CN112662491A - Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof - Google Patents
Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof Download PDFInfo
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- CN112662491A CN112662491A CN202110133813.8A CN202110133813A CN112662491A CN 112662491 A CN112662491 A CN 112662491A CN 202110133813 A CN202110133813 A CN 202110133813A CN 112662491 A CN112662491 A CN 112662491A
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- soap
- eucommia
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- acne
- oil
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
Abstract
The invention belongs to the technical field of eucommia processing, and particularly relates to acne-removing soap prepared by taking byproducts in eucommia oil refining as raw materials and a preparation method thereof. The invention mainly protects the application of eucommia ulmoides soapstock in the acne-removing soap. The acne-removing soap provided by the invention is prepared by using a byproduct in eucommia bark soapstock refining of eucommia bark oil as a main raw material, and the content of eucommia bark oil in the eucommia bark soapstock is lower than 0.4%. The invention has the beneficial effects that: (1) the raw material adopted by the invention is a byproduct generated in the refining process of the eucommia bark oil, namely the eucommia bark soapstock, the raw material is derived from wastes, the cost of the raw material is low, the raw material is easy to obtain, the raw material is utilized, the waste is changed into valuable, the problems that the eucommia bark soapstock cannot be piled up and buried everywhere are solved, the resource reutilization is realized, and the remarkable economic benefit is generated; (2) the raw materials adopted by the invention, in particular to the eucommia bark soapstock, are sourced from eucommia bark trees, belong to natural raw materials and have small irritation to skin.
Description
Technical Field
The invention belongs to the technical field of eucommia ulmoides processing, and particularly relates to application of eucommia ulmoides nigre in acne-removing soap; also relates to acne-removing soap prepared by taking byproducts in eucommia oil refining as raw materials and a preparation method of the acne-removing soap.
Background
The following patent documents disclose eucommia ulmoides soap:
CN107739670A discloses an eucommia oil soap, which is characterized by comprising the following components in parts by weight: eucommia oil: 30-50 parts of olive oil: 5-20 of eucommia ulmoides leaf extract: 5-20 of aloe vera extract: 2-15 parts of lavender essential oil: 1-10 sodium hydroxide: 5-15 deionized water: 20-30. The eucommia oil soap aims to solve the problems that the prepared eucommia oil soap can deeply clean the face, control oil and preserve moisture, resist bacteria and diminish inflammation, fade color spots, resist aging and the like, and has multiple effects. The soap is prepared from eucommia oil and eucommia extract.
In the above patent documents, the eucommia oil soap is produced mainly from eucommia oil and an extract of eucommia leaves, and the eucommia oil soap is produced from eucommia oil and an extract of eucommia leaves, which are relatively high in cost. Because the eucommia seeds belong to woody oil, the growth period is long, the yield is low, and the oil yield is far lower than that of peanuts, soybeans, corns, rapeseeds and the like, the yield of the eucommia oil is limited, and the cost and the selling price of the eucommia oil are correspondingly high due to high nutritional value of the eucommia oil; although the eucommia ulmoides leaves are abundant and easily obtained, the extract containing the active ingredients can be obtained only by multi-stage filtration such as solvent high-temperature extraction, coarse filtration, horizontal spiral centrifugal filtration, membrane filtration and the like in the production process of the extract, and then membrane concentration and low-temperature spray drying are carried out, so that the production process is complex, the energy consumption is high, and the production cost is high; the active ingredients of the eucommia ulmoides leaf extract belong to heat-sensitive substances, the content of the eucommia ulmoides leaf extract is closely related to the control of process conditions, and the improper control of the process conditions can cause the content of the active ingredients to be greatly reduced and even completely lost. If the eucommia oil and the eucommia leaf extract are used as raw materials to produce the soap, although a certain anti-inflammatory effect can be achieved, the soap does not have practicability and popularization significance based on the cost consideration.
In the extraction and refining processes of eucommia oil, the crude oil can generate a byproduct of nigre during deacidification, at present, the nigre is not processed well, a large amount of space is consumed for storing the eucommia nigre, and alkaline substances added in the deacidification process can pollute soil, so the eucommia nigre cannot be buried at will, and certain hidden danger is brought to clean production. If the soap or perfumed soap is produced by taking the byproduct nigre in the eucommia oil processing process as a raw material, the production cost can be obviously reduced, and the active ingredients in the nigre can be reused by people to play a certain specific role, so that certain effects of cleaning, protecting and the like on the skin are achieved.
