CN106381242A - Flaxseed oil handmade soap and preparation method thereof - Google Patents

Flaxseed oil handmade soap and preparation method thereof Download PDF

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Publication number
CN106381242A
CN106381242A CN201610757718.4A CN201610757718A CN106381242A CN 106381242 A CN106381242 A CN 106381242A CN 201610757718 A CN201610757718 A CN 201610757718A CN 106381242 A CN106381242 A CN 106381242A
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oil
handmade soap
semen lini
lini oil
soap
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唐振兴
梁洁玉
施明珠
卞继州
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Cosmetics Co Ltd Hangzhou Su Yan
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Cosmetics Co Ltd Hangzhou Su Yan
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Priority to CN201610757718.4A priority Critical patent/CN106381242A/en
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/14—Shaping
    • C11D13/16—Shaping in moulds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38636—Preparations containing enzymes, e.g. protease or amylase containing enzymes other than protease, amylase, lipase, cellulase, oxidase or reductase
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/005—Synthetic soaps
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/26—Organic compounds, e.g. vitamins containing oxygen
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/26—Organic compounds, e.g. vitamins containing oxygen
    • C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/38—Products in which the composition is not well defined
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/40—Proteins

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
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Abstract

The invention discloses flaxseed oil handmade soap and a preparation method thereof. The flaxseed oil handmade soap is made from the following raw materials, according to a mass ratio, 3.0-15% of flaxseed oil, 20-60% of palm oil, 1.0-20% of olive oil, 5.0-20% of sodium hydroxide, 1.0-20% of glycerin, 0.10-3.0% of a moisturizing component, 0.10-3.0% of an itching-relieving component, and 0.10-3.0% of an anti-oxidant, with the balance being water. The obtained flaxseed oil handmade soap can moisturize the skin and relieve itching, and alpha-linolenic acid in the flaxseed oil can permeate into the skin very easily to develop the function of restoring and reinforcing the skin which is a natural barrier. The flaxseed oil handmade soap is suitable for different groups of people, and particularly suitable for improving or treating xerosis cutis and pruritus which the old people suffer from. The flaxseed oil handmade soap is convenient to use, is durable, and can be used for a long time. The preparation method is simple and mature, and is suitable for industrial production.

Description

A kind of Semen Lini oil handmade soap and preparation method thereof
(1) technical field
The invention belongs to cosmetic technical field and in particular to a kind of Semen Lini oil handmade soap with the antipruritic function of moisturizing and Its preparation method.
(2) background technology
Handmade soap is one of emerging clean skin class product developed in recent years, is deeply liked by people because of its distinctive advantage Love.Traditional fancy soap has preferable clean skin effect, but moistening effect is poor, washes that rear skin is easily tight dry and astringent, and life-time service is on the contrary The irritant reaction of skin instinct can be caused, secrete a large amount of oils and fatss, make skin pore thick, hydropenia is coarse, therefore less and less People uses fancy soap face cleaning.Handmade soap compensate for the shortcoming of fancy soap to a great extent, not only can face cleaning, can also be used to unload Adornment, takes a shower.The natural vegetable oil of the material choice of handmade soap, action temperature and little to skin irritation, and also shape color is diversified, Be translucent shape, and fragrance is suitably it is easier to causing people's concern and using.Handmade soap adds corresponding according to its different function Natural extract or active component, effect variation, make consumer have extensive selection space.
In Semen Lini oil, unsaturated fatty acid content is high, and alpha-linolenic acid and linoleic acid easily penetrate into skin surface to depth Layer, to supplement the lipid nutrient needed for skin, plays and repairs and strengthen Skin Cell natural cover for defense function, reduces percutaneous moisture and damages Lose, ventilative water-retaining film can also be formed in skin surface simultaneously, weaken the moisture loss of deep skin.Alpha-linolenic acid can also delay Solution skin aging, adjusts the cornification processes of human body skin, strengthens skin firmness and consistency comprehensively.Semen Lini oil is as one kind Rare is the crude vegetal of alpha-linolenic acid rich in ω -3, prurituss, allergy coarse to some skin problems such as xerosis cutiss, The repairing and treating of eczema, acne etc. has obvious effect, also can play antiinflammatory action, makes impaired, aged cells non-stimulatedly Peel off, can effectively wrinkle reduction, to defying age, treat the skin problem such as adolescent acne.
