CN1197549C - Powder type bath detergent and its preparation method - Google Patents
Powder type bath detergent and its preparation method Download PDFInfo
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- CN1197549C CN1197549C CN 02122121 CN02122121A CN1197549C CN 1197549 C CN1197549 C CN 1197549C CN 02122121 CN02122121 CN 02122121 CN 02122121 A CN02122121 A CN 02122121A CN 1197549 C CN1197549 C CN 1197549C
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Abstract
The present invention provides a powdery bath detergent product, wherein a salt of natural fatty acid is used as a detergent, and besides, the present invention also contains a nutrient agent, a weight reduction agent, horny layer particles, other functional additives, pigment and essence. The present invention has a cleaning effect when in use; besides, the present invention promotes the blood circulation of the skin by a massage function generated by rubbing the skin to enable a human body to feel heat generation, and has the effects of softening, nourishing, moistening and whitening the skin, improving the flexibility of the skin and making a person lose weight.
Description
Technical field
The invention belongs to daily articles for washing field, relate to the powder type bath cleaning supplies, also claim shower powder, this shower powder can also play massage effect to skin in cleaning skin, thereby has good skin moistening health care and body shaping effect.The invention still further relates to the preparation method of shower powder.
Background technology
Common in the market shower and clean body hygienic article mainly contain liquid, and as bath gel, bulk is as fancy soap or lamellar, as soap wrapper etc.These clean body articles for use generally are made of cleansing (surfactant) and suitable skin moistening and nutritional labeling, its effect mainly is a cleaning skin, and the skin moistening and the nutritional labeling of wherein adding also can cooperate the skin moistening requirement of satisfying the shower process, in use generally can only make health that cool sensation is arranged, skin there is not massage effect, bad for the effect of removing the deep skin dirt.
These body lotions or bath soap all require various compositions to dissolve in soap base in preparation, if therefore having comprised some has the active substance of special efficacy, its activity is difficult in and keeps active in such environment for a long time, that is to say that the effect of product might be given a discount along with the time.
Summary of the invention
The inventor is after having investigated clean body agent market with great concentration and having groped through a large amount of experiments, find to adopt the powder type bath articles for use to address the above problem, promptly use the powder type bath agent, in cleaning skin, can make health that the sensation of heating is arranged owing to rub, thereby can accelerate cutaneous circulation, reach the effect of vigorous and graceful skin.Cooperate and add some functional components, can all produce good nursing care and regulating action the skin and even the bodily form.Because product is powdered solid-state before use, the active matter in the product can keep the longer time.
Therefore the purpose of this invention is to provide a kind of powder type bath cleaning supplies, i.e. powder type bath agent in use can produce massage to skin simultaneously, promotes blood circulation of skin, plays the effect of skin care.
The present invention also provides a kind of powder type bath cleaning supplies simultaneously, by the additive of wherein skin moistening and weight reducing effect, also can receive good elegant body and health-care effect in the cleaning of taking a shower.
Another object of the present invention provides a kind of method for preparing powder type bath detergent.
Above-mentioned purpose of the present invention can realize according to following scheme:
Powder type bath detergent of the present invention is to be soap base with the soap after the saponification of natural animal-plant oil, add the additive that the nutrient with skin moistening function, the weight reducing agent with the effect of elimination body fat and antibacterial and chelating agen etc. have given efficacy, cooperate suitable pigment and essence, become have different size, the grain products of different color, generally can be the irregular particle of 0.01-3.0 millimeter particle diameter, in the washing friction, make health that the sensation of heating be arranged, but reach the effect of massage skin, sterilizing and itch-relieving and skin moistening, weight reducing body shaping.
According to powder type bath detergent of the present invention, its soap that contains natural oil is as soap base, and comprise oatmeal and vitamin E nutrient, comprise weight reducing agent, pigment and the essence of chilli oil.Quality with this powder type bath detergent is a benchmark, and powder type bath detergent of the present invention comprises:
The soap of the natural oil of 20.0-90%;
The nutrient of 0.02-40% is comprising the oatmeal of 0.1-15% and the vitamin E of 0.01-8% weight;
The weight reducing agent of 0.01-23% is comprising the chilli oil of 0.1-5%;
Be no more than 0.02% pigment;
Be no more than 1.5% essence.
