CN106010832A - Aloe-rose essential oil handmade soap and making method thereof - Google Patents

Aloe-rose essential oil handmade soap and making method thereof Download PDF

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Publication number
CN106010832A
CN106010832A CN201610400638.3A CN201610400638A CN106010832A CN 106010832 A CN106010832 A CN 106010832A CN 201610400638 A CN201610400638 A CN 201610400638A CN 106010832 A CN106010832 A CN 106010832A
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parts
oil
fats
oils
handmade soap
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张杨
汪凌
刘馨
樊双鸣
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Dermatology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Detergent Compositions (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses an aloe-rose essential oil handmade soap and a making method thereof, belonging to the field of daily chemicals. The objective of the invention is to overcome the problem that conventional perfumed soap usually lacks nutritional components beneficial for the skin and poses environmental pollution. The handmade soap comprises the following raw materials: vegetable fat, sodium hydroxide, rose essential oil and aloe juice, wherein the usage amounts of sodium hydroxide, rose essential oil and aloe juice are 12 to 15%, 0.5 to 1.0% and 10 to 12% of the total weight of the fat, respectively, and the vegetable fat comprises, by weight, 15 to 25% of vegetable shortening, 10 to 20 parts of refined cocoa butter, 25 to 35 parts of avocado oil, 10 to 20 parts of filbert oil, 15 to 25 parts of coconut oil and 3 to 7 parts of white beeswax. The making method is simple and convenient; the materials used in the invention are easily available and cheap; and the handmade soap is nonirritant, green, environment friendly, safe and convenient to use and qualified and has deep cleaning, moistening and moisture-retaining functions.

Description

Chinese aloe rose quintessence oil handmade soap and manufacture method
Technical field
The invention belongs to household chemicals field, be specifically related to a kind of Chinese aloe rose quintessence oil handmade soap.
Background technology
Soap is the articles for washing that human history is the longest, so far existing thousands of years history, often makes in current people life Fancy soap be typically at high temperature mix with all kinds of animal oils and alkali for primary raw material, through saltouing, filtering, isolate sweet Oil, is allowed to the fastest rapid-result soap, then adds foaming agent, antibacterial, lubricant, synthetic dyestuff, synthetic perfume etc. and be processed into.This Class fancy soap does not contains natural glycerin, lacks the nutritional labeling of useful skin, and this kind of fancy soap of life-time service can make xerosis cutis, affects skin The balance of nature ability of skin, makes skin resistance decline.Secondly, in terms of environmental conservation, after this kind of chemosynthesis fancy soap uses The sewage chemical complicated component of discharge, the most degradable, water quality environment can be affected.
Summary of the invention
It is an object of the invention to provide a kind of Chinese aloe rose quintessence oil handmade soap, to solve, existing fancy soap is logical lacks useful skin Nutritional labeling and exist pollute environment problem.
It is a further object to provide the manufacture method of a kind of Chinese aloe rose quintessence oil handmade soap.
Technical solution of the present invention is as follows: a kind of Chinese aloe rose quintessence oil handmade soap, and it includes following raw materials according: Vegetable oil lipoprotein, hydrogen Sodium oxide, Flos Rosae Rugosae quintessence oil, aloe juice, the consumption of sodium hydroxide be above-mentioned oils and fats gross weight be the 12%-of above-mentioned oils and fats gross weight 15%, the consumption of Flos Rosae Rugosae quintessence oil be above-mentioned oils and fats gross weight be the 0.5%-1.0% of oils and fats gross weight, the consumption of aloe juice is above-mentioned Oils and fats gross weight is the 10%-12% of oils and fats gross weight;Described Vegetable oil lipoprotein is made up of the raw material of following weight portion: plant white oil 15%- 25 parts, 10 parts-20 parts of praeparata cacao fat, American Avocado Tree oil 25 parts-35 parts, hazelnut oil 10 parts-20 parts, Oleum Cocois 15 parts-25 parts, whitish honey 3 parts-7 parts of wax.
