CN110408486A - A kind of Cortex Eucommiae soap and preparation method thereof - Google Patents
A kind of Cortex Eucommiae soap and preparation method thereof Download PDFInfo
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- CN110408486A CN110408486A CN201810387144.5A CN201810387144A CN110408486A CN 110408486 A CN110408486 A CN 110408486A CN 201810387144 A CN201810387144 A CN 201810387144A CN 110408486 A CN110408486 A CN 110408486A
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- cortex eucommiae
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- fine powder
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/444—Dyes; Pigments
Abstract
The present invention relates to a kind of Cortex Eucommiae soap in daily life chemicals field and preparation method thereof；The Cortex Eucommiae soap, the following components comprising parts by weight meter: 100 parts of vegetable fat, 4~16 parts of Cortex Eucommiae fine powder, 4~16 parts of highly basic, 12~28 parts of water, 4~16 parts of milk, 0~2 part of essence, 0~2 part of colouring matter；Cortex Eucommiae fine powder has the function of that Chinese medicine reconciles and nourishes that taste is pure and fresh, tranquilizing the mind QI invigorating, has effects that antiallergy for pruitus and alleviates；Containing fat, protein, minerals, vitamin etc. in milk, it is easy to be absorbed by the skin, there is whitening and moistening skin；Cortex Eucommiae soap provided by the invention not only can be used for washing spot, but also can be used for moistening skin-care, and it is fine and smooth mild to use feeling, product does not have the addition of extra chemicals, human skin is not stimulated, it is not easy to allergy occur, can satisfy the use demand of any type crowd substantially.
Description
Technical field
The present invention relates to daily life chemicals fields, furtherly, are related to a kind of Cortex Eucommiae soap and preparation method thereof.
Background technique
The production of soap product has a long history, and about with regard to useful grease and contains potassium carbonate at B.C. 2500
Plant ass produce potash soap, and the record of wool is washed with this soap.Since 19th century, due to the quick hair of efficient alkaline method
Exhibition, makes the production of soap enter the industrialized stage.Nowadays with the improvement of living standards, people are for material life
Health requirements are also increasingly stringenter, and exploitation has safety, stability, cost performance height, the apparent soap of effect, and it is very good to have
Development prospect.
Commodity soap main component on the market is odium stearate at present, is to be generated by highly basic and fat saponification reaction, separately
The outer soap that various chemical addition agents can be added, various specific functions are made.Sulphur component is added such as in soap base, sulphur medicine is made
Soap, or existing color dulcet perfumed soap again is made in addition fragrance and dyestuff in soap base.But the additive being added is generally right
Skin has side effect injury, can be dried using rear skin, and is easy allergy.Cortex Eucommiae is that the distinctive tradition of China nourishes rare medicine
Material has the various functions such as nourishing liver and kidney, strengthening the bones and muscles, blood pressure lowering, miscarriage prevention；The Chinese patent of Publication No. CN106350312A discloses
A kind of Chinese medicine crease-resistant handmade soap, but it uses chemical reagent to carry out the eucommia ulmoides extracts of soak extraction, it can generation
It learns and extracts reagent residual, being irritating to the skin property in use.
Summary of the invention
In order to solve the above-mentioned problems in the prior art, the present invention proposes a kind of Cortex Eucommiae soap, more particularly to Du
Secondary soap and preparation method thereof.Soap is the sodium salt of higher fatty acids, and molecular structure is made of two parts, and one end is hydrophilic
Polarity carboxyl, the other end are the nonpolar hydroxyls of oleophylic, can be aligned when soap is dissolved in water, due to this higher aliphatic
The presence of silicate layer weakens the intermolecular active force of water surface, plays the role of surfactant, then by mechanically rubbing with the hands
Washing away for water is rubbed up to achieve the purpose that wash dirt.The present invention has perfumed soap and is calmed the nerves by addition natural materials Cortex Eucommiae fine powder
The pure and fresh effect of QI invigorating, taste, is used for a long time that safe and efficient skin is non-stimulated, allergy, target user be not in extensive range.The present invention
The Cortex Eucommiae fine powder used be the direct ball-milling treatment of folium cortex eucommiae after, the toxic action of chemical extraction reagent is reduced in preparation,
More health environment-friendly；The addition of natural constituents milk can effectively improve skin problem, and it is mild fine and smooth to use feeling；To reach
To the double effects for the treatment of and skin nutrition, is not dried using rear skin, do not stimulate skin.
