CN104593178B - A kind of multifunctional manual soap containing the rare saponin(e of ginseng - Google Patents
A kind of multifunctional manual soap containing the rare saponin(e of ginseng Download PDFInfo
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Abstract
The present invention relates to a kind of manual soap composition using the rare saponin(e of ginseng as main active, belong to commodity, it is characterised in that by weight percentage, the manual soap composition contains：65 75% vegetable fat, 10 12% sodium hydroxides, 0.1 3.0% Radix Platycodonis extract, the 0.5 3% rare saponin(e of ginseng, surplus are deionized water.The rare saponin(e of ginseng mainly includes ginsenoside Rk1, Rg5, Rg6 and F4 etc..The handmade soap of the present invention belongs to cold process soap, vegetable oil and the rare saponin(e isoreactivity composition of ginseng are remained to greatest extent, and there are oil control and acne removal, the multiple efficacies such as deep layer cleaning, skin whitening, moisturizing, inhibiting bacteria and diminishing inflammation, it can be used as face cleaning, moisturizing, moisturizing, anti-inflammatory etc., be a kind of multifunctional manual soap.
Description
Technical field
The invention belongs to daily washing product technical field, and in particular to a kind of two kinds of active ingredient of Chinese herbs of balloonflower root and ginseng
Manual soap composition and its its preparation method based on addition.
Background technology
Perfumed soap is a kind of indispensable daily washing product, and people can trace back to B.C. meaning using the history of perfumed soap
Big profit.Perfumed soap has preferable cleaning effect as a kind of daily cleaning products.However, the perfumed soap to circulate in the market
Quality is very different, and effect is more single.Handmade soap is gradually favored as a kind of product newly risen by market, this hand
Work soap belongs to cold process soap, and saponification, which occurs, with alkali using natural plant grease is made, and it has, and foaming characteristic is strong, and foam exquisiteness is rich
Richness, natural epidemic disaster in booth and the features such as（Referring to：Shen Qian, the development and preparation of handmade soap,《Scientific and technological information》, 2011）.With crude drug
Thing studies the increase of temperature, and the artificial traditional Chinese medicine extract that adds turns into a big feature of such handmade soap（Referring to：Chen Jia is right
Some of traditional-handwork soap preparation method are improved and experience,《Chemical learning aid》, 2014）.However, traditional simple addition is present such as
Lower deficiency：（1）Adding ingredient includes part easily corrupt composition, influences the handmade soap shelf-life, and 2）The extraction of active Chinese drug component material can not
Avoiding bringing organic solvent residual, the quality to handmade soap brings hidden danger, and 3）Specific active material does not have clear and definite quality control
System, causes handmade soap quality heterogeneity.Before the present invention, the related patent application of existing ginseng, such as ginseng cosmetic fancy soap
（ZL.201110154474.8）, soap with fragrant of ginseng flower for protecting skin and its manufacturing process (CN. 200710055642.1), panax ginseng extractum perfumed soap
And preparation method（CN. 201110038946.3）, ginseng soap（CN.93100622.8）Deng above-mentioned patent is only simply to add
Add the compositions such as ginseng, its main active is not known, and not using the more preferable rare ginsenoside of wherein activity as main matter
Control targe is measured, the present invention solves above mentioned problem, innovative to propose the specific of the rare saponin(e of ginseng and Radix Platycodonis extract
Addition and main active are formed.
The content of the invention
In order to solve shortcomings and deficiencies present in above-mentioned existing Chinese medicine handmade soap process technology, there is provided in definitely
Pharmaceutically active substance adds, and reaches preferably using feeling and effect, the present invention provide it is a kind of with containing the rare saponin(e Rk1 of ginseng,
Rg5, Rg6 and F4 etc. are manual soap composition of main active and preparation method thereof.The handmade soap of the present invention by planting more
Thing oil and sodium hydroxide are at low temperature by slowly saponification is made for a long time.It contains the natural glycerin of high content
（25%）, and remain to greatest extent the unrighted acid in vegetable oil and ginsenoside thermal cracking etc. composition, make production
Product possess excellent cleaning, moisturizing, skin care and certain therapeutic effect while cleaning action is played, and the quality guarantee period is more
It is long.
