CN106137935A - A kind of hydrogel facial film controlling oil pore cleanser effect - Google Patents

A kind of hydrogel facial film controlling oil pore cleanser effect Download PDF

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CN106137935A
CN106137935A CN201610738892.4A CN201610738892A CN106137935A CN 106137935 A CN106137935 A CN 106137935A CN 201610738892 A CN201610738892 A CN 201610738892A CN 106137935 A CN106137935 A CN 106137935A
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parts
extract
facial film
oil
ferulic acid
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CN106137935B (en
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钱玉连
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Guangdong dense Biology Technology Co., Ltd.
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钱玉连
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/042Gels
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/20Halogens; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4906Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4993Derivatives containing from 2 to 10 oxyalkylene groups
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/731Cellulose; Quaternized cellulose derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/817Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
    • A61K8/8176Homopolymers of N-vinyl-pyrrolidones. Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin

Abstract

The present invention relates to a kind of hydrogel facial film controlling oil pore cleanser effect, belong to cosmetic technical field.Including mask matrix and backing layer, described mask matrix is by made by following component in parts by weight: Caulis Echinopsis Multiplicis meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, Fructus Citri Limoniae quintessence oil, Basil Essential, camomile extract, ferulic acid, azone, glycerol, Aloe extraction solution, polyoxyethylene sorbitan laurate, Margarita powder, sodium carboxymethyl cellulose, methylcellulose, polyvinylpolypyrrolidone, sodium chloride, vitamin E, preservative, essence, water.The facial film that the present invention provides, using natural plant essence as active component, has pore cleanser, control oil, effect of moisturizing, and preservation is long for period.

Description

A kind of hydrogel facial film controlling oil pore cleanser effect
Technical field
The present invention relates to a kind of hydrogel facial film controlling oil pore cleanser effect, belong to cosmetic technical field.
Background technology
One " bolt " the sample thing that blackhead is mainly made up of sebum, cell bits and antibacterial, is blocked in hair follicle opening part and shape Become.Plus the dust in air, dirt and Oxidation so that it is a gradually blackening of ingress of air, so obtaining so One less graceful title blackhead.Blackhead is hardened fat obturator, typically occurs in the portions such as the forehead of face, nose Position, when oils and fats gland is too stimulated, and pore is full of unnecessary oils and fats and causes obstruction, at nose and peripheral part thereof, warp Often have greasy sensation.These oils and fatss eventually harden, oxidized after become the point of black, these points are referred to as exactly The oils and fats obturator of blackhead.Blackhead is exactly a kind of situation of cutin thromboembolism in fact, and the oils and fats secreting surplus in pore mixes always Useless cutin is blocked in pore, Oxidation of Fat and Oils reform into present after the oils and fats obturator of hardening is exposed to the surface oxidation of air black Color, so we are commonly called as its blackhead.Because T word position fat secretion is vigorous, so blackhead typically occurs in our forehead, nose Position, Zi Deng T district.The appearance of blackhead is that individual's skin quality is combined with outside environmental elements and causes, any age, any skin quality People all occur the possibility of blackhead.The sultry meeting of weather causes fuel-displaced more, and pore opens, and makes the excess oil in sebum pipeline It is more prone to oxidized hardening, so blackhead situation just becomes apparent from.So, in terms of the origin cause of formation, remove the blackhead generated It is a way, and is also a requisite ring from root control oil moisturizing.
CN105380890A discloses one and dispels blackhead facial film, calculates in parts by weight, including following raw material: rice vinegar 70-90 part, Rhizoma Dioscoreae concentrate elite 10-12 part, carrageenan 2-4 part, red wine 10-20 part, Ovum Gallus domesticus album 15-25 part, Semen Sesami Nigrum powder 6-8 Part, concentrated pomelo juice 3-5 part, Semen sojae atricolor concentrate elite 3-5 part, pectin 5-7 part.CN104856900A provides a kind of blackhead film, its Including following components: water, polyvinyl alcohol, ethanol, acrylic acid (ester) analog copolymer, Radix Rehmanniae extract, Rhizoma Belamcandae extract, Folium Camelliae sinensis Extract, Fructus Chaenomelis extract, Tremella fructification extract, white carbon black, triethanolamine, phenoxyethanol and essence.
But it is undesirable that above-mentioned facial film remains pore cleanser effect, the shortcoming without control oil effect.
Summary of the invention
It is an object of the invention to: provide a kind of facial film with preferable pore cleanser effect, this facial film is with natural plants essence China, as active component, has control oil, effect of moisturizing, and preservation is long for period.