As the used main cleaning agent of the present invention, the product that the soap of described natural oil can adopt natural animal and vegetable oil to obtain through saponification, wherein animal oil can be Adeps Bovis seu Bubali or Adeps Caprae seu ovis etc., vegetable oil then can be Oleum Cocois, Petiolus Trachycarpi oil, Oleum Ricini, Oleum Glycines, olive oil or camellia oleosa seed wet goods, can obtain sodium salt, potassium salt or ammonium salt through carrying out saponification with different alkali.
The natural oil fat hydrochlorate that the present invention adopts is a kind of outstanding surfactant, use as soap base, it has in the shower process that foam is abundant, zest is little, the effective dirt in the cleaning skin, advantages such as favorable biological degradability, its amount in shower powder is 20-90%, is preferably 50-90%.Oatmeal that the nutrient that the present invention uses comprises (Avena sativa[oat] Kerenl Flour) and vitamin E, wherein, oatmeal has the nutrition skin, makes skin recover elastic effect, and vitamin E then can defying age, skin whitening.Can also optionally comprise in glycerol, lanoline and the Aloe powder one or more in the described nutrient, glycerol and lanoline are known skin moistening wetting agents, and Aloe powder is except that can skin moistening preserving moisture, and also has the effect of healing of wound, sterilization, antiperspirant, antipruritic, antiinflammatory.Wherein the addition of glycerol is no more than 8%, and the addition of Aloe powder is no more than 10%.The emollient that performance and the use crowd concrete according to product, the present invention use can use their mixture of some kinds.
Weight reducing agent in the powder type bath detergent of the present invention is except that using chilli oil, can also add in Sargassum extract, Folium Camelliae sinensis extract and the theobromine one or more, especially green tea extract or theobromine, they all have the health of making heating, deflagrate and the effect that consumes body fat.The total amount of described weight reducing agent in product of the present invention is 0.01-23%, can use chilli oil separately, also chilli oil can be mixed use with in the above-mentioned substance one or more, according to preferred version of the present invention, if you are using, the consumption of Sargassum extract is no more than 8%, and the consumption of green tea extract is no more than 5%.
The pigment among the present invention and the kind of essence and consumption can be determined on demand, can give different fragrance of product and color according to the hobby of user in the production.Wherein pigment is preferably selected food coloring for use, and consumption should be no more than 0.02%.
Can also optionally contain in the powder type bath detergent of the present invention and be selected from destratum corneum particle, antibacterial, chelating agen, brightening agent, suds booster, and in other effective substance one or more.The destratum corneum particle can be selected from one or more or its mixture in silicon dioxide, polyethylene powder, Jojoba particle and the mica powder, this component can increase the massage effect of product of the present invention, help thoroughly removing dead bark on the one hand, softening skin, because rubbing action has increased blood circulation of skin, make skin that vigor more be arranged on the other hand.Particulate size is preferably the 100-150 order, is benchmark with the quality of this powder type bath detergent, and the destratum corneum particle total amount that is added is 0.1-9%, is preferably 1-5%.Mica powder is except can destratum corneum, because itself band pearly-lustre, can also increase outward appearance U.S. of product, and when containing mica powder, its amount is no more than 3%.
Chelating agen can play the effect of demineralized water, can be selected from EDTA sodium salt, sodium citrate or its mixture, is benchmark with the quality of this powder type bath detergent, and addition is 0.1-1%.
Antibacterial has the disinfectant antipruritic effect, should select material for use to human body safety, can be selected from triclosan (Triclosan), sodium trichloro-isocyanurate, ketoconazole, the toluene-sodium-sulfonchloramide (Chloramine T) one or more, quality with this powder type bath detergent is a benchmark, and addition is 0.1-0.5%.
