CN103571657A - Natural soap for removing poxes as well as preparation method thereof - Google Patents

Natural soap for removing poxes as well as preparation method thereof Download PDF

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CN103571657A
CN103571657A CN 201310507097 CN201310507097A CN103571657A CN 103571657 A CN103571657 A CN 103571657A CN 201310507097 CN201310507097 CN 201310507097 CN 201310507097 A CN201310507097 A CN 201310507097A CN 103571657 A CN103571657 A CN 103571657A
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oil
natural
soap
liquor
skin
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CN 201310507097
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CN103571657B (en )
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朱建华
李胜利
杨欢欢
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朱建华
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Abstract

The invention discloses a natural soap for removing poxes as well as a preparation method thereof. The natural soap contains the following substances: shea butter, canola oil, corn oil, coconut oil, sweet almond oil, palm oil, beewax, linseed oil, sodium hydroxide, distilled water, sucrose, absolute ethyl alcohol, glycerol, walnut oil, camellia oleosa seed oil, chrysanthemum indicum extracting liquor, polygonum cuspidatum extracting liquor and salviae miltiorrhizae extracting liquor. Compared with the prior art, the natural soap disclosed by the invention is appropriate in hardness, rich in foams, good in stability, fragrant in smell, semitransparent, fine and uniform. The components are matched and combined to supplement with each other, and cooperate with each other to achieve effects of preventing and treating whelks. Meanwhile, skin nutrient substances are provided to achieve the effects of deeply nourishing, whitening skin primarily and repairing damaged skin secondly.

Description

一种除痘的天然烏及其制备方法 Natural black and preparation method Chudou

技术领域 FIELD

[0001] 本发明涉及一种化妆品及其制备方法,特别涉及一种除痘的天然皂及其制备方法。 [0001] The present invention relates to a cosmetic preparation method thereof, particularly to a natural soap Chudou their preparation.

背景技术 Background technique

[0002] 青春痘[学名痤疮(acne),中医称之为“粉刺”]是一种毛囊皮脂腺的慢性炎症性皮肤病,大约累及85%左右的青少年及50%以上的成年人。 [0002] Acne [Name of acne (Acne), Chinese medicine called "acne"] is a chronic inflammatory skin disease follicular sebaceous glands, involving about 85% of the young people and 50% of the adult. 该病往往病程较长,有的可延续数年,或反复发作,严重的影响到患者的面容及心身健康。 The disease is often longer course, some may continue for several years, or recurrent, severe impact on the patient's face and physical and mental health.

[0003] 青春痘(痤疮)发病原因比较复杂,主要与雄激素、皮脂分泌增多、毛囊皮脂腺导管异常角化、痤疮丙酸杆菌增殖及遗传等因素有关。 [0003] acne (acne) causes complicated, mainly androgens, increased secretion of sebum, abnormal keratinization pilosebaceous duct, the proliferation of Propionibacterium acnes and other genetic factors. 部分患者的发病还与免疫、使用化妆品、饮食刺激和内分泌紊乱等因素有关。 The incidence of some patients is also associated with immunization, use of cosmetics, diet stimulation and endocrine disorders and other factors. 金黄色葡萄球菌的皮肤感染亦与青春痘发病有密切关系。 Staphylococcus aureus skin infections also closely related to the pathogenesis of acne. 临床报道采用单味中药、中药复方水煎液外洗治疗青春痘取得很好疗效。 Clinical reports using single herb, outside the compound decoction of traditional Chinese medicine treatment of acne wash to obtain good results. 体外抑菌试验证实部分清热燥湿、清热解毒、活血化瘀类等中药及其有效成分对痤疮丙酸杆菌、金黄色葡萄球菌等有抑制作用。 Antibacterial test confirmed portion dampness heat, detoxification, blood circulation etc. Chinese medicine and its active ingredients inhibit Propionibacterium acnes, Staphylococcus aureus. 为研制一种含中药复方祛痘天然皂的科学性、可操作性提供理论基础及实验依据。 For the development of traditional Chinese medicine containing natural soap acne scientific, operational and provide a theoretical basis for experimental basis.

发明内容 SUMMARY

[0004] 本发明所要解决的第I个技术问题是提供一种新的含有天然成分提取物的除痘的天然皂。 [0004] The present invention solves the technical problem of I is to provide a new natural soap containing natural ingredients of the extract was Chudou.

