CN110151666A - A kind of ultra micron cleaning mud facial cleanser and preparation method thereof - Google Patents

A kind of ultra micron cleaning mud facial cleanser and preparation method thereof Download PDF

Info

Publication number
CN110151666A
CN110151666A CN201910513092.6A CN201910513092A CN110151666A CN 110151666 A CN110151666 A CN 110151666A CN 201910513092 A CN201910513092 A CN 201910513092A CN 110151666 A CN110151666 A CN 110151666A
Authority
CN
China
Prior art keywords
egg
ultra micron
parts
facial cleanser
extract
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201910513092.6A
Other languages
Chinese (zh)
Other versions
CN110151666B (en
Inventor
张淑云
张灿海
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangzhou Yilumei Cosmetics Co Ltd
Original Assignee
Guangzhou Yilumei Cosmetics Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangzhou Yilumei Cosmetics Co Ltd filed Critical Guangzhou Yilumei Cosmetics Co Ltd
Priority to CN201910513092.6A priority Critical patent/CN110151666B/en
Publication of CN110151666A publication Critical patent/CN110151666A/en
Application granted granted Critical
Publication of CN110151666B publication Critical patent/CN110151666B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/981Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
    • A61K8/982Reproductive organs; Embryos, Eggs
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41Particular ingredients further characterized by their size
    • A61K2800/412Microsized, i.e. having sizes between 0.1 and 100 microns

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Developmental Biology & Embryology (AREA)
  • Reproductive Health (AREA)
  • Zoology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses a kind of ultra micron cleaning mud facial cleanser and preparation method thereof, the ultra micron cleaning mud facial cleanser includes the component of following parts by weight: 5~10 parts of egg-shell meal, 8~15 parts of kaolin, 1~8 part of plant extracts, 1~3 part of anionic surfactant, 3~8 parts of stearic acid, 0.1~1 part of xanthan gum, 0.05~0.5 part of citric acid, 0.3~1 part of Phenoxyethanol and 30~50 parts of deionized water;The plant extracts includes wintergreen extract, honeybee flower extract and Bitter Melon P.E.Facial cleanser of the invention is weakly acidic, the foaming abundancy of generation is careful, easily rinse well, containing with ultra micron mud made of egg-shell meal and kaolin, can mild exfoliating and deeply cleaning pore the effect of, and can adsorb and remove the dirts such as the dust sebum on skin and old waste, it is mildly clean to play the role of deep layer to skin, also contain wintergreen extract, honeybee flower extract and Bitter Melon P.E, can assign skin salubrious feeling when cleaning skin, is moistened using rear skin water not tight.