Other has the material of given efficacy to have no special requirements to brightening agent, suds booster etc. in the present invention, can use according to the known technology that those of ordinary skills understood, and concrete addition is conventional amount used and gets final product.
According to another object of the present invention, the preparation method of this powder type bath detergent is provided, comprise the steps:
1) saponification is good natural oil fat hydrochlorate soap base is pulverized the back screening, collects the soap powder granule of required size;
2) in this soap powder, add the nutrient after measuring and the agent of reducing weight, mix homogeneously;
3) other composition is measured the back respectively and adds step 2) mixture in, abundant mix homogeneously;
4) said mixture oven drying at low temperature, bake out temperature are not higher than 40 ℃;
5) suitably obtain finished product after the cooling.
The manner of packing of finished product and dosage are determined according to actual needs.
Unless otherwise indicated, related amounts of components all is that gross mass with described powder type bath detergent product is a benchmark among the application.The amount of related functional materials all is meant its active component or active constituent content.
Powder type bath cleaning product of the present invention has following advantage:
The present invention has remedied the blank of this series products as a kind of novel shower cleaning supplies.Product particle can produce friction to skin in the use, and make health that the sensation of heating be arranged, thereby when removing the deep skin dirt, can promote blood circulation, during softening skin, product are formed functional materials such as distinctive nutrient and weight reducing agent simultaneously to skin provide moist, brighten, kill virus antipruritic, improve skin elasticity and eliminate multiple effects such as subcutaneous fat.
The present invention is a powder product, can adopt the fractional pack form, and is easy to carry, more helps keeping for a long time of active component simultaneously.
The specific embodiment
The invention provides a kind of powder type bath detergent, its soap base has adopted the soap of natural animal and vegetable oil, as main cleaning agent, can be sodium salt, potassium salt or ammonium salt, described natural animal oil comprises Adeps Bovis seu Bubali, Adeps Caprae seu ovis etc., and crude vegetal comprises Oleum Cocois, Petiolus Trachycarpi oil, Oleum Ricini, Oleum Glycines, olive oil or camellia oleosa seed wet goods.This soap base can adopt above-mentioned oils and fats and corresponding alkali solution to make according to conventional saponification process, for example sodium hydroxide solution, potassium hydroxide solution or Ammonia.This soap base raw material also can directly be purchased.
The preferred saponification process of the present invention is as follows:
Drop into raw oil material to the saponification still, slowly add aqueous slkalis such as the NaOH of metering excessive 2%～3% or KOH (be made in advance 32% concentration) then, feed steam simultaneously to stir, oils and fats is fully contacted, with alkali liquor to reach the saponified purpose of homogeneous phase.Can open greatlyyer at saponification common steam of when beginning operation, turn down then, keep the saponification material up and down slowly circulation stir, temperature remains on about 85 ℃, saponifying process requires to keep in the saponification process a certain amount of free alkali (0.3%～0.5%).Saponification finishes, obtain even, transparent syrupy shape reactant, the soap base that saponification workshop section is sent here (containing 30～32% moisture) drying operation makes moisture drop to 10～15% afterwards, can adopt the chain type drying machine, soap base is delivered to chilling roll to be solidified, make the soap flakes of flakiness shape, again soap flakes are installed to conveyer belt, in hothouse, transport and carry out drying in the process.
Mixing procedure can be: the soap base raw material of saponification gained is pulverized with pulverizer, and screen cloth sieves, select suitable granule (size of particle diameter is 0.1 millimeter～3.0 millimeters), add weight reducing agent, nutrient, with additives such as destratum corneum particle, antibacterial, chelating agen, essence, pigments, abundant mix homogeneously, at least 10 minutes, dry in baking oven afterwards, temperature is 40 ℃.Product is implemented packing according to actual needs.
The raw material that the present invention uses all has industrialization product, and in the embodiment of back, the nutrient oatmeal can come from the far-reaching Food Co., Ltd in Shanghai (active ingredient 95%), and vitamin E can adopt the product (active ingredient 100%) of German BASF AG; Aloe powder adopts the be bestowed by heaven product (active ingredient 90%) of company of Guangzhou; The chilli oil of weight reducing effect is a product (active ingredient 30%) of going up the good company in Haiyang; Sargassum extract, Folium Camelliae sinensis extract, theobromine adopt the product of Shanghai higher-dimension biochemical product company (active ingredient 50%), French EXSYMOL company (active ingredient 50%), French SOLABIA company (active ingredient 60%) respectively, and toluene-sodium-sulfonchloramide uses Jianping, Shanghai chemical industry company limited product.
The equipment that the present invention uses also is conventional, and what use in an embodiment is:
1, saponification still: SM-I (Enping City machinery plant), volume is 1m
3, stainless steel;
2, chain type drying machine: XF-5 type, power 50.0KW/h;
3, pulverizer: F-3 type pulverizer, rotating speed 2800r/min, power 7.5KW/h;
4, mixing machine: SHM bipyramid spiral mixing machine, power 3.0KW/h;
5, baking oven: H8 type, 8000 watts of power, volume 10m
3
Below describe the realization of the object of the invention in detail by specific embodiment, purpose only is to help the reader to understand characteristics of the present invention, does not constitute any qualification to the scope of the present invention.
Embodiment 1
Raw material:
Coco-nut oil fatty acid sodium 57.19kg
Glycerol 5.0kg
Aloe powder 8.0kg
Green tea extractive liquor 3.0kg
Chilli oil 4.0kg
Vitamin E 8.0kg
Oatmeal 10.0kg
Silicon dioxide 3.0kg
Triclosan 0.2kg
EDTA-2Na 0.1kg
Mica powder 1.0kg
Food coloring (bright orchid) 0.01kg
Essence 0.5kg
Manufacture method:
Coco-nut oil fatty acid soda soap base can be according to the method described above with Oleum Cocois and sodium hydroxide solution in 1m
3The saponification still in carry out saponification and obtain.
This soap base places mixer, adds glycerol, Aloe powder, green tea extractive liquor and chilli oil after measuring, stirs 5 minutes; Add vitamin E, oatmeal, silicon dioxide, EDTA-2Na, triclosan, mica powder, bright orchid afterwards, stirred 5 minutes; Adding essence at last stirred 3 minutes; The powder that mixes is placed baking oven, and about 40 ℃ dryings of constant temperature were taken out after 10 minutes, and the cool to room temperature packing gets final product.
The size of product is 0.01 millimeter～3.0 millimeters, and it is shaped as irregular particle.
The batching of embodiment 2-4 sees table
| Name of material | Inventory (kg) | |||
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | |
| Soap | 57.19 | 63.99 | 81.09 | 86.98 |
| Glycerol | 5.0 | 3.0 | -- | -- |
| Aloe powder | 8.0 | -- | 3.0 | 1.5 |
| Seaweed extracted liquor | -- | 6.0 | 4.0 | -- |
| Green tea extractive liquor | 3.0 | 2.0 | -- | 2.0 |
| Chilli oil | 4.0 | 4.0 | 2.5 | 2.5 |
| Vitamin E | 8.0 | 8.0 | 3.0 | 2.0 |
| Oatmeal | 10.0 | 8.0 | 2.0 | 3.0 |
| Silicon dioxide | 3.0 | 3.5 | -- | -- |
| Polyethylene | -- | -- | 3.0 | 1.0 |
| Triclosan | 0.2 | 0.3 | 0.5 | 0.3 |
| EDTA-2Na | 0.1 | 0.2 | 0.1 | 0.2 |
| Mica powder | 1.0 | -- | 0.3 | -- |
| Food coloring | 0.01 | 0.01 | 0.01 | 0.02 |
| Essence | 0.5 | 1.0 | 0.5 | 0.5 |
The test example
Subjects: select 20 village woman in the pool, Malong village, Zhong Jiang town, Enping City to compare test, one group of per 10 people are respectively test group and matched group, the equal main suit of experimenter: long-term housework, it is longer to contact the bigger water time of salt scale part, pachylosis.
Test method: test group is used the about 30g of this shower powder when taking a shower every day, does not re-use any other cleaning agent midway; " virtue wafts " board bath gel that matched group uses Guangzhou color spring Cosmetics Plant to be produced every day uses 15g at every turn when taking a shower, do not re-use other cleaning agent.
Test period: on April 10,2 days to 2002 March in 2002,40 days by a definite date;
Result of the test:
Test group is told: when taking a shower, in friction, feels to have the sensation of heating at every turn, all feels skin lubrication after the bath, and no harsh feeling, skin is soft than before after 40 showers, and exquisiteness bleaches slightly, and than more flexible in the past, subcutaneous fat reduces, and stature is also than slenderrer in the past.
Matched group: dermal sensation is coarse.
Conclusion:
This product to skin have softening, moisten, brighten, improve the effect of skin elasticity, weight reducing.
In addition, find also in the test that long some red miliaria in two bit test objects (test group) the test predecessor always feels that health itches often, the degree of itching after the test reduces greatly, and red miliaria also major part has disappeared.
Claims (11)
1, a kind of powder type bath detergent, its soap that contains natural oil is as soap base and comprise oatmeal and the nutrient of vitamin E, comprise weight reducing agent, pigment and the essence of chilli oil, is benchmark with the quality of this powder type bath detergent, wherein comprises:
The soap of the natural oil of 20.0-90%;
The nutrient of 0.02-40% is comprising the oatmeal of 0.1-15% and the vitamin E of 0.01-8% weight;
The weight reducing agent of 0.01-23% is comprising the chilli oil of 0.1-5%;
Be no more than 0.02% pigment;
Be no more than 1.5% essence.
2, the described powder type bath detergent of claim 1, wherein, the soap of described natural oil is the soap that natural animal oil or crude vegetal obtain through saponification.
3, the described powder type bath detergent of claim 2, wherein, the soap of described crude vegetal is selected from: the soap of Oleum Cocois, Petiolus Trachycarpi oil, Oleum Ricini, Oleum Glycines, olive oil and Oleum Camelliae.
4, the described powder type bath detergent of claim 1, wherein, also optionally comprise in Sargassum extract, Folium Camelliae sinensis extract, the theobromine one or more in the described weight reducing agent, quality with this powder type bath detergent is a benchmark, the consumption of Sargassum extract is no more than 8%, and the consumption of tea extract is no more than 5%.
5, the described powder type bath detergent of claim 1, wherein, also optionally comprising in glycerol, Aloe powder, the lanoline one or more in the described nutrient, is benchmark with the quality of this powder type bath detergent, the amount of glycerol is no more than 8%, and the amount of Aloe powder is no more than 10%.
6, each described powder type bath detergent of claim 1-5, it also optionally contains destratum corneum particle, antibacterial, chelating agen, brightening agent, and in other effective substance one or more.
7, the described powder type bath detergent of claim 6, wherein, the destratum corneum particle can be one or more or its mixture in silicon dioxide, polyethylene powder, Jojoba particle and the mica powder, quality with this powder type bath detergent is a benchmark, its total amount is 0.1-9%, when containing mica powder, the amount of this mica powder is no more than 3%.
8, the described powder type bath detergent of claim 6, wherein, chelating agen is EDTA sodium salt, sodium citrate or its mixture, is benchmark with the quality of this powder type bath detergent, the chelating agen addition is 0.1-1%.
9, the described powder type bath detergent of claim 6, wherein, antibacterial is selected from one or more among triclosan, sodium trichloro-isocyanurate, ketoconazole, the fluorine amine T, is benchmark with the quality of this powder type bath detergent, and addition is 0.1-0.5%.
10, the preparation method of each described powder type bath detergent of claim 1-9, it may further comprise the steps:
1) saponification is good natural oil fat hydrochlorate soap base is pulverized the back screening, and collection cut size is 0.1 millimeter-3.0 millimeters a soap powder granule;
2) in this soap powder, add the nutrient after measuring and the agent of reducing weight, mix homogeneously;
3) other composition is measured the back respectively and adds step 2) mixture in, abundant mix homogeneously;
4) said mixture oven drying at low temperature, bake out temperature are not higher than 40 ℃;
5) obtain finished product after the cooling.
11, the described preparation method of claim 10, wherein, natural oil fat hydrochlorate soap base is natural animal and vegetable oil and aqueous slkali fully to be contacted saponification form, the saponification resultant dehydrate is to water content 10-15%.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02122121 CN1197549C (en) | 2002-05-31 | 2002-05-31 | Powder type bath detergent and its preparation method |
| JP2002205271A JP2004002255A (en) | 2002-05-31 | 2002-07-15 | Powdery bathing cleaning agent and method for producing the same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02122121 CN1197549C (en) | 2002-05-31 | 2002-05-31 | Powder type bath detergent and its preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1462615A CN1462615A (en) | 2003-12-24 |
| CN1197549C true CN1197549C (en) | 2005-04-20 |
Family
ID=29743146
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 02122121 Expired - Fee Related CN1197549C (en) | 2002-05-31 | 2002-05-31 | Powder type bath detergent and its preparation method |
Country Status (2)
| Country | Link |
|---|---|
| JP (1) | JP2004002255A (en) |
| CN (1) | CN1197549C (en) |
Cited By (1)
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| CN103110557A (en) * | 2013-03-21 | 2013-05-22 | 白继良 | Bath rubbing tea with function of refreshing and stopping perspiration and preparation method thereof |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101125893B1 (en) * | 2005-04-13 | 2012-03-21 | (주)아모레퍼시픽 | Medicinal herb cosmetic soap composition |
| CN100372521C (en) * | 2006-02-06 | 2008-03-05 | 高明全 | Bathing agent possessing health and medical function and its preparation method |
| JP2013155369A (en) * | 2012-01-05 | 2013-08-15 | Nippon Eisei Center:Kk | Shirasu soap (volcanic ash soap) |
| CN102776086A (en) * | 2012-07-09 | 2012-11-14 | 启东市中勇机电工具有限公司 | Cleansing soap |
| CN103284919B (en) * | 2013-06-08 | 2014-11-05 | 上海巴方精细化工有限公司 | Tea tree oil bath salt |
| CN103432030A (en) * | 2013-08-23 | 2013-12-11 | 南通华兴石油仪器有限公司 | Natural sterilizing shower gel |
| CN106166127A (en) * | 2016-08-23 | 2016-11-30 | 安徽洁尘日化用品有限公司 | Sea grape absolute oil facial film |
| CN106265251A (en) * | 2016-08-23 | 2017-01-04 | 安徽洁尘日化用品有限公司 | The preparation method of sea grape absolute oil facial film |
| CN107174567A (en) * | 2016-12-30 | 2017-09-19 | 吴玉爱 | Moisten often naked skin and help the strong medicine composition for protecting bullet |
| CN108785180A (en) * | 2018-08-22 | 2018-11-13 | 广州道明研究院有限公司 | A kind of shower cream and preparation method thereof containing wormwood extract and nano silicon dioxide |
| CN111991271A (en) * | 2020-09-17 | 2020-11-27 | 佛山市南海区桂城埃菲尔化妆品有限公司 | Gilding bath cream and preparation method thereof |
-
2002
- 2002-05-31 CN CN 02122121 patent/CN1197549C/en not_active Expired - Fee Related
- 2002-07-15 JP JP2002205271A patent/JP2004002255A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103110557A (en) * | 2013-03-21 | 2013-05-22 | 白继良 | Bath rubbing tea with function of refreshing and stopping perspiration and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2004002255A (en) | 2004-01-08 |
| CN1462615A (en) | 2003-12-24 |
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