As a further improvement on the present invention, described Vegetable oil lipoprotein is made up of the raw material of following weight portion: plant white oil 20 Part, 17 parts of praeparata cacao fat, American Avocado Tree oil 30 parts, hazelnut oil 10 parts, Oleum Cocois 20 parts, 3 parts of whitish honey wax.
The manufacture method of above-mentioned Chinese aloe rose quintessence oil handmade soap, comprises the steps:
A, first the Vegetable oil lipoprotein oils and fats of solid is melted, mixing, be positioned over 50 DEG C of-55 DEG C of stirred in water bath uniform;
B, preparation sodium hydroxide solution: weigh sodium hydroxide, and dissolved with deionized water,
C, the above-mentioned sodium hydroxide solution prepared is poured in the oils and fats of mix homogeneously, and keep being sufficiently stirred for;
D, the mixed liquor of step C is reacted 50 DEG C of-55 DEG C of stirred in water bath, be subsequently added into aloe juice and continue stirring, finally Add Flos Rosae Rugosae quintessence oil, continue stirring;
E into, above-mentioned soap lye is poured die for molding, the demoulding, stand, obtain product.
As a further improvement on the present invention, in step B, the sodium hydroxide solution of preparation is cooled to 30 DEG C-35 DEG C uses.
As a further improvement on the present invention, in step B, deionized water consumption is the 33%-38% of above-mentioned oils and fats gross weight.
As a further improvement on the present invention, in step D, mixed liquor stirs the response time in a water bath is 20-30min,
As a further improvement on the present invention, in step D, mixed liquor mixing time after adding fresh aloe juice liquid is 8- 10min,
As a further improvement on the present invention, in step E, lower time of repose is 7-10 days, and the pH value of handmade soap is 7.5-8.5.
Advantage of the present invention is as follows:
(1) Flos Rosae Rugosae quintessence oil used by product of the present invention is as also having whitening, moistening face while natural perfume material, adds fresh aloe juice Liquid increases moistening effect.
(2) product of the present invention uses cera alba to keep handmade soap self soft or hard balance, and prevents soap body from depositing process Middle cracking.
(3) products material of the present invention easily obtains, and cost of manufacture is low, and technique is simple, and reaction condition is gentle and saves the energy.
(4) product of the present invention be not added with foaming agent, antibacterial, lubricant, synthetic dyestuff, synthetic perfume, surfactant, The auxiliary agents such as preservative, easy to foaming and foaming abundancy, wash and feel salubrious, can quickly wash down, little to skin burden, effectively keep skin certainly So balanced capacity, does not damage keratodermatitis, it is adaptable to chemical sensitivity skin quality and the easy obstructor of pore.There is deep layer cleaning, taste Profit moisture-keeping functions.
(5) product of the present invention (50 DEG C-55 DEG C) under low temperature makes, and relative industrial high temperature preparation method remains to greatest extent The nutritional labeling of skin-friendly, later stage molding, the demoulding to dry in the sun become the time cycle used by soap short.
(6) environment friendly and pollution-free, the sanitary sewage after using, in 24 hours, decomposes under natural conditions.
Detailed description of the invention
The following examples can further illustrate the present invention, but limits the present invention never in any form.Following embodiment Middle raw material is and is purchased.Flos Rosae Rugosae quintessence oil selects Gansu Rose grievances quintessence oil, and aloe juice is that potted plant Fresh leaf of aloe is smashed prepared.
Embodiment 1(preferred example)
Weigh Vegetable oil lipoprotein raw material (solid grease prior in microwave oven melt): plant white oil 20g, praeparata cacao fat 17g, western class Tooth produces American Avocado Tree oil 30g, and Britain produces hazelnut oil 10g, and Philippine produces Oleum Cocois 20g, and Malaysia produces whitish honey wax 3g.
Above-mentioned oils and fats is added in glass drying oven and mixes, and be placed in 53 DEG C of waters bath with thermostatic control, stir;
Weighing top grade pure cerium hydroxide sodium is the 14.4% of oils and fats gross weight, weigh that deionized water is oils and fats gross weight 36%.
It is cooled to 30 DEG C, it is to note that this process should be under conditions of having exhaust equipment after deionized water dissolved hydrogen sodium oxide Operation, and holds with polyethylene can, and the process of adding water should slowly be carried out and by polythene material stirring rod stirring and dissolving.
Then sodium hydroxide solution is slowly added in glyceride stock, allows it be sufficiently stirred for reaction in 53 DEG C of water-baths 25min, adding fresh aloe juice liquid afterwards is the 10% of oils and fats gross weight, continues stirring 10min, and finally adding Flos Rosae Rugosae quintessence oil is oils and fats The 0.7% of gross weight, stirring can draw substantially " 8 " word and stop, above-mentioned soap lye enters mold forming to soap lye surface, de-after placing 2 days Mould, is placed in left at room temperature 7-10 days, and with pH detection paper handmade soap pH value, pH value can use at 7.5-8.5.
Embodiment 2
Weigh Vegetable oil lipoprotein raw material (solid grease prior in microwave oven melt): plant white oil 15g, praeparata cacao fat 20g, western class Tooth produces American Avocado Tree oil 25g, and Britain produces hazelnut oil 17g, and Philippine produces Oleum Cocois 15g, and Malaysia produces whitish honey wax 6g.
Above-mentioned oils and fats is added in glass drying oven and mixes, and be placed in 50 DEG C of waters bath with thermostatic control, stir;Weigh Top grade pure cerium hydroxide sodium is the 12% of oils and fats gross weight, weigh that deionized water is oils and fats gross weight 33%.
It is cooled to 35 DEG C with after deionized water dissolved hydrogen sodium oxide, then sodium hydroxide solution is slowly added into oils and fats former In material, allowing it be sufficiently stirred for reacting 20min in 50 DEG C of water-baths, adding fresh aloe juice liquid afterwards is the 10.5% of oils and fats gross weight, continues Continuous stirring 10min, finally adding Flos Rosae Rugosae quintessence oil is the 1.0% of oils and fats gross weight, and stirring can draw substantially " 8 " word to soap lye surface and stop Only, above-mentioned soap lye is entered mold forming, the demoulding after placing 2 days, it is placed in left at room temperature 7-10 days, with pH detection paper handmade soap pH Value, pH value can use at 7.5-8.5.
Embodiment 3
Weigh Vegetable oil lipoprotein raw material (solid grease prior in microwave oven melt): plant white oil 22g, praeparata cacao fat 15g, western class Tooth produces American Avocado Tree oil 35g, and Britain produces hazelnut oil 15g, and Philippine produces Oleum Cocois 18g, and Malaysia produces whitish honey wax 4g.
Above-mentioned oils and fats is added in glass drying oven and mixes, and be placed in 55 DEG C of waters bath with thermostatic control, stir, weigh Top grade pure cerium hydroxide sodium is the 14% of oils and fats gross weight, weigh that deionized water is oils and fats gross weight 35%.With deionized water dissolved hydrogen oxygen It is cooled to 30 DEG C after changing sodium, then sodium hydroxide solution is slowly added in glyceride stock, make it abundant in 55 DEG C of water-baths Stirring reaction 30min, adding fresh aloe juice liquid afterwards is the 12% of oils and fats gross weight, continues stirring 10min, finally adds rhodamine toner Oil is the 0.5% of oils and fats gross weight, and stirring can draw substantially " 8 " word and stop to soap lye surface, above-mentioned soap lye enters mold forming, places 2 The demoulding after it, is placed in left at room temperature 7-10 days, and with pH detection paper handmade soap pH value, pH value can use at 7.5-8.5.
Embodiment 4
Weigh Vegetable oil lipoprotein raw material (solid grease prior in microwave oven melt): plant white oil 25g, praeparata cacao fat 12g, western class Tooth produces American Avocado Tree oil 28g, and Britain produces hazelnut oil 13g, and Philippine produces Oleum Cocois 23g, and Malaysia produces whitish honey wax 5g.
Above-mentioned oils and fats is added in glass drying oven and mixes, and be placed in 53 DEG C of waters bath with thermostatic control, stir;Weigh Top grade pure cerium hydroxide sodium is the 13% of oils and fats gross weight, weigh that deionized water is oils and fats gross weight 37%.With deionized water dissolved hydrogen oxygen It is cooled to 30 DEG C after changing sodium, then sodium hydroxide solution is slowly added in glyceride stock, make it abundant in 53 DEG C of water-baths Stirring reaction 25min, adding fresh aloe juice liquid afterwards is the 11% of oils and fats gross weight, continues stirring 10min, finally adds rhodamine toner Oil is the 0.8% of oils and fats gross weight, and stirring can draw substantially " 8 " word and stop to soap lye surface, above-mentioned soap lye enters mold forming, places 2 The demoulding after it, is placed in left at room temperature 7-10 days, and with pH detection paper handmade soap pH value, pH value can use at 7.5-8.5.
Embodiment 5
Weigh Vegetable oil lipoprotein raw material (solid grease prior in microwave oven melt): plant white oil 17g, praeparata cacao fat 10g, western class Tooth produces American Avocado Tree oil 22g, and Britain produces hazelnut oil 20g, and Philippine produces Oleum Cocois 25g, and Malaysia produces whitish honey wax 7g.
Above-mentioned oils and fats is added in glass drying oven and mixes, and be placed in 53 DEG C of waters bath with thermostatic control, stir, weigh Top grade pure cerium hydroxide sodium is the 15% of oils and fats gross weight, weigh that deionized water is oils and fats gross weight 38%.
It is cooled to 30 DEG C with after deionized water dissolved hydrogen sodium oxide, then sodium hydroxide solution is slowly added into oils and fats former In material, allowing it be sufficiently stirred for reacting 25min in 53 DEG C of water-baths, adding fresh aloe juice liquid afterwards is the 11.5% of oils and fats gross weight, continues Continuous stirring 10min, finally adding Flos Rosae Rugosae quintessence oil is the 0.9% of oils and fats gross weight, and stirring can draw substantially " 8 " word to soap lye surface and stop Only, above-mentioned soap lye is entered mold forming, the demoulding after placing 2 days, it is placed in left at room temperature 7-10 days, with pH detection paper handmade soap pH Value, pH value can use at 7.5-8.5.
Product of the present invention each volume of production at least 500g, each container at most 3000g during batch making, comparison test: by Table 1 Data Comparison show that product of the present invention meets and meets country's QB/T 2485-2008 II type all technical through detection It is qualified products.Using safe and non-stimulating, life-time service can improve sensitivity, be dried skin quality, and balance skin fat secretion moistens and protects Wet, whitening.
Being contrasted by experimental data, the present invention has 5 advantages: 1. total working substance content is more than commercially available two types fancy soap, Prove that this product cleaning force is strong;2. moisture and volatile matter are less than commercially available two types fancy soap, it was demonstrated that this product maintains good Aesthetic appearance and product hardness, the degree of balance of quality;3. total free alkali and free caustic alkali index are low, it was demonstrated that this product safety is not Can corrode and stimulate skin, manufacturing process is rigorous simultaneously, and 4. chloride is less than commercially available two types fancy soap, it was demonstrated that product of the present invention Manufacturing process, without saltouing, can guarantee that it contains 20%-30% glycerol and is of value to skin moisture-keeping and moistens, will not make pachylosis; 5. total phosphorus pentoxide index is low, it was demonstrated that product of the present invention is the most phosphorous.