Description

A kind of ultra micron cleaning mud facial cleanser and preparation method thereof
Technical field
The present invention relates to cosmetic technical field more particularly to a kind of ultra micron cleaning mud facial cleanser and its preparation sides Method.
Background technique
With the raising of people's life and educational level, skin nursing is increasingly by everybody attention, and skin cleans It is the mostly important step of skin nursing.If skin cleaning is not thorough, the dirt remained on skin can block hair follicle, make skin Seem coarse, lackluster, it is also possible to cause acne, pimples or derivative other skin problems.
Facial cleanser belongs to clean skin class cosmetics, and effect is the dirt removed on skin, makes skin refreshing, facilitates skin Keep normal physiological condition.Face's cleaning products at present on the market are many kinds of, and portioned product, for main detergent, is steeped with soap base Foam is abundant, strong detergency, but degreasing use by force after feel to tighten, part emulsifying product property is mild, but clean effect is poor, very Difficulty makes foam abundant, feels greasy after washing.Mildly to wash away therefore, it is necessary to develop a kind of mild safety-type product While dirty, cleaning products are preferably minimized the injury of skin.
Eggshell is porous structure, and it is the high-sequential being mainly made of calcium carbonate and protein that biological safety is high Biological mineral matter.Also containing polysaccharide, amine-galactose, hexosamine, gucosamine, mannose, galactolipin and fructose etc. in eggshell Nutritional ingredient, and contain various trace elements such as zinc, copper, manganese, iron etc..7 kinds of vitamins, lot of trace member can be measured in eggshell Plain and some important enzymes, peptide matters are all nutriments necessary to human body though content is micro-.China is in the world The most country of fowl is supported, egg production is first of the world continuous 20 Nian Ju.However, although there is eggshell resource abundant in China, but Developmental research and recycling to eggshell is unsatisfactory.Eggshell is generally taken as rubbish discarding, not only pollutes environment, also results in The waste of resource.
Summary of the invention
To solve above-mentioned shortcoming and defect existing in the prior art, the purpose of the present invention is to provide a kind of ultra micron is clear Clean mud facial cleanser.Facial cleanser of the invention contains ultra micron mud, can deep layer cleaning skin with excellent absorption property Skin, softening and removal old useless cutin, it is mildly non-stimulated to skin, in addition, facial cleanser of the invention also contains the plant of protection skin Object extract keeps skin water profit after face cleaning not tight.
To realize its purpose, the technical scheme adopted by the invention is as follows:
A kind of ultra micron cleaning mud facial cleanser comprising the component of following parts by weight: 5~10 parts of egg-shell meal, kaolin 8 ~15 parts, 1~8 part of plant extracts, 1~3 part of anionic surfactant, 3~8 parts of stearic acid, 0.1~1 part of xanthan gum, lemon 0.05~0.5 part of lemon acid, 0.3~1 part of Phenoxyethanol and 30~50 parts of deionized water;The plant extracts includes that wintergreen mentions Take object, honeybee flower extract and Bitter Melon P.E.
Kaolin has pearly luster, and quality is soft, and large specific surface area, absorption property is excellent, from a wealth of sources, use cost It is low, it is readily dispersed in water or other liquid.And egg-shell meal calcium component containing high carbon acid and multi-layer microporous structure, it may have excellent Different absorption property can effectively adsorb the dirt on skin, moreover it is possible to adsorbing metal ions.The present invention is with egg-shell meal and kaolin On the one hand eggshell can be carried out waste utilization by main skin cleansing, on the other hand, egg-shell meal has certain hardness, It can play the role of frosted, remove skin dead skin and cuticula, accelerate skin metabolism, the soft kaolinite of quality of being arranged in pairs or groups Soil can reduce egg-shell meal to the irritation of skin, facial cleanser is made to reach soft skin friendly, mild exfoliating, go deep into free wool Pore, the effect for removing old useless cutin and dirt.Meanwhile the present invention also utilizes ultra micron pulverization process technology by egg-shell meal and height Ridge soil ultra micro granulation, further increases egg-shell meal and kaolinic specific surface area, keeps its absorption property stronger, mildness is more Height, while preferable frosted effect is also maintained, easily rinse well.
When dispersing in water due to the granulated egg-shell meal of ultra micro and kaolin again, adhesivity can be shown, is easy agglomeration.Cause This, the present invention joined anionic surfactant in facial cleanser, kaolinic to reduce ultra micron egg-shell meal and ultra micron Adhesivity improves its dispersed homogeneous degree, prevents from agglomerating.