One of the object of the invention is to provide a kind of Cortex Eucommiae soap, may include the following components of parts by weight meter:
100 parts of vegetable fat；
4~16 parts of Cortex Eucommiae fine powder, preferably 8~12 parts；
4~16 parts of highly basic, preferably 8~12 parts；
12~28 parts of water, preferably 18~22 parts；
4~16 parts of milk, preferably 8~12 parts；
0~2 part of essence, preferably 0.2~2 part, more preferable 0.8~1.2 part；
0~2 part of colouring matter, preferably 0.2~2 part, more preferable 0.8~1.2 part.
Most preferably, the Cortex Eucommiae soap includes following components:
100 parts of vegetable fat；
8~12 parts of Cortex Eucommiae fine powder；
8~12 parts of highly basic；
18~22 parts of water；
8~12 parts of milk；
0.8~1.2 part of essence；
0.8~1.2 part of colouring matter.
In the above component, vegetable fat and highly basic are to generate the soap with washing decontamination in order to which saponification occurs
Base；Water plays the role of mitigating saponification, prevents reaction excessively acutely without can control；Cortex Eucommiae fine powder is crucial additive
Matter, the special role for making the finished product soap being eventually fabricated that there is tranquilizing the mind QI invigorating, moisturizing to be depressured；In milk containing fat, protein,
Minerals, vitamin etc. are easy to be absorbed by the skin, and play the role of whitening and moistening skin, smooth away wrinkles；Essence makes soap scent more preferably；
Colouring matter keeps soapy appearance moulding more prominent.
The vegetable fat can be selected from including rapeseed oil and olive oil.The cost of rapeseed oil is not high but hardness is low, if singly making
With rapeseed oil then soap can not stable molding, if singly too long cooling time using soap lye if the higher olive oil of hardness.Specifically may be used
To be mixed with finished product by rapeseed oil and olive oil weight ratio (1.5~6): 1, preferably (3.5~4.5): 1, more preferable 4:1.
The Cortex Eucommiae fine powder is to be ground by dry Cortex Eucommiae raw material (can be made by fresh leaf dryness in the sun) by ball mill
Mill, the screen to filtrate and be made.The Cortex Eucommiae raw material is at least one of Folium Eucommiae, eucommia bark, preferably Folium Eucommiae.Institute
Stating drum's speed of rotation is 300~500r/min, can be ground 15~25 minutes；It is miniature comprehensive that Fu Kasi can be selected in ball mill model
Planetary type ball-milling instrument F-P400E；Sieve mesh number is 100 mesh.More safety and sanitation are processed with ball milling physical method, are not contacted toxic
Chemical reagent, Cortex Eucommiae fine powder uniform particle sizes, appearance are completely fine and smooth.
The highly basic is in the pure rank sodium hydroxide of use for laboratory chemistry, potassium hydroxide, barium hydroxide, calcium hydroxide
At least one, preferred sodium hydroxide herein, because it is common chemical products, raw material is easily obtained.
Water is not done overcritical in the soap, one of preferable natural water, pure water, distilled water, tap water or
A variety of mixing；The milk is selected from least one of milk, goat milk, preferred milk, in milk containing there are many nutriments such as
Vitamin, amino acid etc. itself have the moist effect of whitening, and milk constituents can neutralize the various mixtures inside soap,
Cortex Eucommiae fine powder is set preferably to play a role.Have the function of washing spot, the milk being furthermore added in addition to similar with common product
Component can effectively improve skin problem, and it is fine and smooth mild to use feeling.
The essence can be selectively added without particular/special requirement under conditions of meeting safety by itself hobby.
The colouring matter can be selectively added without particular/special requirement under conditions of meeting safety by itself hobby.
