CN103462856B - There is the Radix et Caulis Opuntiae Dillenii mud, facial film and preparation method thereof of clean skin-care effect - Google Patents
There is the Radix et Caulis Opuntiae Dillenii mud, facial film and preparation method thereof of clean skin-care effect Download PDFInfo
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- CN103462856B CN103462856B CN201310446600.6A CN201310446600A CN103462856B CN 103462856 B CN103462856 B CN 103462856B CN 201310446600 A CN201310446600 A CN 201310446600A CN 103462856 B CN103462856 B CN 103462856B
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- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 230000000694 effects Effects 0.000 title abstract description 8
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- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 15
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- 241000219357 Cactaceae Species 0.000 claims description 6
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- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 6
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- 239000000843 powder Substances 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 4
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims description 3
- 229940058015 1,3-butylene glycol Drugs 0.000 claims description 3
- HIQIXEFWDLTDED-UHFFFAOYSA-N 4-hydroxy-1-piperidin-4-ylpyrrolidin-2-one Chemical compound O=C1CC(O)CN1C1CCNCC1 HIQIXEFWDLTDED-UHFFFAOYSA-N 0.000 claims description 3
- OQILCOQZDHPEAZ-UHFFFAOYSA-N Palmitinsaeure-octylester Natural products CCCCCCCCCCCCCCCC(=O)OCCCCCCCC OQILCOQZDHPEAZ-UHFFFAOYSA-N 0.000 claims description 3
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims description 3
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 claims description 3
- 235000019437 butane-1,3-diol Nutrition 0.000 claims description 3
- 229940081733 cetearyl alcohol Drugs 0.000 claims description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 3
- 229940008099 dimethicone Drugs 0.000 claims description 3
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 3
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 230000001804 emulsifying effect Effects 0.000 claims description 3
- GJQLBGWSDGMZKM-UHFFFAOYSA-N ethylhexyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(CC)CCCCC GJQLBGWSDGMZKM-UHFFFAOYSA-N 0.000 claims description 3
- YQEMORVAKMFKLG-UHFFFAOYSA-N glycerine monostearate Natural products CCCCCCCCCCCCCCCCCC(=O)OC(CO)CO YQEMORVAKMFKLG-UHFFFAOYSA-N 0.000 claims description 3
- SVUQHVRAGMNPLW-UHFFFAOYSA-N glycerol monostearate Natural products CCCCCCCCCCCCCCCCC(=O)OCC(O)CO SVUQHVRAGMNPLW-UHFFFAOYSA-N 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
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- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 3
- 229940100460 peg-100 stearate Drugs 0.000 claims description 3
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 3
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- 235000010384 tocopherol Nutrition 0.000 claims description 3
- 239000011732 tocopherol Substances 0.000 claims description 3
- 239000000230 xanthan gum Substances 0.000 claims description 3
- 229920001285 xanthan gum Polymers 0.000 claims description 3
- 235000010493 xanthan gum Nutrition 0.000 claims description 3
- 229940082509 xanthan gum Drugs 0.000 claims description 3
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 3
- 230000004936 stimulating effect Effects 0.000 abstract description 5
- 208000003251 Pruritus Diseases 0.000 description 7
- 238000012360 testing method Methods 0.000 description 6
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- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 2
- 239000004141 Sodium laurylsulphate Substances 0.000 description 2
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- ZZVUWRFHKOJYTH-UHFFFAOYSA-N diphenhydramine Chemical compound C=1C=CC=CC=1C(OCCN(C)C)C1=CC=CC=C1 ZZVUWRFHKOJYTH-UHFFFAOYSA-N 0.000 description 1
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- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
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Abstract
The invention provides a kind of the Radix et Caulis Opuntiae Dillenii mud, facial film and preparation method thereof with clean skin-care effect.In this pureed facial film, operating weight is raw material than the Radix et Caulis Opuntiae Dillenii mud for 10-30%.Facial film provided by the present invention for primary raw material with natural Radix et Caulis Opuntiae Dillenii, is made by original artisan craftsmanship, can effectively clean skin of face, have the function of calm skin simultaneously.Radix et Caulis Opuntiae Dillenii mud provided by the present invention and facial film thereof, safe and non-stimulating, life-time service does not have dependency, can use for sensitive group.