In order to lift the quality of traditional-handwork soap and overcome original handmade soap to state technical problem, the present invention passes through following technology
Scheme is realized：
A kind of manual soap composition, it is characterised in that by weight percentage, the manual soap composition contains：
65-75% vegetable fat, 10-12% sodium hydroxides, 1.0-3.0% Radix Platycodonis extract, the 0.5-3% rare soap of ginseng
Glycosides, surplus are water.
The rare saponin(e of ginseng involved in the present invention derives from but is not limited to ginseng, gen-seng haulms, ginseng fruit, pseudo-ginseng
The general ginsenoside of the extractions such as root, notoginseng haulm, American ginseng root, stem and leaves of American ginseng and American Ginseng Fruit, thereafter through thermal cracking
Obtain the rare saponin(e of ginseng used in the present invention.The rare saponin(e of ginseng of acquisition mainly includes ginsenoside Rk1, Rg5,
Rg6 and F4 etc., different rare ginsenosides, which are made an addition in handmade soap, can play good oil control and acne removal, skin whitening, moisturizing and antibacterial disappear
Inflammation and other effects.
Radix Platycodonis extract involved in the present invention derives from the dry root of Campanulaceae balloonflower root, thereafter through water or low dense
Ethanol extraction gained is spent, balloonflower root root extract is obtained and mainly includes platycodin and lobetyolin, also comprising polysaccharide, amino acid,
The compositions such as flavones, the addition of balloonflower root root extract help that good oil control and acne removal, skin whitening, moisturizing and suppression can be played in handmade soap
Bacterium anti-inflammatory and other effects.
In a preferred embodiment of the invention, the vegetable fat is selected from coconut oil, palm oil, grape-kernel oil, seen the moon
At least one of careless oil, olive oil, Sweet Almond Oil, shea butter.
In a preferred embodiment of the invention, the vegetable fat by weight percentage, by 10-20% coconut oil,
10-30% palm oils, 10-30% olive oil, 15-20% grape-kernel oils, 10-20% evening primrose oil, 10-20% Sweet Almond Oils, 5-10%
Shea butter forms.
The method for preparing handmade soap using above-mentioned manual soap composition, it is characterised in that comprise the following steps：
（1）The vegetable fat is added in the reactor, after stirring, is warming up to 30~40 degree, constant temperature is stand-by；
（2）The sodium hydrate aqueous solution that temperature is 30~40 degree is added into step（1）Solution in, quick stirring, until
Soap lye thickens（Viscosity 6000mPa.s~8000mPa.s）;
（3）The rare saponin(e of ginseng and balloonflower root root extract that water in advance is disperseed add step（2）In obtained soap lye,
And stir；
（4）Step（3）Soap lye pour into preprepared mould, it is 30~40 DEG C of incubator to be put into temperature, is treated
After soap lye solidification completely, the demoulding, then it is put into place more than 4 weeks under air drying environment and treats its full maturity（Soap blank is stiff, PH
In alkalescent, PH7~9）, obtain the multifunctional manual soap mainly using the rare saponin(e of ginseng as main active.
The handmade soap according to made from the above method.
Handmade soap produced by the present invention reflects that using effect is very dry and comfortable, without tight after 100 people are on probation one month
Taut sense, moistening effect is good, no allergic reaction, and skin quality tool is improved significantly.
Compared with prior art, manual soap composition of the invention remains vegetable oil, Radix Platycodonis extract to greatest extent
With the high-activity compound such as the rare saponin(e of ginseng, product is set to possess oil control and acne removal, skin whitening, moisturizing while cleaning action is played
And inhibiting bacteria and diminishing inflammation and other effects.
Embodiment
With reference to embodiment to for a more detailed description of the present invention, but embodiments of the present invention are not limited to
This, for especially not dated technological parameter or condition, can refer to routine techniques progress.
The preparation and constituent analysis of the rare saponin(e of the ginseng of embodiment 1
Extracted by raw material in fact, gen-seng haulms of gen-seng haulms through routine techniques, obtain ginseng stem and leave general saponin, ginseng stem
Leaf total saposins prepare the rare saponin(e of ginseng through HTHP heat scission reaction again, and caused rare ginsenoside mainly includes ginseng
The compositions such as saponin(e Rk1, Rg5, Rg6 and F4.
Concrete operations are as follows：Gen-seng haulms coarse powder 5kg, made solvent with 10 times of water measured or dilute alcohol and carried out refluxing extraction 3 times,
Each 4h, merge extract solution, be concentrated into medicinal extract, it is water-dispersible, D101 macroreticular resins are crossed, successively with water, the ethanol of various concentrations
Eluted, collect the component containing ginsenoside, be further concentrated to dry, obtain ginseng stem and leave general saponin 950g.Ginseng stem-leaf total soap
Glycosides 500g, after adding dilute alcohol to be dissolved, progress HIGH PRESSURE TREATMENT 2-4h in autoclave is put into, produces ginseng thermal cracking saponin(e,
After evaporating into no alcohol taste, it is freeze-dried and produces the rare saponin(e of ginseng.Detected through HPLC, mainly contain ginsenoside Rk1, Rg5,
Rg6 and F4 etc. is shown in, accompanying drawing 1.
The preparation and constituent analysis of the balloonflower root root extract of embodiment 2
Using the balloonflower root root of 2-3 lifes as raw material, extracted through routine techniques, obtain balloonflower root root extract.Concrete operation step
It is as follows：
Balloonflower root dry root coarse powder 5kg, ultrasonic wave extraction 3 times, each 1h is carried out with the aqueous solvent of 10 times of amounts, merges extraction
Liquid, it is concentrated into without alcohol taste, is freeze-dried and produces water extract 750g of balloonflower root root or so, mainly contained through HPLC detections abundant
Platycodin and the composition such as lobetyolin, see accompanying drawing 2.
The preparation method of the handmade soap of embodiment 3 is preferred
A kind of manual soap composition, it is consisted of the following components in percentage by weight：
| Sequence number（NO.） | Additive | Addition（%） |
| 1 | Coconut oil | 10.0 |
| 2 | Palm oil | 25.0 |
| 3 | Olive oil | 30.0 |
| 4 | Sodium hydroxide | 10.0 |
| 5 | The rare saponin(e of ginseng | 1.0 |
| 6 | Balloonflower root root extract | 2.0 |
| 7 | Deionized water | 22.0 |
Above-mentioned coconut oil, palm oil, olive oil are put into reactor successively, turn on agitator（10rpm）Stir,
30 DEG C are warming up to, heat preservation for standby use；
Under fast stirring（30rpm）, sodium hydroxide is dissolved in appropriate water, after being completely dissolved, is cooled to 30 DEG C；
Above-mentioned sodium hydroxide solution is slowly added in reactor, quick to stir (30rpm), until soap lye thickens（Viscosity
6000~8000mPa.s）；
After the rare saponin(e of ginseng and balloonflower root root extract are disperseed with remaining deionized water, it is added into reactor,
Stir；
Soap lye is poured into preprepared mould, after covering mould with plastic sheeting, is put into quiet in 30 DEG C of incubators
Put；
It is stripped after 48 hours, is then put into place more than 4 weeks under air drying environment and treats its full maturity（Soap blank is done
Firmly, PH is in alkalescent, PH 7~9）, obtain mainly containing the multifunctional manual soap of the rare saponin(e of ginseng.
The preparation method of the handmade soap of embodiment 4 is preferred
A kind of manual soap composition, it is consisted of the following components in percentage by weight：
| Sequence number（NO.） | Additive | Addition（%） |
| 1 | Coconut oil | 10.0 |
| 2 | Sweet Almond Oil | 30.0 |
| 3 | Wooden fruit oil | 25.0 |
| 4 | Sodium hydroxide | 10.0 |
| 5 | The rare saponin(e of ginseng | 1.5 |
| 6 | Balloonflower root root extract | 1.5 |
| 7 | Deionized water | 22.0 |
Above-mentioned coconut oil, Sweet Almond Oil, wooden fruit oil are put into reactor successively, turn on agitator（10rpm）Stirring is equal
It is even, 30 DEG C are warming up to, heat preservation for standby use；
Under fast stirring（30rpm）, sodium hydroxide is dissolved in appropriate water, after being completely dissolved, is cooled to 30 DEG C；
Above-mentioned sodium hydroxide solution is slowly added in reactor, quick to stir (30rpm), until soap lye thickens（Viscosity
6000~8000mPa.s）；
After the rare saponin(e of ginseng and balloonflower root root extract are disperseed with remaining deionized water, it is added into reactor,
Stir；
Soap lye is poured into preprepared mould, after covering mould with plastic sheeting, is put into quiet in 30 DEG C of incubators
Put；
It is stripped after 48 hours, is then put into place more than 4 weeks under air drying environment and treats its full maturity（Soap blank is done
Firmly, PH is in alkalescent, PH 7~9）, obtain mainly containing the multifunctional manual soap of the rare saponin(e of ginseng.
The preparation method of the handmade soap of embodiment 5 is preferred
A kind of manual soap composition, it is consisted of the following components in percentage by weight：
| Sequence number（NO.） | Additive | Addition（%） |
| 1 | Coconut oil | 10.0 |
| 2 | Palm oil | 30.0 |
| 3 | Olive oil | 15.0 |
| 4 | Wooden fruit oil | 10.0 |
| 5 | Sodium hydroxide | 10.0 |
| 6 | The rare saponin(e of ginseng | 2.0 |
| 7 | Balloonflower root root extract | 2.0 |
| 8 | Deionized water | 21.0 |
Above-mentioned coconut oil, palm oil, olive oil, wooden fruit oil are put into reactor successively, turn on agitator（10rpm）Stir
Mix uniformly, be warming up to 30 DEG C, heat preservation for standby use；
Under fast stirring（30rpm）, sodium hydroxide is dissolved in appropriate water, after being completely dissolved, is cooled to 30 DEG C；
Above-mentioned sodium hydroxide solution is slowly added in reactor, quick to stir (30rpm), until soap lye thickens（Viscosity
6000~8000mPa.s）；
After the rare saponin(e of ginseng and balloonflower root root extract are disperseed with remaining deionized water, it is added into reactor,
Stir；
Soap lye is poured into preprepared mould, after covering mould with plastic sheeting, is put into quiet in 30 DEG C of incubators
Put；
It is stripped after 48 hours, is then put into place more than 4 weeks under air drying environment and treats its full maturity（Soap blank is done
Firmly, PH is in alkalescent, PH 7~9）, obtain mainly containing the multifunctional manual soap of the rare saponin(e of ginseng.
The invention is not limited in above-mentioned embodiment, without departing from the spirit and scope of the present invention, to this
Invent the various modifications made and/or deformation belongs to protection scope of the present invention.
The preparation method of the handmade soap of embodiment 6 is preferred
A kind of manual soap composition, it is consisted of the following components in percentage by weight：
| Sequence number（NO.） | Additive | Addition（%） |
| 1 | Coconut oil | 10.0 |
| 2 | Olive oil | 15.0 |
| 3 | Evening primrose oil | 20.0 |
| 4 | Grape-kernel oil | 10.0 |
| 5 | Sodium hydroxide | 10.0 |
| 6 | The rare saponin(e of ginseng | 2.0 |
| 7 | Balloonflower root root extract | 2.0 |
| 8 | Deionized water | 21.0 |
Above-mentioned coconut oil, olive oil, evening primrose oil and grape-kernel oil are put into reactor successively, turn on agitator
（10rpm）Stir, be warming up to 30 DEG C, heat preservation for standby use；
Under fast stirring（30rpm）, sodium hydroxide is dissolved in appropriate water, after being completely dissolved, is cooled to 30 DEG C；
Above-mentioned sodium hydroxide solution is slowly added in reactor, quick to stir (30rpm), until soap lye thickens（Viscosity
6000~8000mPa.s）；
After the rare saponin(e of ginseng and balloonflower root root extract are disperseed with remaining deionized water, it is added into reactor,
Stir；
Soap lye is poured into preprepared mould, after covering mould with plastic sheeting, is put into quiet in 30 DEG C of incubators
Put；
It is stripped after 48 hours, is then put into place more than 4 weeks under air drying environment and treats its full maturity（Soap blank is done
Firmly, PH is in alkalescent, PH 7~9）, obtain mainly containing the multifunctional manual soap of the rare saponin(e of ginseng.
The using effect evaluation of the handmade soap of embodiment 6
Fed back after the crowd of 100 all ages and classes is continuously on probation 30 days with ginseng multifunctional manual soap provided by the invention
Work well, main fast and fine and smooth including foaming, skin quality clearly improves, and with certain oil control and acne removal, deep layer cleaning, U.S.
Multiple efficacies, the specific data such as white moisturizing, inhibiting bacteria and diminishing inflammation are as follows：
| Effect assessment | Using effect statistical analysis | Using effect statistical analysis | Using effect statistical analysis | Efficient % |
| Substantially | Typically | It is invalid | ||
| Foam is fine and smooth abundant | 98 | 2 | 100 | |
| Oil control and acne removal | 75 | 17 | 8 | 92.0 |
| Deep layer cleaning | 78 | 18 | 4 | 96.0 |
| Skin whitening, moisturizing | 85 | 10 | 5 | 95.0 |
| Inhibiting bacteria and diminishing inflammation | 76 | 15 | 9 | 91.0 |
The invention is not limited in above-mentioned embodiment, without departing from the spirit and scope of the present invention, to this
Invent the various modifications made and/or deformation belongs to protection scope of the present invention.
Brief description of the drawings：Fig. 1 be ginsenoside it is hot cracked after HPLC chromatogram；Fig. 2 is balloonflower root root extract
HPLC chromatogram.
Claims (1)
1. a kind of manual soap composition, it is characterised in that by weight percentage, the manual soap composition is：65-75% plants
Thing grease, 10-12% sodium hydroxides, the rare saponin(e of 0.5-3% ginseng, 0.1-3.0% Radix Platycodonis extract
Described Radix Platycodonis extract comes from Campanulaceae balloonflower root（Platycodon grandiflorum）Root extraction
Thing, described balloonflower root root extract are mainly that water extracts obtained extract, mainly contain 0.1~3% platycodin, system
Preparation Method is：Using the balloonflower root root of 2-3 lifes as raw material, extracted through routine techniques, obtain balloonflower root root extract, specific preparation manipulation
Step is as follows：Balloonflower root dry root coarse powder 5kg, ultrasonic wave extraction 3 times, each 1h is carried out with the aqueous solvent of 10 times of amounts, merges extraction
Liquid, no alcohol taste is concentrated into, is freeze-dried the water extract 750g for producing balloonflower root root；
The rare saponin(e of described ginseng be mainly general ginsenoside by mixture caused by HTHP thermal cracking, mainly include
Ginsenoside Rk1, Rg5, Rg6 and F4, its 4 kinds of saponin content summations are 0.01~5%, and specific preparation method is：Gen-seng haulms
Coarse powder 5kg, make solvent with 10 times of water measured or dilute alcohol and carry out refluxing extraction 3 times, each 4h, merge extract solution, be concentrated into medicinal extract,
It is water-dispersible, D101 macroreticular resins are crossed, is eluted successively with the ethanol of water, various concentrations, collects the group containing ginsenoside
Point, it is further concentrated to dry, obtains ginseng stem and leave general saponin 950g；Ginseng stem and leave general saponin 500g, after adding dilute alcohol to be dissolved, it is put into height
Press and HIGH PRESSURE TREATMENT 2-4h is carried out in sterilizer, produce ginseng thermal cracking saponin(e, after evaporating into no alcohol taste, be freeze-dried and produce ginseng
Rare saponin(e；
The vegetable fat is in coconut oil, palm oil, grape-kernel oil, evening primrose oil, olive oil, Sweet Almond Oil, wooden fruit oil
At least one, surplus are deionized water；
The handmade soap is prepared by following preparation method, is comprised the following steps：
（1）The vegetable fat is added in the reactor, after stirring, is warming up to 30~40 DEG C, constant temperature is stand-by；
（2）The sodium hydrate aqueous solution that temperature is 30~40 DEG C is added into step（1）Solution in, quick stirring, until soap lye
Thicken；
（3）The rare saponin(e of ginseng and balloonflower root root extract that water in advance is disperseed add step（2）In obtained soap lye, and stir
Mix uniformly；
（4）Step（3）Soap lye pour into preprepared mould, it is in 30~40 degree of incubator to be put into temperature, treats soap
After liquid solidification completely, the demoulding, then it is put under air drying environment and places more than 4 weeks, treat its full maturity, produce handmade soap.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022268401A1 (en) * | 2021-06-22 | 2022-12-29 | Beiersdorf Ag | Substrates containing soapworts |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106833971A (en) * | 2016-12-28 | 2017-06-13 | 贵州艾力康中草药开发有限公司 | It is a kind of with swelling and pain relieving, the Chinese medicine handmade soap of anti-inflammation and preparation method thereof |
| CN108467803A (en) * | 2017-12-19 | 2018-08-31 | 苏州纳贝通环境科技有限公司 | A kind of environment-friendly type natural liquid detergent and preparation method thereof |
| CN109651481A (en) * | 2018-12-27 | 2019-04-19 | 湖州市食品药品检验研究院 | A kind of ginsenoside extracting method and its application |
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|---|---|---|---|---|
| CN1269835C (en) * | 2002-12-13 | 2006-08-16 | 中国科学院大连化学物理研究所 | Method for preparing low-polarity ginseng saponin and its aglycone by catalytic pyrolysis |
| CN103194342A (en) * | 2013-04-25 | 2013-07-10 | 上海巴方精细化工有限公司 | Skin whitening platycodon root compound soap |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101238825B1 (en) * | 2010-02-10 | 2013-03-04 | 수성대학교 산학협력단 | The Composite make natural korean herb cosmetics from genseng saponin Rg1 and polia coccos ferment |
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2014
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1269835C (en) * | 2002-12-13 | 2006-08-16 | 中国科学院大连化学物理研究所 | Method for preparing low-polarity ginseng saponin and its aglycone by catalytic pyrolysis |
| CN103194342A (en) * | 2013-04-25 | 2013-07-10 | 上海巴方精细化工有限公司 | Skin whitening platycodon root compound soap |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022268401A1 (en) * | 2021-06-22 | 2022-12-29 | Beiersdorf Ag | Substrates containing soapworts |
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Effective date of registration: 20180820 Address after: 134500 Lazi river village, Fusong, Baishan City, Jilin Patentee after: FUSONG ANDONG GINSENG INDUSTRY CO., LTD. Address before: 130118 2888 New Town Street, Changchun, Jilin Patentee before: Jilin Agricultural University |