104042525 A CN104042525 A CN 104042525A CN 201410321178 A CN201410321178 A CN 201410321178A CN 104042525 A CN104042525 A CN 104042525A
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- chinese medicine
- extraction liquid
- medicine extraction
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- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000006260 foam Substances 0.000 title abstract description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 33
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 22
- 239000007788 liquid Substances 0.000 claims abstract description 18
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 17
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229960002152 chlorhexidine acetate Drugs 0.000 claims abstract description 12
- MCSINKKTEDDPNK-UHFFFAOYSA-N propyl propionate Chemical compound CCCOC(=O)CC MCSINKKTEDDPNK-UHFFFAOYSA-N 0.000 claims abstract description 12
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229930003316 Vitamin D Natural products 0.000 claims abstract description 11
- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 claims abstract description 11
- 125000000217 alkyl group Chemical group 0.000 claims abstract description 11
- 239000011780 sodium chloride Substances 0.000 claims abstract description 11
- 235000019166 vitamin D Nutrition 0.000 claims abstract description 11
- 239000011710 vitamin D Substances 0.000 claims abstract description 11
- 150000003710 vitamin D derivatives Chemical class 0.000 claims abstract description 11
- 229940046008 vitamin d Drugs 0.000 claims abstract description 11
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 20
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims description 20
- 239000003814 drug Substances 0.000 claims description 17
- 238000000605 extraction Methods 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 244000060011 Cocos nucifera Species 0.000 claims description 10
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 10
- 239000005639 Lauric acid Substances 0.000 claims description 10
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 10
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims description 10
- 239000001632 sodium acetate Substances 0.000 claims description 10
- 235000017281 sodium acetate Nutrition 0.000 claims description 10
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 10
- 235000011152 sodium sulphate Nutrition 0.000 claims description 10
- 238000005352 clarification Methods 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 238000010025 steaming Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 1
- 239000000284 extract Substances 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 2
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 2
- 229960001484 edetic acid Drugs 0.000 abstract 2
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 abstract 1
- 241000218691 Cupressaceae Species 0.000 abstract 1
- 244000303040 Glycyrrhiza glabra Species 0.000 abstract 1
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 abstract 1
- 244000007853 Sarothamnus scoparius Species 0.000 abstract 1
- SMVRDGHCVNAOIN-UHFFFAOYSA-L disodium;1-dodecoxydodecane;sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O.CCCCCCCCCCCCOCCCCCCCCCCCC SMVRDGHCVNAOIN-UHFFFAOYSA-L 0.000 abstract 1
- GLSRFBDXBWZNLH-UHFFFAOYSA-L disodium;2-chloroacetate;2-(4,5-dihydroimidazol-1-yl)ethanol;hydroxide Chemical compound [OH-].[Na+].[Na+].[O-]C(=O)CCl.OCCN1CCN=C1 GLSRFBDXBWZNLH-UHFFFAOYSA-L 0.000 abstract 1
- 235000013399 edible fruits Nutrition 0.000 abstract 1
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 abstract 1
- 235000011477 liquorice Nutrition 0.000 abstract 1
- 229940041616 menthol Drugs 0.000 abstract 1
- 229940096501 sodium cocoamphoacetate Drugs 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 4
- 230000003115 biocidal effect Effects 0.000 description 3
- 230000001954 sterilising effect Effects 0.000 description 3
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000002453 shampoo Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Medicinal Preparation (AREA)
- Cosmetics (AREA)
Abstract
The invention provides antibacterial bath foam and a preparation method thereof. The bath foam comprises the following components in percentage by weight: 10-25 percent of sodium lauryl ether sulfate, 10-20 parts of traditional Chinese medicinal extract liquid, 5-10 percent of alkyl polyglucoside, 5-8 percent of sodium cocoamphoacetate, 2-8 percent of 1,2-propylene glycol, 0.5-1.0 percent of sodium chloride, 0.3-0.5 percent of menthol, 0.1-1.0 percent of vitamin D, 0.1-0.3 percent of EDTA (ethylene diamine tetraacetic acid), 0.1-0.5 percent of chlorhexidine acetate and 0.1-0.3 percent of citric acid, wherein the traditional Chinese medicinal extract liquid contains extracts of radix sophorae flavescentis, radix scutellariae, broom cypress fruit, fructus cnidii, cortex phellodendri and liquorice. The antibacterial bath foam has the effect of antibacteria and disinfection, is good in stability, does not irritate skin, and is suitable for various skins.
