CN106137935B - A kind of hydrogel facial mask of oil-control pore cleanser effect - Google Patents

A kind of hydrogel facial mask of oil-control pore cleanser effect Download PDF

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CN106137935B
CN106137935B CN201610738892.4A CN201610738892A CN106137935B CN 106137935 B CN106137935 B CN 106137935B CN 201610738892 A CN201610738892 A CN 201610738892A CN 106137935 B CN106137935 B CN 106137935B
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extract
oil
facial mask
ferulic acid
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CN106137935A (en
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钱玉连
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Guangdong dense Biology Technology Co., Ltd.
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
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    • A61K8/345Alcohols containing more than one hydroxy group
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
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    • A61K8/4993Derivatives containing from 2 to 10 oxyalkylene groups
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    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
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Abstract

The present invention relates to a kind of hydrogel facial masks of oil-control pore cleanser effect, belong to cosmetic technical field.Include mask matrix and back sheet, the mask matrix is made by following component in parts by weight:Cactus with globular meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, lemon, Basil Essential, camomile extract, ferulic acid, azone, glycerine, extract solution from aloe, polyoxyethylene sorbitan laurate, pearl powder, sodium carboxymethylcellulose, methylcellulose, crospovidone, sodium chloride, vitamin E, preservative, essence, water.Facial mask provided by the invention has effects that pore cleanser, oil-control, moisturizing, preservation period are long using natural plant essence as active constituent.

Description

A kind of hydrogel facial mask of oil-control pore cleanser effect
Technical field
The present invention relates to a kind of hydrogel facial masks of oil-control pore cleanser effect, belong to cosmetic technical field.
Background technology
Blackhead is mainly one kind " bolt " the sample object being made of sebum, cell bits and bacterium, is blocked at hair follicle opening and shape At.In addition the dust, dirt in air and oxidation, make a gradual blackening of its ingress of air, so obtaining so One less graceful title --- blackhead.Blackhead is hardened fat obturator, typically occurs in the portions such as forehead, the nose of face Position, when grease gland swashs by intermuscular needling, and pore causes obstruction full of extra grease, in nose and its peripheral part, warp Often have greasy feeling.These greases eventually harden, and become the dot of black after oxidized, these dots are exactly to be referred to as The grease obturator of blackhead.Blackhead is exactly a kind of situation of cutin embolism in fact, and superfluous grease is secreted in pore and is mixed always Useless cutin is blocked in pore, Oxidation of Fat and Oils reform into hardening grease obturator be exposed to after the surface oxidation of air present it is black Color, so we are commonly called as its blackhead.Because T words position fat secretion is vigorous, blackhead typically occurs in our forehead, nose The areas Zi Deng T position.The appearance of blackhead be personal skin quality with outside environmental elements in conjunction with and caused by, any age, any skin quality People all occur the possibility of blackhead.Weather is sultry to be caused fuel-displaced more, and pore opens, and enables the excess oil in sebum pipeline It is more prone to be aoxidized to be hardened, so blackhead situation is with regard to more obvious.So in terms of the origin cause of formation, the blackhead generated is removed A method, and from root oil-control moisturizing be also an essential ring.
CN105380890A discloses one kind and dispels blackhead facial mask, according to the number of parts by weight, including the following raw material:Rice vinegar 70-90 parts, Chinese yam concentration 10-12 parts of essence, 2-4 parts of carragheen, 10-20 parts of red wine, 15-25 parts of egg white, black sesame powder 6-8 Part, 3-5 parts of essence of 3-5 parts of concentrated pomelo juice, black soya bean concentration, 5-7 parts of pectin.CN104856900A provides a kind of blackhead film, Including following components:Water, polyvinyl alcohol, ethyl alcohol, acrylic acid (ester) analog copolymer, glutinous rehmannia root extract, belamcanda chinensis extract, tealeaves Extract, papaya extractives, Tremella fructification extract, carbon black, triethanolamine, Phenoxyethanol and essence.
But to remain pore cleanser effect undesirable for above-mentioned facial mask, does not have the shortcomings that oil-control effect.
Invention content
The purpose of the present invention is:A kind of facial mask with preferable pore cleanser effect is provided, the facial mask is with natural plants essence China is used as active constituent, has effects that oil-control, moisturizing, preservation period are long.
