CN106221967A - A kind of pure plant extract strong dirt-removing cleaning agent and preparation method thereof - Google Patents
A kind of pure plant extract strong dirt-removing cleaning agent and preparation method thereof Download PDFInfo
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- CN106221967A CN106221967A CN201610645883.0A CN201610645883A CN106221967A CN 106221967 A CN106221967 A CN 106221967A CN 201610645883 A CN201610645883 A CN 201610645883A CN 106221967 A CN106221967 A CN 106221967A
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- cleaning agent
- plant extract
- removing cleaning
- strong dirt
- acid
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2079—Monocarboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38618—Protease or amylase in liquid compositions only
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
Abstract
The present invention proposes a kind of pure plant extract strong dirt-removing cleaning agent, including each component of following mass percent: natural surfactant 32 38%；Cocinic acid 10 15%；Natural glycine betaine 3 5%；Thickening agent 0 1%；Proteinase-10 1%；Acid-base modifier 1 2%；Plant fragrance quintessence oil 0 1%；Deionized water adds to 100%.This product, while high-effective cleansing, also has plant health, skin friendly effect.And form physical damnification hardly at article surface after decontamination, and effectively maintain the apparent glossiness of article, the invention also discloses the preparation method of described pure plant extract strong dirt-removing cleaning agent, relatively simple, be conducive to implementing and expanding production.
Description
Technical field
The present invention relates to filed of daily-use chemical industry, particularly relate to a kind of pure plant extract strong dirt-removing cleaning agent, the present invention is also
Relate to the preparation method of a kind of pure plant extract strong dirt-removing cleaning agent.
Background technology
Strong dirt-removing cleaning agent is the product going stain on the market for decontamination, because of its fast decontaminating.Cleaning effect is good, is deeply subject to
The favor of people.Decontamination cleanser in the market compounds based on heavy chemicals, and its component not only includes bleach, grinds
Grinding agent, Surfactant preparations, be the most also corrosive and the sodium tripolyphosphate of toxicity, normal hexane etc..Due to its composition mainly by
Chemicals is compounding to be formed, and this type of detergent defines secondary pollution to environment, health is formed harm simultaneously, is retained in
Chemicals on household articles, utensil, human body skin is difficult to eliminate, and the life that user is later is brought strong by long-time use
Health hidden danger.It is thus desirable to research and development one is polluted few, more environmentally-friendly decontamination cleaning product.
Summary of the invention
The present invention proposes a kind of pure plant extract strong dirt-removing cleaning agent, and clean effect is good, and environment-protecting asepsis, do not hinder skin
Skin and health.
The technical scheme is that and be achieved in that: a kind of pure plant extract strong dirt-removing cleaning agent, including following matter
Each component of amount percentage ratio: natural surfactant 28-42%；Cocinic acid 10-15%；Natural glycine betaine 3-5%；Thickening agent 0-
1%；Proteinase-10-1%；Acid-base modifier 1-2%；Plant fragrance quintessence oil 0-1%, deionized water adds to 100%.
Further, the preferred 32-38% of the proportioning of natural surfactant.
Further, described natural surfactant is in APG, oil tea saponin, aescine, Tsubaki-saponin
At least one.
Wherein, described oil tea saponin (Tea Saponin) is a kind of pentacyclic triterpene chemical combination extracted from camellia seed meal
Thing, it is the natural surfactant of a kind of function admirable, not only have good emulsifying, foam, disperse, permeate, lubrication etc.
Active function, but also have antiinflammatory, ease pain, sterilize, the pharmacological action such as antipruritic.Among the people once utilized the soaked hair washing of tea seed cake, washed
Clothing, also has the record of " bar seed is smash core and washed agriculture oil removal " in Compendium of Material Medica.Commercial synthesis surfactant is mainly used at it
As decontamination cleaning action bulk composition, it is frequently accompanied by the secondary dirt that industrial surface activity agent biodegradability difference causes
Dye.The scale produced along with Camellia oil, it is the deepest that the improvement of tea saponin enrichment extraction process and its applied research work
Enter, its characteristic make its both can as matrix components for shampoo, natural herb shampoo, sun-proof antiinflammatory skin lotion, wash one's hair
Body lotions etc., can be widely applied to again the industry such as textile washing, medicine.