In addition, facial cleanser of the invention also contains including wintergreen extract, honeybee flower extract and Bitter Melon P.E Plant extracts.The extraction source of wintergreen extract is Pyrolaceae plant wintergreen (Pyrola calliantha H.Andr. herb) is a kind of water-soluble extractive.Studies have shown that wintergreen extract have brighten, anti-inflammatory and antibacterial etc. Effect.The extraction source of honeybee flower extract is Lamiaceae plant lemon balm (Melissa axillaris (Benth.) Bakh.f. herb and a kind of water-soluble extractive).Studies have shown that honeybee flower extract has awake skin of refreshing oneself, balance skin Skin oil and other effects.The extraction source of Bitter Melon P.E is the fruit of cucurbitaceous plant balsam pear (Momordica charantiaL.) Real and a kind of water-soluble extractive.Studies have shown that Bitter Melon P.E contains Momordica charantial, glucokinin, balsam pear flavones The nutritional ingredients such as class, bitter melon polysaccharide, organic acid, amino acid, protein and peptides have hypoglycemic, anti-oxidant, antitumor and adjust Save the multiple pharmacological effects such as immune function.The present invention passes through the study found that wintergreen extract, honeybee flower extract and balsam pear mention It takes object to be used in compounding, there are good moisturizing moisturizing effects, be added in facial cleanser, facial cleanser can be made when cleaning skin It assigns skin salubrious feeling, is moistened using rear skin water not tight.
Stearic acid plays the role of stablizing and be emulsified in inventive formulation, and facial cleanser is made to become stable lotion.Xanthan Glue plays thickening power in inventive formulation, so that facial cleanser is had certain consistency, it is promoted to become stable lotion.Lemon Acid plays pH adjustment effect in inventive formulation, keeps facial cleanser weakly acidic, close to the pH value of skin.Phenoxyethanol is a kind of Mildly, the preservative of low sensitization, the bactericidal effect with broad-spectrum high efficacy.Since the plant extracts in inventive formulation also has There is certain bacteriostasis, thus, compounding Phenoxyethanol can play effective antisepsis to facial cleanser.
Preferably, the ultra micron cleaning mud facial cleanser includes the component of following parts by weight: 7~9 parts of egg-shell meal, kaolinite Native 10~13 parts, 4~6 parts of plant extracts, 1.5~2.5 parts of anionic surfactant, 4~6 parts of stearic acid, xanthan gum 0.4 ~0.6 part, 0.2~0.4 part of citric acid, 0.5~0.8 part of Phenoxyethanol and 40~45 parts of deionized water;The plant extracts Including wintergreen extract, honeybee flower extract and Bitter Melon P.E.The present invention is found through experiments that, the facial cleanser of above-mentioned formula Foaming abundancy is fine and smooth, mild non-stimulated, and cleans more excellent with moistening effect.
Most preferably, the ultra micron cleaning mud facial cleanser includes the component of following parts by weight: 8 parts of egg-shell meal, kaolinite Native 12 parts, 5 parts of plant extracts, 2 parts of anionic surfactant, 5 parts of stearic acid, 0.5 part of xanthan gum, 0.3 part of citric acid, benzene 0.6 part and 42 parts of deionized water of oxyethanol.The present invention is found through experiments that the facial cleanser foaming abundancy of above-mentioned formula is fine and smooth, temperature With it is non-stimulated, and clean and moistening effect it is optimal.
Preferably, in the plant extracts, the weight of wintergreen extract, honeybee flower extract and Bitter Melon P.E it Than are as follows: wintergreen extract: honeybee flower extract: Bitter Melon P.E=1:1:(4~8).The present invention is found through experiments that, deer hoof When careless extract, honeybee flower extract and Bitter Melon P.E are compounded with said ratio, moistening effect is more significant.
Most preferably, in the moisture-keeping composition, the weight of wintergreen extract, honeybee flower extract and Bitter Melon P.E The ratio between are as follows: wintergreen extract: honeybee flower extract: Bitter Melon P.E=1:1:6.The present invention is found through experiments that, wintergreen When extract, honeybee flower extract and Bitter Melon P.E are compounded with said ratio, moistening effect is best.
Preferably, the egg-shell meal is the egg-shell meal of birds, beasts and eggs.Preferably, the egg-shell meal is selected from goose egg-shell powder, Ovum Anas domestica putamina At least one of powder, egg shell powder.Most preferably, the egg-shell meal is egg shell powder.Micropore on egg shell is finer and closely woven, and Powder hardness is smaller, it is easier to process, and more preferable to the frosted finish effect of skin, irritation is smaller.
Preferably, the kaolin is white kaolin.White kaolin is one kind most fine in kaolin, quality It is the softest, purity is high.It also has other than with excellent absorption property and alleviates red capillary, softens skin and highlights Colour of skin and other effects.
Preferably, the egg-shell meal and the kaolinic weight ratio are as follows: egg-shell meal: kaolin=(1:2)~(5: 6).The present invention is found through experiments that, when egg-shell meal and kaolin are compounded with said ratio, the cleaning effect of facial cleanser is preferable, and Property is mild, non-stimulated to skin.
Most preferably, the egg-shell meal and the kaolinic weight ratio are as follows: egg-shell meal: kaolin=2:3.The present invention It is found through experiments that, when egg-shell meal and kaolin are compounded with said ratio, the cleaning effect of facial cleanser is best.
Preferably, the anionic surfactant is selected from sodium secondary alkyl sulfonate, sodium sulfate of polyethenoxy ether of fatty alcohol (AES), at least one of AEO carboxylic acid sodium.The anionic surfactant that the present invention uses is green Surfactant, it is environmentally friendly to human temperature and non-stimulated, it can also increase the foaming abundancy of facial cleanser to a certain extent Degree.
The present invention also provides a kind of preparation methods of ultra micron cleaning mud facial cleanser comprising following steps:
(1) egg-shell meal and kaolin are subjected to ultra micron pulverization process respectively, obtain the ultra micro that partial size is respectively 5~10 μm Grain egg-shell meal and ultra micron kaolin;