There is no disclosure in the literature regarding the soap or soap made from eucommia ulmoides soapstock. The eucommia ulmoides soapstock needs to consume a large amount of space for storage, alkaline substances added in the deacidification process pollute soil, so the eucommia ulmoides soapstock cannot be buried at will, certain hidden dangers are brought to clean production, if the soap which takes the eucommia ulmoides soapstock and the soap base as raw materials can be invented, the cost is low, the stimulation to skin can be reduced as little as possible, the waste is changed into valuable, the material is fully used, the problem of storage of the soap is solved, and great economic benefits can be generated.
Disclosure of Invention
In order to solve the technical problems, the invention provides the soap which is prepared by taking the byproduct generated in the refining process of the eucommia bark oil as the raw material, the soap is prepared from the byproduct, namely the eucommia bark soapstock, which is low in cost and is obtained in the processing process of natural plants, so that the irritation to the skin of a human body is reduced; the soap produced by utilizing the eucommia bark soapstock has obvious acne removing effect;
the invention also provides a preparation method of the eucommia ulmoides soap.
When the inventor researches and develops the invention, just when the applicant conducts the whole industry chain development of eucommia ulmoides, a byproduct namely eucommia ulmoides nigre is generated in the deacidification process in the eucommia ulmoides seed oil refining process, at present, a good treatment mode is not provided for the eucommia ulmoides nigre, a large amount of space is consumed for storing the eucommia ulmoides nigre, and alkaline substances added in the deacidification process pollute soil, so the eucommia ulmoides nigre cannot be buried at will, and certain hidden troubles are brought to clean production.
Therefore, the eucommia ulmoides soap is utilized along the idea of making the best use of the eucommia ulmoides soap, and is processed and utilized by taking the eucommia ulmoides soap stock and the soap base as raw materials through a specific process, so that the eucommia ulmoides soap is invented, and has a remarkable acne removing effect.
Application of cortex Eucommiae nigre in soap for removing acne; and acne-removing soap containing cortex Eucommiae nigre; are all the key points to be protected by the invention.
The invention is realized by the following technical scheme:
the acne-removing soap is characterized in that a byproduct eucommia bark nigre in eucommia bark oil refining is adopted, the dosage of the byproduct eucommia bark nigre is 5-30 parts, and a soap base is adopted: 70-95 parts. The soap of the invention has the efficacy which is not possessed by other common soaps, namely the acne-removing efficacy. In the eucommia ulmoides soapstock, the content of eucommia ulmoides oil is 0.1-0.4%; preferably 0.1%.
The soap is obtained by the steps of: removing oil from cortex Eucommiae soapstock; heating the soap base to melt, placing the eucommia bark soapstock in the melted soap base, uniformly mixing, continuously heating, cooling, shaping and curing to obtain the finished product of the acne-removing soap.
The specific step of removing the grease in the eucommia bark soapstock is to carry out vacuum filtration on the eucommia bark soapstock to remove the redundant grease.
In the step of removing the grease in the eucommia ulmoides soapstock, the vacuum degree is 0.6-0.9 MPa.
The preparation method of the acne-removing soap prepared by taking the byproduct in the refining of the eucommia ulmoides oil as the raw material comprises the following steps:
(1) removing redundant grease in the eucommia bark soapstock by vacuum filtration to obtain the eucommia bark soapstock;
when a laboratory is used for a small test, filter paper is placed in a Buchner funnel, the funnel is placed on a filter flask with a sealing ring, and the filter flask and a vacuum pump are connected by a rubber pipe;
(2) weighing soap base, putting into a beaker, and heating with a digital display constant temperature water bath kettle to melt the soap base;
(3) weighing the filtered eucommia ulmoides soapstock in the step (1) and placing the eucommia ulmoides soapstock in the dissolved soap base in the step (2), and continuously heating to dissolve and uniformly mix the eucommia ulmoides soapstock to obtain a soap solution;
(4) pouring the uniformly mixed soap liquid into a mould, and cooling and shaping the soap liquid;
(5) and taking the cooled and shaped eucommia bark soapstock out of the mould, and curing for 28-32 days in a cool and dry place to obtain the finished product acne removing soap.
(1) And (3) putting the eucommia ulmoides soapstock in vacuum filtration equipment, opening a vacuum pump, and filtering redundant grease in the eucommia ulmoides soapstock.