(3) content of the invention
It is an object of the invention to provide a kind of Semen Lini oil handmade soap and preparation method thereof.The Semen Lini oil of present invention exploitation Handmade soap using natural vegetable oil as raw material, alpha-linolenic acid easily skin permeation in one side Semen Lini oil, play repair and Strengthen skin natural cover for defense function, reduce moisture loss, adjust skin keratin process, in another aspect handmade soap, add moisturizing And antipruritic active ingredients, thoroughly cleaning skin can also can not only effectively repair or treat xerosis cutiss, prurituss, allergy etc. and ask Topic, this product is suitable for different crowd, is especially suitable for improving or treating old people's xerosis cutiss prurituss problem, easy to use, Durable.
The technical solution used in the present invention is：
The present invention provides a kind of Semen Lini oil handmade soap, and described Semen Lini oil handmade soap is by the raw material system of following quality proportioning Become：Semen Lini oil 3.0～15%, Petiolus Trachycarpi oil 20～60%, olive oil 1.0～20%, sodium hydroxide 5.0～20%, glycerol 1.0 ～20%, moisturizing ingredient 0.10～3.0%, antipruritic composition 0.10～3.0%, antioxidant 0.10～3.0%, water surplus.Institute State moisturizing ingredient be Herba Lysimachiae foenum-graeci quintessence oil, jasmine essential oil, hyaluronic acid, hyaluronic acid, collagen protein, aminoacid, Sargassum elite and The mixing of one or more in Aloe extract, in the acid of preferably clear matter, hyaluronic acid, collagen protein and Aloe extract a kind of or Several mixing；Described antipruritic composition is a kind of in Folium Artemisiae Argyi leaf, Sucus Zingberis, Flos Lonicerae, propolis, essential oil of traditional Chinese medicine, allantoin and carbamide Or several mixing, the preferably mixing of one or more in propolis, allantoin and carbamide；Described antioxidant is Vitamin E, dimension The mixing of one or more in raw element C and superoxide dismutase.
Further, described antioxidant is vitamin C and Vitamin E with mass ratio 0.5～1:1 mixing.
Further, described antipruritic composition is propolis, allantoin and carbamide with mass ratio 0.5～2:0.5～2:1 mixing.
Further, described Semen Lini oil handmade soap is made up of the raw material of following quality proportioning：Semen Lini oil 5.0～10%, Petiolus Trachycarpi oil 25～50%, olive oil 3.0～15%, sodium hydroxide 6.0～18%, glycerol 3.0～15%, moisturizing ingredient 0.50～ 2.5%th, antipruritic composition 0.50～2.5%, antioxidant 0.20～2.0%, water surplus.
Further, described Semen Lini oil handmade soap is made up of the raw material of following quality proportioning：Semen Lini oil 6.0～ 8.0%th, Petiolus Trachycarpi oil 30～40%, olive oil 8.0～12%, sodium hydroxide 8.0～15%, glycerol 7.0～13%, moisturizing ingredient 1.0～2.0%, antipruritic composition 1.0～2.0%, antioxidant 0.50～1.5%, water surplus.
Further, described Semen Lini oil handmade soap is made up of the raw material of following quality proportioning：Semen Lini oil 7.0%, palm fibre Palmitic acid oil 35%, olive oil 10%, sodium hydroxide 13%, glycerol 11%, hyaluronic acid 1.5%, antipruritic composition 1.6%, antioxidation Agent 0.9%, water 20%；Described antipruritic composition is propolis, allantoin and carbamide with mass ratio 1.4:0.8:1 mixing；Described anti- Oxidant is for vitamin C and Vitamin E with mass ratio 0.8:1 mixing.
The present invention also provides a kind of preparation method of described Semen Lini oil handmade soap, and methods described is：
(1) press formula ratio, by Semen Lini oil, olive oil, Petiolus Trachycarpi oil mixing, heating in water bath, to 30～40 DEG C, obtains mixing Oil, constant temperature is stand-by；
(2) press formula ratio, sodium hydroxide distillation water dissolution be heated to 30～40 DEG C, obtain sodium hydrate aqueous solution, Constant temperature is stand-by；
(3) sodium hydrate aqueous solution of step (2) is added in the miscella in step (1), stirs saponification, until soap Liquid thickens, and obtains mixed liquor；
(4) press formula ratio, glycerol, moisturizing ingredient, antipruritic composition and antioxidant are added to the mixed liquor of step (3) In, it is uniformly mixed, obtain mixture；
(5) mixture of step (4) is poured into molding in mould (preferably oval, packing less silica gel mould), put into The couveuse that 30～40 DEG C of temperature, after soap lye solidifies completely, the demoulding；
(6) handmade soap after the demoulding is placed 4～8 weeks under normal temperature drying environment and treat its full maturity, that is, obtain Caulis et Folium Lini Seed oil handmade soap.