(2) appropriate amount of deionized water dissolved anion surfactant is used, ultra micron kaolin and ultra micron egg is then added Shell powder, stirs evenly, and stands swelling, obtains ultra micron mud;
(3) by wintergreen extract, honeybee flower extract, Bitter Melon P.E, xanthan gum, citric acid and remaining deionization Water mixes, and heating stirring obtains water phase to dissolving at 35~45 DEG C;
(4) stearic acid and Phenoxyethanol are mixed, is heated to dissolving, be then added in water phase, be uniformly dispersed, then while hot It is added the ultra micron mud of step (1), homogeneous cleans mud to get the ultra micron to obtaining the fine and smooth uniform emulsifiable paste shape of quality Facial cleanser.
The present invention also provides a kind of application methods of ultra micron cleaning mud facial cleanser comprising following steps: After drenching face with warm water, the product of 2cm or so is taken, face is applied to after adding water to blister, massage washes with water clean in a moment.
Compared with prior art, the invention has the benefit that
1, facial cleanser of the invention carries out waste eggshell using egg-shell meal and kaolin as major skin cleansing The problem of efficiently using, alleviating environmental pollution and the wasting of resources;
2, facial cleanser of the invention contains with ultra micron mud made of egg-shell meal and kaolin, soft skin friendly, Have effects that mild exfoliating and deeply clean pore, can adsorb and remove dust, harmful substance, the sebum on skin And the dirts such as old waste, it is mildly clean to play the role of deep layer to skin;
3, facial cleanser of the invention contains the plant including wintergreen extract, honeybee flower extract and Bitter Melon P.E and mentions Object is taken, can assign skin salubrious feeling when cleaning skin, is moistened using rear skin water not tight;
4, facial cleanser of the invention is weakly acidic, and the foaming abundancy of generation is careful, easily rinses well, can mildly clean flesh Skin, the materials safety of use, green are safe to the human body harmless, environmentally friendly.
Detailed description of the invention
Fig. 1 is the facial cleanser of Examples 1 to 5 and comparative example 1~2 to the cleaning effect figure of skin.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, the present invention passes through the following example furtherly It is bright.Obviously, the following example is only a part of the embodiments of the present invention, instead of all the embodiments.It should be understood that the present invention is real It applies example and is merely to illustrate technical effect of the invention, protection scope and is not intended to limit the present invention.
Embodiment 1
A kind of ultra micron cleaning mud facial cleanser, is grouped as by the group of following parts by weight: 8 parts of egg shell powder, white are high Ridge soil 12 parts, 5 parts of plant extracts, 2 parts of sodium secondary alkyl sulfonate, 5 parts of stearic acid, 0.5 part of xanthan gum, 0.3 part of citric acid, benzene oxygen 0.6 part and 42 parts of deionized water of ethyl alcohol.The plant extracts is by wintergreen extract, honeybee flower extract and Bitter Melon P.E Composition, and the weight ratio of wintergreen extract, honeybee flower extract and Bitter Melon P.E are as follows: wintergreen extract: lemon balm Extract: Bitter Melon P.E=1:1:6.
The preparation method of the ultra micron cleaning mud facial cleanser, includes the following steps:
(1) egg shell powder and white kaolin are subjected to ultra micron pulverization process with ultra micron pulverizer, obtain partial size point Ultra micron egg-shell meal and ultra micron kaolin that Wei be 5~10 μm;
(2) sodium secondary alkyl sulfonate is dissolved with appropriate amount of deionized water, ultra micron kaolin and ultra micron egg-shell meal is then added, It stirs evenly, stands 30min, make its swelling, obtain ultra micron mud;
(3) by wintergreen extract, honeybee flower extract, Bitter Melon P.E, xanthan gum, citric acid and remaining deionization Water mixes, and heating stirring obtains water phase to dissolving at 40 DEG C;
(4) stearic acid and Phenoxyethanol are mixed, is heated to dissolving, be then added in water phase, be uniformly dispersed, then while hot The ultra micron mud of step (1) is added, homogeneous cleans mud facial cleanser to the cream ultra micron paste is obtained.
Embodiment 2
A kind of ultra micron cleaning mud facial cleanser, is grouped as by the group of following parts by weight: 7 parts of egg shell powder, white are high Ridge soil 10 parts, 4 parts of plant extracts, 2.5 parts of sodium secondary alkyl sulfonate, 6 parts of stearic acid, 0.4 part of xanthan gum, 0.2 part of citric acid, benzene 0.5 part and 40 parts of deionized water of oxyethanol.The plant extracts is extracted by wintergreen extract, honeybee flower extract and balsam pear Object composition, and the weight ratio of wintergreen extract, honeybee flower extract and Bitter Melon P.E are as follows: wintergreen extract: honeybee Flower extract: Bitter Melon P.E=1:1:6.
The preparation method of the ultra micron cleaning mud facial cleanser, includes the following steps:
(1) egg shell powder and white kaolin are subjected to ultra micron pulverization process with ultra micron pulverizer, obtain partial size point Ultra micron egg-shell meal and ultra micron kaolin that Wei be 5~10 μm;
(2) sodium secondary alkyl sulfonate is dissolved with appropriate amount of deionized water, ultra micron kaolin and ultra micron egg-shell meal is then added, It stirs evenly, stands 30min, make its swelling, obtain ultra micron mud;
(3) by wintergreen extract, honeybee flower extract, Bitter Melon P.E, xanthan gum, citric acid and remaining deionization Water mixes, and heating stirring obtains water phase to dissolving at 40 DEG C;