In a laboratory lab, the specific steps for removing the grease in the eucommia bark soapstock are that filter paper is placed in a Buchner funnel, then the funnel is placed on a filter flask with a sealing ring, and the filter flask is connected with a vacuum pump by a rubber tube;
(2) heating in water bath to 60-70 ℃, and heating in water bath until the soap base is melted;
(3) and continuously heating to 60-70 ℃ until the materials are melted.
More preferably, the acne-removing soap prepared by using byproducts in eucommia oil refining as raw materials comprises the following steps:
(1) removing redundant grease in the eucommia ulmoides soapstock by vacuum filtration, wherein the vacuum degree is 0.6-0.9 MPa during vacuum filtration; performing suction filtration until the oil content in the eucommia ulmoides soapstock is 0.1-0.4%, preferably 0.1%;
(2) putting the soap base into a container, and heating the soap base in a water bath to 60-70 ℃ to melt the soap base;
(3) putting the eucommia ulmoides soapstock in the step (1) into the soap base dissolved in the step (2), continuously heating to 60-70 ℃ until the materials are dissolved, and uniformly mixing to obtain a soap solution;
(4) pouring the uniformly mixed soap liquid into a mould, cooling and shaping;
(5) and (4) taking the eucommia ulmoides soap which is cooled and shaped in the step (4) out of the mold, and curing the eucommia ulmoides soap in a cool and dry place for 28-32 days to obtain the finished product acne removing soap.
According to the invention, effective components in the eucommia bark soapstock are utilized, a reasonable matching ratio of the eucommia bark soapstock and the soap base is explored through a plurality of tests, the preparation process is determined through a series of experiments, and the prepared eucommia bark handmade soap can leave a protective film of natural eucommia bark grease on the skin while properly cleaning the skin, and can fully play the anti-inflammatory role of eucommia bark, so that the handmade soap has the acne removing effect, can clean stains and moisten the skin, and most importantly, the effect of removing acne can be achieved, and the eucommia bark handmade soap is good news of acne muscle crowds.
The acne is caused by various reasons, is not caused by a single inflammatory reason, and has limited effect on acne-growing skin even by adopting anti-inflammatory drugs. The secretion of oil is more, and the oil is easy to block pores when the face is not cleaned frequently, so that the secretion of the oil is not smooth, and further the acne on the face, namely acne on the face, is caused. In addition, if the skin care product is resident in a place with poor air environment quality and high pollution, pollutants in the air are easy to adhere to the skin of the face, and if the skin care product cannot be cleaned in time, the pollutants block pores, and the phenomenon of growing acne is also caused. Therefore, acne can be successfully removed without diminishing inflammation.
The eucommia ulmoides soap provided by the invention has an anti-inflammatory effect, and can play a positive role in promoting the healing of skin repair wounds due to active ingredients contained in eucommia ulmoides soap stock, wherein the effect is achieved by a common anti-inflammatory product. In addition, the eucommia ulmoides soap also has the effects of deeply cleaning and repairing skin.
The invention has the beneficial effects that:
(1) the raw material adopted by the invention is a byproduct generated in the refining process of the eucommia bark oil, namely the eucommia bark soapstock, and the raw material is waste; in the eucommia ulmoides soap in the background art, eucommia ulmoides fine powder is adopted, and is not a byproduct or waste, so that the cost is high;
(2) the raw material adopted by the invention is eucommia bark soapstock which is derived from byproducts in the refining process of natural plant eucommia bark and is not a chemical synthetic product, so that the irritation to the skin is reduced;
(3) the soap prepared by the invention has the cleaning effect of common soap, can leave a protective film of natural eucommia oil on skin, fully exerts the anti-inflammatory effect of eucommia, and has the anti-inflammatory and acne-removing effects at the same time; compared with the common soap, the soap disclosed by the invention has the greatest difference of acne removing effect.
Detailed Description
The present invention will be further described with reference to specific examples so that those skilled in the art may better understand the present invention, but the present invention is not limited thereto.