Technical solution is:
A kind of hydrogel facial mask of oil-control pore cleanser effect includes mask matrix and back sheet, the mask matrix It is made by following component in parts by weight:1~2 part of cactus with globular meat extract, 0.5~1 part of Eucalyptus globulus Labill.extract, tea tree 0.5~1 part of essential oil, 0.5~1 part of lemon, 0.5~1 part of Basil Essential, 0.5~1 part of camomile extract, ferulic acid 0.2 ~0.4 part, 2~4 parts of azone, 7~12 parts of glycerine, 4~6 parts of extract solution from aloe, polyoxyethylene sorbitan laurate 0.05~1 part, 0.5~0.8 part of pearl powder, 0.5~1 part of sodium carboxymethylcellulose, 4~10 parts of methylcellulose, the poly- dimension of crosslinking 0.5~0.8 part of ketone, 0.5~1 part of sodium chloride, 2~4 parts of vitamin E, 0.05~0.1 part of preservative, 0.1~0.2 part of essence, 50~80 parts of water.
The back sheet is silk fiber cloth.
The ferulic acid is that Glucosamine is modified ferulic acid.
Modified amido glucose be modified ferulic acid preparation method be:By weight, take aminoglucose hydrochloride 5~ 9 parts, be dissolved in 60~80 parts of deionized water, then pH to 11~13 adjusted with the aqueous solution of 5wt%NaOH, add Ah 3~6 parts of Wei's acid is warming up to reflux and carries out 20~60min of reaction, then reactant is evaporated under reduced pressure and is removed water, and obtained powder is used The immersion of 6~10 parts of ethyl alcohol, solids is filtered, then after solids is dried, both.
The cactus with globular meat extract be by the way that cactus with globular meat is extracted in water after, after extracting solution is concentrated under reduced pressure Obtained extract.Eucalyptus globulus Labill.extract will obtain after Eucalyptus globulus Labill leaf flooding, reduced pressure, drying;Camomile extract It will be obtained after chamomile flooding, reduced pressure, drying.
The preparation method of the hydrogel facial mask, includes the following steps:
S1 extracts cactus with globular meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, lemon, Basil Essential, chamomile Object, ferulic acid, azone, extract solution from aloe, water are uniformly mixed, and are warming up to 65~75 DEG C, and glycerine, polyoxyethylene sorbitan is added Alcohol laurate is cooled to 30~40 DEG C after mixing, adds pearl powder, modified carboxy methyl cellulose sodium, Methyl cellulose Element, crospovidone, sodium chloride, vitamin E, preservative, essence are uniformly mixed, obtain mask matrix;
S2 after mask matrix is applied on back sheet, obtains facial mask.
《Luchuan book on Chinese herbal medicine》Described in cactus with globular have effects that eliminating inflammation and expelling toxin, apocenosis myogenic, in facial mask of the invention, use Cactus with globular meat extract is allowed to penetrate into as main component inside skin, so that it is promoted skin oil and fat, purulence blood discharge, has simultaneously There is the effect of removing toxic substances, anti-inflammatory, blackhead is promoted to disappear;Tea tree ethereal oil has effects that anti-inflammatory, oil-control, can prevent blackhead from regenerating; Ferulic acid has the function of anti-oxidation, and the storage life of facial mask is made to extend;Modified carboxy methyl cellulose sodium and methylcellulose are The main component for forming hydrogel can effectively make facial mask have uniform quality, promote active ingredient draws.
Advantageous effect
Facial mask provided by the invention is using natural plant essence as active constituent, the work(with pore cleanser, oil-control, moisturizing Effect, preservation period are long.
Specific implementation mode
Embodiment 1
Hydrogel facial mask, includes mask matrix and back sheet silk fiber cloth, and the mask matrix is by according to weight Made by the following component for measuring part meter:1 part of cactus with globular meat extract, 0.5 part of Eucalyptus globulus Labill.extract, 0.5 part of tea tree ethereal oil, lemon extract 0.5 part of oil, 0.5 part of Basil Essential, 0.5 part of camomile extract, 0.2 part of ferulic acid, 2 parts of azone, 7 parts of glycerine, aloe extraction 4 parts of liquid, 0.05 part of polyoxyethylene sorbitan laurate, 0.5 part of pearl powder, 0.5 part of sodium carboxymethylcellulose, methyl are fine 4 parts of dimension element, 0.5 part of crospovidone, 0.5 part of sodium chloride, 2 parts of vitamin E, 0.05 part of preservative, 0.1 part of essence, water 50 Part.