Description
Technical field
The present invention relates to a kind of Radix et Caulis Opuntiae Dillenii mud, specifically a kind ofly can play Radix et Caulis Opuntiae Dillenii mud that is clean, skin effect, by clay standby external-use skin care preparation of this Radix et Caulis Opuntiae Dillenii and preparation method thereof.
Background technology
Along with the raising of people's living standard, beauty and skin care becomes the thing that numerous personage of liking to be beautiful pays close attention to jointly, and the skin care item of pure natural are pursuing a goal of consumer always.
At present, although the skin care formulation kind of pureed facial film is enriched on market, what mainly use is not natural material, and such pureed facial film does not also meet the pursuit of consumer to natural skin care product.And, existing pureed facial film is mainly through adding a large amount of Kaolin, final products are made to have pureed outward appearance, although such pureed facial film also has good cleaning efficacy, but its adsorptivity is too strong, uses the very dry even pruritus of rear skin, so, existing pureed facial film after a procedure, needs to select other products to nurse face further.
In sum, a kind of skin care item can not realize again well nursing effect while effectively clean at present.Therefore, work out one and can clean skin, and the facial film raw material simultaneously with nursing effect just has profound significance.
Summary of the invention
Primary technical problem to be solved by this invention is to provide a kind of Radix et Caulis Opuntiae Dillenii mud.
Another technical problem to be solved by this invention is the preparation method providing above-mentioned Radix et Caulis Opuntiae Dillenii mud.
Another technical problem to be solved by this invention is to provide a kind of facial film using Radix et Caulis Opuntiae Dillenii mud to be raw material.
Invention thinking of the present invention is as follows:
Effect brief introduction of Radix et Caulis Opuntiae Dillenii is as follows: heat-clearing and toxic substances removing, relaxing muscles and tendons and activating QI and blood in the collateral, dissipating blood stasis for subsidence of swelling, intestinal detoxication, cooling blood and relieving pain, and intestine moistening is stopped blooding, benefiting stomach and stopping pain, antitussive.
The present invention selects natural Radix et Caulis Opuntiae Dillenii to be raw material, by original artisan craftsmanship, thus effectively can play cleaning skin, has calm skin effect simultaneously.
For realizing above-mentioned goal of the invention, the present invention adopts following technical scheme:
Use the facial film that Radix et Caulis Opuntiae Dillenii mud is prepared as raw material, be grouped into by the one-tenth of following weight ratio:
Oil phase: PEG-100 stearate 1-4%, ceteareth-250.5-2%, cetearyl alcohol 1-5%, glycerol monostearate 1-3%, dimethicone 1-4%, isopropyl myristate 2-4%, tocopherol 0.2-1%, ethylhexyl palmitate 1-4%;
Aqueous phase: xanthan gum 0.1-0.3%, glycerol 1-5%, trehalose 1-2%, 1,3 butylene glycol 2-4%, Radix et Caulis Opuntiae Dillenii mud 10-30%, water 30-60%;
Antiseptic 0.1-0.2%;
The weight ratio sum of above-mentioned all the components is 100%;
Wherein, described Radix et Caulis Opuntiae Dillenii mud is obtained by following steps:
(1) raw material is taken by following proportioning: dry cactus powder 20-40 weight portion, deionized water 60-80 weight portion;
(2) extraction process: dry cactus powder is added in deionized water, extracting liq nutrient after heating, Extracting temperature 50 DEG C, 1 hour extraction time;
(3) according to the reduction of feed volume extracted in step (2), the gellan gum of 0.1% reduction of feed volume is claimed; First with the glycerol of 2% reduction of feed volume, gellan gum is disperseed, then add 20 times of pure water stir 30 minutes swelling, obtain swelling after gellan gum solution; Gellan gum solution after swelling is added in the liquid nutrient that step (2) obtains, stir and obtain Radix et Caulis Opuntiae Dillenii mud.