Table 1
QB/T 2485-2008 fancy soap (II type) project Index Product measuring index of the present invention Commercially available soap base soap measuring index Commercially available fancy soap measuring index
Total working substance content/% 53 82 68 78
Moisture and volatile matter/% 30 18 22 20
Total free alkali (in terms of NaOH)/% 0.30 0.16 Do not detect Do not detect
Free caustic alkali (in terms of NaOH)/% 0.10 0.01 Do not detect Do not detect
Chloride (in terms of NaCl)/% 1.0 0.01 0.2 0.1
Total phosphorus pentoxide/% 1.1 0.04 0.1 Do not detect

Claims (8)

1. a Chinese aloe rose quintessence oil handmade soap, it is characterised in that it includes following raw materials according: Vegetable oil lipoprotein, sodium hydroxide, Flos Rosae Rugosae Quintessence oil, aloe juice, the consumption of sodium hydroxide be above-mentioned oils and fats gross weight be the 12%-15% of above-mentioned oils and fats gross weight, Flos Rosae Rugosae quintessence oil Consumption be above-mentioned oils and fats gross weight be the 0.5%-1.0% of oils and fats gross weight, the consumption of aloe juice is that above-mentioned oils and fats gross weight is The 10%-12% of oils and fats gross weight;Described Vegetable oil lipoprotein is made up of the raw material of following weight portion: plant white oil 15%-25 part, refined can Can 10 parts-20 parts of fat, American Avocado Tree oil 25 parts-35 parts, hazelnut oil 10 parts-20 parts, Oleum Cocois 15 parts-25 parts, 3 parts-7 parts of whitish honey wax.
Chinese aloe rose quintessence oil handmade soap the most according to claim 1, it is characterised in that: described Vegetable oil lipoprotein is by following weight The raw material composition of part: plant white oil 20 parts, 17 parts of praeparata cacao fat, American Avocado Tree oil 30 parts, hazelnut oil 10 parts, Oleum Cocois 20 parts, in vain Apis cerana Fabricius 3 parts.
3. the manufacture method of the Chinese aloe rose quintessence oil handmade soap described in claim 1, it is characterised in that it comprises the steps:
A, first the Vegetable oil lipoprotein oils and fats of solid is melted, mixing, be positioned over 50 DEG C of-55 DEG C of stirred in water bath uniform;
B, preparation sodium hydroxide solution: weigh sodium hydroxide, and dissolved with deionized water,
C, the above-mentioned sodium hydroxide solution prepared is poured in the oils and fats of mix homogeneously, and keep being sufficiently stirred for;
D, the mixed liquor of step C is reacted 50 DEG C of-55 DEG C of stirred in water bath, be subsequently added into aloe juice and continue stirring, finally Add Flos Rosae Rugosae quintessence oil, continue stirring;
E into, above-mentioned soap lye is poured die for molding, the demoulding, stand, obtain product.
The manufacture method of Chinese aloe rose quintessence oil handmade soap the most according to claim 3, it is characterised in that: step B is prepared Sodium hydroxide solution be cooled to 30 DEG C-35 DEG C uses.
5. according to the manufacture method of the Chinese aloe rose quintessence oil handmade soap described in claim 3 or 4, it is characterised in that: in step B Ionized water consumption is the 33%-38% of above-mentioned oils and fats gross weight.
The manufacture method of Chinese aloe rose quintessence oil handmade soap the most according to claim 5, it is characterised in that: step D mixes It is 20-30min that liquid stirs the response time in a water bath.
The manufacture method of Chinese aloe rose quintessence oil handmade soap the most according to claim 6, it is characterised in that: step D mixes Liquid mixing time after adding fresh aloe juice liquid is 8-10min.
The manufacture method of Chinese aloe rose quintessence oil handmade soap the most according to claim 7, it is characterised in that: quiet under in step E The time of putting is 7-10 days, and the pH value of handmade soap is 7.5-8.5.
CN201610400638.3A 2016-06-08 2016-06-08 Aloe-rose essential oil handmade soap and making method thereof Pending CN106010832A (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106520416A (en) * 2016-10-28 2017-03-22 楚雄乌蛮渡农垦有限公司 Elsholtzia rugulosa hemsl essential oil soap and preparing method thereof
CN106883957A (en) * 2017-04-17 2017-06-23 帝善圆农业科技(苏州)有限公司 A kind of soap and preparation method thereof
CN106906083A (en) * 2017-02-21 2017-06-30 安徽安龙基因医学检验所有限公司 A kind of natural no stimulation aloe refined jasmine oil handmade soap and preparation method thereof
CN107523445A (en) * 2017-09-27 2017-12-29 中国林业科学研究院林产化学工业研究所 A kind of preparation method of cape jasmine humidity-preserving type craft cold process soap
CN107629900A (en) * 2017-09-27 2018-01-26 中国林业科学研究院林产化学工业研究所 A kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap
CN107760497A (en) * 2017-09-27 2018-03-06 中国林业科学研究院林产化学工业研究所 A kind of preparation method of the crease-resistant type craft cold process soap of cape jasmine
CN108456597A (en) * 2017-10-24 2018-08-28 浙江康鸿生物科技有限公司 A kind of preparation method of cape jasmine antiphlogistic craft cold process soap
CN109022180A (en) * 2017-10-24 2018-12-18 浙江康鸿生物科技有限公司 A kind of preparation method of cape jasmine skin-protection type craft cold process soap
CN109749899A (en) * 2017-11-06 2019-05-14 广西民族大学 A kind of face cleaning handmade soap formula and preparation method thereof
CN115737485A (en) * 2022-11-23 2023-03-07 深圳市洁依源科技有限公司 Dry skin foam bath washing block and preparation method thereof

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CN104388213A (en) * 2014-11-14 2015-03-04 浙江久晟茶业发展有限公司 Handmade camellia oil soap and preparation method thereof
CN105062726A (en) * 2015-08-05 2015-11-18 广西大学 Medicated soap for conditioning skin and weakening melanin
CN105400617A (en) * 2015-12-17 2016-03-16 宁波工程学院 Preparation method of cold-formed soap
FR3035118A1 (en) * 2015-04-16 2016-10-21 Fabrice Balland PROCESS FOR PRODUCING DERMATOLOGICAL SOAP DERMATOLOGICAL SOAP

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CN104388213A (en) * 2014-11-14 2015-03-04 浙江久晟茶业发展有限公司 Handmade camellia oil soap and preparation method thereof
FR3035118A1 (en) * 2015-04-16 2016-10-21 Fabrice Balland PROCESS FOR PRODUCING DERMATOLOGICAL SOAP DERMATOLOGICAL SOAP
CN105062726A (en) * 2015-08-05 2015-11-18 广西大学 Medicated soap for conditioning skin and weakening melanin
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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106520416A (en) * 2016-10-28 2017-03-22 楚雄乌蛮渡农垦有限公司 Elsholtzia rugulosa hemsl essential oil soap and preparing method thereof
CN106906083A (en) * 2017-02-21 2017-06-30 安徽安龙基因医学检验所有限公司 A kind of natural no stimulation aloe refined jasmine oil handmade soap and preparation method thereof
CN106883957A (en) * 2017-04-17 2017-06-23 帝善圆农业科技(苏州)有限公司 A kind of soap and preparation method thereof
CN107523445A (en) * 2017-09-27 2017-12-29 中国林业科学研究院林产化学工业研究所 A kind of preparation method of cape jasmine humidity-preserving type craft cold process soap
CN107629900A (en) * 2017-09-27 2018-01-26 中国林业科学研究院林产化学工业研究所 A kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap
CN107760497A (en) * 2017-09-27 2018-03-06 中国林业科学研究院林产化学工业研究所 A kind of preparation method of the crease-resistant type craft cold process soap of cape jasmine
CN108456597A (en) * 2017-10-24 2018-08-28 浙江康鸿生物科技有限公司 A kind of preparation method of cape jasmine antiphlogistic craft cold process soap
CN109022180A (en) * 2017-10-24 2018-12-18 浙江康鸿生物科技有限公司 A kind of preparation method of cape jasmine skin-protection type craft cold process soap
CN109749899A (en) * 2017-11-06 2019-05-14 广西民族大学 A kind of face cleaning handmade soap formula and preparation method thereof
CN115737485A (en) * 2022-11-23 2023-03-07 深圳市洁依源科技有限公司 Dry skin foam bath washing block and preparation method thereof

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Application publication date: 20161012