The preparation method of the hydrogel facial mask, includes the following steps:
S1 extracts cactus with globular meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, lemon, Basil Essential, chamomile Object, ferulic acid, azone, extract solution from aloe, water are uniformly mixed, and are warming up to 65 DEG C, and glycerine, the polyoxyethylene sorbitan moon is added Cinnamic acid ester is cooled to 30 DEG C after mixing, adds pearl powder, modified carboxy methyl cellulose sodium, methylcellulose, crosslinking Povidone, sodium chloride, vitamin E, preservative, essence are uniformly mixed, obtain mask matrix;
S2 after mask matrix is applied on back sheet, obtains facial mask.
Embodiment 2
Hydrogel facial mask, includes mask matrix and back sheet silk fiber cloth, and the mask matrix is by according to weight Made by the following component for measuring part meter:2 parts of cactus with globular meat extract, 1 part of Eucalyptus globulus Labill.extract, 1 part of tea tree ethereal oil, lemon 1 Part, is gathered 1 part of Basil Essential, 1 part of camomile extract, 0.4 part of ferulic acid, 4 parts of azone, 12 parts of glycerine, 6 parts of extract solution from aloe 1 part of ethylene oxide anhydrous sorbitol laurate, 0.8 part of pearl powder, 1 part of sodium carboxymethylcellulose, 10 parts of methylcellulose, crosslinking 0.8 part of povidone, 1 part of sodium chloride, 4 parts of vitamin E, 0.1 part of preservative, 0.2 part of essence, 80 parts of water.
The preparation method of the hydrogel facial mask, includes the following steps:
S1 extracts cactus with globular meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, lemon, Basil Essential, chamomile Object, ferulic acid, azone, extract solution from aloe, water are uniformly mixed, and are warming up to 75 DEG C, and glycerine, the polyoxyethylene sorbitan moon is added Cinnamic acid ester is cooled to 40 DEG C after mixing, adds pearl powder, modified carboxy methyl cellulose sodium, methylcellulose, crosslinking Povidone, sodium chloride, vitamin E, preservative, essence are uniformly mixed, obtain mask matrix;
S2 after mask matrix is applied on back sheet, obtains facial mask.
Embodiment 3
Hydrogel facial mask, includes mask matrix and back sheet silk fiber cloth, and the mask matrix is by according to weight Made by the following component for measuring part meter:2 parts of cactus with globular meat extract, 0.8 part of Eucalyptus globulus Labill.extract, 0.8 part of tea tree ethereal oil, lemon extract 0.7 part of oil, 0.7 part of Basil Essential, 0.7 part of camomile extract, 0.3 part of ferulic acid, 3 parts of azone, 9 parts of glycerine, aloe extraction 5 parts of liquid, 0.07 part of polyoxyethylene sorbitan laurate, 0.6 part of pearl powder, 0.6 part of sodium carboxymethylcellulose, methyl are fine 5 parts of dimension element, 0.6 part of crospovidone, 0.6 part of sodium chloride, 3 parts of vitamin E, 0.08 part of preservative, 0.15 part of essence, water 70 Part.
The preparation method of the hydrogel facial mask, includes the following steps:
S1 extracts cactus with globular meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, lemon, Basil Essential, chamomile Object, ferulic acid, azone, extract solution from aloe, water are uniformly mixed, and are warming up to 70 DEG C, and glycerine, the polyoxyethylene sorbitan moon is added Cinnamic acid ester is cooled to 35 DEG C after mixing, adds pearl powder, modified carboxy methyl cellulose sodium, methylcellulose, crosslinking Povidone, sodium chloride, vitamin E, preservative, essence are uniformly mixed, obtain mask matrix;
S2 after mask matrix is applied on back sheet, obtains facial mask.
Embodiment 4
With embodiment 3 difference lies in:The ferulic acid is that Glucosamine is modified ferulic acid.Modified amido glucose Being modified the preparation method of ferulic acid is:By weight, 5~9 parts of aminoglucose hydrochloride is taken, deionized water is dissolved in In 60~80 parts, then with the aqueous solution of 5wt%NaOH pH to 11~13 is adjusted, adds 3~6 parts of ferulic acid, be warming up to and flow back into Row 20~60min of reaction, then reactant is evaporated under reduced pressure and is removed water, by 6~10 parts of immersions of ethyl alcohol of obtained powder, by solids Filter, then after solids is dried to get.