Eucommia bark soapstock: a byproduct of the deacidification process in the eucommia oil extraction process;
the soap base is a common soap base sold in the market;
example 1
Taking laboratory experiments as an example, the preparation method of the acne-removing soap prepared by taking byproducts in eucommia oil refining as raw materials comprises the following steps:
(1) putting filter paper in a Buchner funnel, putting the funnel on a filter flask with a sealing ring, and connecting the filter flask with a vacuum pump by using a rubber tube; filtering out redundant grease in the eucommia ulmoides soapstock until the grease content in the eucommia ulmoides soapstock is about 0.1%;
(2) putting 20 parts of eucommia ulmoides soapstock into a Buchner funnel, opening a vacuum pump, and filtering redundant grease in the eucommia ulmoides soapstock; setting the vacuum degree of a vacuum pump to be about 0.8 MPa;
(3) 80 parts of soap base, putting into a beaker, and heating by using a digital display constant temperature water bath kettle to melt the soap base; heating in water bath until soap base is melted at 65 deg.C;
(4) putting the weighed and filtered eucommia bark soapstock into the dissolved soap base, and continuously heating to dissolve and uniformly mix the eucommia bark soapstock; the heating temperature is about 65 ℃;
(5) pouring the uniformly mixed soap liquid obtained in the step (4) into a mould, and cooling and shaping the soap liquid;
(6) and (5) taking the eucommia bark soapstock soap which is cooled and shaped in the step (5) out of the mould, and curing the eucommia bark soapstock soap in a cool and dry place for about 30 days to obtain the finished product acne removing soap.
TABLE 1 eucommia ulmoides soap test data in example 1
In example 1 of the present invention, not only the ingredients in the eucommia ulmoides oil were not used, but also the excess oil and fat in the raw material soapstock was filtered off in the process of manufacturing the soap until the oil and fat content was about 0.1%, and it was found that the soap of the present invention utilized not the eucommia ulmoides oil but the active ingredients in the soapstock.
In the preparation method of the eucommia oil soap in the background art, the eucommia oil accounts for 30-50 parts, and the proportion of the eucommia oil is about 31.25-44.1% after conversion. The content of the eucommia ulmoides oil is controlled to be about 0.1%, so that the soap achieves the effect of removing acnes, active ingredients of the eucommia ulmoides oil are not utilized, the cost is greatly reduced compared with the scheme in the background technology, different effects are achieved, the scheme in the background technology only plays a role in diminishing inflammation, and the eucommia ulmoides soap further achieves the effects of deep cleaning and removing acnes.
Example 2
Taking laboratory experiments as an example, the preparation method of the acne-removing soap prepared by taking byproducts in eucommia oil refining as raw materials comprises the following steps:
(1) putting filter paper in a Buchner funnel, putting the funnel on a filter flask with a sealing ring, and connecting the filter flask with a vacuum pump by using a rubber tube;
(2) putting 15 parts of eucommia ulmoides soapstock into a Buchner funnel, opening a vacuum pump, and filtering redundant grease in the eucommia ulmoides soapstock; setting the vacuum degree of a vacuum pump to be 0.6 MPa;
(3) 85 parts of soap base is put into a beaker and heated to about 60 ℃ by a digital display constant temperature water bath kettle to be dissolved;
(4) putting the weighed and filtered eucommia bark soapstock into a dissolved soap base, and continuously heating to about 60 ℃ to dissolve and mix the eucommia bark soapstock evenly;
(5) pouring the uniformly mixed soap liquid obtained in the step (4) into a mould, and cooling and shaping the soap liquid;
(6) and (5) taking the eucommia bark soapstock soap which is cooled and shaped in the step (5) out of the mould, and curing the eucommia bark soapstock soap in a cool and dry place for about 28 days to obtain the finished product acne removing soap.
Example 3
Taking laboratory experiments as an example, the preparation method of the acne-removing soap prepared by taking byproducts in eucommia oil refining as raw materials comprises the following steps:
(1) putting filter paper in a Buchner funnel, putting the funnel on a filter flask with a sealing ring, and connecting the filter flask with a vacuum pump by using a rubber tube;
(2) putting 15 parts of eucommia ulmoides soapstock into a Buchner funnel, opening a vacuum pump, and filtering redundant grease in the eucommia ulmoides soapstock; the vacuum degree of the vacuum pump is set to be 0.9MPa,
(3) 85 parts of soap base is put into a beaker and heated to about 70 ℃ by a digital display constant temperature water bath kettle to be dissolved;
(4) putting the weighed and filtered eucommia bark soapstock into a dissolved soap base, and continuously heating to about 70 ℃ to dissolve and mix the eucommia bark soapstock evenly;
(5) pouring the uniformly mixed soap liquid obtained in the step (4) into a mould, and cooling and shaping the soap liquid;
(6) and (5) taking the eucommia bark soapstock soap which is cooled and shaped in the step (5) out of the mould, and curing the eucommia bark soapstock soap in a cool and dry place for 30 days to obtain the finished product acne removing soap.