Semen Lini oil of the present invention is the seed flax seed of flax family (Linaceae) plant Caulis et Folium Lini, squeezes through cold press or hot pressing and extracts Refined oily liquids.
Compared with prior art, the present invention has the advantages that：
The invention provides a kind of Semen Lini oil handmade soap and preparation method thereof, the Semen Lini oil handmade soap of gained has guarantor Wet and antipruritic function, alpha-linolenic acid easily skin permeation in Semen Lini oil simultaneously, play and repair and strengthen skin natural cover for defense work( Energy.This product is suitable for different crowd, is especially suitable for improving or treating old people's xerosis cutiss prurituss problem, easy to use, Durable.This Product Process is simple, technology maturation, suitable industrialized production.
(4) specific embodiment
With reference to specific embodiment, the present invention is described further, but protection scope of the present invention is not limited in This：
Semen Lini oil used by the embodiment of the present invention is the seed flax seed of flax family (Linaceae) plant Caulis et Folium Lini, squeezes through cold press or hot pressing The oily liquids of Hydrolysis kinetics.
Glycerol, molecular formula C3H8O3, it is purchased from Guangzhou Sheng Xin Chemical Industry Science Co., Ltd.
Carbamide, molecular formula CO (NH2)2, it is purchased from Guangzhou Sheng Xin Chemical Industry Science Co., Ltd.
Hyaluronic acid, molecular formula C28H44N2O23, it is purchased from Guangzhou Sheng Xin Chemical Industry Science Co., Ltd.
Allantoin, is purchased from Zhejiang Wu Mei bio tech ltd.
Hyaluronic acid, is purchased from Guangzhou Pin Ding Chemical Industry Science Co., Ltd.
Aloe extract, is purchased from Zhengzhou Zheng Ya chemical products company limited.
Collagen protein, is purchased from Jiangsu Fu Shengde biological engineering company limited.
Propolis, is purchased from Lantian County chin or cheek honeybee hall ecology Apiss garden company limited.
Embodiment 1
1st, proportioning raw materials：Semen Lini oil 6.0g, Petiolus Trachycarpi oil 40g, olive oil 10.0g, sodium hydroxide 10g, glycerol 8.0g, glass Uric acid 1.50g, propolis 0.40g, allantoin 0.40g, carbamide 0.40g, vitamin C 0.40g, Vitamin E 0.50g, water 22.4g.
2nd, Semen Lini oil handmade soap preparation：
(1) press formula ratio, by Semen Lini oil, olive oil, Petiolus Trachycarpi oil mixing, heating in water bath, to 30～40 DEG C, obtains mixing Oil, constant temperature is stand-by；
(2) press formula ratio, sodium hydroxide is distilled water dissolution with 22.4g, be heated to 30～40 DEG C, obtain sodium hydroxide water Solution, constant temperature is stand-by；
(3) sodium hydrate aqueous solution of step (2) is added in the miscella in step (1), stirs saponification, until soap Liquid thickens, and obtains mixed liquor；
(4) press formula ratio, glycerol, moisturizing ingredient, antipruritic composition and antioxidant are added to the mixed liquor of step (3) In, it is uniformly mixed, obtain mixture；
(5) mixture of step (4) is poured in oval, packing less silica gel mould, put into 30～40 DEG C of temperature Couveuse, after soap lye solidifies completely, the demoulding；
(6) handmade soap after the demoulding is placed 4～8 weeks under normal temperature drying environment and treat its full maturity, that is, obtain Caulis et Folium Lini Seed oil handmade soap.
The Semen Lini oil handmade soap being obtained by above-mentioned formula, different triers are 93 points of (standards of grading to its comprehensive grading Reference implementation example 6), in the shelf-life, oxidation stain phenomenon does not occur in two years.
Embodiment 2
1st, proportioning raw materials：Semen Lini oil 7.0g, Petiolus Trachycarpi oil 35g, olive oil 10g, sodium hydroxide 13g, glycerol 11g, transparent Matter acid 1.5g, propolis 0.70g, allantoin 0.40g, carbamide 0.50g, vitamin C 0.40g, Vitamin E 0.50g, water 20g.