Hydrogel facial mask, includes mask matrix and back sheet silk fiber cloth, and the mask matrix is by according to weight Made by the following component for measuring part meter:2 parts of cactus with globular meat extract, 0.8 part of Eucalyptus globulus Labill.extract, 0.8 part of tea tree ethereal oil, lemon extract 0.7 part of oil, 0.7 part of Basil Essential, 0.7 part of camomile extract, Glucosamine are modified 0.3 part of ferulic acid, 3 parts of azone, sweet 9 parts of oil, 5 parts of extract solution from aloe, 0.07 part of polyoxyethylene sorbitan laurate, 0.6 part of pearl powder, carboxymethyl cellulose 0.6 part of sodium, 5 parts of methylcellulose, 0.6 part of crospovidone, 0.6 part of sodium chloride, 3 parts of vitamin E, 0.08 part of preservative, perfume Smart 0.15 part, 70 parts of water.
The preparation method of the hydrogel facial mask, includes the following steps:
S1 extracts cactus with globular meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, lemon, Basil Essential, chamomile Object, Glucosamine are modified ferulic acid, azone, extract solution from aloe, water and are uniformly mixed, and are warming up to 70 DEG C, and glycerine, polyoxy second is added Alkene anhydrous sorbitol laurate is cooled to 35 DEG C after mixing, adds pearl powder, modified carboxy methyl cellulose sodium, first Base cellulose, crospovidone, sodium chloride, vitamin E, preservative, essence are uniformly mixed, obtain mask matrix;
S2 after mask matrix is applied on back sheet, obtains facial mask.
Reference examples 1
With embodiment 3 difference lies in:Basil Essential is not added.
Hydrogel facial mask, includes mask matrix and back sheet silk fiber cloth, and the mask matrix is by according to weight Made by the following component for measuring part meter:2 parts of cactus with globular meat extract, 0.8 part of Eucalyptus globulus Labill.extract, 0.8 part of tea tree ethereal oil, lemon extract 0.7 part of oil, 0.7 part of camomile extract, 0.3 part of ferulic acid, 3 parts of azone, 9 parts of glycerine, 5 parts of extract solution from aloe, polyoxyethylene 0.07 part of anhydrous sorbitol laurate, 0.6 part of pearl powder, 0.6 part of sodium carboxymethylcellulose, 5 parts of methylcellulose, crosslinking are poly- Tie up 0.6 part of ketone, 0.6 part of sodium chloride, 3 parts of vitamin E, 0.08 part of preservative, 0.15 part of essence, 70 parts of water.
The preparation method of the hydrogel facial mask, includes the following steps:
S1 extracts cactus with globular meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, lemon, Basil Essential, chamomile Object, ferulic acid, azone, extract solution from aloe, water are uniformly mixed, and are warming up to 70 DEG C, and glycerine, the polyoxyethylene sorbitan moon is added Cinnamic acid ester is cooled to 35 DEG C after mixing, adds pearl powder, modified carboxy methyl cellulose sodium, methylcellulose, crosslinking Povidone, sodium chloride, vitamin E, preservative, essence are uniformly mixed, obtain mask matrix;
S2 after mask matrix is applied on back sheet, obtains facial mask.
The effect of blackhead is removed to verify product of the present invention to Eradicates, the present inventor has organized 160 volunteers for having blackhead Clinical test is carried out, 3 groups of embodiment, 4 groups of embodiment, 1 group of reference examples and blank group, every group of each 40 people are randomly divided into.
Embodiment 3, embodiment 4, reference examples 1 use the pore cleanser facial mask of embodiment 3, embodiment 4, reference examples 1 respectively, right According to the commercially available moisture saver mask of group use.
Application method is to open facial mask packaging after drying the cleaning of nose, facial mask is fitted on nose, absolutely empty side by side Gas removes facial mask after twenty minutes, and nose is cleaned with clear water, uses 2 times daily, is used continuously 2 months.All volunteers before test There is blackhead position to take pictures, taking pictures again at same position after test, then with the picture taken pictures twice It is compared.In this contrast test, to judge effective standard preceding reduction work(blackhead is obviously relatively used using rear blackhead Disappear, judge the standard to take effect to have a degree of reduction using rear blackhead, after judging invalid standard for use with use Preceding blackhead changes unobvious.If as follows:
Effectively It takes effect In vain Efficient %
Embodiment 3 17 18 5 87.5
Embodiment 4 23 15 2 95
Reference examples 1 16 17 7 82.5
Control group 0 0 40
As can be seen from the table, facial mask provided by the invention has the effect of preferable pore cleanser, and embodiment 3 is relative to right As usual 1 and control group all have conspicuousness P<0.05, by being modified to ferulic acid Glucosamine in embodiment 4, can promote The absorption and effect of drug, improve the effect of pore cleanser.