[0005] 本发明所要解决的第2个技术问题是上述除痘的天然皂的制备方法。 [0005] The present invention is to solve the second technical problem is the preparation of a natural soap Chudou.

[0006] 本发明解决的技术问题是:一种除痘的天然皂,94g除痘的天然皂中含有以下物 [0006] The technical problem underlying the present invention is: A Chudou natural soap, 94g Chudou natural soap containing the following composition

质: quality:

[0007]乳木果油 1-1Og [0007] Shea Butter 1-1Og

芥花油 1-1Og Canola oil 1-1Og

玉米油 1-1Og Corn oil 1-1Og

椰子油 2-19g Coconut oil 2-19g

甜杏仁油 1-1bg Sweet almond oil 1-1bg

棕榈油 8.3-22g Palm oil 8.3-22g

蜂蜡 0.8-1 Ig Beeswax 0.8-1 Ig

亚麻籽油 l-5g Linseed oil l-5g

氢氧化钠 3-8g蒸馏水 l_19ml Distilled water and sodium hydroxide 3-8g l_19ml

蔗糖 6_18g Sucrose 6_18g

无水乙醇 6-20ml Ethanol 6-20ml

甘油 10-2 Oni L Glycerol 10-2 Oni L

核桃油 l-5ml L-5ml walnut oil

油茶籽油 1-5ml Camellia seed oil 1-5ml

菊花提取液 l_5ml Chrysanthemum extract l_5ml

虎杖提取液 1-5ml Polygonum cuspidatum extract 1-5ml

丹参提取液 l-5ml Salvia extract l-5ml

[0008] 所述的菊花提取液通过以下方法制备: [0008] The extract of Chrysanthemum prepared by the following method:

[0009] 称取菊花一定量,置容器中,加热60_85°C,第1次加7-14倍量水,提取l_2h,第2次加5-10倍量水,提取l_2h,第3次加4-8倍量水,提取0.5_lh,每次用3层纱布滤过,合并滤液,加热浓缩至菊花重量的1-4倍体积(g/ml),用3层纱布滤过,待用。 [0009] Chrysanthemum weighed amount, the storage container and heated 60_85 ° C, 1st 7-14 times the amount of water added, extracted l_2h, 2nd 5-10 times the amount of water added, extracted l_2h, 3rd plus 4-8 times the amount of water and extracted 0.5_lh, each with 3 layers of gauze filtration, the combined filtrate was heated and concentrated to 1-4 times the volume (g / ml) by weight of chrysanthemum, with 3 layers of gauze filtration and set aside.

[0010] 所述的丹参提取液通过以下方法制备: [0010] Salvia extract prepared according to the following method:

[0011] 称取丹参一定量,置回流提取器中,加热50-85°C第1次加7-14倍量50_85%乙醇,提取l_2h,第2次加5-10倍量50-85%乙醇,提取l_2h,第3次加4_8倍量50-85%乙醇,提取0.5-lh,每次用3层纱布滤过,合并滤液,加热浓缩至丹参重量的1-4倍体积(g/ml),用3层纱布滤过,待用。 [0011] Salvia amount weighed, placed reflux extractor, heated 50-85 ° C 1st plus an amount equal to 7-14 times 50_85% ethanol, extraction l_2h, 2nd added 5-10 times the amount of 50-85% ethanol, extraction l_2h, 3rd dosage 4_8 times 50-85% ethanol extract 0.5-lh, each with 3 layers of gauze filtration, the combined filtrate was heated and concentrated to a volume of 1-4 times the weight of Salvia miltiorrhiza (g / ml ), with 3 layers of gauze filtration and set aside.

[0012] 所述的虎杖提取液通过以下方法制备: [0012] The Polygonum cuspidatum extract was prepared by the following method:

[0013] 称取虎杖一定量,置回流提取器中,加热60_80°C第1次加6-15倍量50-85%乙醇,提取l_2h,第2次加8-10倍量50-85%乙醇,提取l_2h,第3次加7_12倍量50-85%乙醇,提取l_2h,每次用3层纱布滤过,合并滤液,加热浓缩至虎杖重量的1-5倍体积(g/ml),用3层纱布滤过,待用。 [0013] Polygonum cuspidatum amount weighed, placed reflux extraction vessel heated 60_80 ° C 1st added 6-15 times the amount of 50-85% ethanol, extraction l_2h, 2nd added 8-10 times the amount of 50-85% ethanol, extraction l_2h, 3rd times the amount of 50-85% 7_12 added ethanol extraction l_2h, each with 3 layers of gauze filtration, the combined filtrate was heated and concentrated to 1-5 times the volume (g / ml) by weight of Polygonum cuspidatum, with 3 layers of gauze filtration and set aside.