(4) stearic acid and Phenoxyethanol are mixed, is heated to dissolving, be then added in water phase, be uniformly dispersed, then while hot The ultra micron mud of step (1) is added, homogeneous cleans mud facial cleanser to the cream ultra micron paste is obtained.
Embodiment 3
A kind of ultra micron cleaning mud facial cleanser, is grouped as by the group of following parts by weight: 9 parts of egg shell powder, white are high Ridge soil 13 parts, 6 parts of plant extracts, 1.5 parts of sodium secondary alkyl sulfonate, 4 parts of stearic acid, 0.6 part of xanthan gum, 0.4 part of citric acid, benzene 0.8 part and 45 parts of deionized water of oxyethanol.The plant extracts is extracted by wintergreen extract, honeybee flower extract and balsam pear Object composition, and the weight ratio of wintergreen extract, honeybee flower extract and Bitter Melon P.E are as follows: wintergreen extract: honeybee Flower extract: Bitter Melon P.E=1:1:6.
The preparation method of the ultra micron cleaning mud facial cleanser, includes the following steps:
(1) egg shell powder and white kaolin are subjected to ultra micron pulverization process with ultra micron pulverizer, obtain partial size point Ultra micron egg-shell meal and ultra micron kaolin that Wei be 5~10 μm;
(2) sodium secondary alkyl sulfonate is dissolved with appropriate amount of deionized water, ultra micron kaolin and ultra micron egg-shell meal is then added, It stirs evenly, stands 30min, make its swelling, obtain ultra micron mud;
(3) by wintergreen extract, honeybee flower extract, Bitter Melon P.E, xanthan gum, citric acid and remaining deionization Water mixes, and heating stirring obtains water phase to dissolving at 42 DEG C;
(4) stearic acid and Phenoxyethanol are mixed, is heated to dissolving, be then added in water phase, be uniformly dispersed, then while hot The ultra micron mud of step (1) is added, homogeneous cleans mud facial cleanser to the cream ultra micron paste is obtained.
Embodiment 4
A kind of ultra micron cleaning mud facial cleanser, is grouped as by the group of following parts by weight: 5 parts of egg shell powder, white are high Ridge soil 8 parts, 1 part of plant extracts, 1 part of sodium sulfate of polyethenoxy ether of fatty alcohol, 3 parts of stearic acid, 1 part of xanthan gum, citric acid 0.05 part, 0.3 part of Phenoxyethanol and 30 parts of deionized water.The plant extracts is by wintergreen extract, honeybee flower extract It is formed with Bitter Melon P.E, and the weight ratio of wintergreen extract, honeybee flower extract and Bitter Melon P.E are as follows: wintergreen mentions Take object: honeybee flower extract: Bitter Melon P.E=1:1:6.
The preparation method of the ultra micron cleaning mud facial cleanser, includes the following steps:
(1) egg shell powder and white kaolin are subjected to ultra micron pulverization process with ultra micron pulverizer, obtain partial size point Ultra micron egg-shell meal and ultra micron kaolin that Wei be 5~10 μm;
(2) appropriate amount of deionized water dissolved fat alcohol polyethenoxy ether sodium sulfate is used, ultra micron kaolin is then added and is surpassed Particle egg-shell meal, stirs evenly, and stands 30min, makes its swelling, obtain ultra micron mud;
(3) by wintergreen extract, honeybee flower extract, Bitter Melon P.E, xanthan gum, citric acid and remaining deionization Water mixes, and heating stirring obtains water phase to dissolving at 35 DEG C;
(4) stearic acid and Phenoxyethanol are mixed, is heated to dissolving, be then added in water phase, be uniformly dispersed, then while hot The ultra micron mud of step (1) is added, homogeneous cleans mud facial cleanser to the cream ultra micron paste is obtained.
Embodiment 5
A kind of ultra micron cleaning mud facial cleanser, is grouped as by the group of following parts by weight: 10 parts of egg shell powder, white are high Ridge soil 15 parts, 8 parts of plant extracts, 3 parts of AEO carboxylic acid sodium, 8 parts of stearic acid, 0.1 part of xanthan gum, citric acid 0.5 part, 1 part of Phenoxyethanol and 50 parts of deionized water.The plant extracts is by wintergreen extract, honeybee flower extract and hardship Melon extract composition, and the weight ratio of wintergreen extract, honeybee flower extract and Bitter Melon P.E are as follows: wintergreen is extracted Object: honeybee flower extract: Bitter Melon P.E=1:1:6.
The preparation method of the ultra micron cleaning mud facial cleanser, includes the following steps:
(1) egg shell powder and white kaolin are subjected to ultra micron pulverization process with ultra micron pulverizer, obtain partial size point Ultra micron egg-shell meal and ultra micron kaolin that Wei be 5~10 μm;
(2) appropriate amount of deionized water dissolved fat alcohol polyoxyethylene ether carboxylic acid sodium is used, ultra micron kaolin is then added and is surpassed Particle egg-shell meal, stirs evenly, and stands 30min, makes its swelling, obtain ultra micron mud;
(3) by wintergreen extract, honeybee flower extract, Bitter Melon P.E, xanthan gum, citric acid and remaining deionization Water mixes, and heating stirring obtains water phase to dissolving at 45 DEG C;
(4) stearic acid and Phenoxyethanol are mixed, is heated to dissolving, be then added in water phase, be uniformly dispersed, then while hot The ultra micron mud of step (1) is added, homogeneous cleans mud facial cleanser to the cream ultra micron paste is obtained.
Comparative example 1
A kind of facial cleanser is grouped as by the group of following parts by weight: 5 parts of plant extracts, 2 parts of sodium secondary alkyl sulfonate, hard 5 parts of resin acid, 0.5 part of xanthan gum, 0.3 part of citric acid, 0.6 part of Phenoxyethanol and 42 parts of deionized water.The plant extracts by Wintergreen extract, honeybee flower extract and Bitter Melon P.E composition, and wintergreen extract, honeybee flower extract and balsam pear mention Take the weight ratio of object are as follows: wintergreen extract: honeybee flower extract: Bitter Melon P.E=1:1:6.Preparation method is referring to implementation Example 1.
