CN104388213A - Handmade camellia oil soap and preparation method thereof - Google Patents
Handmade camellia oil soap and preparation method thereof Download PDFInfo
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Abstract
The invention relates to handmade camellia oil soap and a preparation method thereof. The handmade camellia oil soap is prepared from the following raw materials in parts by mass: 40-80 parts of camellia oil, 1-30 parts of palm oil, 1-30 parts of coconut oil, 5-30 parts of an alkaline solution and a proper amount of essential oil. The handmade camellia oil soap disclosed by the invention is simple in preparation process, diversified in product shape, flavor and color, moderate in hardness, convenient to store, durable in use, quite high in practicability and quite high in economic efficiency; the method disclosed by the invention is simple in preparation process, easy to implement, high in production efficiency, high in safety and capable of rapidly and efficiently preparing the handmade camellia oil soap which is good in cleaning, wetting and nourishing effects, moderate in hardness and durable in use.
Description
(1) technical field
The present invention relates to a kind of Camellia oil handmade soap and preparation method thereof.
(2) background technology
Camellia oil, another name camellia seed oil is the natural plant oil extracting gained from tea seed, belong to high-grade plant health-care oil, not only having quite high nutritive value, also have very high pharmaceutical use simultaneously, is the safest externally applied agent that has no side effect and cosmetics and skincare product.Camellia oil contains abundant VITAMIN and oleic acid, is very easily absorbed by the skin; But also containing mineral elements such as biologically active substance and potassium, zinc, selenium such as squalene, tea saponin, tea-polyphenol, amino acid.Now commercially all contain the composition of Camellia oil in a lot of makeup, such as cleansing milk, shampoo, handmade soap, skin care product etc.
The Chinese patent of publication No. CN 103897896A discloses the making method that a kind of tea oil, Jojoba oil and tea essential oil and sodium hydroxide saponification make tea oil perfumed soap; Use and be rich in the Camellia oil saponification gained sodium palmitate cleaning capacity of unsaturated fatty acids, whipability is poor, soap body quality is softer at normal temperatures, easily softens, and not easily preserves, and clean of daily shower, is less than 4 weeks/100g work-ing life;
The Chinese patent of publication No. CN 103589534A discloses the manufacture method adopting highly purified cold press Camellia oil, sodium hydroxide, pure water and Camellia oil essential oil to manufacture a kind of Camellia oil perfumed soap of green health; This soap receives composition primarily of unsaturated fatty acids, and soap body is soft at normal temperatures, and hardness is low, easily softens, moisture-sensitive, clean of daily shower, work-ing life about 3 weeks/100g, foam is tiny, rare, and cleaning force is undesirable.
The Chinese patent of publication No. CN 103333752A discloses and adopts natural phant Camellia oil, palm wet goods vegetables oil is raw material, with sodium hydroxide with physiological saline through low temperature cold system, and add the camellia oil skin care soap of effective skin-care nutrient composition such as honey, aloe; The plam oil saponification gained saturated fatty acid being rich in saturated fatty acid receive with Camellia oil saponification after unsaturated fatty acids sodium arrange in pairs or groups, substantially increase soap body hardness, clean of daily shower, work-ing life about 5 weeks/100g; But foaming effect and cleaning force are all undesirable; And the natural glycerin because of saponification generation is partially soluble in excessive physiological saline and runs off, and causes moistening degree poor.
The Chinese patent of publication No. CN 103937626A discloses a kind ofly fires the alkali lye after knot alkali and Camellia oil, sweet oil, olive seed oil, Rice pollard oil, greatly Rice & peanut milk low temperature cold natural phant handmade soap by paulownia shell or mangosteen, also discloses the preparation method of this natural handmade soap.Alkali lye saponification after this patent selects paulownia shell or mangosteen to fire knot alkali, performance obviously comparatively gentle, the safety of sodium hydroxide; But, alkali lye raw material sources not easily and complicated operation.Gained handmade soap cleaning force is poor, and soap body hardness is low, and clean of daily shower, be less than 4 weeks/100g work-ing life, foaming effect is undesirable, and cost is higher.