Example 4
Taking industrial production as an example, the preparation method of the acne-removing soap prepared by taking byproducts in eucommia oil refining as raw materials comprises the following steps:
(1) placing the eucommia ulmoides soapstock in a vacuum filtration device, and carrying out vacuum filtration under the condition that the vacuum degree is about 0.8 MPa; room temperature; filtering out redundant grease in the eucommia ulmoides soapstock until the grease content in the eucommia ulmoides soapstock is about 0.4%;
(2) weighing soap base, heating in water bath at 65 deg.C for melting;
(3) placing the filtered eucommia ulmoides soapstock in the step (1) into a dissolved soap base, and continuously heating to about 65 ℃ to dissolve and mix the eucommia ulmoides soapstock uniformly;
(4) pouring the uniformly mixed soap liquid into a mould, and cooling and shaping the soap liquid;
(5) taking out the cooled and shaped eucommia bark soap stock soap from the mould, and curing the eucommia bark soap stock soap in a cool and dry place for about 30 days to obtain the finished product acne-removing soap.
Comparative example 1
The inventor adjusts the weight ratio of the soapstock and the soap base in the experimental process, and finds that the weight ratio of the soapstock and the soap base has a relatively obvious influence on the efficacy of the soap.
Taking laboratory experiments as an example, the preparation method of the acne-removing soap prepared by taking byproducts in eucommia oil refining as raw materials comprises the following steps:
(1) putting filter paper in a Buchner funnel, putting the funnel on a filter flask with a sealing ring, and connecting the filter flask with a vacuum pump by using a rubber tube;
(2) putting 1 part of eucommia ulmoides soapstock into a Buchner funnel, opening a vacuum pump, and filtering redundant grease in the eucommia ulmoides soapstock; setting the vacuum degree of the vacuum pump to be about 0.8MPa,
(3) 99 parts of soap base, putting the soap base into a beaker, and heating the soap base by using a digital display constant temperature water bath kettle to melt the soap base; heating in water bath until the soap base is melted at about 65 deg.C;
(4) putting the weighed and filtered eucommia bark soapstock into the dissolved soap base, and continuously heating to dissolve and uniformly mix the eucommia bark soapstock; heating to about 65 ℃;
(5) pouring the uniformly mixed soap liquid obtained in the step (4) into a mould, and cooling and shaping the soap liquid;
(6) and (5) taking the eucommia bark soapstock soap which is cooled and shaped in the step (5) out of the mould, and curing the eucommia bark soapstock soap in a cool and dry place for 28-32 days to obtain the finished product acne-removing soap.
The soap produced by combining the soapstock and the soap base has the acne removing effect when the soap is used by a tester and does not achieve the acne removing effect, which shows that the soap produced by combining the soapstock and the soap base has the acne removing effect when the proportion of the soapstock and the soap base is within a certain range.
Comparative example 2
Likewise, the amounts of soapstock and soap base in comparative example 2 are outside the scope of the present invention; as a result, the soap produced by combining the two has still not ideal acne-removing effect.
Taking laboratory experiments as an example, the preparation method of the acne-removing soap prepared by taking byproducts in eucommia oil refining as raw materials comprises the following steps:
(1) putting filter paper in a Buchner funnel, putting the funnel on a filter flask with a sealing ring, and connecting the filter flask with a vacuum pump by using a rubber tube;
(2) putting 3 parts of eucommia ulmoides soapstock into a Buchner funnel, opening a vacuum pump, and filtering redundant grease in the eucommia ulmoides soapstock; setting the vacuum degree of a vacuum pump to be about 0.8 MPa;
(3) 97 parts of soap base, putting the soap base into a beaker, and heating the soap base by using a digital display constant temperature water bath kettle to melt the soap base; heating in water bath until the soap base is melted at about 65 deg.C;
(4) putting the weighed and filtered eucommia bark soapstock into the dissolved soap base, and continuously heating to dissolve and uniformly mix the eucommia bark soapstock; the heating temperature is about 65 ℃;
(5) pouring the uniformly mixed soap liquid obtained in the step (4) into a mould, and cooling and shaping the soap liquid;
(6) and (5) taking the eucommia bark soapstock soap which is cooled and shaped in the step (5) out of the mould, and curing the eucommia bark soapstock soap in a cool and dry place for 30 days to obtain the finished product acne removing soap.