Comparative example 2
A kind of facial cleanser is grouped as by the group of following parts by weight: 8 parts of egg shell powder, 12 parts of white kaolin, secondary alkyl 2 parts of sodium sulfonate, 5 parts of stearic acid, 0.5 part of xanthan gum, 0.3 part of citric acid, 0.6 part of Phenoxyethanol and 42 parts of deionized water.Preparation Method is referring to embodiment 1.
Experimental example
The facial cleanser of Examples 1 to 5 and comparative example 1~2 is evaluated and tested, evaluation and test project includes mildness (patch examination Test), quality/foam, pH value, cleaning effect and moisturizing degree (skin water before skin moisture content-face cleaning after moisturizing degree=face cleaning Divide content, moisture content is measured using skin moisture detector).The evaluating method of cleaning effect are as follows: apply the lipstick on skin On, it is applied to after suitable facial cleanser is blistered with water on the skin of lipstick, after massaging 30s, is rinsed with water clean, observation lip Remaining situation after cream is cleaned.Evaluation result see the table below 1 and attached drawing 1.
The evaluation result of 1 facial cleanser of table
It can be seen that from evaluation result, facial cleanser of the invention is weakly acidic, the weak acid environment of skin can be protected, to skin Mild non-stimulated, the foaming abundancy of generation can effectively clear the lipstick on skin, and dirt-removing power is strong, and moisture retention is good, the energy after Keep skin water profit not tight.It is preferable with the comprehensive performance of Examples 1 to 3 in above-mentioned evaluation and test sample, and embodiment 1 is comprehensive Can be best, therefore, optimization formula of the present invention using embodiment 1 as facial cleanser.Comparing embodiment 1 and comparative example 1 are it is found that comparison The lipstick of example 1 remains the clean skin effect for obviously illustrating that the addition of egg shell powder and white kaolin can be obviously improved facial cleanser.Than Compared with embodiment 1 and comparative example 2 it is found that the moisturizing degree of comparative example 2 significantly reduces, illustrate wintergreen extract, honeybee flower extract The moistening effect of facial cleanser can be obviously improved with the addition of Bitter Melon P.E.
For probe into the group of the plant extracts be grouped as and each component between with compare facial cleanser moistening effect shadow It rings, designs the test group of table 2.
2 test group of table
The test group of table 2 is prepared into facial cleanser according to the formula and preparation method of embodiment 1, then tests each facial cleanser Moisturizing degree, test result are shown in Table 3.
The moisturizing degree of 3 facial cleanser of table
From the test result of upper table it is found that compared in wintergreen extract, honeybee flower extract and Bitter Melon P.E Any one, the compounding of wintergreen extract, honeybee flower extract and Bitter Melon P.E can be obviously improved the moisture retention of facial cleanser Energy.Moreover, wintergreen extract: honeybee flower extract: Bitter Melon P.E=1:1:(4~8) when moistening effect it is more significant, deer hoof Careless extract: honeybee flower extract: moistening effect is most significant when Bitter Melon P.E=1:1:6.
To probe into the influence with the mildness and cleaning effect for comparing facial cleanser between egg-shell meal and kaolin, table is designed 4 test group.
4 test group of table
Facial cleanser is prepared according to the egg-shell meal and kaolinic dosage of each test group in table 4, remaining component and preparation method According to embodiment 1, the cleaning effect and mildness of each facial cleanser are then evaluated and tested, test method is commented referring to experimental example, cleaning effect Price card standard is shown in Table 5, and evaluation result is shown in Table 6.
5 cleaning effect evaluation criterion of table
Opinion rating Standard
No lipstick residual Lipstick naked eyes on skin are invisible
There is micro lipstick to remain Lipstick naked eyes on skin are as it can be seen that but unobvious
There is a small amount of lipstick to remain Lipstick naked eyes on skin are as it can be seen that and obvious
The evaluation result of 6 facial cleanser of table
From the test result of upper table it is found that the cleaning effect and mildness of test group 2~4 are preferable, the cleaning of test group 1 is imitated Fruit is slightly inferior, but mildness is still fine, and the cleaning effect and mildness of test group 5 are all slightly inferior.Illustrate, the powder hardness of eggshell Larger, if egg-shell meal accounting is excessive, the cleaning effect and mildness that will affect facial cleanser also can if the accounting of egg-shell meal is very few Influence the cleaning effect of facial cleanser.And egg-shell meal: when kaolin=(1:2)~(5:6), the cleaning effect and mildness of facial cleanser All preferably, reach balance.Egg-shell meal: when kaolin=2:3, the cleaning effect of facial cleanser is best.
Finally it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention The limitation of range, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should be managed Solution, can with modification or equivalent replacement of the technical solution of the present invention are made, without departing from technical solution of the present invention essence and Range.

