CN104042525B - A kind of antibacterial bath liquor and preparation method thereof - Google Patents

A kind of antibacterial bath liquor and preparation method thereof Download PDF

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CN104042525B
CN104042525B CN201410321178.6A CN201410321178A CN104042525B CN 104042525 B CN104042525 B CN 104042525B CN 201410321178 A CN201410321178 A CN 201410321178A CN 104042525 B CN104042525 B CN 104042525B
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chinese medicine
extraction liquid
medicine extraction
liquor
preparation
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CN104042525A (en
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章家民
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Foochow Green Field Biochemical Technology Co Ltd
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Foochow Green Field Biochemical Technology Co Ltd
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Abstract

The invention provides a kind of antibacterial bath liquor and preparation method thereof, containing lauric acid ether sulfate 10-25wt.% in bath foam, Chinese medicine extraction liquid 10-20wt.%, alkyl polyglycoside 5-10wt.%, cocos nucifera oil both sexes sodium acetate 5-8wt.%, 1, 2-propylene glycol 2-8wt.%, sodium chloride 0.5-1.0wt.%, Mentholum 0.3-0.5wt.%, vitamin D 0.1-1.0wt.%, EDTA 0.1-0.3wt.%, chlorhexidine acetate 0.1-0.5wt.%, citric acid 0.1-0.3wt.%, described Chinese medicine extraction liquid is Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, the extract of Radix Glycyrrhizae.Product has an antibiotic and sterilizing effect, and good stability is non-stimulated to skin, is suitable for various skin quality.