In addition, being also determined to the fat content in skin using skin oil and fat analyzer, according to above-mentioned same side Method uses 2 facial masks, each 20min to measure skin oil and fat content after 6 weeks again daily, and the data in each group are averaged, Difference group grease situation of change is as follows:
Grease variable quantity %
Embodiment 3 -58.9±6.5*
Embodiment 4 -67.8±7.8*#
Reference examples 1 -45.1±6.8*
Control group +2.2±0.8
* relative to control group P<0.01, # relative to 3 P of embodiment<0.01.
As can be seen that the facial mask of the present invention also has good inhibiting effect, embodiment 4 for the fat secretion of skin of face Facial mask be better than embodiment 3.

Claims (6)

1. a kind of hydrogel facial mask of oil-control pore cleanser effect, which is characterized in that include mask matrix and back sheet, it is described Mask matrix is made by following component in parts by weight:1~2 part of cactus with globular meat extract, Eucalyptus globulus Labill.extract 0.5~ 1 part, 0.5~1 part of tea tree ethereal oil, 0.5~1 part of lemon, 0.5~1 part of Basil Essential, 0.5~1 part of camomile extract, 0.2~0.4 part of ferulic acid, 2~4 parts of azone, 7~12 parts of glycerine, 4~6 parts of extract solution from aloe, the polyoxyethylene sorbitan moon 0.05~1 part of cinnamic acid ester, 0.5~1 part of sodium carboxymethylcellulose, 4~10 parts of methylcellulose, is handed over 0.5~0.8 part of pearl powder 0.5~0.8 part of povidone of connection, 0.5~1 part of sodium chloride, 2~4 parts of vitamin E, 0.05~0.1 part of preservative, essence 0.1~ 0.2 part, 50~80 parts of water.
2. the hydrogel facial mask of oil-control pore cleanser effect according to claim 1, which is characterized in that the back sheet is Silk fiber cloth.
3. the hydrogel facial mask of oil-control pore cleanser effect according to claim 1, which is characterized in that the ferulic acid is Glucosamine is modified ferulic acid.
4. the hydrogel facial mask of oil-control pore cleanser effect according to claim 3, which is characterized in that Glucosamine is modified The preparation method of ferulic acid is:By weight, take 5~9 parts of aminoglucose hydrochloride, be dissolved in deionized water 60~ In 80 parts, then with the aqueous solution of 5wt%NaOH adjust pH to 11~13, add 3~6 parts of ferulic acid, be warming up to reflux carry out it is anti- 20~60min is answered, then reactant is evaporated under reduced pressure and is removed water, 6~10 parts of immersions of ethyl alcohol of obtained powder filter out solids , then after solids is dried, both.
5. the hydrogel facial mask of oil-control pore cleanser effect according to claim 1, which is characterized in that the cactus with globular meat Extract be by the way that cactus with globular meat is extracted in water after, the extract that is obtained after extracting solution is concentrated under reduced pressure;Blue gum extracts Object will obtain after Eucalyptus globulus Labill leaf flooding, reduced pressure, drying;Camomile extract is by chamomile flooding, subtracts It is obtained after pressure concentration, drying.
6. the preparation method of the hydrogel facial mask of oil-control pore cleanser effect described in claim 1, which is characterized in that including as follows Step:S1, by cactus with globular meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, lemon, Basil Essential, camomile extract, Ferulic acid, azone, extract solution from aloe, water are uniformly mixed, and are warming up to 65~75 DEG C, and glycerine, polyoxyethylene sorbitan is added Laurate is cooled to 30~40 DEG C after mixing, adds pearl powder, sodium carboxymethylcellulose, methylcellulose, friendship Join povidone, sodium chloride, vitamin E, preservative, essence, is uniformly mixed, obtains mask matrix;Mask matrix is applied to the back of the body by S2 After on lining, facial mask is obtained.
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