The acne removing effect is not obvious after the test is carried out.
Comparative example 3
Taking laboratory experiments as an example, the preparation method of the acne-removing soap prepared by taking byproducts in eucommia oil refining as raw materials comprises the following steps:
(1) putting filter paper in a Buchner funnel, putting the funnel on a filter flask with a sealing ring, and connecting the filter flask with a vacuum pump by using a rubber tube;
(2) putting 50 parts of eucommia ulmoides soapstock into a Buchner funnel, opening a vacuum pump, and filtering redundant grease in the eucommia ulmoides soapstock; setting the vacuum degree of the vacuum pump to be about 0.8MPa,
(3) 50 parts of soap base is put into a beaker and heated by a digital display constant temperature water bath kettle to be melted; heating in water bath until the soap base is melted at about 65 deg.C;
(4) putting the weighed and filtered eucommia bark soapstock into the dissolved soap base, and continuously heating to dissolve and uniformly mix the eucommia bark soapstock; the heating temperature is about 65 ℃;
(5) pouring the uniformly mixed soap liquid obtained in the step (4) into a mould, and cooling and shaping the soap liquid;
(6) and (5) taking the eucommia bark soapstock soap which is cooled and shaped in the step (5) out of the mould, and curing the eucommia bark soapstock soap in a cool and dry place for 30 days to obtain the finished product acne removing soap.
The acne removing effect is obvious when the soap is used by a tester, but the soap is too soft and is inconvenient to use.
By people with long acne, the eucommia bark soap stock soap with different proportions has poor acne removing effect when the proportion of the eucommia bark soap stock is less than 5 parts, has good acne removing effect when the proportion of the eucommia bark soap stock is more than 30 parts, but is soft and easy to deform.
From the above comparison, it can be concluded that: the acne-removing soap prepared by the method has the characteristics of good acne-removing effect in a certain proportion range, easiness in forming and no condition that the higher the content of eucommia bark soapstock is, the better the acne-removing soap is.
Example 4
Through the soap prepared by the invention, the inventor verifies the acne removing effect of the soap, and the acne removing effect is as follows:
in the invention, a person with 10 bits of pox is selected, and the basic condition and the using effect of the person with 10 bits of pox are as follows:
use example 1: junxin, male, 50 years old, professional: national enterprise staff; whelk exists on the face, the whelk is grown for more than 30 years, and various acne removing products are used and are ineffective; the soap is used for washing the face once in the morning and at night; the soap of example 1 was continuously used for 7 days, and after 7 days, the face was observed again for whelks, and it was found that: the soap of the invention is basically free from acne when the acne-growing place is dark in color and the acne is dry and flat, and the experiments prove that the soap of the invention has excellent acne-removing effect.
Use example 2: lie somewhere, male, age 27, occupation: a company employee; whelk exists on the face, the whelk is grown for more than 10 years, and the whelk is not effective when other acne removing products are used; the soap in the embodiment 1 of the invention is used for washing the face once in the morning and once in the evening; after 10 days of continuous use, the face was observed again for whelks after 10 days, and it was found that: the soap of the invention is basically free from acne when the acne-growing place is dark in color and the acne is dry and flat, and the experiments prove that the soap of the invention has excellent acne-removing effect.
Use example 3: somersault guo, male, 24 years old, occupation: a company employee; whelk exists on the face, the whelk is grown for more than 10 years, and the whelk is not effective when other acne removing products are used; the soap in the embodiment 1 of the invention is used for washing the face once in the morning and once in the evening; after 10 days of continuous use, the face was observed again for whelks after 10 days, and it was found that: the soap of the invention is basically free from acne when the acne-growing place is dark in color and the acne is dry and flat, and the experiments prove that the soap of the invention has excellent acne-removing effect.
Use example 4: wang certain month, female, 30 years old, occupation: a company employee; whelk exists on the face, the whelk is grown for more than 10 years, and the whelk is not effective when other acne removing products are used; the soap in the embodiment 1 of the invention is used for washing the face once in the morning and once in the evening; after 7 days of continuous use, the face of the patient was observed again for whelk, and it was found that: the soap of the invention is basically free from acne when the acne-growing place is dark in color and the acne is dry and flat, and the experiments prove that the soap of the invention has excellent acne-removing effect.