Technical scheme is:
A kind of control oil pore cleanser effect hydrogel facial film, include mask matrix and backing layer, described mask matrix be by Made by following component in parts by weight: Caulis Echinopsis Multiplicis meat extract 1~2 parts, Eucalyptus globulus Labill.extract 0.5~1 part, tea tree ethereal oil 0.5~1 part, Fructus Citri Limoniae quintessence oil 0.5~1 part, Basil Essential 0.5~1 part, camomile extract 0.5~1 part, ferulic acid 0.2~ 0.4 part, azone 2~4 parts, glycerol 7~12 parts, Aloe extraction solution 4~6 parts, polyoxyethylene sorbitan laurate 0.05 ~1 part, Margarita powder 0.5~0.8 part, sodium carboxymethyl cellulose 0.5~1 part, methylcellulose 4~10 parts, polyvinylpolypyrrolidone 0.5 ~0.8 part, sodium chloride 0.5~1 part, vitamin E 2~4 parts, preservative 0.05~0.1 part, essence 0.1~0.2 part, water 50~ 80 parts.
Described backing layer is silk fiber cloth.
Described ferulic acid is glucosamine modification ferulic acid.
The preparation method of modified amido glucose modification ferulic acid is: by weight, take glucosamine hydrochloride 5~ 9 parts, be dissolved in deionized water 60~80 parts, then regulate pH to 11~13 with the aqueous solution of 5wt%NaOH, add Ah Acid 3~6 parts Wei, is warming up to backflow and carries out reacting 20~60min, then be evaporated under reduced pressure by reactant except water, used by the powder obtained Ethanol 6~10 parts of immersions, filter solids, then solids is dried, both.
Described Caulis Echinopsis Multiplicis meat extract be by Caulis Echinopsis Multiplicis meat is extracted in water after, after extracting solution concentrating under reduced pressure The extract obtained.Eucalyptus globulus Labill.extract is by Eucalyptus globulus Labill leaf flooding, concentrating under reduced pressure, obtain after drying;Camomile extract By Flos Matricariae chamomillae flooding, concentrating under reduced pressure, obtain after drying.
The preparation method of described hydrogel facial film, comprises the steps:
S1, by Caulis Echinopsis Multiplicis meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, Fructus Citri Limoniae quintessence oil, Basil Essential, camomile extract, Ah Acid Wei, azone, Aloe extraction solution, water mix homogeneously, be warming up to 65~75 DEG C, adds glycerol, the polyoxyethylene sorbitan moon Cinnamic acid ester, after mix homogeneously, is cooled to 30~40 DEG C, add Margarita powder, modified carboxy methyl cellulose sodium, methylcellulose, Polyvinylpolypyrrolidone, sodium chloride, vitamin E, preservative, essence, mix homogeneously, obtain mask matrix;
S2, after being applied on backing layer by mask matrix, obtains facial film.
Caulis Echinopsis Multiplicis described in " Luchuan book on Chinese herbal medicine " has eliminating inflammation and expelling toxin, effect of evacuation of pus granulation promoting, in the facial film of the present invention, uses Caulis Echinopsis Multiplicis meat extract is as main component so that it is penetrate into inside skin so that it is promotes that skin oil and fat, pus and blood are discharged, has simultaneously There is effect of removing toxic substances, antiinflammatory, promote that blackhead disappears;Tea tree ethereal oil has antiinflammatory, effect of control oil, is possible to prevent blackhead to regenerate; Ferulic acid has anti-oxidation effect, makes the storage life of facial film extend;Modified carboxy methyl cellulose sodium and methylcellulose are Form the main component of hydrogel, can effectively make facial film have uniform quality, promote active ingredient draws.
Beneficial effect
The facial film that the present invention provides, using natural plant essence as active component, has pore cleanser, control oil, effect of moisturizing, protects Tibetan is long for period.
Detailed description of the invention
Embodiment 1
Hydrogel facial film, includes mask matrix and backing layer silk fiber cloth, and described mask matrix is by according to weight portion Made by the following component of meter: Caulis Echinopsis Multiplicis meat extract 1 part, Eucalyptus globulus Labill.extract 0.5 part, tea tree ethereal oil 0.5 part, Fructus Citri Limoniae quintessence oil 0.5 part, Basil Essential 0.5 part, camomile extract 0.5 part, ferulic acid 0.2 part, azone 2 parts, glycerol 7 parts, Aloe extraction solution 4 Part, polyoxyethylene sorbitan laurate 0.05 part, Margarita powder 0.5 part, sodium carboxymethyl cellulose 0.5 part, Methyl cellulose Element 4 parts, polyvinylpolypyrrolidone 0.5 part, 0.5 part of sodium chloride, vitamin E 2 parts, preservative 0.05 part, 0.1 part of essence, 50 parts of water.