Wherein more preferably, in described step (1), the dry Radix et Caulis Opuntiae Dillenii selecting more than 3 years is raw material.
Wherein more preferably, described Radix et Caulis Opuntiae Dillenii mud accounts for the weight ratio of facial film all the components is 25%.
A preparation method for above-mentioned facial film, comprises the steps:
(1) by oil phase, aqueous phase is biphase adds in oil cauldron and kettle respectively, heated and stirred is all dissolved completely to 80 ~ 85 DEG C to raw material;
(2) first by Aqueous Phase Raw Material suction emulsifying pot, then suction oil phase raw material while stirring, treat that oil phase raw material all exhausts, evacuation, stirring, homogenizing, after 4 ~ 7 minutes, are incubated and within 15 minutes, start cooling;
(3) add antiseptic when temperature drops to 40 ~ 45 DEG C, stir discharging.
Different according to use approach, the external-use skin care preparation that the present invention uses Radix et Caulis Opuntiae Dillenii mud to make, is not limited to facial film, also can be made into cleansing milk, facial cream etc.According to method known in skin care industry field, above-mentioned Radix et Caulis Opuntiae Dillenii mud can be made various different external-use skin care preparation by known method.
The recommendation method of facial film provided by the present invention is: according to individual demand on ordinary days nursing use, smear invention formulation in right amount, is as the criterion all to cover.
Advantage of the present invention and benefit:
Radix et Caulis Opuntiae Dillenii mud provided by the invention and by the clay standby external-use skin care preparation of Radix et Caulis Opuntiae Dillenii, with natural Radix et Caulis Opuntiae Dillenii for primary raw material, is obtained by original artisan craftsmanship, has the function of calm skin while effectively clean skin of face.The present invention is safe and non-stimulating, and life-time service does not have dependency, can use for sensitive group.
Detailed description of the invention
Foregoing invention content part of the present invention has done detailed description to technical scheme of the present invention, and those skilled in the art can repeat the present invention according to foregoing and obtain technique effect of the present invention.Be further explained the technology of the present invention content below by detailed description of the invention, to make, those skilled in the art are clearer understands content of the present invention, not limitation of the present invention, and any equivalent replacement or known change all belong to scope.
The present embodiment medical material used all enough can buy from China Medicament Group Corp., meets Pharmacopoeia of People's Republic of China 2005 editions standards.Other compositions are skin care item and cosmetic field customary adjuvant, all obtain by commercially available purchase.
The preparation of embodiment 1 Radix et Caulis Opuntiae Dillenii mud
(1) Radix et Caulis Opuntiae Dillenii pretreatment
The Radix et Caulis Opuntiae Dillenii selecting more than 3 years is raw material, except thorn, smashs to pieces.
(2) raw material is taken by following proportioning: dry cactus powder, 20-40 weight portion, deionized water 60-80 weight portion.
(3) extraction process: dry cactus powder is added in deionized water, extracting liq nutrient after heating, Extracting temperature 50 DEG C, 1 hour extraction time.
(4) according to the reduction of feed volume extracted in step (3), the gellan gum of 0.1% reduction of feed volume is claimed; First with the glycerol of 2% reduction of feed volume, gellan gum is disperseed, then add 20 times of pure water stir 30 minutes swelling, obtain swelling after gellan gum solution; Gellan gum solution after swelling is added in the liquid nutrient that step (3) obtains, stir and obtain Radix et Caulis Opuntiae Dillenii mud.
Obtain Radix et Caulis Opuntiae Dillenii mud, there is following Testing index: abnormal smells from the patient: hay-scented; Dry thing content: > 20; PH:4.0-6.0.
The preparation of the facial film of embodiment 2 containing Radix et Caulis Opuntiae Dillenii mud
The component of the facial film that embodiment 2 provides and weight ratio:
Oil phase: PEG-100 stearate 1-4%, ceteareth-250.5-2%, cetearyl alcohol 1-5%, glycerol monostearate 1-3%, dimethicone 1-4%, isopropyl myristate 2-4%, tocopherol 0.2-1%, ethylhexyl palmitate 1-4%;
Aqueous phase: xanthan gum 0.1-0.3%, glycerol 1-5%, trehalose 1-2%, 1,3 butylene glycol 2-4%, Radix et Caulis Opuntiae Dillenii mud 10-30%, water 30-60%;
Antiseptic 0.1-0.2%.
Preparation method:
1) by oil phase, aqueous phase is biphase adds in oil cauldron and kettle respectively, heated and stirred is all dissolved completely to 80 ~ 85 DEG C to raw material;
2) first by Aqueous Phase Raw Material suction emulsifying pot, then suction oil phase raw material while stirring, treat that oil phase raw material all exhausts, evacuation, stirring, homogenizing, after 4 ~ 7 minutes, are incubated and within 15 minutes, start cooling;
3) add antiseptic when temperature drops to 40 ~ 45 DEG C, stir discharging.
The cleaning efficacy experiment of the facial film of embodiment 3 containing 25% Radix et Caulis Opuntiae Dillenii mud
Experimental technique:
Volunteer's number is 30, wherein male volunteers 15, female volunteers 15.Using left face as test zone, smear the facial film added containing Radix et Caulis Opuntiae Dillenii mud 25% in embodiment 2; The corresponding symmetrical region of right face is blank, smears not containing the facial film of Radix et Caulis Opuntiae Dillenii mud.Wash away after 15min, volunteer's subjective assessment cleaning efficacy.
Statistics volunteer subjective evaluation result: all volunteers think that the cleaning effect containing 25% Radix et Caulis Opuntiae Dillenii mud facial film is better than matched group, and skin feel is clearly breathed freely.
The calm Efficacy experiments of the facial film of embodiment 4 containing 25% Radix et Caulis Opuntiae Dillenii mud
Test method: volunteer's number is 30, wherein male volunteers 15, female volunteers 15.Before test, half an hour enters laboratory, sits quietly 30 minutes time.After stimulating and cause by 10% sodium lauryl sulphate (SDS) solution paster (area: 2cm × 2cm) and itch, smear the facial film adding embodiment 2 Radix et Caulis Opuntiae Dillenii mud 25%; Be the blank facial film of Radix et Caulis Opuntiae Dillenii mud (not containing) with corresponding symmetrical region.Observe the skin pruritus situation in 30min.Main suit's linear Evaluating grade of pruritus degree companion's skin lesion symptom 0-3 level is adopted to calculate calm efficacy outcomes.Wherein, table 1 is depicted as the criterion of the linear Evaluating grade of clinic trial pruritus degree companion's skin lesion symptom 0-3 level, and score value is lower shows that Lavender Extract effect is better.
The criterion of table 1. pruritus
The experimental result of the calm contrast test of table 2.
Table 2 is the calm comparative test result containing 25% Radix et Caulis Opuntiae Dillenii mud facial film and blank group, and result shows to smear the facial film adding embodiment 2 Radix et Caulis Opuntiae Dillenii mud 25% and has obviously instant Lavender Extract effect.After smearing the facial film 5min adding embodiment 2 Radix et Caulis Opuntiae Dillenii mud 25%, have significantly instant sedation to skin pruritus, effective percentage reaches 70%.Within the test period of 30min, can obviously reduce because stimulating the uncomfortable phenomenon of the skin caused, overall efficiency about 93%.