(3) summary of the invention
For above deficiency, the present invention coordinates with the Camellia oil being rich in oleic acid is rich in the Oleum Cocois of lauric acid and tetradecanoic acid, the high-melting-point plam oil being rich in palmitinic acid and the cold system of alkali lye low-temperature saponification, and add the effective skin care ingredient of essential oil, there is provided a kind of formula rationally, preparation is simple, be easy to realize, performance is gentle, and clean, moisturizing, nourishing is respond well and soap body hardness suitable, fine and smooth, the long-lived Camellia oil handmade soap of foaming abundancy and preparation method thereof.The preparation technology of the method is simple, and safety easily realizes, it is clean rapidly and efficiently to prepare and moisturizing and nourishing is respond well and the Camellia oil handmade soap that hardness is suitable.
The technical solution used in the present invention is:
A kind of Camellia oil handmade soap, the raw material following by quality proportioning is made:
Described plam oil is the one in 58 degree of plam oils, 52 degree of plam oils, 44 degree of plam oils, 33 degree of plam oils;
The solute of described alkali lye is sodium hydroxide, solvent is that water, hydrosol are (also known as flower water, refer to the water that essential oil stays in distillation extraction process, it is a kind of byproduct of essential oil, refining a kind of 100% saturated hydrosol separated in essential oil process, composition is natural pure), at least one in milk, goat milk, liquid distilled from honeysuckle flowers or lotus leaves, jasmine tea, solute is 1:2 ~ 3 with the ratio of solvent quality;
Described essential oil is at least one in Herba Lysimachiae foenumgraeci quintessence oil, lemon quintessence oil, rosemary ethereal oil, Flos Rosae Rugosae quintessence oil, chamomile essential oil, Salvia japonica Thunb. essential oil, Cananga odorata quintessence oil.
In the present invention, described Camellia oil is that tea seed warp directly squeezes the oil produced, and namely squeezes Camellia oil, remains crude substance composition wherein and trophic component completely.Sodium oleate also has the effect of nourishing lubrication while having good cleaning function, sodium laurate and Sodium tetradecanoate have good cleaning capacity and latherability, high-melting-point plam oil is solid-state under normal temperature (25 DEG C) state, be commonly called " hard oil ", Sodium pentadecanecarboxylate improves the hardness of soap body to a certain extent while as natural surface active agent to such an extent as to is convenient to deposit, thus the work-ing life extending handmade soap was at 6 weeks/more than 100g.
Preferably, described handmade soap raw material is composed as follows:
More preferred, described handmade soap raw materials quality is composed as follows:
The invention still further relates to the method preparing described Camellia oil handmade soap, described method comprises the steps:
(1) weighing sodium hydroxide and coordinative solvent prepare alkali lye in proportion;
(2) take Camellia oil, Oleum Cocois, plam oil by formula, add in container, water proof is heated to 40 ~ 60 DEG C, obtained mixed vegetable oil;
(3) get the alkali lye of formula ratio, be heated to 40 ~ 60 DEG C;
(4) alkali lye is slowly poured in mixed vegetable oil, 40 ~ 60 DEG C of insulated and stirred 1 ~ 2h, form saponification liquor;
(5) get formula ratio essential oil, add in saponification liquor, stir, then inject 40 ~ 60 DEG C of insulation 12 ~ 24h in mould, until saponification is shaping, then take out in air-dry 60 ~ 90 days of 25 ~ 35 DEG C of constant temperature, obtained described Camellia oil handmade soap.
Abovementioned steps (2), (3) are without sequencing.
The hardness that the present invention obtains handmade soap is moderate, is convenient to preserve and durable, and every 100g work-ing life is more than 6 weeks, cleaning force, foaming power are strong, and containing natural glycerin, can while clean dirt, skin is formed the protective membrane that one deck is natural, skin is had to the effects such as moisturizing; Adopt low temperature cold technology, remain nutritive substance wherein to greatest extent, as polysaccharide, phenolic compound, vitamin A, C, D, E and vitamin B group, mineral element (as potassium, zinc, selenium etc.), amino acid etc.In penetrating to the skin through pore in use, thus reach clean, maintenance skin effect unique.This handmade soap both can be used as washing one's face, and makeup removing, can be used as again shower use, and foam exquisiteness is abundant, thoroughly can remove the greasy dirt of pore depths.Make skin moisten gloss, high resilience, camellia handmade soap is not containing sanitas, and the chemical compositions such as tensio-active agent are one very safety and effective skin clean and cosmetics.Not only performance is gentle, and environmental protection.Use the sodium soap of rear discharge to have good biological degradability, in 48h, be directly bacterially decomposed into water and carbonic acid gas.
Beneficial effect of the present invention is mainly reflected in: Camellia oil handmade soap manufacture craft of the present invention is simple, the variation of shape of product, fragrance, color, and hardness is moderate, is convenient to preservation, durable, has very strong practicality and very high economic benefit; The inventive method preparation technology is simple and easy, be easy to realize, and production efficiency is high, and security is high, rapidly and efficiently can prepare clean, moisturizing, nourishing is respond well and hardness is suitable for, the Camellia oil handmade soap of durable.
(4) embodiment
Below in conjunction with specific embodiment, the present invention is described further, but protection scope of the present invention is not limited in this:
Embodiment 1:
A kind of Camellia oil handmade soap, described Camellia oil handmade soap every 100g finished product handmade soap raw material dosage is as follows: squeezing Camellia oil (Zhejiang Choisun Tea Development Co., Ltd.'s production): 50g; 33 degree of plam oil: 20g; Oleum Cocois: 20g; Alkali lye: 10g; Essential oil: 2mL.
Described alkali lye is aqueous sodium hydroxide solution.
Described essential oil is Peppermint essential oil.
The preparation method of this Camellia oil handmade soap is as follows:
(1) by metering weighing sodium hydroxide, with water in mass ratio 1:3 be mixed and made into alkali lye.
(2) take out the Camellia oil of corresponding formula ratio, Oleum Cocois, 33 degree of plam oils add in container, water proof is heated to 40 DEG C, obtained mixed vegetable oil;
(3) take out the alkali lye of corresponding formula ratio, be heated to 40 DEG C;
(4) alkali lye is slowly poured in mixed vegetable oil, and Keep agitation action and 40 DEG C of insulation 2h, form saponification liquor;
(5) get the Peppermint essential oil of respective amount, add in saponification liquor, and stir, then inject 40 DEG C of insulation 12h in mould, until saponification is shaping, constant temperature 28 DEG C, after air-dry 90 days, obtains Camellia oil handmade soap;
Described step (2), (3) are without sequencing.
Gained Camellia oil handmade soap pH 6.8, through 40 personnel (wherein, dry skin 10; 10, oiliness skin; 10, mixed type skin; 10, susceptibility skin.), take a shower voluntarily clean and use six weeks.All users of service reflection, this soap hardness is moderate, and cleaning force is strong, and foam is fine and smooth, abundant, and performance is gentle, refrigerant skin toner, moisturizing and nourishing skin care and have the distinctive fragrance of peppermint, every 100g work-ing life (about 85 days) more than six weeks.Without interference, tight sense, without allergic phenomena, rear skin is used to have obviously finer and smoother, smooth, glossy.
Embodiment 2:
A kind of Camellia oil handmade soap, described Camellia oil handmade soap every 100g finished product handmade soap raw material dosage is as follows: squeezing Camellia oil: 60g; 44 degree of plam oil: 15g; Oleum Cocois: 10g; Alkali lye: 15g; Essential oil: 3mL.
Described sodium hydroxide rose wate solution.
Described essential oil is lemon quintessence oil.
The preparation method of this Camellia oil handmade soap is as follows:
(1) by metering weighing sodium hydroxide, with rose wate in mass ratio 1:2.5 be mixed and made into alkali lye.
(2) take out the Camellia oil of corresponding formula ratio, Oleum Cocois, 44 degree of plam oils, then add in container, water proof is heated to 45 DEG C, obtained mixed vegetable oil;
(3) take out the alkali lye of corresponding formula ratio, be heated to 45 DEG C;
(4) alkali lye is slowly poured in mixed vegetable oil, Keep agitation and 45 DEG C insulation 1.5h, formed saponification liquor;
(5) get respective amount lemon quintessence oil, add in saponification liquor, and stir, then inject 45 DEG C of insulation 12h in mould, until saponification is shaping, the demoulding, constant temperature 30 DEG C, after air-dry 90 days, obtains Camellia oil handmade soap;
Described step (2), (3) are without sequencing.
Gained Camellia oil handmade soap pH 7.0, through 40 personnel (wherein, dry skin 10; 10, oiliness skin; 10, mixed type skin; 10, susceptibility skin.), take a shower voluntarily clean and use six weeks.All users of service reflection, this soap hardness is moderate, and cleaning force is strong, and foam is fine and smooth, abundant, and performance is gentle, refrigerant skin toner, moisturizing and nourishing skin care and have rose, the distinctive fragrance of lemon, every 100g work-ing life (about 72 days) more than six weeks.Without interference, tight sense, without allergic phenomena, rear skin is used to have obviously finer and smoother, smooth, glossy.
Embodiment 3:
A kind of Camellia oil handmade soap, described Camellia oil handmade soap every 100g finished product handmade soap raw material dosage is as follows: squeezing Camellia oil: 75g; 52 degree of plam oil: 5g; Oleum Cocois: 5g; Alkali lye: 15g; Essential oil: 2mL.
Described alkali lye is aqueous sodium hydroxide solution.
Described essential oil is Herba Lysimachiae foenumgraeci quintessence oil.
The preparation method of this Camellia oil handmade soap is as follows:
(1) by metering weighing sodium hydroxide, with water in mass ratio 1:2.5 be mixed and made into alkali lye.
(2) take out the Camellia oil of corresponding formula ratio, Oleum Cocois, 52 degree of plam oils, then add in container, water proof is heated to 55 DEG C, obtained mixed vegetable oil;
(3) take out the alkali lye of corresponding formula ratio, be heated to 55 DEG C;
(4) alkali lye is slowly poured in mixed vegetable oil, and Keep agitation action and 55 DEG C of insulation 1h, form saponification liquor;
(5) get respective amount Herba Lysimachiae foenumgraeci quintessence oil, add in saponification liquor, and stir, inject 45 DEG C of insulation 12h in mould subsequently, until saponification is shaping, take out constant temperature 30 DEG C after air-dry 90 days, obtained Camellia oil handmade soap goods;
Described step (2), (3) are without sequencing.
Gained Camellia oil handmade soap pH 7.1, through 40 personnel (wherein, dry skin 10; 10, oiliness skin; 10, mixed type skin; 10, susceptibility skin.), take a shower voluntarily clean and use six weeks.All users of service reflection, this soap hardness is moderate, and cleaning force is strong, and foam is fine and smooth, abundant, and performance is gentle, refrigerant skin toner, moisturizing and nourishing skin care and have the distinctive fragrance of lavandula angustifolia, and every 100g takes a shower clean work-ing life (about 65 days) more than six weeks.Without interference, tight sense, without allergic phenomena, rear skin is used to have obviously finer and smoother, smooth, glossy.
Embodiment 4:
A kind of Camellia oil handmade soap, described Camellia oil handmade soap every 100g finished product handmade soap raw material dosage is as follows: squeezing Camellia oil: 80g; 58 degree of plam oil: 8g; Oleum Cocois: 2g; Alkali lye: 15g; Essential oil: 2mL.
Described alkali lye is the sodium hydroxide anthemidis flos aqueous solution.
Described essential oil is Flos Rosae Rugosae quintessence oil.
The preparation method of this Camellia oil handmade soap is as follows:
(1) by metering weighing sodium hydroxide, with anthemidis flos water in mass ratio 1:2.5 be mixed and made into alkali lye.
(2) take out the Camellia oil of corresponding formula ratio, Oleum Cocois, 58 degree of plam oils, then add in container, be heated to 60 DEG C, obtained mixed vegetable oil;
(3) take out the alkali lye of corresponding formula ratio, be heated to 60 DEG C;
(4) alkali lye is slowly poured in mixed vegetable oil, and Keep agitation action and 60 DEG C of insulation 1h, form saponification liquor;
(5) get respective amount Flos Rosae Rugosae quintessence oil, add in saponification liquor, and stir, then inject 45 DEG C of insulation 12h in mould, until saponification is shaping, take out constant temperature 30 DEG C after air-dry 90 days, obtained Camellia oil handmade soap goods;
Described step (2), (3) are without sequencing.
Gained Camellia oil handmade soap pH 7.2, through 40 personnel (wherein, dry skin 10; 10, oiliness skin; 10, mixed type skin; 10, susceptibility skin.), take a shower voluntarily clean and use six weeks.All users of service reflection, this soap hardness is moderate, and cleaning force is strong, and foam is fine and smooth, abundant, and performance is gentle, refrigerant skin toner, moisturizing and nourishing skin care and have Flos Matricariae chamomillae, the distinctive fragrance of rose, every 100g work-ing life (about 70 days) more than six weeks.Without interference, tight sense, without allergic phenomena, rear skin is used to have obviously finer and smoother, smooth, glossy.
Embodiment 5:
A kind of Camellia oil handmade soap, described Camellia oil handmade soap every 100g finished product handmade soap raw material dosage is as follows: squeezing Camellia oil: 80g; 44 degree of plam oil: 8g; Oleum Cocois: 2g; Alkali lye: 15g; Essential oil: 5mL.
Described alkali lye is sodium hydroxide milk soln.
Described essential oil is rosemary ethereal oil, Salvia japonica Thunb. essential oil (volume ratio 2:3).
The preparation method of this Camellia oil handmade soap is as follows:
(1) by weighing balance sodium hydroxide, with milk in mass ratio 1:2.4 be mixed and made into alkali lye.
(2) take out the Camellia oil of corresponding formula ratio, Oleum Cocois, 44 degree of plam oils, add in container, water proof is heated to 45 DEG C and is incubated, obtained mixed vegetable oil;
(3) take out the alkali lye of corresponding formula ratio, be heated to 45 DEG C;
(4) alkali lye is slowly poured in mixed vegetable oil, and Keep agitation action and 45 DEG C of insulation 2h, form saponification liquor;
(5) get respective amount rosemary ethereal oil, Salvia japonica Thunb. essential oil, add in saponification liquor, and stir, then inject 45 DEG C of insulation 12h in mould, until saponification is shaping, take out constant temperature 30 DEG C after air-dry 90 days, obtained tea oil handmade soap goods;
Described step (2), (3) are without sequencing.
Gained Camellia oil handmade soap pH 6.6, through 40 personnel (wherein, dry skin 10; 10, oiliness skin; 10, mixed type skin; 10, susceptibility skin.), take a shower voluntarily clean and use six weeks.All user of service's reflections, this soap hardness is moderate, and cleaning force is strong, foam is fine and smooth, abundant, and performance is gentle, refrigerant skin toner, moisturizing and nourishing skin care and have Rosmarinus officinalis, Salvia japonica Thunb., the distinctive fragrance of milk, every 100g work-ing life (about 68 days) more than six weeks.Without interference, tight sense, without allergic phenomena, rear skin is used to have obviously finer and smoother, smooth, glossy.
Wherein optimum optimization case is embodiment 1.
Below be only several concrete preferred embodiment of the present invention; these embodiments should be understood only be not used in for illustration of the present invention and limit the scope of the invention; after having read the present invention; the amendment of those skilled in the art to the various equivalent form of value of the present invention all falls within claims of the present invention and limited, and protection scope of the present invention should be as the criterion with claim of the present invention.
Claims (4)
1. a Camellia oil handmade soap, the raw material following by quality proportioning is made:
Described plam oil is the one in 58 degree of plam oils, 52 degree of plam oils, 44 degree of plam oils, 33 degree of plam oils;
The solute of described alkali lye is sodium hydroxide, and solvent is at least one in water, hydrosol, milk, goat milk, liquid distilled from honeysuckle flowers or lotus leaves, jasmine tea, and solute is 1:2 ~ 3 with the ratio of solvent quality;
Described essential oil is at least one in Herba Lysimachiae foenumgraeci quintessence oil, lemon quintessence oil, rosemary ethereal oil, Flos Rosae Rugosae quintessence oil, chamomile essential oil, Salvia japonica Thunb. essential oil, Cananga odorata quintessence oil.
2. Camellia oil handmade soap as claimed in claim 1, is characterized in that its raw materials quality is composed as follows:
3. Camellia oil handmade soap as claimed in claim 1, is characterized in that its raw materials quality is composed as follows:
4. prepare the method for Camellia oil handmade soap described in claim 1, described method comprises the steps:
(1) weighing sodium hydroxide and coordinative solvent prepare alkali lye in proportion;
(2) take Camellia oil, Oleum Cocois, plam oil by formula, add in container, water proof is heated to 40 ~ 60 DEG C, obtained mixed vegetable oil;
(3) get the alkali lye of formula ratio, be heated to 40 ~ 60 DEG C;
(4) alkali lye is slowly poured in mixed vegetable oil, 40 ~ 60 DEG C of insulated and stirred 1 ~ 2h, form saponification liquor;
(5) get formula ratio essential oil, add in saponification liquor, stir, then inject 40 ~ 60 DEG C of insulation 12 ~ 24h in mould, until saponification is shaping, then take out in air-dry 60 ~ 90 days of 25 ~ 35 DEG C of constant temperature, obtained described Camellia oil handmade soap.
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