[0014] 所述的一种除痘的天然皂的制备方法,包括以下步骤: Preparation of [0014] the method of a natural soap Acne, comprising the steps of:

[0015] a)称取椰子油2_19g、棕榈油3_22g、芥花油l_10g、乳木果油l_10g、蜂蜡0.8_llg、玉米油l-10g、甜杏仁油l-16g,亚麻籽油l-5g。 [0015] a) Weigh coconut oil 2_19g, palm oil 3_22g, canola oil l_10g, shea butter l_10g, beeswax 0.8_llg, corn oil l-10g, sweet almond oil l-16g, linseed oil l-5g. 于烧杯中置于60-95°C的水浴锅中让固体油融化,得油溶液A ; 60-95 ° C was placed in the beaker water bath to melt the solid oil allows to obtain an oil solution A;

[0016] b)称取3_8g氢氧化钠于烧杯加入蒸馏水l_19ml,搅拌待其完全溶解,冷却,得溶液B ; [0016] b) was weighed into a beaker of sodium hydroxide was added distilled water 3_8g l_19ml, dissolved completely with stirring, cooled to obtain a solution B;

[0017] c)称取蔗糖6_18g,研成过60-80目筛的细粉;取无水乙醇6_20ml,置于烧杯中,将蔗糖细粉加入烧杯中,搅拌使其溶解; [0017] c) sucrose weighed 6_18g, research into a fine powder through a 60-80 mesh sieve; Anhydrous ethanol 6_20ml, placed in a beaker, sucrose powder into a beaker and dissolved with stirring;

[0018] d)将溶液B在搅拌下呈细流状倒入油溶液A中,边加边搅拌,然后将溶液C加入,加入甘油10-20ml、核桃油l_5ml、油茶籽油l_5ml,菊花提取液l_5ml、虎杖提取液l_5ml、丹参提取液l_5ml,与此同时在模具中加入液状石蜡,涂抹均匀,待用。 [0018] d) Solution B was small streams into the oil solution A, with stirring, and then the solution C was added, with stirring at 10-20ml glycerin, walnut oil l_5ml, camellia oil l_5ml, Chrysanthemum liquid l_5ml, Polygonum cuspidatum extract l_5ml, Salvia miltiorrhiza extract l_5ml, liquid paraffin was added at the same time in the mold, spread evenly, until use. 搅拌5-10分钟,待混合液面划8字能清晰可见时,倒入模中,待其凝固,就可以形成所需要的除痘的天然皂。 Stirring for 5-10 minutes, until the surface of the mixture, 8 draw clearly visible, was poured into the mold and letting it solidify and form the desired Chudou natural soap.

[0019] 本发明中的各种成分如下: [0019] The various components of the present invention are as follows:

[0020] 野菊花含野菊花内酯、野菊花醇、野菊花酮、菊油环酮、顺-螺烯醇醚、当归酰豚草素、当归酰亚菊素、刺槐苷、木樨草素、槲皮素_β-D葡萄糖苷、矢车菊苷、菊黄质、胡萝卜苷、熊果酸、棕榈酸等成分。 [0020] Chrysanthemum indicum lactone-containing chrysanthemum, chrysanthemum alcohols, ketones chrysanthemum, chrysanthenone, cis - spiro enol ether, angelic acid ragweed Su, Su Angelica imide chrysanthemum, locust glycosides, luteolin, quercetin _β-D-glucoside, cyanidin, chrysanthemum zeaxanthin, daucosterol, ursolic acid, palmitic acid and the like. 美容功效清热解毒,疏风平肝。 Cosmetic effect detoxification, Shufeng Pinggan. 本品为外科疮肿要药,针对疔疮、痈疽、丹毒、湿疹、皮炎等,用本品单味或复方水煎内服、或水煎液外洗、或鲜药捣烂外敷治之效果显著。 This product is a surgical sores to the drug, for out-wash boils, carbuncle, erysipelas, eczema, dermatitis, using this single herb or compound decoction taken orally, or decoction, or the effect of fresh drug smashed topical rule significantly. 本品水剂对引起青春痘的致病菌金黄色葡萄球菌等有抑制作用,并有抗炎、抗氧化、解热、增强免疫功能、降压等作用。 The product has to cause acne agent pathogen inhibition of Staphylococcus aureus, and have anti-inflammatory, antioxidant, antipyretic, enhance immune function, blood pressure and the like. 部分临床治疗青春痘疗效较好的内服或外用复方中药中均含野菊花。 Some clinical treatment of acne better efficacy of Chinese Traditional Medicine in internal or external inclusive chrysanthemum. 上述为野菊花外用清洗治疗青春痘有效提供依据。 Chrysanthemum above is effective to provide a topical treatment of acne wash basis. 本品含熊果酸可以有效的抑制皮肤黑色素的生成,有助于美白肌肤。 This product contains ursolic acid can effectively inhibit the formation of melanin in the skin, helps to skin whitening.