In traditional industrial soap preparation process, dirt-removing functions are mainly considered, our innovation is Cortex Eucommiae essence
The addition of powder and milk avoids the toxic side effect of other chemical synthesis additives, while keeping cleaning function, obtains
The special efficacy that Cortex Eucommiae tranquilizing the mind QI invigorating, moisturizing decompression and milk whitening are moistened.
The second object of the present invention is to providing the preparation method of the Cortex Eucommiae soap, specifically can comprise the following steps that
1) load weighted highly basic is added to the water dissolution, lye is made；The process is exothermic reaction, can be subsequent soap
Change reaction and a part of heat is provided, to accelerate the preparation of product.
2) it pours into container, dissolves by heating after mixing load weighted vegetable fat, until oil temperature is 45~55 DEG C；Heating
Being stirred in the process to it can be allowed to be heated evenly, and promote the dissolution of monounsaturated fatty acid molecule.
3) vegetable fat dissolved is poured into after lye is cooled to 45~55 DEG C, this operation is to keep close for the two
Temperature, both make preferably fusion, saponification occur and obtains mixed solution.
4) the Cortex Eucommiae raw material after being dried is put into ball mill and is ground, then remove impurity with the screen to filtrate, obtained
The powder of quality exquisiteness is obtained to get Cortex Eucommiae fine powder；The sieve is 100 mesh；
5) mixed solution is added in load weighted Cortex Eucommiae fine powder, be sufficiently stirred, specifically available glass bar is taken quick and slow
The mode (quickly under per minute 200, at a slow speed per minute 100 under) of speed alternately each stirring 5min, until the soap lye is in the pasty state simultaneously
And its surface without grease layer, it is then slowly added into milk reconciliation, obtains thick soap lye；
6) thick soap lye is poured into mold, room temperature ventilating and thermal insulating can specifically be protected under 20~25 DEG C of ventilation cool environments
Temperature 2~3 days, prolonged air-dry hangs the stable formation that can promote soap, later takes out the solid in mold, after slice
Up to Cortex Eucommiae soap.
Effect of the invention
Cortex Eucommiae fine powder has the function of that Chinese medicine reconciles and nourishes that taste is pure and fresh, tranquilizing the mind QI invigorating, has antiallergy to pruitus
The effect of with alleviating, makes soap be provided with excellent comprehensive performance after soap is added, widely applicable, safe and efficient.The present invention mentions
The Cortex Eucommiae soap of confession not only can be used for washing spot, but also can be used for moistening skin-care, use feeling exquisiteness mildly, product does not have
The addition of extra chemicals does not stimulate human skin, and allergy is less likely to occur for long-time service, can satisfy various crowds
Use demand.
Compared with existing soap preparing process, the preparation method reaction temperature of the application product is low, and more conducively control operation does not have
Using extra chemical addition agent, no waste material generates more health environment-friendly, and equipment is simple, and fabrication cycle is shorter.
Detailed description of the invention
Fig. 1 is that Cortex Eucommiae soap products of the invention prepare simple process figure.
Specific embodiment
Below with reference to embodiment, the present invention is further illustrated.But the present invention is not restricted by the embodiments.Prepare Cortex Eucommiae
Fine powder
By after fresh Folium Eucommiae dryness in the sun by ball mill grinding, the screen to filtrate and the powdery for obtaining quality exquisiteness
Object is to get Cortex Eucommiae fine powder.The drum's speed of rotation is 500r/min, is ground 20 minutes；Ball mill model selects Fu Kasi miniature
Comprehensive planetary type ball-milling instrument F-P400E.Filtering sieve mesh number is 100 mesh.
Embodiment 1
It weighs in parts by weight: 80 parts of rapeseed oil, 20 parts of olive oil, 10 parts of Cortex Eucommiae fine powder, 10 parts of sodium hydroxide, distilled water
20 parts, 10 parts of plain chocolate.
The specific preparation method of Cortex Eucommiae soap, including the following steps:
1, sodium hydroxide is added in distilled water, lye is made；
2, beaker is added after mixing rapeseed oil and olive oil, is heated to 50 DEG C on electromagnetic heating set；
3, the compound lard being cooled to lye after pouring into heating after 50 DEG C, stirs evenly, obtains mixed solution；
4, load weighted Cortex Eucommiae fine powder is added above-mentioned mixed solution, stirring to paste and its surface without grease layer, then
It is slowly added to plain chocolate, obtains thick soap lye；
5, thick soap lye is poured into resin die, keeps the temperature 48h under 25 DEG C of ventilation cool environments, it later will be in mold
Solid takes out, and Cortex Eucommiae soap is made after slice.
Embodiment 2
It weighs in parts by weight: 60 parts of rapeseed oil, 40 parts of olive oil, 10 parts of Cortex Eucommiae fine powder, 10 parts of sodium hydroxide, tap water
20 parts, 10 parts of plain chocolate.
The specific preparation method of Cortex Eucommiae soap, including the following steps:
1, sodium hydroxide is added in tap water, lye is made；
2, beaker is added after mixing rapeseed oil and olive oil, is heated to 50 DEG C on electromagnetic heating set；
3, the compound lard being cooled to lye after pouring into heating after 50 DEG C, stirs evenly, obtains mixed solution；
4, load weighted Cortex Eucommiae fine powder is added above-mentioned mixed solution, stirring to paste and its surface without grease layer, then
It is slowly added to plain chocolate, obtains thick soap lye；
5, thick soap lye is poured into resin die, keeps the temperature 72h under 25 DEG C of ventilation cool environments, it later will be in mold
Solid takes out, and Cortex Eucommiae soap is made after slice.
Embodiment 3
It weighs in parts by weight: 80 parts of rapeseed oil, 20 parts of olive oil, 10 parts of Cortex Eucommiae fine powder, 10 parts of sodium hydroxide, tap water
20 parts, 10 parts of plain chocolate, fragrant refined 1 part of house milk flavour of U.S., fragrant refined 1 part of house green pigment of U.S..
The specific preparation method of Cortex Eucommiae soap, including the following steps:
1, sodium hydroxide is added in tap water, lye is made；
2, beaker is added after mixing rapeseed oil and olive oil, is heated to 50 DEG C on electromagnetic heating set；
3, the compound lard being cooled to lye after pouring into heating after 50 DEG C, stirs evenly, and obtains mixing soap lye；
4, mixing soap lye, stirring to paste and its surface without grease layer is added in load weighted Cortex Eucommiae fine powder；
5, above-mentioned mixing soap lye is added in plain chocolate, essence, colouring matter, stirring is uniform and stable to soap lye color, obtains dense
Thick soap lye；
6, thick soap lye is poured into mold, 48h is kept the temperature under 25 DEG C of ventilation cool environments, then by the production in mold
Product take out, and Cortex Eucommiae soap is made after slice.
Embodiment performance test
(1) face cleaning aptitude tests
Long Liqi sulphur facial soap is bought in the market, as comparative experiments.From the masses that voluntary participation is tested,
Randomly select 10 Oily masses, 10 allergic skin masses；The masses of every kind of skin quality are divided equally, A, B two is combined into
Group, every group includes 5 Oily masses, 5 allergic skin masses, all applies to every masses face and spreads identical ink
Pattern, then, the soap face cleaning that A group uses embodiment 3 to provide, the Long Liqi sulphur facial soap face cleaning that B group is bought using market.
After two groups of A, B of masses' face cleaning, its skin of face is detected using skinanalysis apparatus, the result of detection is as follows: A group
Many facial residues are lower than 1%, and the face of the allergic skin masses has no discomfort, and the faint scent taste for having Cortex Eucommiae special, enable
People's spirit and QI cleaning；The facial residue of the B group masses is 8~12%, the face of the allergic skin masses slightly itch sense of discomfort.
(2) washing hand test
Purchase carving board soap in the market, as comparative experiments.From the masses that voluntary participation is tested, randomly select
40 masses, are divided into two groups, first group of soap scouring of wool towel provided using embodiment 3, second group of fertilizer bought using market
It soaps towel.After 20min, stop washing, first group of masses feels that both hands have no discomfort, also without dry sensation, second group of masses
Feel after prolonged washing, hand is relatively dry.
Comprehensively consider the above test, when soap provided in this embodiment is used for face cleaning, more completely, noresidue, Er Qiefei
Room temperature and, allergic skin is also suitable.In addition, not hurt hands, practicability good to skin sparing when being washed using the soap yet
Height is suitble to promote.
In addition, the soap that Examples 1 and 2 are provided is tested, the result of acquisition is consistent with above-mentioned test result.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, for the skill of this field
For art personnel, the invention may be variously modified and varied.All within the spirits and principles of the present invention, made any to repair
Change, equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of Cortex Eucommiae soap, the following components comprising parts by weight meter:
100 parts of vegetable fat；
4~16 parts of Cortex Eucommiae fine powder；
4~16 parts of highly basic；
12~28 parts of water；
4~16 parts of milk；
0~2 part of essence；
0~2 part of colouring matter.
2. Cortex Eucommiae soap according to claim 1, it is characterised in that the following components comprising parts by weight meter:
100 parts of vegetable fat；
8~12 parts of Cortex Eucommiae fine powder；
8~12 parts of highly basic；
18~22 parts of water；
8~12 parts of milk；
0.8~1.2 part of essence；
0.8~1.2 part of colouring matter.
3. Cortex Eucommiae soap according to claim 1 or 2, it is characterised in that:
The vegetable fat selects rapeseed oil with olive oil by weight (1.5~6): 1 mixes and is made.
4. Cortex Eucommiae soap according to claim 3, it is characterised in that:
The vegetable fat selects rapeseed oil with olive oil by weight (3.5~4.5): 1 mixes and is made.
5. Cortex Eucommiae soap according to claim 1 or 2, it is characterised in that:
The Cortex Eucommiae fine powder is by Cortex Eucommiae raw material by ball mill grinding, the screen to filtrate and be made.
6. Cortex Eucommiae soap according to claim 5, it is characterised in that:
The Cortex Eucommiae raw material is Folium Eucommiae；
The revolving speed of the ball mill is 300~500r/min；The sieve mesh number is 100 mesh.
7. Cortex Eucommiae soap according to claim 1 or 2, it is characterised in that:
The highly basic is selected from least one of sodium hydroxide, potassium hydroxide, barium hydroxide, calcium hydroxide；
The wet concentration is from least one of natural water, pure water, distilled water, tap water；
The milk is selected from least one of milk, goat milk.
8. the preparation method of described in any item Cortex Eucommiae soap according to claim 1~7, it is characterised in that including following step
It is rapid:
1) load weighted highly basic is added to the water dissolution, lye is made；
2) load weighted vegetable fat is poured into container, is dissolved by heating；
3) vegetable fat dissolved is poured into after lye is cooling, obtains mixed solution；
4) Cortex Eucommiae raw material is put into ball mill grinding, then removes impurity with the screen to filtrate, obtain the flour of quality exquisiteness, i.e.,
Obtain Cortex Eucommiae fine powder；
5) by load weighted Cortex Eucommiae fine powder be added mixed solution, be sufficiently stirred, until the soap lye in the pasty state and its surface without
Oil layer is then slowly added into milk reconciliation, obtains thick soap lye；
6) thick soap lye is poured into mold, room temperature ventilating and thermal insulating later takes out the solid in mold, up to Cortex Eucommiae fertilizer after slice
Soap.
9. the preparation method of Cortex Eucommiae soap according to claim 8, it is characterised in that:
In the step 2), the oil temperature after heating for dissolving is 45~55 DEG C；
In the step 3), the lye is spare after being cooled to 45~55 DEG C；
In the step 4), the Cortex Eucommiae raw material is spare after being dried.
10. soap made of the preparation method of Cortex Eucommiae soap according to claim 8 or claim 9.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810387144.5A CN110408486A (en) | 2018-04-26 | 2018-04-26 | A kind of Cortex Eucommiae soap and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810387144.5A CN110408486A (en) | 2018-04-26 | 2018-04-26 | A kind of Cortex Eucommiae soap and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111440680A (en) * | 2020-04-24 | 2020-07-24 | 山东贝隆杜仲生物工程有限公司 | Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof |
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| CN111440680A (en) * | 2020-04-24 | 2020-07-24 | 山东贝隆杜仲生物工程有限公司 | Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof |
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