Description
Technical field
The invention belongs to cosmetics of everyday use field, be specifically related to a kind of antibacterial bath liquor and preparation method thereof.
Background technology
Existing antibacterial bath liquor kind is a lot, but usefulness differs, often the valid density of high-efficiency antimicrobial bath foam is high, price is also high, and easily skin is produced to certain damage or stimulation, and people wish that scientific research personnel can develop the bath foam of a kind of not only antibiotic and sterilizing but also safety and stability always.
Summary of the invention
The object of the present invention is to provide a kind of antibacterial bath liquor and preparation method thereof, product has antibiotic and sterilizing effect, and good stability is non-stimulated to skin, is suitable for various skin quality.
For achieving the above object, the present invention adopts following technical scheme:
In a kind of antibacterial bath liquor, lauric acid alcohol ether sodium sulfate 10-25wt.%, Chinese medicine extraction liquid 10-20wt.%, alkyl polyglycoside 5-10wt.%, cocos nucifera oil both sexes sodium acetate 5-8wt.%, 1,2-propylene glycol 2-8wt.%, sodium chloride 0.5-1.0wt.%, Mentholum 0.3-0.5wt.%, vitamin D 0.1-1.0 wt.%, EDTA 0.1-0.3 wt.%, chlorhexidine acetate 0.1-0.5 wt.%, citric acid 0.1-0.3 wt.%, add water to 100%; The preparation method of described Chinese medicine extraction liquid: be 3:2:1:1:1:1 mixing in mass ratio by Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, Radix Glycyrrhizae, be soaked in 3-5 hour in the water of 12 times of quality, add 1 of 3 times of quality, 2-propylene glycol, twice of steaming and decocting, filter, clarification, is concentrated into 1/3-1/5.
Preparation method comprises the following steps:
(1) chlorhexidine acetate is dissolved in the 1,2-PD of 50-80 ℃, adds Mentholum;
(2) under stirring, add water, lauric acid alcohol ether sodium sulfate, alkyl polyglycoside and cocos nucifera oil both sexes sodium acetate, treat to dissolve completely, be warming up to 80 ℃, add the mixed liquor of Chinese medicine extraction liquid and step (1);
(3) after mix homogeneously, with citric acid, be adjusted to pH=4.5 ~ 6.5;
(4) after cooling, add EDTA and vitamin D;
(5) use sodium chloride adjusting viscosity, make antibacterial bath liquor.
Remarkable advantage of the present invention is: product has antibiotic and sterilizing effect, and good stability is non-stimulated to skin, is suitable for various skin quality.Chlorhexidine acetate is a kind of shallow table antibacterial, and character is gentle, is used in conjunction with herb liquid, and anti-fungistatic effect is good.Product pH value is 4.5 ~ 6.5, is conducive to improve the stability of product.During Chinese medicine extraction, adopt 1,2-PD to carry out instead of ethanol, not only can extract the liposoluble substance in Chinese medicine, and without recycling step, reduced production cost.
The specific embodiment
embodiment 1
In a kind of antibacterial bath liquor, lauric acid alcohol ether sodium sulfate 10wt.%, Chinese medicine extraction liquid 10wt.%, alkyl polyglycoside 5wt.%, cocos nucifera oil both sexes sodium acetate 5wt.%, 1,2-propylene glycol 2wt.%, sodium chloride 0.5wt.%, Mentholum 0.3wt.%, vitamin D 0.1wt.%, EDTA 0.1wt.%, chlorhexidine acetate 0.1wt.%, citric acid 0.1wt.%, add water to 100%; The preparation method of described Chinese medicine extraction liquid: Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, Radix Glycyrrhizae are to 3:2:1:1:1:1 mixes in mass ratio, are soaked in the water of 12 times of quality 3 hours, add 1 of 3 times of quality, 2-propylene glycol, steaming and decocting twice, filters, clarification, is concentrated into 1/3.
Preparation method comprises the following steps:
(1) chlorhexidine acetate is dissolved in the 1,2-PD of 50 ℃, adds Mentholum;
(2) under stirring, add water, lauric acid alcohol ether sodium sulfate, alkyl polyglycoside and cocos nucifera oil both sexes sodium acetate, treat to dissolve completely, be warming up to 80 ℃, add the mixed liquor of Chinese medicine extraction liquid and step (1);
(3) after mix homogeneously, with citric acid, be adjusted to pH=4.5;
(4) after cooling, add EDTA and vitamin D;
(5) use sodium chloride adjusting viscosity, make antibacterial bath liquor.
embodiment 2
In a kind of antibacterial bath liquor, lauric acid alcohol ether sodium sulfate 25wt.%, Chinese medicine extraction liquid 20wt.%, alkyl polyglycoside 10wt.%, cocos nucifera oil both sexes sodium acetate 8wt.%, 1,2-propylene glycol 8wt.%, sodium chloride 1.0wt.%, Mentholum 0.5wt.%, vitamin D 1.0 wt.%, EDTA 0.3 wt.%, chlorhexidine acetate 0.5 wt.%, citric acid 0.3 wt.%, add water to 100%; The preparation method of described Chinese medicine extraction liquid: Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, Radix Glycyrrhizae are to 3:2:1:1:1:1 mixes in mass ratio, are soaked in the water of 12 times of quality 5 hours, add 1 of 3 times of quality, 2-propylene glycol, steaming and decocting twice, filters, clarification, is concentrated into 1/5.
Preparation method comprises the following steps:
(1) chlorhexidine acetate is dissolved in the 1,2-PD of 80 ℃, adds Mentholum;
(2) under stirring, add water, lauric acid alcohol ether sodium sulfate, alkyl polyglycoside and cocos nucifera oil both sexes sodium acetate, treat to dissolve completely, be warming up to 80 ℃, add the mixed liquor of Chinese medicine extraction liquid and step (1);
(3) after mix homogeneously, with citric acid, be adjusted to pH=6.5;
(4) after cooling, add EDTA and vitamin D;
(5) use sodium chloride adjusting viscosity, make antibacterial bath liquor.
embodiment 3
In a kind of antibacterial bath liquor, lauric acid alcohol ether sodium sulfate 20wt.%, Chinese medicine extraction liquid 15wt.%, alkyl polyglycoside 8wt.%, cocos nucifera oil both sexes sodium acetate 6wt.%, 1,2-propylene glycol 5wt.%, sodium chloride 0.8wt.%, Mentholum 0.4wt.%, vitamin D 0.5wt.%, EDTA 0.2 wt.%, chlorhexidine acetate 0.3wt.%, citric acid 0.2 wt.%, add water to 100%; The preparation method of described Chinese medicine extraction liquid: Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, Radix Glycyrrhizae are to 3:2:1:1:1:1 mixes in mass ratio, are soaked in the water of 12 times of quality 4 hours, add 1 of 3 times of quality, 2-propylene glycol, steaming and decocting twice, filters, clarification, is concentrated into 1/4.
Preparation method comprises the following steps:
(1) chlorhexidine acetate is dissolved in the 1,2-PD of 65 ℃, adds Mentholum;
(2) under stirring, add water, lauric acid alcohol ether sodium sulfate, alkyl polyglycoside and cocos nucifera oil both sexes sodium acetate, treat to dissolve completely, be warming up to 80 ℃, add the mixed liquor of Chinese medicine extraction liquid and step (1);
(3) after mix homogeneously, with citric acid, be adjusted to pH=5.5;
(4) after cooling, add EDTA and vitamin D;
(5) use sodium chloride adjusting viscosity, make antibacterial bath liquor.
Product meets the extraordinary bath shampoo > of GB 19877.2-2005 < < >, the disposable use hygienic article of GB15979-2002 < < sanitary standard > > and < < disinfection technology standard > > (Ministry of Public Health 2007).
The foregoing is only preferred embodiment of the present invention, all equalizations of doing according to the present patent application the scope of the claims change and modify, and all should belong to covering scope of the present invention.
Claims (2)
1. an antibacterial bath liquor, it is characterized in that: lauric acid alcohol ether sodium sulfate 10-25wt.%, Chinese medicine extraction liquid 10-20wt.%, alkyl polyglycoside 5-10wt.%, cocos nucifera oil both sexes sodium acetate 5-8wt.%, 1,2-propylene glycol 2-8wt.%, sodium chloride 0.5-1.0wt.%, Mentholum 0.3-0.5wt.%, vitamin D 0.1-1.0 wt.%, EDTA 0.1-0.3 wt.%, chlorhexidine acetate 0.1-0.5 wt.%, citric acid 0.1-0.3 wt.%, add water to 100%; The preparation method of described Chinese medicine extraction liquid: be 3:2:1:1:1:1 mixing in mass ratio by Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, Radix Glycyrrhizae, be soaked in 3-5 hour in the water of 12 times of quality, add 1 of 3 times of quality, 2-propylene glycol, twice of steaming and decocting, filter, clarification, is concentrated into 1/3-1/5.
2. a method of preparing antibacterial bath liquor as claimed in claim 1, is characterized in that: comprise the following steps:
(1) chlorhexidine acetate is dissolved in the 1,2-PD of 50-80 ℃, adds Mentholum;
(2) under stirring, add water, lauric acid alcohol ether sodium sulfate, alkyl polyglycoside and cocos nucifera oil both sexes sodium acetate, treat to dissolve completely, be warming up to 80 ℃, add the mixed liquor of Chinese medicine extraction liquid and step (1);
(3) after mix homogeneously, with citric acid, be adjusted to pH=4.5 ~ 6.5;
(4) after cooling, add EDTA and vitamin D;
(5) use sodium chloride adjusting viscosity, make antibacterial bath liquor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410321178.6A CN104042525B (en) | 2014-07-08 | 2014-07-08 | A kind of antibacterial bath liquor and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410321178.6A CN104042525B (en) | 2014-07-08 | 2014-07-08 | A kind of antibacterial bath liquor and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104042525A true CN104042525A (en) | 2014-09-17 |
| CN104042525B CN104042525B (en) | 2016-06-29 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410321178.6A Expired - Fee Related CN104042525B (en) | 2014-07-08 | 2014-07-08 | A kind of antibacterial bath liquor and preparation method thereof |
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| CN (1) | CN104042525B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105748355A (en) * | 2016-03-10 | 2016-07-13 | 蚌埠团结日用化学有限公司 | Chinese herbal medicine shower gel and preparation method thereof |
| CN108056965A (en) * | 2018-02-28 | 2018-05-22 | 深圳市川中王中医药科技发展有限公司 | Chinese medicine bath cream |
| CN111388385A (en) * | 2020-03-30 | 2020-07-10 | 山东消博士消毒科技股份有限公司 | Disinfecting bath foam and preparation process thereof |
| CN112716867A (en) * | 2021-03-05 | 2021-04-30 | 孔静波 | Bath lotion containing Chinese herbal medicine components and preparation process thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102247564A (en) * | 2010-11-29 | 2011-11-23 | 吴克 | Liquid preparation for treating dermatitis, eczema and the like and preparation method thereof |
| CN103315932A (en) * | 2013-06-05 | 2013-09-25 | 片仔癀（上海）生物科技研发有限公司 | Itching-relieving body wash and preparation method thereof |
-
2014
- 2014-07-08 CN CN201410321178.6A patent/CN104042525B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102247564A (en) * | 2010-11-29 | 2011-11-23 | 吴克 | Liquid preparation for treating dermatitis, eczema and the like and preparation method thereof |
| CN103315932A (en) * | 2013-06-05 | 2013-09-25 | 片仔癀（上海）生物科技研发有限公司 | Itching-relieving body wash and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 王秀琴: "《过敏性疾病知识》", 31 July 1989, 人民卫生出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105748355A (en) * | 2016-03-10 | 2016-07-13 | 蚌埠团结日用化学有限公司 | Chinese herbal medicine shower gel and preparation method thereof |
| CN108056965A (en) * | 2018-02-28 | 2018-05-22 | 深圳市川中王中医药科技发展有限公司 | Chinese medicine bath cream |
| CN111388385A (en) * | 2020-03-30 | 2020-07-10 | 山东消博士消毒科技股份有限公司 | Disinfecting bath foam and preparation process thereof |
| CN112716867A (en) * | 2021-03-05 | 2021-04-30 | 孔静波 | Bath lotion containing Chinese herbal medicine components and preparation process thereof |
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| Publication number | Publication date |
|---|---|
| CN104042525B (en) | 2016-06-29 |
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