[0021] 丹参含丹参酮,隐丹参酮,异丹参酮,异隐丹参酮,丹参醛,丹参酚,原儿茶醛,原儿茶酸,丹参素,维生素Ε,β-谷留醇等。 [0021] Salvia containing tanshinone, Cryptotanshinone, tanshinone isopropyl, isobutyl Cryptotanshinone, Salvia aldehyde, phenol Salvia, protocatechuic aldehyde, protocatechuic acid, Salvia, vitamin Ε, β- valley leaving alcohol. 美容功效活血祛瘀,止痛调经,养血安神,清心除烦,凉血消痈。 Cosmetic effect stasis, menstruation pain, nourishing the nerves, pure heart Chufan, cooling carbuncle. 主治疮痈肿痛,粉刺,酒渣鼻,黧黑斑,瘢痕疙瘩,瘙痒性皮肤病,各种化脓性感染,月经不调,烦燥不寐。 Attending carbuncle sore throat, acne, rosacea, dark spots, keloids, itching of the skin, various purulent infection, irregular menstruation, irritability, insomnia. 丹参主要有效成分丹参酮能抑制中性粒细胞的趋化运动,降低血浆中前列腺素E2 (PGE2)和PGE2的含量,减轻炎症反应,并对多种致病菌如金葡菌、痤疮丙酸杆菌等有抑制作用,长期使用不产生耐药性;并作用于体内的性腺靶器官,调节其激素分泌,维持体内激素平衡,因而在青春痘致病的3个环节都能发挥作用。 Salvia tanshinone main active ingredient capable of inhibiting neutrophil chemotaxis and decreased plasma prostaglandin E2 (PGE2) and PGE2 levels, reduce inflammation, and a variety of pathogenic bacteria such as Staphylococcus aureus, Propionibacterium acnes are inhibited, no resistance to long-term use; gonad and acts on the target organ in the body, which hormone regulation, to maintain the hormone balance, and thus can play a role in the pathogenesis of acne three links. 体外实验证明外用3%丹参酮能明显缩小皮脂腺的体积,通过抑制皮脂腺细胞的增殖或直接抑制脂质合成起作用。 In vitro experiments show that topical tanshinone 3% significantly reduced the volume of the sebaceous glands, proliferation of sebaceous cells by inhibiting the direct inhibition of lipid synthesis or function. 有人发现丹参酮可能通过直接抑制皮脂腺细胞的增殖与脂质合成或间接下调皮脂腺细胞雄激素受体,而具有抗皮脂腺活性的作用,调控油脂分泌,对治疗青春痘有较好效果。 It was found possible tanshinone sebocytes or indirectly androgen receptor downregulation by directly inhibiting lipid synthesis and proliferation of sebocytes, and the role of having anti-sebaceous gland activity, regulation of oil production, a better effect on the treatment of acne. 总之丹参及其有效成分丹参酮内服或外用均是治疗青春痘的要药。 In short Salvia tanshinone and its active ingredients are internal or external to the drug treatment of acne.

[0022] 虎杖含游离蒽醌及蒽醌苷:大黄素,大黄素甲醚,大黄酚。 [0022] Polygonum cuspidatum containing free anthraquinone and anthraquinone glycoside: emodin, emodin, chrysophanol. 蒽苷Α,蒽苷B,迷人醇, [Alpha] anthracene glycosides, anthracene glycosides B, attractive alcohol,