The preparation method of described hydrogel facial film, comprises the steps:
S1, by Caulis Echinopsis Multiplicis meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, Fructus Citri Limoniae quintessence oil, Basil Essential, camomile extract, Ah Acid Wei, azone, Aloe extraction solution, water mix homogeneously, be warming up to 65 DEG C, adds glycerol, polyoxyethylene sorbitan lauric acid Ester, after mix homogeneously, is cooled to 30 DEG C, adds Margarita powder, modified carboxy methyl cellulose sodium, methylcellulose, the poly-dimension of crosslinking Ketone, sodium chloride, vitamin E, preservative, essence, mix homogeneously, obtain mask matrix;
S2, after being applied on backing layer by mask matrix, obtains facial film.
Embodiment 2
Hydrogel facial film, includes mask matrix and backing layer silk fiber cloth, and described mask matrix is by according to weight portion Made by the following component of meter: Caulis Echinopsis Multiplicis meat extract 2 parts, Eucalyptus globulus Labill.extract 1 part, tea tree ethereal oil 1 part, Fructus Citri Limoniae quintessence oil 1 part, sieve Strangle quintessence oil 1 part, camomile extract 1 part, ferulic acid 0.4 part, azone 4 parts, glycerol 12 parts, Aloe extraction solution 6 parts, polyoxyethylene Anhydrous sorbitol laurate 1 part, Margarita powder 0.8 part, sodium carboxymethyl cellulose 1 part, methylcellulose 10 parts, polyvinylpolypyrrolidone 0.8 part, 1 part of sodium chloride, vitamin E 4 parts, preservative 0.1 part, 0.2 part of essence, 80 parts of water.
The preparation method of described hydrogel facial film, comprises the steps:
S1, by Caulis Echinopsis Multiplicis meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, Fructus Citri Limoniae quintessence oil, Basil Essential, camomile extract, Ah Acid Wei, azone, Aloe extraction solution, water mix homogeneously, be warming up to 75 DEG C, adds glycerol, polyoxyethylene sorbitan lauric acid Ester, after mix homogeneously, is cooled to 40 DEG C, adds Margarita powder, modified carboxy methyl cellulose sodium, methylcellulose, the poly-dimension of crosslinking Ketone, sodium chloride, vitamin E, preservative, essence, mix homogeneously, obtain mask matrix;
S2, after being applied on backing layer by mask matrix, obtains facial film.
Embodiment 3
Hydrogel facial film, includes mask matrix and backing layer silk fiber cloth, and described mask matrix is by according to weight portion Made by the following component of meter: Caulis Echinopsis Multiplicis meat extract 2 parts, Eucalyptus globulus Labill.extract 0.8 part, tea tree ethereal oil 0.8 part, Fructus Citri Limoniae quintessence oil 0.7 part, Basil Essential 0.7 part, camomile extract 0.7 part, ferulic acid 0.3 part, azone 3 parts, glycerol 9 parts, Aloe extraction solution 5 Part, polyoxyethylene sorbitan laurate 0.07 part, Margarita powder 0.6 part, sodium carboxymethyl cellulose 0.6 part, Methyl cellulose Element 5 parts, polyvinylpolypyrrolidone 0.6 part, 0.6 part of sodium chloride, vitamin E 3 parts, preservative 0.08 part, 0.15 part of essence, 70 parts of water.
The preparation method of described hydrogel facial film, comprises the steps:
S1, by Caulis Echinopsis Multiplicis meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, Fructus Citri Limoniae quintessence oil, Basil Essential, camomile extract, Ah Acid Wei, azone, Aloe extraction solution, water mix homogeneously, be warming up to 70 DEG C, adds glycerol, polyoxyethylene sorbitan lauric acid Ester, after mix homogeneously, is cooled to 35 DEG C, adds Margarita powder, modified carboxy methyl cellulose sodium, methylcellulose, the poly-dimension of crosslinking Ketone, sodium chloride, vitamin E, preservative, essence, mix homogeneously, obtain mask matrix;
S2, after being applied on backing layer by mask matrix, obtains facial film.
Embodiment 4
Difference with embodiment 3 is: described ferulic acid is glucosamine modification ferulic acid.Modified amido glucose is modified The preparation method of ferulic acid is: by weight, takes glucosamine hydrochloride 5~9 parts, be dissolved in deionized water 60~ In 80 parts, then regulate pH to 11~13 with the aqueous solution of 5wt%NaOH, add ferulic acid 3~6 parts, be warming up to backflow and carry out instead Answer 20~60min, then reactant be evaporated under reduced pressure except water, by the powder ethanol 6 obtained~10 parts of immersions, solids is filtered, Again that solids is dried, to obtain final product.
Hydrogel facial film, includes mask matrix and backing layer silk fiber cloth, and described mask matrix is by according to weight Made by the following component of amount part meter: Caulis Echinopsis Multiplicis meat extract 2 parts, Eucalyptus globulus Labill.extract 0.8 part, tea tree ethereal oil 0.8 part, lemon extract Oil 0.7 part, Basil Essential 0.7 part, camomile extract 0.7 part, glucosamine modification ferulic acid 0.3 part, azone 3 parts, sweet Oil 9 parts, Aloe extraction solution 5 parts, polyoxyethylene sorbitan laurate 0.07 part, Margarita powder 0.6 part, carboxymethyl cellulose 0.6 part of sodium, methylcellulose 5 parts, polyvinylpolypyrrolidone 0.6 part, 0.6 part of sodium chloride, vitamin E 3 parts, preservative 0.08 part, perfume Essence 0.15 part, 70 parts of water.
The preparation method of described hydrogel facial film, comprises the steps:
S1, by Caulis Echinopsis Multiplicis meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, Fructus Citri Limoniae quintessence oil, Basil Essential, camomile extract, ammonia The glucose modified ferulic acid of base, azone, Aloe extraction solution, water mix homogeneously, be warming up to 70 DEG C, adds glycerol, polyoxyethylene mistake Water sorbitan laurate, after mix homogeneously, is cooled to 35 DEG C, adds Margarita powder, modified carboxy methyl cellulose sodium, methyl fibre Dimension element, polyvinylpolypyrrolidone, sodium chloride, vitamin E, preservative, essence, mix homogeneously, obtain mask matrix;
S2, after being applied on backing layer by mask matrix, obtains facial film.
Reference examples 1
Difference with embodiment 3 is: do not add Basil Essential.
Hydrogel facial film, includes mask matrix and backing layer silk fiber cloth, and described mask matrix is by according to weight Made by the following component of amount part meter: Caulis Echinopsis Multiplicis meat extract 2 parts, Eucalyptus globulus Labill.extract 0.8 part, tea tree ethereal oil 0.8 part, lemon extract Oil 0.7 part, camomile extract 0.7 part, ferulic acid 0.3 part, azone 3 parts, glycerol 9 parts, Aloe extraction solution 5 parts, polyoxyethylene Anhydrous sorbitol laurate 0.07 part, Margarita powder 0.6 part, sodium carboxymethyl cellulose 0.6 part, methylcellulose 5 parts, crosslinking gather Dimension ketone 0.6 part, 0.6 part of sodium chloride, vitamin E 3 parts, preservative 0.08 part, 0.15 part of essence, 70 parts of water.
The preparation method of described hydrogel facial film, comprises the steps:
S1, by Caulis Echinopsis Multiplicis meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, Fructus Citri Limoniae quintessence oil, Basil Essential, camomile extract, Ah Acid Wei, azone, Aloe extraction solution, water mix homogeneously, be warming up to 70 DEG C, adds glycerol, polyoxyethylene sorbitan lauric acid Ester, after mix homogeneously, is cooled to 35 DEG C, adds Margarita powder, modified carboxy methyl cellulose sodium, methylcellulose, the poly-dimension of crosslinking Ketone, sodium chloride, vitamin E, preservative, essence, mix homogeneously, obtain mask matrix;
S2, after being applied on backing layer by mask matrix, obtains facial film.
In order to verify product of the present invention to except the effect of blackhead, the present inventor has organized 160 volunteers having blackhead to carry out Clinical trial, is randomly divided into embodiment 3 groups, embodiment 4 groups, reference examples 1 group and blank group, often organizes each 40 people.
Embodiment 3, embodiment 4, reference examples 1 use the pore cleanser facial film of embodiment 3, embodiment 4, reference examples 1 respectively, right Commercially available moisture saver mask is used according to group.
Using method be the cleaning of nose is dried after, open facial film packaging, mask sheet is combined on nose, absolutely the most empty Gas, took off facial film after 20 minutes, cleaned nose with clear water, used every day 2 times, used 2 months continuously.All volunteers before test All having blackhead position to take pictures, test is taken pictures at same position after terminating again, then with the picture taken pictures for twice Contrast.With in this contrast test, it is judged that effective standard is for reducing merit blackhead before blackhead the most relatively uses after using Disappear, it is judged that the standard taken effect for use after blackhead have a certain degree of minimizing, it is judged that invalid standard for use after with use Front blackhead change is inconspicuous.If as follows:
Effectively Take effect Invalid Effective percentage %
Embodiment 3 17 18 5 87.5
Embodiment 4 23 15 2 95
Reference examples 1 16 17 7 82.5
Matched group 0 0 40
As can be seen from the table, the facial film that the present invention provides has the effect of preferable pore cleanser, and embodiment 3 is relative to reference examples 1 and matched group all there is significance P < 0.05, by modified to ferulic acid glucosamine in embodiment 4, medicine can be promoted Absorption and effect, improve pore cleanser effect.