Claims (10)

1. a kind of ultra micron cleans mud facial cleanser, which is characterized in that the component including following parts by weight: 5~10 parts of egg-shell meal, 8~15 parts of kaolin, 1~8 part of plant extracts, 1~3 part of anionic surfactant, 3~8 parts of stearic acid, xanthan gum 0.1 ~1 part, 0.05~0.5 part of citric acid, 0.3~1 part of Phenoxyethanol and 30~50 parts of deionized water;The plant extracts includes Wintergreen extract, honeybee flower extract and Bitter Melon P.E.
2. ultra micron as described in claim 1 cleans mud facial cleanser, which is characterized in that the facial cleanser includes following weight The component of part: 8 parts of egg-shell meal, 12 parts of kaolin, 5 parts of plant extracts, 2 parts of anionic surfactant, 5 parts of stearic acid, Huang 0.5 part of virgin rubber, 0.3 part of citric acid, 0.6 part of Phenoxyethanol and 42 parts of deionized water.
3. ultra micron as described in claim 1 cleans mud facial cleanser, which is characterized in that in the plant extracts, deer hoof The weight ratio of careless extract, honeybee flower extract and Bitter Melon P.E are as follows: wintergreen extract: honeybee flower extract: balsam pear Extract=1:1:(4~8).
4. ultra micron as claimed in claim 3 cleans mud facial cleanser, which is characterized in that in the moisture-keeping composition, deer hoof The weight ratio of careless extract, honeybee flower extract and Bitter Melon P.E are as follows: wintergreen extract: honeybee flower extract: balsam pear Extract=1:1:6.
5. ultra micron as described in claim 1 cleans mud facial cleanser, which is characterized in that the egg-shell meal is the eggshell of birds, beasts and eggs Powder;Preferably, the egg-shell meal is selected from least one of goose egg-shell powder, duck egg powder, egg shell powder;Most preferably, described Egg-shell meal is egg shell powder.
6. ultra micron as described in claim 1 cleans mud facial cleanser, which is characterized in that the kaolin is white kaolinite Soil.
7. ultra micron as described in claim 1 cleans mud facial cleanser, which is characterized in that the egg-shell meal and the kaolin Weight ratio are as follows: egg-shell meal: kaolin=(1:2)~(5:6).
8. ultra micron as claimed in claim 7 cleans mud facial cleanser, which is characterized in that the egg-shell meal and the kaolin Weight ratio are as follows: egg-shell meal: kaolin=2:3.
9. ultra micron as described in claim 1 cleans mud facial cleanser, which is characterized in that the anionic surfactant choosing From at least one of sodium secondary alkyl sulfonate, sodium sulfate of polyethenoxy ether of fatty alcohol, AEO carboxylic acid sodium.
10. a kind of preparation method of ultra micron cleaning mud facial cleanser as described in any one of claims 1 to 9, feature exist In including the following steps:
(1) egg-shell meal and kaolin are subjected to ultra micron pulverization process respectively, obtain the ultra micron egg that partial size is respectively 5~10 μm Shell powder and ultra micron kaolin;
(2) appropriate amount of deionized water dissolved anion surfactant is used, ultra micron kaolin and ultra micron egg-shell meal is then added, It stirs evenly, stands swelling, obtain ultra micron mud;
(3) wintergreen extract, honeybee flower extract, Bitter Melon P.E, xanthan gum, citric acid and remaining deionized water are mixed It closes, heating stirring obtains water phase to dissolving at 35~45 DEG C;
(4) stearic acid and Phenoxyethanol are mixed, is heated to dissolving, be then added in water phase while hot, be uniformly dispersed, be then added The ultra micron mud of step (1), homogeneous clean mud facial cleanser to the cream ultra micron paste is obtained.
CN201910513092.6A 2019-06-13 2019-06-13 Ultra-fine particle cleaning slurry facial cleanser and preparation method thereof Active CN110151666B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910513092.6A CN110151666B (en) 2019-06-13 2019-06-13 Ultra-fine particle cleaning slurry facial cleanser and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910513092.6A CN110151666B (en) 2019-06-13 2019-06-13 Ultra-fine particle cleaning slurry facial cleanser and preparation method thereof