2nd, Semen Lini oil handmade soap preparation：
(1) press formula ratio, by Semen Lini oil, olive oil, Petiolus Trachycarpi oil mixing, heating in water bath, to 30～40 DEG C, obtains mixing Oil, constant temperature is stand-by；
(2) press formula ratio, sodium hydroxide is distilled water dissolution with 20g, be heated to 30～40 DEG C, constant temperature is stand-by, obtain hydrogen Aqueous solution of sodium oxide；
(3) sodium hydrate aqueous solution of step (2) is added in the miscella in step (1), stirs saponification, until soap Liquid thickens, and obtains mixed liquor；
(4) press formula ratio, glycerol, moisturizing ingredient, antipruritic composition and antioxidant are added to the mixed liquor of step (3) In, it is uniformly mixed, obtain mixture；
(5) mixture of step (4) is poured in oval, packing less silica gel mould, put into 30～40 DEG C of temperature Couveuse, after soap lye solidifies completely, the demoulding；
(6) handmade soap after the demoulding is placed 4～8 weeks under normal temperature drying environment and treat its full maturity, that is, obtain Caulis et Folium Lini Seed oil handmade soap.
The Semen Lini oil handmade soap being obtained by above-mentioned formula, different triers are 98 points of (standards of grading to its comprehensive grading Reference implementation example 6), in the shelf-life, oxidation stain phenomenon does not occur in two years.
Embodiment 3
1st, proportioning raw materials：Semen Lini oil 8.0g, Petiolus Trachycarpi oil 38g, olive oil 9g, sodium hydroxide 12g, glycerol 10g, collagen egg White 1.0g, propolis 0.70g, allantoin 0.60g, carbamide 0.50g, vitamin C 0.40g, Vitamin E 0.50g, water 19.3g.
2nd, Semen Lini oil handmade soap preparation：
(1) press formula ratio, by Semen Lini oil, olive oil, Petiolus Trachycarpi oil mixing, heating in water bath, to 30～40 DEG C, obtains mixing Oil, constant temperature is stand-by；
(2) press formula ratio, sodium hydroxide is distilled water dissolution with 19.3g, be heated to 30～40 DEG C, constant temperature is stand-by, obtain Sodium hydrate aqueous solution；
(3) sodium hydrate aqueous solution of step (2) is added in the miscella in step (1), stirs saponification, until soap Liquid thickens, and obtains mixed liquor；
(4) press formula ratio, glycerol, moisturizing ingredient, antipruritic composition and antioxidant are added to the mixed liquor of step (3) In, it is uniformly mixed, obtain mixture；
(5) mixture of step (4) is poured in oval, packing less silica gel mould, put into 30～40 DEG C of temperature Couveuse, after soap lye solidifies completely, the demoulding；
(6) handmade soap after the demoulding is placed 4～8 weeks under normal temperature drying environment and treat its full maturity, that is, obtain Caulis et Folium Lini Seed oil handmade soap.
The Semen Lini oil handmade soap being obtained by above-mentioned formula, different triers are 94 points of (standards of grading to its comprehensive grading Reference implementation example 6), in the shelf-life, oxidation stain phenomenon does not occur in two years.
Embodiment 4
1st, proportioning raw materials：Semen Lini oil 11g, Petiolus Trachycarpi oil 35g, olive oil 12g, sodium hydroxide 10g, glycerol 10g, Aloe carry Take thing 1.2g, propolis 0.70g, allantoin 0.60g, carbamide 0.50g, vitamin C 0.50g, Vitamin E 0.50g, water 18g.
2nd, Semen Lini oil handmade soap preparation：
(1) press formula ratio, by Semen Lini oil, olive oil, Petiolus Trachycarpi oil mixing, heating in water bath, to 30～40 DEG C, obtains mixing Oil, constant temperature is stand-by；
(2) press formula ratio, sodium hydroxide is distilled water dissolution with 18g, be heated to 30～40 DEG C, obtain sodium hydroxide water-soluble Liquid, constant temperature is stand-by；
(3) sodium hydrate aqueous solution of step (2) is added in the miscella in step (1), stirs saponification, until soap Liquid thickens, and obtains mixed liquor；
(4) press formula ratio, glycerol, moisturizing ingredient, antipruritic composition and antioxidant are added to the mixed liquor of step (3) In, it is uniformly mixed, obtain mixture；
(5) mixture of step (4) is poured in oval, packing less silica gel mould, put into 30～40 DEG C of temperature Couveuse, after soap lye solidifies completely, the demoulding；
(6) handmade soap after the demoulding is placed 4～8 weeks under normal temperature drying environment and treat its full maturity, that is, obtain Caulis et Folium Lini Seed oil handmade soap.