It addition, also use skin oil and fat analyzer the fat content in skin to be determined, according to above-mentioned same side Method, uses 2 facial films, each 20min every day, again measures skin oil and fat content after 6 weeks, and the data in each group are averaged, Different group oils and fats situations of change are as follows:
Oils and fats variable quantity %
Embodiment 3 -58.9±6.5*
Embodiment 4 -67.8±7.8*#
Reference examples 1 -45.1±6.8*
Matched group +2.2±0.8
* relative to matched group P < 0.01, # relative to embodiment 3 P < 0.01.
It can be seen that the facial film of the present invention also has good inhibiting effect, embodiment 4 for the fat secretion of skin of face Facial film be better than embodiment 3.

Claims (7)

1. the hydrogel facial film controlling oil pore cleanser effect, it is characterised in that include mask matrix and backing layer, described Mask matrix is by made by following component in parts by weight: Caulis Echinopsis Multiplicis meat extract 1~2 parts, Eucalyptus globulus Labill.extract 0.5~ 1 part, tea tree ethereal oil 0.5~1 part, Fructus Citri Limoniae quintessence oil 0.5~1 part, Basil Essential 0.5~1 part, camomile extract 0.5~1 part, Ferulic acid 0.2~0.4 part, azone 2~4 parts, glycerol 7~12 parts, Aloe extraction solution 4~6 parts, the polyoxyethylene sorbitan moon Cinnamic acid ester 0.05~1 part, Margarita powder 0.5~0.8 part, sodium carboxymethyl cellulose 0.5~1 part, methylcellulose 4~10 parts, friendship Connection polyvidone 0.5~0.8 part, sodium chloride 0.5~1 part, vitamin E 2~4 parts, preservative 0.05~0.1 part, essence 0.1~ 0.2 part, water 50~80 parts.
The hydrogel facial film of control oil pore cleanser effect the most according to claim 1, it is characterised in that described backing layer is Silk fiber cloth.
The hydrogel facial film of control oil pore cleanser effect the most according to claim 1, it is characterised in that described ferulic acid is Glucosamine modification ferulic acid.
The hydrogel facial film of control oil pore cleanser effect the most according to claim 3, it is characterised in that modified amido glucose The preparation method of modified ferulic acid is: by weight, takes glucosamine hydrochloride 5~9 parts, is dissolved in deionized water In 60~80 parts, then regulate pH to 11~13 with the aqueous solution of 5wt%NaOH, add ferulic acid 3~6 parts, be warming up to flow back into Row reaction 20~60min, then reactant is evaporated under reduced pressure except water, by the powder ethanol 6 obtained~10 parts of immersions, by solids Filter, then solids is dried, both.
The hydrogel facial film of control oil pore cleanser effect the most according to claim 1, it is characterised in that described Caulis Echinopsis Multiplicis meat Extract be by Caulis Echinopsis Multiplicis meat is extracted in water after, the extract that will obtain after extracting solution concentrating under reduced pressure.
6. Eucalyptus globulus Labill.extract is by Eucalyptus globulus Labill leaf flooding, concentrating under reduced pressure, obtain after drying;Camomile extract is that ocean is sweet Chrysanthemum flooding, concentrating under reduced pressure, obtain after drying.
7. the preparation method of the hydrogel facial film of the control oil pore cleanser effect described in claim 1, it is characterised in that include as follows Step: S1, by Caulis Echinopsis Multiplicis meat extract, Eucalyptus globulus Labill.extract, tea tree ethereal oil, Fructus Citri Limoniae quintessence oil, Basil Essential, camomile extract, Ferulic acid, azone, Aloe extraction solution, water mix homogeneously, be warming up to 65~75 DEG C, adds glycerol, polyoxyethylene sorbitan Laurate, after mix homogeneously, is cooled to 30~40 DEG C, adds Margarita powder, modified carboxy methyl cellulose sodium, Methyl cellulose Element, polyvinylpolypyrrolidone, sodium chloride, vitamin E, preservative, essence, mix homogeneously, obtain mask matrix;S2, by mask matrix After being applied on backing layer, obtain facial film.
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