Use example 5: zhengzhiyang, female, 24 years old, occupational: a company employee; whelk exists on the face, the whelk is grown for more than 10 years, and the whelk is not effective when other acne removing products are used; the soap in the embodiment 1 of the invention is used for washing the face once in the morning and once in the evening; after 7 days of continuous use, the face of the patient was observed again for whelk, and it was found that: the soap of the invention is basically free from acne when the acne-growing place is dark in color and the acne is dry and flat, and the experiments prove that the soap of the invention has excellent acne-removing effect.
Use example 6: spaniansen, male, 24 years old, occupation: a company employee; whelk exists on the face, the whelk is grown for more than 10 years, and the whelk is not effective when other acne removing products are used; the soap in the embodiment 1 of the invention is used for washing the face once in the morning and once in the evening; after 10 days of continuous use, the face was observed again for whelks after 10 days, and it was found that: the soap of the invention is basically free from acne when the acne-growing place is dark in color and the acne is dry and flat, and the experiments prove that the soap of the invention has excellent acne-removing effect.
Use example 7: hades, maid, 24 years old, occupational: a company employee; whelk exists on the face, the whelk is grown for more than 10 years, and the whelk is not effective when other acne removing products are used; the soap in the embodiment 1 of the invention is used for washing the face once in the morning and once in the evening; after 7 days of continuous use, the face of the patient was observed again for whelk, and it was found that: the soap of the invention is basically free from acne when the acne-growing place is dark in color and the acne is dry and flat, and the experiments prove that the soap of the invention has excellent acne-removing effect.
Use example 8: lie, a wisdom, female, 23 years old, occupation: a company employee; whelk exists on the face, the whelk is grown for more than 10 years, and the whelk is not effective when other acne removing products are used; the soap in the embodiment 1 of the invention is used for washing the face once in the morning and once in the evening; after 7 days of continuous use, the face of the patient was observed again for whelk, and it was found that: the soap of the invention is basically free from acne when the acne-growing place is dark in color and the acne is dry and flat, and the experiments prove that the soap of the invention has excellent acne-removing effect.
Use example 9: boy, 36 years old, occupation: a company employee; whelk exists on the face, the whelk is grown for more than 20 years, and the whelk is not effective when other acne removing products are used; the soap in the embodiment 1 of the invention is used for washing the face once in the morning and once in the evening; after 7 days of continuous use, the face of the patient was observed again for whelk, and it was found that: the soap of the invention is basically free from acne when the acne-growing place is dark in color and the acne is dry and flat, and the experiments prove that the soap of the invention has excellent acne-removing effect.
Use example 10: old east, male, 37 years old, occupation: a company employee; whelk exists on the face, the whelk is grown for more than 20 years, and the whelk is not effective when other acne removing products are used; the soap in the embodiment 1 of the invention is used for washing the face once in the morning and once in the evening; after 7 days of continuous use, the face of the patient was observed again for whelk, and it was found that: the soap of the invention is basically free from acne when the acne-growing place is dark in color and the acne is dry and flat, and the experiments prove that the soap of the invention has excellent acne-removing effect.
The product has more number of people to be tried, which is not listed; the inventor summarizes the use of the product of the present invention by the following table, which is specifically shown in table 2 below:
TABLE 2 Change in use
Note: the above control group was a group using a common soap; experiment 1 group (some acne removal product on the market); experiment 2 group: the eucommia ulmoides soap of example 1 of the present invention. Subjects were randomly divided into 3 groups of 20 subjects each; the above products were used separately. The effect thereof after use will be described.
Through the use of the use cases, the eucommia ulmoides soap disclosed by the invention is proved to have a remarkable and satisfactory acne removing effect.
Therefore, the method utilizes byproducts in the processing of eucommia ulmoides products as raw materials, changes waste into valuable, and realizes the comprehensive utilization of resources; the obtained soap is mild and has remarkable anti-inflammatory and acne-removing effects.
Claims (10)
1. Application of cortex Eucommiae nigre in soap for removing acne is provided.
2. The use of claim 1, wherein the eucommia ulmoides soapstock contains 0.1-0.4% of eucommia ulmoides oil; preferably, the eucommia ulmoides oil content in the eucommia ulmoides soapstock is 0.1%.