Description

A kind of antibacterial bath liquor and preparation method thereof
Technical field
The invention belongs to cosmetics of everyday use field, be specifically related to a kind of antibacterial bath liquor and preparation method thereof.
Background technology
Existing antibacterial bath liquor kind is a lot, but usefulness differs, often the valid density of high-efficiency antimicrobial bath foam is high, price is also high, and skin easily produces certain damage or stimulation, and people wish that scientific research personnel can develop a kind of not only antibiotic and sterilizing but also the bath foam of safety and stability always.
Summary of the invention
It is an object of the invention to provide a kind of antibacterial bath liquor and preparation method thereof, product has an antibiotic and sterilizing effect, and good stability is non-stimulated to skin, is suitable for various skin quality.
For achieving the above object, the present invention adopts the following technical scheme that
In a kind of antibacterial bath liquor, lauric acid ether sulfate 10-25wt.%, Chinese medicine extraction liquid 10-20wt.%, alkyl polyglycoside 5-10wt.%, cocos nucifera oil both sexes sodium acetate 5-8wt.%, 1,2-propylene glycol 2-8wt.%, sodium chloride 0.5-1.0wt.%, Mentholum 0.3-0.5wt.%, vitamin D 0.1-1.0wt.%, EDTA0.1-0.3wt.%, chlorhexidine acetate 0.1-0.5wt.%, citric acid 0.1-0.3wt.%, add water to 100%;The preparation method of described Chinese medicine extraction liquid: Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, Radix Glycyrrhizae are mixed for 3:2:1:1:1:1 in mass ratio, be soaked in the water of 12 times of quality 3-5 hour, adds the 1 of 3 times of quality, 2-propylene glycol, steaming and decocting twice, filter, clarification, is concentrated into 1/3-1/5.
Preparation method comprises the following steps:
(1) chlorhexidine acetate is dissolved in the 1,2-PD of 50-80 DEG C, adds Mentholum;
(2) under stirring, add water, lauric acid ether sulfate, alkyl polyglycoside and cocos nucifera oil both sexes sodium acetate, wait to be completely dissolved, be warming up to 80 DEG C, add the mixed liquor of Chinese medicine extraction liquid and step (1);
(3), after mix homogeneously, regulate to pH=4.5~6.5 with citric acid;
(4) EDTA and vitamin D are added after cooling;
(5) regulate viscosity with sodium chloride, prepare antibacterial bath liquor.
The product that has the great advantage that of the present invention has an antibiotic and sterilizing effect, and good stability is non-stimulated to skin, is suitable for various skin quality.Chlorhexidine acetate is a kind of shallow table antibacterial, and character is gentle, with herb liquid with the use of, anti-fungistatic effect is good.Product pH value is 4.5~6.5, is conducive to improving the stability of product.Adopt 1,2-PD to substitute ethanol during Chinese medicine extraction, be possible not only to extract the liposoluble substance in Chinese medicine, and without recycling step, reduce production cost.
Detailed description of the invention
Embodiment 1
In a kind of antibacterial bath liquor, lauric acid ether sulfate 10wt.%, Chinese medicine extraction liquid 10wt.%, alkyl polyglycoside 5wt.%, cocos nucifera oil both sexes sodium acetate 5wt.%, 1,2-propylene glycol 2wt.%, sodium chloride 0.5wt.%, Mentholum 0.3wt.%, vitamin D 0.1wt.%, EDTA0.1wt.%, chlorhexidine acetate 0.1wt.%, citric acid 0.1wt.%, add water to 100%;The preparation method of described Chinese medicine extraction liquid: Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, Radix Glycyrrhizae are mixed for 3:2:1:1:1:1 in mass ratio, be soaked in the water of 12 times of quality 3 hours, adds the 1 of 3 times of quality, 2-propylene glycol, steaming and decocting twice, filter, clarification, is concentrated into 1/3.
Preparation method comprises the following steps:
(1) chlorhexidine acetate is dissolved in the 1,2-PD of 50 DEG C, adds Mentholum;
(2) under stirring, add water, lauric acid ether sulfate, alkyl polyglycoside and cocos nucifera oil both sexes sodium acetate, wait to be completely dissolved, be warming up to 80 DEG C, add the mixed liquor of Chinese medicine extraction liquid and step (1);
(3), after mix homogeneously, regulate to pH=4.5 with citric acid;
(4) EDTA and vitamin D are added after cooling;
(5) regulate viscosity with sodium chloride, prepare antibacterial bath liquor.
Embodiment 2
In a kind of antibacterial bath liquor, lauric acid ether sulfate 25wt.%, Chinese medicine extraction liquid 20wt.%, alkyl polyglycoside 10wt.%, cocos nucifera oil both sexes sodium acetate 8wt.%, 1,2-propylene glycol 8wt.%, sodium chloride 1.0wt.%, Mentholum 0.5wt.%, vitamin D1 .0wt.%, EDTA0.3wt.%, chlorhexidine acetate 0.5wt.%, citric acid 0.3wt.%, add water to 100%;The preparation method of described Chinese medicine extraction liquid: Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, Radix Glycyrrhizae are mixed for 3:2:1:1:1:1 in mass ratio, be soaked in the water of 12 times of quality 5 hours, adds the 1 of 3 times of quality, 2-propylene glycol, steaming and decocting twice, filter, clarification, is concentrated into 1/5.
Preparation method comprises the following steps:
(1) chlorhexidine acetate is dissolved in the 1,2-PD of 80 DEG C, adds Mentholum;
(2) under stirring, add water, lauric acid ether sulfate, alkyl polyglycoside and cocos nucifera oil both sexes sodium acetate, wait to be completely dissolved, be warming up to 80 DEG C, add the mixed liquor of Chinese medicine extraction liquid and step (1);
(3), after mix homogeneously, regulate to pH=6.5 with citric acid;
(4) EDTA and vitamin D are added after cooling;
(5) regulate viscosity with sodium chloride, prepare antibacterial bath liquor.
Embodiment 3
In a kind of antibacterial bath liquor, lauric acid ether sulfate 20wt.%, Chinese medicine extraction liquid 15wt.%, alkyl polyglycoside 8wt.%, cocos nucifera oil both sexes sodium acetate 6wt.%, 1,2-propylene glycol 5wt.%, sodium chloride 0.8wt.%, Mentholum 0.4wt.%, vitamin D 0.5wt.%, EDTA0.2wt.%, chlorhexidine acetate 0.3wt.%, citric acid 0.2wt.%, add water to 100%;The preparation method of described Chinese medicine extraction liquid: Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, Radix Glycyrrhizae are mixed for 3:2:1:1:1:1 in mass ratio, be soaked in the water of 12 times of quality 4 hours, adds the 1 of 3 times of quality, 2-propylene glycol, steaming and decocting twice, filter, clarification, is concentrated into 1/4.
Preparation method comprises the following steps:
(1) chlorhexidine acetate is dissolved in the 1,2-PD of 65 DEG C, adds Mentholum;
(2) under stirring, add water, lauric acid ether sulfate, alkyl polyglycoside and cocos nucifera oil both sexes sodium acetate, wait to be completely dissolved, be warming up to 80 DEG C, add the mixed liquor of Chinese medicine extraction liquid and step (1);
(3), after mix homogeneously, regulate to pH=5.5 with citric acid;
(4) EDTA and vitamin D are added after cooling;
(5) regulate viscosity with sodium chloride, prepare antibacterial bath liquor.
Product meets GB19877.2-2005 " extraordinary bath shampoo ", GB15979-2002 " Disposable Sanitary Accessory sanitary standard " and " disinfection technology standard " (Ministry of Public Health 2007).
The foregoing is only presently preferred embodiments of the present invention, all equalizations done according to the present patent application the scope of the claims change and modify, and all should belong to the covering scope of the present invention.