Additionally, aescine, Tsubaki-saponin belong to Saponin class natural surfactant, there is good surface activity effect
Really, and natural environmental-protective.
APG (APG) is a kind of by Renewable resource (starch and oils and fats or their derivant glucose and fat
Fat alcohol) be raw material and prepared nonionic surfactant, be α and beta isomer mixture it live except having conventional surface
Property agent excellent properties outside, also there is many unique performances, be therefore referred to as world-class surfactant.APG is except self
Outside to human body skin and eye irritation, also can reduce the zest of anion surfactant compounding with it.In low stimulation
Property cleaning wash and protect in product configuration, APG is requisite primary raw material.In decontamination cleanser, live with anionic surface
Property agent reach good compatibility effect, the product zest to skin can be reduced simultaneously well, improve the mildness of product.
Further, described thickening agent is carboxymethyl cellulose, native cellulose be nature is distributed the widest, content is most
Polysaccharide, originate the abundantest.Cellulose obtains carboxymethyl cellulose (CMC) after carboxy methylation, its aqueous solution have thickening,
The effect such as the protection of film forming, gluing, water tariff collection, colloid, emulsifying and suspension, be widely used in oil, food, medicine, weaving and
The industries such as papermaking, are commonly called as " industry monosodium glutamate ".In formula for a product, the uniform of material in process of producing product can be effectively improved
Dispersion, is effectively improved product stability, reaches certain thickening power.
Further, described acid-base modifier is citric acid, and natural lemon acid is distributed very wide in nature, natural Fructus Citri Limoniae
Acid is present in the fruits such as plant such as Fructus Citri Limoniae, Citrus, Fructus Ananadis comosi and the skeleton of animal, muscle, blood.Citric acid is main in formula
Serve the effect of regulation product acid base number, while keeping product fine dirt-removing power, maintain product pH=6 ~ 7.
Further, described plant fragrance quintessence oil is to extract a kind of natural perfume (or spice) with Titian or flavouring effect to plant
Essence, such as Flos Rosae Rugosae quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil, Fructus Citri Limoniae quintessence oil etc., gives the plant fragrance that plant is special in this product.
Additionally, other components in formula, it may have very important effect and effect, as wherein protease is most important
A kind of industrial enzyme preparation, energy catalytic proteins and many hydrolase polypeptides, it is widely present in pluck, plant stem-leaf, fruit and micro-life
In thing.The most substantial amounts of use protease in cheesemaking, tenderization and vegetable protein modification.The interpolation of protease can be effective
Improve cleaning decontamination product the specific aim of the protein-based spots such as bloodstain is removed, be effectively improved dirt-removing power.
The formula that another one is important, natural glycine betaine, is the important composition composition of cereal product in nature, Ke Yicong
The sugared slag that beet sugar manufacture is later extracts, is found for the first time in sugar beet juice in 19th century.Give up from beet sugar manufacture
Honey extracts and separates the method for glycine betaine a lot, have chemical method, electrolysis, chromatography etc..Natural glycine betaine is to have life
The vitamin of thing activity morphology, for the formation of protein, the activity of enzyme is very important, has the osmotic pressure regulation of brilliance to make
With, stability, water solublity and humectant.In vegetable cleanser, it is effectively improved the biological activity of protease, forms material
Effectively altogether the most molten, skin is had certain moisture retention simultaneously.
The vegetable oil acid that cocinic acid is squeezed after pulverizing and steaming by the endosperm of Petiolus Trachycarpi kind plant Cortex cocois radicis, local in the torrid zone
For white liquid, it is then the solid of Adeps Bovis seu Bubali sample at cold place, has special odor, fragrant time fresh.Cocinic acid can be as day
Often food oil, is the oils and fats being uniquely made up of medium-chain fatty acid in food oil, has natural comprehensive antibacterial ability and resists
Oxidability, has good protective effect to skin.
The preparation method of a kind of described pure plant extract strong dirt-removing cleaning agent, comprises the following steps:
(1) cleaning agent stock solution is prepared: in proportion by thickening agent water mixed dissolution, weigh Natural surfactant the most in proportion
Agent, natural glycine betaine stirring and dissolving, mix homogeneously；Weigh cocinic acid in proportion with after appropriate 95% ethanol stirring and dissolving, mixing
Uniformly；Above two mixed liquor is mixed, uniformly mixes under constant temperature；
(2) mixture is placed room temperature ventilation, after natural cooling, weigh citric acid regulation mixed solution soda acid in proportion
Value；Weigh protease in proportion to be dissolved in appropriate amount of deionized water, two kinds of solution mixing, stir；
(3) storage, the inspection of semifinished product, fill, product inspection, warehouse-in.
Further, in step (1), described constant temperature is in the range of 70-80 DEG C.
Further, in step (2), it is cooled to 50 DEG C.
Further, in step (2), regulation pH-value is to pH=6 ~ 7.
The described pure plant extract strong dirt-removing cleaning agent of the present invention, the various different environmental protection of well-chosen, natural
Component, and creativeness carry out compatibility, bring into play mutually collaborative for the different-effect of each component, having reached can be efficient
Decontamination, the most also has environmental protection, skin friendly, healthy effect.And decontamination rear portion mark, article surface also will not be formed
Physical damnification, efficiently nurses, and improves the apparent glossiness of product, the described pure plant extract strong dirt-removing cleaning agent of the present invention
Preparation method is the most relatively simple, can convenient to carry out and expanding production.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, all
Belong to the scope of protection of the invention.
Embodiment 1
Formula one: Tsubaki-saponin (Contents of Main Components 85-90%) 32；Cocinic acid 10；Aescine 10；Natural glycine betaine 3；
Carboxymethyl cellulose 0.5；Proteinase-10 .5；Citric acid 1；Plant fragrance quintessence oil 0.5, deionized water adds to 100.
Preparation technology:
1) cleaning agent stock solution is prepared: in proportion by carboxymethyl cellulose with 3 times of water mixed dissolutions, weigh Flos Camelliae Japonicae soap the most in proportion
Glycosides, alkylglycoside, natural glycine betaine stirring and dissolving, mix homogeneously；Weigh the appropriate 95% ethanol stirring and dissolving of cocinic acid in proportion
After, mix homogeneously；Above two mixed liquor is mixed, uniformly mixes at 70-80 DEG C of constant temperature.
2) mixture is placed room temperature ventilation, when natural cooling is cooled to 50 DEG C, weigh citric acid regulation in proportion
Mixed solution pH-value is to pH=6 ~ 7；Weigh protease in proportion to be dissolved in appropriate amount of deionized water, mix with the mixed liquor of pH=6 ~ 7
Close, stir.
3) storage, the inspection of semifinished product, fill, product inspection, warehouse-in.
Embodiment 2
Formula three: oil tea saponin (Contents of Main Components 80-85%) 30；Cocinic acid 15；APG (APG) 7；Crude sweet
Dish alkali 5；Carboxymethyl cellulose 1；Protease 1；Citric acid 2；Plant fragrance quintessence oil 1, deionized water adds to 100.
Preparation technology is with embodiment 1.
Embodiment 3
Formula four: oil tea saponin (Contents of Main Components 80-85%) 30；Cocinic acid 10；APG (APG) 7；Crude sweet
Dish alkali 3；Carboxymethyl cellulose 0.5；Proteinase-10 .5；Citric acid 1；Plant fragrance quintessence oil 0.5, deionized water adds to 100.
Preparation technology is with embodiment 1.
Embodiment 4
Formula five: oil tea saponin (Contents of Main Components 80-85%) 25；Cocinic acid 10；APG (APG) 8；Crude sweet
Dish alkali 4；Carboxymethyl cellulose 0.5；Proteinase-10 .5；Citric acid 1.5；Plant fragrance quintessence oil 0.5, deionized water adds to 100.
Preparation technology is with embodiment 1.
Embodiment 5
Formula six: oil tea saponin (Contents of Main Components 80-85%) 22；Cocinic acid 10；APG (APG) 6；Crude sweet
Dish alkali 4；Carboxymethyl cellulose 0.5；Proteinase-10 .5；Citric acid 1.5；Plant fragrance quintessence oil 0.5, deionized water adds to 100.
Preparation technology is with embodiment 1.
Comparative example 6
Pure plant extract strong dirt-removing cleaning agent contrasts (oily waste treatment situation pair with the main performance of tradition decontamination cleaning product
Than):
PH pH-value detergency corrosivity
Kitchen heavy oil decontamination commodity 12-13 93.6 0.081
Furniture detergent commodity 13-14 91.7 0.032
Pure plant extract strong dirt-removing cleaning agent (using formula 4) 7-8 95.2 0.015
Wherein, dependence test is described as follows:
Erosion test:
It is 50mm*25mm*3mm to metal testing plate used in the testing experiment of metal protection.Each metal testing plate is cleaned, and
Drying in baking oven (105 ± 2) DEG C, weigh (M1), test piece is hung on respectively in different abluent working solutions, is placed in constant temperature
Water-bath (60 ± 2) DEG C is taken out after 2h.First wash with clear water, then with absolute ethanol washing, be finally placed in baking oven (105 ± 2)
Drying in DEG C, weigh (M2).Calculate rate of corrosion according to formula (M1-M2)/M1*100%, determine abluent corrosivity
Energy.
The detergency of abluent measures:
Standard intraocular's dirt is uniformly attached on the sheet metal of known certain mass (parallel test 3 groups, often dirt on the dirty sheet of group
Amount should ensure that as (0.5 ± 0.05) g, when in washing tube, abluent liquid temp rises to 30 DEG C, rapidly by the dirty sheet of known quality
Put into washing tube together with wash stand, after last wash stand puts into washing tube, start to calculate soak time, soak 1min,
Starting spotter, at the uniform velocity vibration washing 3min, takes out wash stand, and wash stand and sheet metal are together put into the perseverance of (40 ± 2) DEG C
In temperature drying baker, it is dried 2h, is cooled to room temperature, weighs, measure sheet metal mass change before and after washing, utilize formula
δm=[(M1-M2)/(M1-M0)] *100%
Calculate dirt clearance (relative average debiation ± 5% of 3 groups of results).In formula, δ m is oil removal rate (%), after M1 is for defiling
Metal testing plate quality, M2 for washing after metal testing plate quality, M0 is the initial mass of metal testing plate.
This products application scope is wide, can be used for the surface cleaning nursing of furniture, stone material etc..
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention
Within god and principle, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.
Claims (9)
1. a pure plant extract strong dirt-removing cleaning agent, it is characterised in that include each component of following mass percent: natural
Surfactant 28-42%；Cocinic acid 10-15%；Natural glycine betaine 3-5%；Thickening agent 0-1%；Proteinase-10-1%；Acid-alkali accommodation
Agent 1-2%；Plant fragrance quintessence oil 0-1%, deionized water adds to 100%.
The purest plant extract strong dirt-removing cleaning agent, it is characterised in that: accounting for of natural surfactant
Ratio is 32-38%.
The purest plant extract strong dirt-removing cleaning agent, it is characterised in that: described natural surfactant
At least one in APG, oil tea saponin, aescine, Tsubaki-saponin.
The purest plant extract strong dirt-removing cleaning agent, it is characterised in that: described thickening agent is selected from carboxylic first
At least one in base sodium cellulosate, cycloheptaamylose, sodium alginate, carboxymethyl starch sodium, propylene glycol alginate.
The purest plant extract strong dirt-removing cleaning agent, it is characterised in that: described acid-base modifier is selected from
In citric acid, sodium citrate, potassium citrate, sorbic acid, tartaric acid any one.
6. the preparation method of pure plant extract strong dirt-removing cleaning agent as described in arbitrary in claim 1-5, it is characterised in that bag
Include following steps: (1) prepares cleaning agent stock solution: in proportion by thickening agent water mixed dissolution, weigh natural table the most in proportion
Face activating agent, natural glycine betaine stirring and dissolving, mix homogeneously；Weigh the appropriate 95% ethanol stirring and dissolving of cocinic acid in proportion
After, mix homogeneously；Above two mixed liquor is mixed, uniformly mixes under constant temperature；(2) mixture is placed room temperature to lead to
At wind, after natural cooling, weigh citric acid regulation mixed solution pH-value in proportion；Weigh protease in proportion to be dissolved in right amount
In deionized water, two kinds of solution mixing, stir；(3) storage, the inspection of semifinished product, fill, product inspection, warehouse-in.
The preparation method of the purest plant extract strong dirt-removing cleaning agent, it is characterised in that: step (1)
In, described constant temperature is in the range of 70-80 DEG C.
The preparation method of the purest plant extract strong dirt-removing cleaning agent, it is characterised in that: step (2)
In, it is cooled to 45-55 DEG C.
The preparation method of the purest plant extract strong dirt-removing cleaning agent, it is characterised in that: step (2)
In, regulation pH-value is to pH=6 ~ 7.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610645883.0A CN106221967A (en) | 2016-08-08 | 2016-08-08 | A kind of pure plant extract strong dirt-removing cleaning agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610645883.0A CN106221967A (en) | 2016-08-08 | 2016-08-08 | A kind of pure plant extract strong dirt-removing cleaning agent and preparation method thereof |
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| CN201610645883.0A Pending CN106221967A (en) | 2016-08-08 | 2016-08-08 | A kind of pure plant extract strong dirt-removing cleaning agent and preparation method thereof |
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Cited By (4)
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| CN105670834A (en) * | 2016-03-16 | 2016-06-15 | 江西雾源生态农业有限公司 | Application of camellia seed oil in washing product, washing liquid product and preparation method of washing liquid product |
| CN106753825A (en) * | 2016-12-30 | 2017-05-31 | 江阴市本特塞缪森生命科学研究院有限公司 | A kind of composition for cleaning underwear |
| CN108531301A (en) * | 2018-06-08 | 2018-09-14 | 海南侯臣生物科技有限公司 | A kind of natural neutral vegetables and fruits cleaning agent and preparation method thereof |
| CN108587799A (en) * | 2017-12-25 | 2018-09-28 | 北京欧美中科学技术研究院 | A kind of military strong dirt-removing cleaning agent |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105670834A (en) * | 2016-03-16 | 2016-06-15 | 江西雾源生态农业有限公司 | Application of camellia seed oil in washing product, washing liquid product and preparation method of washing liquid product |
| CN106753825A (en) * | 2016-12-30 | 2017-05-31 | 江阴市本特塞缪森生命科学研究院有限公司 | A kind of composition for cleaning underwear |
| CN108587799A (en) * | 2017-12-25 | 2018-09-28 | 北京欧美中科学技术研究院 | A kind of military strong dirt-removing cleaning agent |
| CN108531301A (en) * | 2018-06-08 | 2018-09-14 | 海南侯臣生物科技有限公司 | A kind of natural neutral vegetables and fruits cleaning agent and preparation method thereof |
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Application publication date: 20161214 |