3. The acne-removing soap contains eucommia ulmoides soapstock as a main raw material, and the content of eucommia ulmoides oil in the eucommia ulmoides soapstock is less than or equal to 0.1%.
4. The acne-removing soap prepared by taking byproducts in eucommia oil refining as raw materials is characterized by comprising the following raw materials in parts by weight: eucommia bark soapstock: 5-30, soap base: 70-95; the eucommia bark soapstock is a byproduct in eucommia bark oil refining.
5. The acne-removing soap made from a by-product of refining eucommia ulmoides oil as claimed in claim 1,
the soap is obtained by the steps of:
removing oil from cortex Eucommiae soapstock; heating the soap base to melt, placing the eucommia bark soapstock with the grease removed in the melted soap base, uniformly mixing, continuously heating, cooling, shaping, and curing to obtain the finished product of the acne-removing soap.
6. The acne-removing soap made from a by-product of refining eucommia ulmoides oil as claimed in claim 5,
the method for removing oil from eucommia bark soapstock comprises the following specific steps of carrying out vacuum filtration on eucommia bark soapstock to remove redundant oil; the eucommia bark soapstock is a byproduct of a deacidification process in the eucommia bark oil extraction and refining process.
7. The acne-removing soap made from a by-product of refining eucommia ulmoides oil as claimed in claim 6,
in the step of removing the grease in the eucommia bark soapstock through vacuum filtration, the vacuum degree is 0.6-0.9 MPa.
8. The acne-removing soap made from by-products of eucommia ulmoides oil refining as claimed in claim 4,
the method comprises the following steps:
(1) removing redundant grease in the eucommia bark soapstock through vacuum filtration;
(2) putting soap base in a container, and heating in water bath to melt the soap base;
(3) putting the eucommia ulmoides soapstock in the step (1) into the soap base dissolved in the step (2), continuously heating and dissolving, and uniformly mixing to obtain a soap solution;
(4) pouring the uniformly mixed soap liquid into a mould, cooling and shaping;
(5) and (4) taking the eucommia ulmoides soap which is cooled and shaped in the step (4) out of the mold, and curing the eucommia ulmoides soap in a cool and dry place for 28-32 days to obtain the finished product acne removing soap.
9. The acne-removing soap made from a by-product of refining eucommia ulmoides oil as claimed in claim 7,
(1) putting the eucommia ulmoides soapstock in vacuum filtration equipment, opening a vacuum pump, and filtering redundant grease in the eucommia ulmoides soapstock;
preferably, in the step (2), heating in water bath to 60-70 ℃ until the soap base is melted;
preferably, in the step (3), the heating is continued to 60-70 ℃ until the material is melted.
10. The acne-removing soap made from a by-product of refining eucommia ulmoides oil as claimed in claim 7,
the method comprises the following steps:
(1) removing redundant grease in the eucommia ulmoides soapstock by vacuum filtration, wherein the vacuum degree is 0.6-0.9 MPa during vacuum filtration; performing suction filtration until the oil content in the eucommia ulmoides soapstock is 0.1-0.4%;
(2) putting the soap base into a container, heating in a water bath to 60-70 ℃ to melt the soap base;
(3) putting the eucommia ulmoides soapstock in the step (1) into the soap base dissolved in the step (2), continuously heating to 60-70 ℃ until the materials are dissolved, and uniformly mixing to obtain a soap solution;
(4) pouring the uniformly mixed soap liquid into a mould, cooling and shaping;
(5) and (4) taking the eucommia ulmoides soap which is cooled and shaped in the step (4) out of the mold, and curing the eucommia ulmoides soap in a cool and dry place for 28-32 days to obtain the finished product acne removing soap.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2020103310804 | 2020-04-24 | ||
| CN202010331080.4A CN111440680A (en) | 2020-04-24 | 2020-04-24 | Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof |
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| CN112662491A true CN112662491A (en) | 2021-04-16 |
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| CN202010331080.4A Withdrawn CN111440680A (en) | 2020-04-24 | 2020-04-24 | Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof |
| CN202110133813.8A Pending CN112662491A (en) | 2020-04-24 | 2021-02-01 | Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202010331080.4A Withdrawn CN111440680A (en) | 2020-04-24 | 2020-04-24 | Acne-removing soap prepared from byproduct in eucommia oil refining and preparation method thereof |
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| CN111440680A (en) | 2020-07-24 |
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