The Semen Lini oil handmade soap being obtained by above-mentioned formula, different triers are 90 points of (standards of grading to its comprehensive grading Reference implementation example 6), in the shelf-life, oxidation stain phenomenon does not occur in two years.
Embodiment 5
1st, proportioning raw materials：Semen Lini oil 14g, Petiolus Trachycarpi oil 36g, olive oil 10g, sodium hydroxide 10g, glycerol 8g, hyalomitome Sour 1.2g, propolis 0.80g, allantoin 0.70g, carbamide 0.50g, vitamin antagonist C 0.40g, Vitamin E 0.40g, water 18g.
2nd, Semen Lini oil handmade soap preparation：
(1) press formula ratio, by Semen Lini oil, olive oil, Petiolus Trachycarpi oil mixing, heating in water bath, to 30～40 DEG C, obtains mixing Oil, constant temperature is stand-by；
(2) press formula ratio, sodium hydroxide is distilled water dissolution with 18g, be heated to 30～40 DEG C, constant temperature is stand-by, obtain hydrogen Aqueous solution of sodium oxide；
(3) sodium hydrate aqueous solution of step (2) is added in the miscella in step (1), stirs saponification, until soap Liquid thickens, and obtains mixed liquor；
(4) press formula ratio, glycerol, moisturizing ingredient, antipruritic composition and antioxidant are added to the mixed liquor of step (3) In, it is uniformly mixed, obtain mixture；
(5) mixture of step (4) is poured in oval, packing less silica gel mould, put into 30～40 DEG C of temperature Couveuse, after soap lye solidifies completely, the demoulding；
(6) handmade soap after the demoulding is placed 4～8 weeks under normal temperature drying environment and treat its full maturity, that is, obtain Caulis et Folium Lini Seed oil handmade soap.
The Semen Lini oil handmade soap being obtained by above-mentioned formula, different triers are 80 points of (standards of grading to its comprehensive grading Reference implementation example 6), when handmade soap room temperature deposits ten months, handmade soap starts to occur some and occurs because Semen Lini oil aoxidizes Yellow fleck, as time went on, spot extension is much.
Embodiment 6
Product of the present invention selects teenager, young people and each 12 people of old people to be tried out respectively, is substantially carried out face Cleaning, sooner or later respectively once, the cycle on probation is 1 year, tries out and according to the standards of grading of table 1, corresponding formulation product is carried out after finishing Marking, teenager and young people tend to Semen Lini oil handmade soap cleaning effect and moistening effect are evaluated, old people Tend to moistening effect and antipruritic effect are evaluated, then statistical analysiss draw the comprehensive score of Semen Lini oil handmade soap.
Table 1 Semen Lini oil handmade soap sense organ and functional effect standards of grading
Because alpha-linolenic acid is easily affected by environment, for investigating product with stable quality, respectively with embodiment 2 and embodiment 5 formulation products, as object of study, analyze Semen Lini oil handmade soap organoleptic quality situation of change during room temperature storage, result Find that embodiment 2 formulation product the ANOMALOUS VARIATIONS such as abnormal smells from the patient, color and quality within the shelf-life depositing 2 years, and sub- When depositing ten months, product surface starts fleck yellow to the higher embodiment of hemp seed oil content 5 formulation product, with Time lengthening, speckle becomes larger, less, when 12 months, yellow spotting accounts for the 1/3 of handmade soap surface area, sternly for abnormal smells from the patient change Ghost image rings product appearance, and quality starts deliquescing simultaneously, and handmade soap can not use substantially.

Claims (7)

1. a kind of Semen Lini oil handmade soap it is characterised in that described Semen Lini oil handmade soap by following quality proportioning raw material system Become：Semen Lini oil 3.0～15%, Petiolus Trachycarpi oil 20～60%, olive oil 1.0～20%, sodium hydroxide 5.0～20%, glycerol 1.0 ～20%, moisturizing ingredient 0.10～3.0%, antipruritic composition 0.10～3.0%, antioxidant 0.10～3.0%, water surplus；Institute State moisturizing ingredient be Herba Lysimachiae foenum-graeci quintessence oil, jasmine essential oil, hyaluronic acid, hyaluronic acid, collagen protein, aminoacid, Sargassum elite and The mixing of one or more in Aloe extract；Described antipruritic composition be Folium Artemisiae Argyi leaf, Sucus Zingberis, Flos Lonicerae, propolis, essential oil of traditional Chinese medicine, The mixing of one or more in allantoin and carbamide；Described antioxidant is Vitamin E, vitamin C and superoxide dismutase In the mixing of one or more.