6-羟基芦荟大黄素等。 6-hydroxy-aloe-emodin like. 还含白藜芦醇,虎杖苷,原儿茶酸,右旋儿茶素,β_谷留醇葡萄糖苷等。 Also contains resveratrol, polydatin, protocatechuic acid, D-catechin, β_ Valley remain alcohol-glucoside and so on. 美容功效活血祛瘀,利湿退黄,清热解毒。 Cosmetic effect stasis, dampness jaundice, detoxification. 主治疮疡肿毒,水火烫伤,跌扑损伤,湿疹,银屑病,闭经,风湿痹痛,湿热黄疸等。 Indications sore swollen poison, water and fire burns, injury or flutter, eczema, psoriasis, menopause, rheumatism, hot and humid jaundice. 体外抑菌试验证实:虎杖主要有效成分大黄素对痤疮丙酸杆菌(抑菌圈直径在10_20mm间,属中敏范围)、金黄色葡萄球菌均有抑制作用。 Antibacterial test confirmed: the main active ingredient emodin from Polygonum Propionibacterium acnes (inhibition zone diameter between 10_20mm, genus sensitive range), Staphylococcus aureus was inhibited. 白藜芦醇对顽癣、汗疱状癣的深红色发癣菌、趾间发癣菌有很强的抑菌作用。 Resveratrol Trichophyton tinea of ​​crimson, sweat blister-like ringworm, interdigital ringworm has a strong inhibitory effect. 本品尚有抗炎、止血收敛、抗病毒等作用。 This product is still anti-inflammatory, astringent to stop bleeding, anti-viral effect. 临床证明含虎杖的中药复方内服或外用治疗青春痘均取得较好疗效。 Clinically proven herbal compound containing knotweed internal or external treatment of acne have achieved good results.

[0023] 亚麻籽油不饱和脂肪酸含量高,对皮肤具有优良的亲和力和渗透力,其所含的多种脂肪酸容易被皮肤吸收,用来补充皮肤所需要的脂质成分,修复干性皮肤和由于接触表面活性剂而损伤的皮肤脂肪酸水平,维持和增强皮肤细胞膜及间质的正常结构和功能;同时,亚麻籽油还可以在皮肤表面形成透气保水膜,减弱皮肤深层的水分损失,使皮肤保持湿润、光滑和弹性。 [0023] The high unsaturated fatty acid content of the linseed oil, and has excellent affinity to the skin penetration, it contains various fatty acids readily absorbed by the skin, used to supplement the required lipid component of the skin, and dry skin repair Since fatty acid levels in the skin contacting surfactant damaged, maintain and enhance the skin cell membrane and normal structure and function of interstitial; Meanwhile, linseed oil may also form a breathable film of water retention in the skin surface, reduced moisture loss deep skin, the skin moist, smooth and elastic. 除作为优良的调理剂和保湿剂外,亚麻籽油还有一些特殊的治疗功效,如亚麻籽油可以发挥消炎和抗增生作用,对减轻由紫外线引起的红斑症及炎症反应有很好的效果。 In addition to a good conditioning agents and humectants, but there are some special linseed oil therapeutic efficacy, such as linseed oil may exert anti-inflammatory and antiproliferative action, have a good effect in reducing UV-induced erythema and inflammation . 作为一种稀有的含ω -3脂肪酸的天然植物油,亚麻籽油对一些皮肤缺陷湿疹、痤疮、过敏、皲裂等具有明显的功效,优质冷榨亚麻籽油对于治疗皮肤过敏症、湿疹、皲裂、婴儿尿疹、皮肤烧伤等多种炎症有明显的作用。 As a rare ω -3 fatty acids containing natural vegetable oil, flaxseed oil on some skin defects eczema, acne, allergies, chapped has obvious effect, high-quality cold-pressed flaxseed oil for the treatment of skin allergies, eczema, chapped, baby diaper rash, burns and other skin inflammation have a significant role.

[0024] 核桃油有美容养颜的作用:这是由于核桃油富含人体必需脂肪酸,同时还富含一种与皮肤亲和力很强的角鲨烯。 [0024] walnut oil has beauty effects: This is due to the walnut oil rich in essential fatty acids, also enriched in one strong affinity with the skin of squalene. 这两种物质能迅速被皮肤吸收,能有效保护皮肤的弹性和润泽,能消除面部皱纹,防止肌肤衰老。 Both substances can be quickly absorbed by the skin, can effectively protect the skin's elasticity and moisture, can eliminate facial wrinkles, prevent skin aging.