Claims (2)

1. an antibacterial bath liquor, it is characterized in that: lauric acid ether sulfate 10-25wt.%, Chinese medicine extraction liquid 10-20wt.%, alkyl polyglycoside 5-10wt.%, cocos nucifera oil both sexes sodium acetate 5-8wt.%, 1,2-propylene glycol 2-8wt.%, sodium chloride 0.5-1.0wt.%, Mentholum 0.3-0.5wt.%, vitamin D 0.1-1.0wt.%, EDTA0.1-0.3wt.%, chlorhexidine acetate 0.1-0.5wt.%, citric acid 0.1-0.3wt.%, add water to 100%;The preparation method of described Chinese medicine extraction liquid: Radix Sophorae Flavescentis, Radix Scutellariae, the Fructus Kochiae, Fructus Cnidii, Cortex Phellodendri, Radix Glycyrrhizae are mixed for 3:2:1:1:1:1 in mass ratio, be soaked in the water of 12 times of quality 3-5 hour, adds the 1 of 3 times of quality, 2-propylene glycol, steaming and decocting twice, filter, clarification, is concentrated into 1/3-1/5.
2. the method preparing antibacterial bath liquor as claimed in claim 1, it is characterised in that: comprise the following steps:
(1) chlorhexidine acetate is dissolved in the 1,2-PD of 50-80 DEG C, adds Mentholum;
(2) under stirring, add water, lauric acid ether sulfate, alkyl polyglycoside and cocos nucifera oil both sexes sodium acetate, wait to be completely dissolved, be warming up to 80 DEG C, add the mixed liquor of Chinese medicine extraction liquid and step (1);
(3), after mix homogeneously, regulate to pH=4.5~6.5 with citric acid;
(4) EDTA and vitamin D are added after cooling;
(5) regulate viscosity with sodium chloride, prepare antibacterial bath liquor.
CN201410321178.6A 2014-07-08 2014-07-08 A kind of antibacterial bath liquor and preparation method thereof Active CN104042525B (en)

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Publication number Priority date Publication date Assignee Title
CN105748355A (en) * 2016-03-10 2016-07-13 蚌埠团结日用化学有限公司 Chinese herbal medicine shower gel and preparation method thereof
CN108056965A (en) * 2018-02-28 2018-05-22 深圳市川中王中医药科技发展有限公司 Chinese medicine bath cream
CN111388385A (en) * 2020-03-30 2020-07-10 山东消博士消毒科技股份有限公司 Disinfecting bath foam and preparation process thereof
CN112716867A (en) * 2021-03-05 2021-04-30 孔静波 Bath lotion containing Chinese herbal medicine components and preparation process thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102247564A (en) * 2010-11-29 2011-11-23 吴克 Liquid preparation for treating dermatitis, eczema and the like and preparation method thereof
CN103315932A (en) * 2013-06-05 2013-09-25 片仔癀(上海)生物科技研发有限公司 Itching-relieving body wash and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102247564A (en) * 2010-11-29 2011-11-23 吴克 Liquid preparation for treating dermatitis, eczema and the like and preparation method thereof
CN103315932A (en) * 2013-06-05 2013-09-25 片仔癀(上海)生物科技研发有限公司 Itching-relieving body wash and preparation method thereof

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