2. Semen Lini oil handmade soap as claimed in claim 1 is it is characterised in that described antioxidant is vitamin C and Vitamin E With mass ratio 0.5～1:1 mixing.
3. Semen Lini oil handmade soap as claimed in claim 1 is it is characterised in that described antipruritic composition is propolis, allantoin and carbamide With mass ratio 0.5～2:0.5～2:1 mixing.
4. Semen Lini oil handmade soap as claimed in claim 1 is it is characterised in that described Semen Lini oil handmade soap is joined by following quality The raw material of ratio is made：Semen Lini oil 5.0～10%, Petiolus Trachycarpi oil 25～50%, olive oil 3.0～15%, sodium hydroxide 6.0～ 18%th, glycerol 3.0～15%, moisturizing ingredient 0.50～2.5%, antipruritic composition 0.50～2.5%, antioxidant 0.20～ 2.0%th, water surplus.
5. Semen Lini oil handmade soap as claimed in claim 1 is it is characterised in that described Semen Lini oil handmade soap is joined by following quality The raw material of ratio is made：Semen Lini oil 6.0～8.0%, Petiolus Trachycarpi oil 30～40%, olive oil 8.0～12%, sodium hydroxide 8.0～ 15%th, glycerol 7.0～13%, moisturizing ingredient 1.0～2.0%, antipruritic composition 1.0～2.0%, antioxidant 0.50～1.5%, Water surplus.
6. Semen Lini oil handmade soap as claimed in claim 1 is it is characterised in that described Semen Lini oil handmade soap is joined by following quality The raw material of ratio is made：Semen Lini oil 7.0%, Petiolus Trachycarpi oil 35%, olive oil 10%, sodium hydroxide 13%, glycerol 11%, hyalomitome Acid 1.5%, antipruritic composition 1.6%, antioxidant 0.9%, water 20%；Described antipruritic composition is propolis, allantoin and carbamide with Mass ratio 1.4:0.8:1 mixing；Described antioxidant is for vitamin C and Vitamin E with mass ratio 0.8:1 mixing.
7. a kind of preparation method of Semen Lini oil handmade soap described in claim 1 is it is characterised in that methods described is：
(1) press formula ratio, by Semen Lini oil, olive oil, Petiolus Trachycarpi oil mixing, heating in water bath, to 30～40 DEG C, obtains miscella, permanent Temperature is stand-by；
(2) press formula ratio, sodium hydroxide distillation water dissolution is heated to 30～40 DEG C, makes sodium hydrate aqueous solution, constant temperature Stand-by；
(3) sodium hydrate aqueous solution of step (2) is added in the miscella in step (1), stirs saponification, until soap lye becomes Thick, obtain mixed liquor；
(4) press formula ratio, glycerol, moisturizing ingredient, antipruritic composition and antioxidant are added in the mixed liquor of step (3), stir Mix mix homogeneously, obtain mixture；
(5) mixture of step (4) is poured into die for molding, put into the couveuse of 30～40 DEG C of temperature, treat that soap lye is completely solidifying Gu after, the demoulding；
(6) handmade soap after the demoulding is placed 4～8 weeks under normal temperature drying environment and treat its full maturity, that is, obtain Semen Lini oil Handmade soap.
CN201610757718.4A 2016-08-29 2016-08-29 Flaxseed oil handmade soap and preparation method thereof Pending CN106381242A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111057626A (en) * 2018-10-16 2020-04-24 李倩 Handmade perfumed soap

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102002452A (en) * 2010-11-23 2011-04-06 陈巍 Method for preparing beautifying perfumed soap
CN103571657A (en) * 2013-10-24 2014-02-12 朱建华 Natural soap for removing poxes as well as preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102002452A (en) * 2010-11-23 2011-04-06 陈巍 Method for preparing beautifying perfumed soap
CN103571657A (en) * 2013-10-24 2014-02-12 朱建华 Natural soap for removing poxes as well as preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111057626A (en) * 2018-10-16 2020-04-24 李倩 Handmade perfumed soap

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Application publication date: 20170208