Publications (2)

Publication Number Publication Date
CN110151666A true CN110151666A (en) 2019-08-23
CN110151666B CN110151666B (en) 2022-05-06

Family

ID=67628927

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910513092.6A Active CN110151666B (en) 2019-06-13 2019-06-13 Ultra-fine particle cleaning slurry facial cleanser and preparation method thereof

Country Status (1)

Country Link
CN (1) CN110151666B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110893159A (en) * 2019-12-03 2020-03-20 山东中医药大学 Traditional Chinese medicine mask with heat-clearing and detoxifying effects and preparation method thereof
CN113908101A (en) * 2021-11-09 2022-01-11 广州大唐化妆品有限公司 Anti-dandruff composition containing ginger granules and application thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1074824A (en) * 1992-01-27 1993-08-04 南京大学 Egg-shell emulsion and preparation method thereof and purposes
CN101191047A (en) * 2006-12-01 2008-06-04 上海宇盛科技有限公司 Application of eggshell in preparing friction agent
CN103599012A (en) * 2013-10-25 2014-02-26 徐花 Whitening and spot removing facial cleanser

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1074824A (en) * 1992-01-27 1993-08-04 南京大学 Egg-shell emulsion and preparation method thereof and purposes
CN101191047A (en) * 2006-12-01 2008-06-04 上海宇盛科技有限公司 Application of eggshell in preparing friction agent
CN103599012A (en) * 2013-10-25 2014-02-26 徐花 Whitening and spot removing facial cleanser

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110893159A (en) * 2019-12-03 2020-03-20 山东中医药大学 Traditional Chinese medicine mask with heat-clearing and detoxifying effects and preparation method thereof
CN110893159B (en) * 2019-12-03 2022-05-27 山东中医药大学 Traditional Chinese medicine mask with heat-clearing and detoxifying effects and preparation method thereof
CN113908101A (en) * 2021-11-09 2022-01-11 广州大唐化妆品有限公司 Anti-dandruff composition containing ginger granules and application thereof

Also Published As

Publication number Publication date
CN110151666B (en) 2022-05-06

Similar Documents

Publication Publication Date Title
CN105267085B (en) Skin makeup mildy wash and preparation method thereof
CN109528523B (en) Amino acid facial cleanser
CN106265360B (en) A kind of facial cleanser of the product containing fermentation of seaweed and preparation method thereof
CN104173250B (en) Skin-nourishing liquid soap containing natural bacteriostatic components and preparation method thereof
CN110420152A (en) A kind of salubrious mild double-deck make up remover and preparation method thereof
CN107638362A (en) A kind of amino acid mildy wash based on hydrolysis shell nacre powder and preparation method thereof
CN105476950B (en) Moisturizing foam mildy wash and preparation method thereof
CN108815054B (en) Bath lotion and preparation method thereof
CN103637940A (en) Shower gel
CN101011319A (en) Mineral salt shampoo
CN111265439A (en) Oil-control, dandruff-removing and itching-relieving shampoo and preparation method thereof
CN109044935A (en) A kind of mildly clean micella makeup remover and its production technology
CN107982086A (en) One kind makeup removing gel and preparation method thereof
CN105687054A (en) Addition-free facial cleansing powder and preparation method thereof
CN110151666A (en) A kind of ultra micron cleaning mud facial cleanser and preparation method thereof
CN109528562A (en) A kind of ozone wire drawing cleansing mousse of use in personal care and preparation method thereof
CN109394619A (en) A kind of composition and its preparation method and application of anti-scalp and hair aging
JP4551053B2 (en) Moisturizing plant extract and moisturizing external preparation, cosmetic, bath preparation and detergent composition containing the extract
KR101908408B1 (en) A cosmetic composition for skin desquamation comprising spicule powder and natural powder
CN103340764A (en) Shampoo containing tea seed cake extract and preparation method thereof
CN106635563A (en) Weak acid crystal soap for skin health and purification
CN109512764A (en) Natural plants ferment essence hydrosol and the preparation method and application thereof
JP4072594B2 (en) Oxidized active oxygen scavenger composition for hair
CN105476895B (en) A kind of hair-washing composition containing lotus active constituent
CN104146931A (en) Natural nourishment and maintenance type hair conditioner and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant