CN108685834B

CN108685834B - Traditional Chinese medicine dentifrice and preparation method thereof

Info

Publication number: CN108685834B
Application number: CN201810866463.4A
Authority: CN
Inventors: 任旻琼
Original assignee: Individual
Current assignee: Individual
Priority date: 2018-08-01
Filing date: 2018-08-01
Publication date: 2021-06-25
Anticipated expiration: 2038-08-01
Also published as: CN108685834A

Abstract

The invention discloses a traditional Chinese medicine dentifrice, which comprises 9-17 parts of a traditional Chinese medicine composition, 1.5-2 parts of a surfactant, 0.02-0.06 part of a sweetening agent, 18-30 parts of an abrasive agent and 0.02-0.08 part of spice; the traditional Chinese medicine composition comprises 1.8-2.5 parts of blackberry lily, 2-3 parts of spreading hedyotis herb, 1-2 parts of walnut kernel, 0.2-0.5 part of cubeb, 0.2-0.3 part of baical skullcap root, 0.1-0.2 part of fragrant solomonseal rhizome, 0.5-1.5 parts of lotus root, 0.5-1 part of boat-fruited sterculia seed, 1-2 parts of tangerine peel, 1-2 parts of eucommia bark, 0.1-0.2 part of tabasheer, 0.1-0.3 part of clove mother and 0.5-1.5 parts of red yeast rice. The invention aims to provide a traditional Chinese medicine dentifrice which is prepared by mixing a plurality of Chinese herbal medicines, and can clear away heat and toxic materials, resist bacteria, diminish inflammation, relieve pain, prevent dental ulcer and gingival bleeding, protect throat, relieve sore throat and the like on the basis of cleaning teeth and preventing decayed teeth.

Description

Traditional Chinese medicine dentifrice and preparation method thereof

Technical Field

The invention belongs to a dentifrice, and particularly relates to a traditional Chinese medicine dentifrice and a preparation method thereof.

Background

Toothpaste is a common cleaning product in daily life and has a long history. With the continuous development of scientific technology, various types of toothpaste come out successively, and the quality and grade of products are improved continuously. Toothpaste is a necessity of life, and a considerable part of toothpaste in the market is fluorine-containing toothpaste, however, experts point out that children under 6 years old are at a high risk of using fluorine-containing toothpaste, and excessive fluorine not only causes the thinness of teeth but also reduces the hardness of bones because fluorine is a toxic substance.

In addition, the existing toothpaste only has the function of cleaning teeth, but cannot discharge fire, and has no function of preventing dental ulcer and the like. The traditional Chinese medicine dentifrice provided by the invention does not contain fluorine, not only can clean teeth and prevent decayed teeth, but also can purge fire, resist bacteria, diminish inflammation and relieve pain, and has the effects of preventing dental ulcer, gingival bleeding and the like.

Disclosure of Invention

The invention aims to provide a traditional Chinese medicine dentifrice which is prepared by mixing a plurality of Chinese herbal medicines, and can clear away heat and toxic materials, resist bacteria, diminish inflammation, relieve pain, prevent dental ulcer and gingival bleeding, protect throat, relieve sore throat and the like on the basis of cleaning teeth and preventing decayed teeth.

The invention also discloses a preparation method of the traditional Chinese medicine dentifrice.

In order to realize the purpose, the invention adopts the technical scheme that: a traditional Chinese medicine dentifrice comprises the following components in parts by weight: 9-17 parts of a traditional Chinese medicine composition, 1.5-2 parts of a surfactant, 0.02-0.06 part of a sweetening agent, 18-30 parts of an abrasive agent and 0.02-0.08 part of a spice; the traditional Chinese medicine composition comprises 1.8-2.5 parts of blackberry lily, 2-3 parts of spreading hedyotis herb, 1-2 parts of walnut kernel, 0.2-0.5 part of cubeb, 0.2-0.3 part of baical skullcap root, 0.1-0.2 part of fragrant solomonseal rhizome, 0.5-1.5 parts of lotus root, 0.5-1 part of boat-fruited sterculia seed, 1-2 parts of tangerine peel, 1-2 parts of eucommia bark, 0.1-0.2 part of tabasheer, 0.1-0.3 part of clove mother and 0.5-1.5 parts of red yeast rice.

Preferably, the surfactant is tea saponin.

Preferably, the sweetener is xylitol.

Preferably, the rubbing agent is lithopone and calcium hydrophosphate in a ratio of 1: 1.

Preferably, the flavor is cinnamon.

A preparation method of traditional Chinese medicine dentifrice is characterized by comprising the following steps:

1) soaking: pulverizing herba Hedyotidis Diffusae, semen Juglandis, fructus Litseae, Scutellariae radix, rhizoma Polygonati Odorati, semen Scaphii Lychnophori, pericarpium Citri Tangerinae, rhizoma Belamcandae, Eucommiae cortex and fructus Caryophylli, sieving with 20 mesh sieve, dicing rhizoma Nelumbinis, and soaking in the soaking solution for 30-40 min;

2) extraction: heating and extracting soaking solution of herba Hedyotidis Diffusae, semen Juglandis, fructus Litseae, Scutellariae radix, rhizoma Polygonati Odorati, rhizoma Nelumbinis, semen Scaphii Lychnophori, pericarpium Citri Tangerinae, rhizoma Belamcandae, Eucommiae cortex, and fructus Caryophylli for 3 times, each for 1 hr, filtering, and mixing filtrates;

3) concentration: concentrating, making into paste, adding concretio silicea Bambusae seu Schizostachyi fine powder, kneading into ball, placing the ball on a screen, granulating, air drying, pulverizing, and mixing with red rice fine powder to obtain Chinese medicinal composition;

4) preparation of a friction agent: calcining Concha Haliotidis at 100-120 deg.C, spraying 5-10 wt% saline water, drying, grinding, sieving with 400 mesh sieve, and mixing with calcium hydrogen phosphate;

5) mixing: mixing the Chinese medicinal composition, surfactant, sweetener, abradant, and perfume uniformly to obtain Chinese medicinal dentifrice.

Preferably, the soaking solution is prepared by mixing forging range ash and water.

Preferably, the forging stove ash is firstly contained in a basin or other vessels, is placed on fire for heating, and then is added with water and uniformly mixed; the ratio of the forging stove ash to the water is 1: 2-3.

Has the advantages that: (1) the invention provides a traditional Chinese medicine dentifrice which is prepared by mixing a plurality of Chinese herbal medicines, and has the effects of clearing away heat and toxic materials, resisting bacteria and diminishing inflammation, preventing dental ulcer and gingival bleeding, protecting throat and relieving sore throat. The invention adopts Chinese herbal medicines to be soaked in a specific soaking solution (ash water of a forging stove), has very good fire-purging effect, and can not cause excessive internal heat when gargling with the dentifrice of the invention every day.

(2) The oral problems such as dental caries, halitosis and periodontal disease are closely related to oral bacteria, the oral bacteria can be inhibited or killed by using antibiotics, but drug resistance is easy to generate and the use is limited, and many traditional Chinese medicines have the effects of resisting bacteria and diminishing inflammation, so that the activity of the oral bacteria can be reduced by using the traditional Chinese medicines in combination.

The Chinese herbal medicine prescription of the invention: the oldenlandia diffusa has the functions of clearing heat and decomposing stasis, resolving carbuncle and dissipating stagnation, promoting urination and removing dampness, the scutellaria baicalensis has the functions of clearing heat and drying dampness, purging intense heat and removing toxicity, stopping bleeding and the like, the blackberrykiky rhizome has the functions of clearing heat and removing toxicity, eliminating phlegm and relieving sore throat, and the effects of clearing heat and removing toxicity, resisting bacteria and diminishing inflammation and preventing dental ulcer are stronger when the three medicines are used together; the fructus Caryophylli has effects of warming spleen and stomach, lowering adverse qi, invigorating kidney, and tonifying yang, and can be used for treating toothache, halitosis, etc., the fructus Litseae has effects of warming spleen and stomach, dispelling cold, activating qi-flowing, relieving pain, and antibacterial and analgesic effects; cortex Eucommiae and semen Juglandis have effects of nourishing liver and kidney, and can be used for strengthening teeth and preventing dental caries; rhizoma Polygonati Odorati has effects of nourishing yin, moistening dryness, promoting fluid production, quenching thirst, semen Scaphii Lychnophori has effects of clearing lung-heat, eliminating phlegm, relieving sore throat, and restoring voice, rhizoma Nelumbinis has effects of clearing heat, promoting fluid production, cooling blood, and stopping bleeding, pericarpium Citri Tangerinae has effects of activating qi-flowing, invigorating spleen, eliminating dampness, eliminating phlegm, and the four medicines can moisten oral cavity, and protect throat. Concretio silicea Bambusae seu Schizostachyi has adsorbability, can adsorb dirt on teeth, remove dirt and fragment in oral cavity, and also has heat clearing, antibacterial, analgesic and antiinflammatory effects, and can be used in combination with herba Hedyotidis Diffusae and flos Caryophylli to enhance antibacterial and analgesic effects; the red yeast rice is prepared from rice serving as a raw material by fermenting with monascus enzyme, has strong antibacterial effect, can be used as a preservative, is beneficial to destroying protein, starch and lipid in the oral cavity, reduces the accumulation of secretion in the oral cavity and prevents dental caries.

(3) The rubbing agent adopts the lithospermum and the calcium hydrophosphate, the lithospermum has the rubbing effect to remove stained tooth pellicle and dental plaque, and simultaneously has the functions of antibiosis, antiphlogosis and hemostasis, and the hemostasis effect is better when the lithospermum is used together with the scutellaria baicalensis and the lotus root.

(4) The surfactant adopts natural tea saponin, and has functions of cleaning teeth and inhibiting bacteria while foaming.

(5) The traditional Chinese medicine composition and part of single medicines are used for in vitro experiments

The MIC of the traditional Chinese medicine composition and part of single medicines for determining the bacteriostatic ability of the traditional Chinese medicine composition to common oral pathogenic bacteria streptococcus mutans, lactobacillus acidophilus, fusobacterium nucleatum and porphyromonas gingivalis₅₀The results are as follows (μ g/L) values:

	chinese medicinal composition	All-grass of spreading hedyotis	Radix Scutellariae	Blackberry lily	Clove bud	Piper cubeba	Concretio silicea Bambusae seu Schizostachyi
								Streptococcus mutans	100	600	800	400	600	400	1000
Lactobacillus acidophilus	200	800	400	400	400	600	800
								Fusobacterium nucleatum	100	800	400	800	1000	600	1600
Porphyromonas gingivalis	200	1200	1000	600	800	1000	2000

Detailed Description

The present invention is described in detail below for the purpose of better understanding technical solutions of the present invention by those skilled in the art, and the description of the present invention is only exemplary and explanatory and should not be construed as limiting the scope of the present invention in any way.

The following are specific examples

Example 1

A traditional Chinese medicine dentifrice comprises the following components in parts by weight: 9 parts of a traditional Chinese medicine composition, 1.5 parts of tea saponin, 0.02 part of xylitol, 18 parts of an abrasive and 0.02 part of cinnamon; the traditional Chinese medicine composition comprises 1.8 parts of blackberry lily, 2 parts of spreading hedyotis herb, 1 part of walnut kernel, 0.2 part of cubeb, 0.2 part of baical skullcap root, 0.1 part of fragrant solomonseal rhizome, 0.5 part of lotus root, 0.5 part of scaphium scaphigerum, 1 part of tangerine peel, 1 part of eucommia bark, 0.1 part of tabasheer, 0.1 part of clove mother and 0.5 part of red yeast rice.

The friction agent is composed of lithospermum and calcium hydrophosphate in a ratio of 1: 1.

A preparation method of traditional Chinese medicine dentifrice comprises the following steps:

1) soaking: pulverizing herba Hedyotidis Diffusae, semen Juglandis, fructus Litseae, Scutellariae radix, rhizoma Polygonati Odorati, semen Scaphii Lychnophori, pericarpium Citri Tangerinae, rhizoma Belamcandae, Eucommiae cortex and fructus Caryophylli, sieving with 20 mesh sieve, dicing rhizoma Nelumbinis, and soaking in the soaking solution for 30 min; the soaking liquid is prepared by mixing forging furnace ash and water, wherein the forging furnace ash is firstly contained in a basin or other vessels, is placed on fire for heating, and then is added with water and is uniformly mixed; the ratio of the forging stove ash to the water is 1:2.

4) preparation of a friction agent: calcining Concha Haliotidis at 100 deg.C, spraying 5 wt% saline water, drying, grinding, sieving with 400 mesh sieve, and mixing with calcium hydrogen phosphate;

Example 2

A traditional Chinese medicine dentifrice comprises the following components in parts by weight: 17 parts of a traditional Chinese medicine composition, 2 parts of tea saponin, 0.06 part of xylitol, 30 parts of an abrasive and 0.08 part of cinnamon; the traditional Chinese medicine composition comprises 2.5 parts of blackberry lily, 3 parts of spreading hedyotis herb, 2 parts of walnut kernel, 0.5 part of cubeb, 0.3 part of baical skullcap root, 0.2 part of fragrant solomonseal rhizome, 1.5 parts of lotus root, 1 part of scaphium scaphigerum, 2 parts of tangerine peel, 2 parts of eucommia bark, 0.2 part of tabasheer, 0.3 part of clove mother and 1.5 parts of red yeast rice.

1) soaking: pulverizing herba Hedyotidis Diffusae, semen Juglandis, fructus Litseae, Scutellariae radix, rhizoma Polygonati Odorati, semen Scaphii Lychnophori, pericarpium Citri Tangerinae, rhizoma Belamcandae, Eucommiae cortex and fructus Caryophylli, sieving with 20 mesh sieve, dicing rhizoma Nelumbinis, and soaking in the soaking solution for 40 min; the soaking liquid is prepared by mixing forging furnace ash and water, wherein the forging furnace ash is firstly contained in a basin or other vessels, is placed on fire for heating, and then is added with water and is uniformly mixed; the ratio of the forging stove ash to the water is 1: 3.

4) preparation of a friction agent: calcining Concha Haliotidis at 120 deg.C, spraying 10 wt% saline water, drying, grinding, sieving with 400 mesh sieve, and mixing with calcium hydrogen phosphate;

Example 3

A traditional Chinese medicine dentifrice comprises the following components in parts by weight: 13 parts of a traditional Chinese medicine composition, 1.8 parts of tea saponin, 0.04 part of xylitol, 20 parts of an abrasive and 0.05 part of cinnamon; the traditional Chinese medicine composition comprises 2 parts of blackberry lily, 2.5 parts of spreading hedyotis herb, 1.5 parts of walnut kernel, 0.3 part of cubeb, 0.3 part of baical skullcap root, 0.2 part of fragrant solomonseal rhizome, 1.2 parts of lotus root, 0.8 part of boat-fruited sterculia seed, 1.2 parts of tangerine peel, 1.5 parts of eucommia bark, 0.2 part of tabasheer, 0.3 part of clove mother and 1 part of red yeast rice.

1) soaking: pulverizing herba Hedyotidis Diffusae, semen Juglandis, fructus Litseae, Scutellariae radix, rhizoma Polygonati Odorati, semen Scaphii Lychnophori, pericarpium Citri Tangerinae, rhizoma Belamcandae, Eucommiae cortex and fructus Caryophylli, sieving with 20 mesh sieve, dicing rhizoma Nelumbinis, and soaking in the soaking solution for 35 min; the soaking liquid is prepared by mixing forging furnace ash and water, wherein the forging furnace ash is firstly contained in a basin or other vessels, is placed on fire for heating, and then is added with water and is uniformly mixed; the ratio of the forging stove ash to the water is 1: 2.5.

4) preparation of a friction agent: calcining Concha Haliotidis at 110 deg.C, spraying 8 wt% saline water, drying, grinding, sieving with 400 mesh sieve, and mixing with calcium hydrogen phosphate;

It should be noted that, in this document, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

The principles and embodiments of the present invention are explained herein using specific examples, which are presented only to assist in understanding the method and its core concepts of the present invention. The foregoing is only a preferred embodiment of the present invention, and it should be noted that there are objectively infinite specific structures due to the limited character expressions, and it will be apparent to those skilled in the art that a plurality of modifications, decorations or changes may be made without departing from the principle of the present invention, and the technical features described above may be combined in a suitable manner; such modifications, variations, combinations, or adaptations of the invention using its spirit and scope, as defined by the claims, may be directed to other uses and embodiments.

Claims

1. The traditional Chinese medicine dentifrice is characterized by comprising the following components in parts by weight: 9-17 parts of a traditional Chinese medicine composition, 1.5-2 parts of a surfactant, 0.02-0.06 part of a sweetening agent, 18-30 parts of an abrasive agent and 0.02-0.08 part of a spice; the traditional Chinese medicine composition comprises the following raw materials: 1.8-2.5 parts of blackberry lily, 2-3 parts of spreading hedyotis herb, 1-2 parts of walnut kernel, 0.2-0.5 part of cubeb, 0.2-0.3 part of baical skullcap root, 0.1-0.2 part of fragrant solomonseal rhizome, 0.5-1.5 parts of lotus root, 0.5-1 part of boat-fruited sterculia seed, 1-2 parts of tangerine peel, 1-2 parts of eucommia bark, 0.1-0.2 part of tabasheer, 0.1-0.3 part of mother clove and 0.5-1.5 parts of red yeast rice;

the surfactant is tea saponin; the sweetener is xylitol; the spice is cinnamon;

the friction agent is composed of lithospermum and calcium hydrogen phosphate, and the ratio of the lithospermum to the calcium hydrogen phosphate is 1: 1.

2. The preparation method of the traditional Chinese medicine dentifrice according to claim 1, which is characterized by comprising the following steps:

1) soaking: pulverizing herba Hedyotidis Diffusae, semen Juglandis, fructus Litseae, Scutellariae radix, rhizoma Polygonati Odorati, semen Scaphii Lychnophori, pericarpium Citri Tangerinae, rhizoma Belamcandae, Eucommiae cortex and fructus Caryophylli, sieving with 20 mesh sieve, dicing rhizoma Nelumbinis, and soaking in the soaking solution for 30-40 min; the soaking solution is prepared by mixing forging stove ash and water;

2) extraction: heating and extracting soaking solution of herba Hedyotidis Diffusae, semen Juglandis, fructus Litseae, Scutellariae radix, rhizoma Polygonati Odorati, rhizoma Nelumbinis, semen Scaphii Lychnophori, pericarpium Citri Tangerinae, rhizoma Belamcandae, Eucommiae cortex, and flos Caryophylli for 3 times, each for 1 hr, filtering, and mixing filtrates;

3) concentration: concentrating, making into paste, adding concretio silicea Bambusae seu Schizostachyi fine powder, kneading into pellet, sieving, granulating, air drying, pulverizing, and mixing with red rice fine powder to obtain Chinese medicinal composition;

4) preparation of a friction agent: calcining Concha Haliotidis at 100-120 deg.C, spraying 5-10 wt% of saline water, drying, grinding, sieving with 400 mesh sieve, and mixing with calcium hydrogen phosphate;

3. The method for preparing a traditional Chinese medicine dentifrice according to claim 2, wherein the calcined ash is first contained in a basin or other vessel, and then is heated by fire, and then water is added to the basin or vessel and mixed uniformly; the ratio of the forging stove ash to the water is 1: 2-3.