In sum, Radix et Caulis Opuntiae Dillenii mud provided by the invention and by the clay standby external-use skin care preparation of Radix et Caulis Opuntiae Dillenii, with natural Radix et Caulis Opuntiae Dillenii for primary raw material, is obtained by original artisan craftsmanship, has the function of calm skin while effectively clean skin of face.The present invention is safe and non-stimulating, and life-time service does not have dependency, can use for sensitive group.
Above Radix et Caulis Opuntiae Dillenii mud provided by the present invention, facial film and preparation method thereof are described in detail.For one of ordinary skill in the art, to any apparent change that it does under the prerequisite not deviating from connotation of the present invention, all by formation to infringement of patent right of the present invention, corresponding legal responsibility will be born.
Claims (4)
1. the facial film prepared as raw material by Radix et Caulis Opuntiae Dillenii mud, is characterized in that, is grouped into by the one-tenth of following weight ratio:
Oil phase: PEG-100 stearate 1-4%, ceteareth-250.5-2%, cetearyl alcohol 1-5%, glycerol monostearate 1-3%, dimethicone 1-4%, isopropyl myristate 2-4%, tocopherol 0.2-1%, ethylhexyl palmitate 1-4%;
Aqueous phase: xanthan gum 0.1-0.3%, glycerol 1-5%, trehalose 1-2%, 1,3 butylene glycol 2-4%, Radix et Caulis Opuntiae Dillenii mud 10-30%, water 30-60%;
Antiseptic 0.1-0.2%;
The weight ratio sum of above-mentioned all the components is 100%;
Wherein, described Radix et Caulis Opuntiae Dillenii mud is prepared by following steps:
(1) raw material is taken by following proportioning: dry cactus powder 20-40 weight portion, deionized water 60-80 weight portion;
(2) extraction process: dry cactus powder is added in deionized water, extracting liq nutrient after heating, Extracting temperature 50 DEG C, 1 hour extraction time;
(3) according to the reduction of feed volume extracted in step (2), the gellan gum of 0.1% reduction of feed volume is claimed; First with the glycerol of 2% reduction of feed volume, gellan gum is disperseed, then add 20 times of pure water stir 30 minutes swelling, obtain swelling after gellan gum solution; Gellan gum solution after swelling is added in the liquid nutrient that step (2) obtains, stir and obtain Radix et Caulis Opuntiae Dillenii mud.
2. facial film as claimed in claim 1, is characterized in that:
In described step (1), the dry Radix et Caulis Opuntiae Dillenii selecting more than 3 years is raw material.
3. facial film as claimed in claim 1, it is characterized in that, the weight ratio that described Radix et Caulis Opuntiae Dillenii mud accounts for facial film all the components is 25%.
4. a preparation method for facial film as claimed in claim 1, is characterized in that, comprises the steps:
(1) by the oil phase in claim 1, aqueous phase is biphase adds in oil cauldron and kettle respectively, heated and stirred is all dissolved completely to 80 ~ 85 DEG C to raw material;
(2) first by Aqueous Phase Raw Material suction emulsifying pot, then suction oil phase raw material while stirring, treat that oil phase raw material all exhausts, evacuation, stirring, homogenizing, after 4 ~ 7 minutes, are incubated and within 15 minutes, start cooling;
(3) add antiseptic when temperature drops to 40 ~ 45 DEG C, stir discharging.
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| CN201310446600.6A CN103462856B (en) | 2013-09-26 | 2013-09-26 | There is the Radix et Caulis Opuntiae Dillenii mud, facial film and preparation method thereof of clean skin-care effect |
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| CN102552076A (en) * | 2010-12-13 | 2012-07-11 | 烟台新时代健康产业日化有限公司 | Anti-allergy preparation and preparation method and application thereof |
| CN102631300A (en) * | 2012-04-05 | 2012-08-15 | 北京工商大学 | External traditional Chinese medicine (TCM) composition and mask with effect of improving skin textures and preparation methods thereof |
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|---|---|---|---|---|
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