[0025] 油茶籽油是安全可靠的美容佳品。 [0025] camellia seed oil is safe and reliable beauty to share. 它富含单不饱和脂肪酸和维生素Ε,能抗紫外线,养颜、延缓衰老,民间历来外用于消炎、去肿,有强大的护肤美容的作用,能让皮肤保湿、润滑,防止晒斑和干纹的出现,去除细纹、淡化斑印和妊娠纹,去除面部黄气,对黄褐斑、晒斑很有效果,长期应用使皮肤光滑、润泽。 It is rich in monounsaturated fatty acids and vitamin Ε, resistant to UV, beauty, anti-aging, anti-inflammatory for folk always outside, to the swelling, skin care and beauty have a powerful effect, make the skin moisture, lubrication, prevents sunburn and dry lines appears, remove fine lines, fade spots and stretch marks printed, remove facial yellow gas, chloasma, sunburn very effective, long-term use make the skin smooth and moist.

[0026] 经实验验证,菊花提取液、丹参提取液、虎杖提取液等在护肤、祛痘等方面有很好的协同效果。 [0026] The experiments prove, chrysanthemum extract, Salvia extract, Polygonum cuspidatum extract and the like have a good synergistic effect in skin, acne and the like.

[0027] 控制炎症是控制青春痘的关键环节。 [0027] The control of inflammation is the key to the control of acne. 痤疮丙酸杆菌、促炎症因子、脂质、白三烯Β4、过氧化物酶体增生物激活受体-α及神经因素等均可能与青春痘炎症有关。 P. acnes, pro-inflammatory cytokines, lipids, [beta] 4 leukotriene, receptor peroxisome proliferator-activated -α and neurological factors etc. may be associated with inflammatory acne. 在遵循中医外治原理、中医对青春痘的施治原则并结合临床经验的基础上,筛选中药野菊花、虎杖、丹参配伍组方,具有清热解毒、活血化瘀、美容功效。 On the basis of the principle to follow the Chinese foreign rule, the principles of traditional Chinese medicine and treatment for acne and clinical experience, the screening of Chinese medicine Chrysanthemum, Polygonum cuspidatum, Salvia compatibility group parties, with detoxification, blood circulation, cosmetic effect. 三味中药均有抗炎、抑菌作用(对多种致病菌如金葡菌、痤疮丙酸杆菌等有抑制作用);丹参主要有效成分丹参酮有抗雄激素及温和的雌激素活性,有抗皮脂腺活性的作用,调控油脂分泌。 Shamisen medicine have anti-inflammatory, antibacterial (inhibition variety of pathogens such as Staphylococcus aureus, Propionibacterium acnes); the main active ingredients Salvia Tanshinone antiandrogen and mild estrogenic activity, anti- sebaceous gland activity, regulation of sebum secretion. 三味中药配伍相辅相成,可产生抗炎、抑菌的相互协同作用,并抑制皮脂分泌而控油,在青春痘致病的3个环节都能发挥作用,从而增强疗效。 Shamisen compatibility complementary medicine, interact synergistically produces anti-inflammatory, antibacterial, oil control and inhibition of sebum secretion, can play a role in acne pathogenic link 3, thereby enhancing efficacy. 因此,三味中药提取液与优质制皂基质配伍制成的除痘的天然皂,既便于清洁局部或全身部位,又可长期使用预防青春痘复发;既可抑菌、抗炎、控油而祛痘,又有滋润、美白功效。 Thus, extracts of Chinese medicines Acne shamisen made with high-quality liquid soap natural soap matrix compatibility, either local or systemic sites to facilitate cleaning, but also long-term prevention of recurrence of acne; both antibacterial, anti-inflammatory, and acne Oil , there moisturizing, whitening effect.

[0028] 本发明与现有技术相比,所制成的除痘的天然皂硬度适宜,泡沫丰富,稳定性好,气味芬芳,半透明,细腻均匀。 [0028] Compared with the prior art, Chudou natural soap made of suitable hardness, rich foam, good stability, fragrant, translucent, fine uniform. 方中诸药合用,对于问题性皮肤有显著治疗作用,它能供给皮肤营养物质,使皮肤深层滋养,从而使皮肤更加富有弹性,更加美白。 Various drugs prescription for problem skin have a significant therapeutic effect, it can supply nutrients to the skin, nourish the skin, making the skin more elastic, more whitening. 其成分具有极强的渗透力、供给皮肤均衡的营养,改善微循环功能,深层滋养调理皮肤,改善肤质、肤色,使皮肤更加健康、亮白。 Its composition has a strong penetration, skin balanced nutrition supply, improve microcirculation function, conditioning nourish the skin, improve skin texture, color, make the skin more healthy, white. 总之处方中各成分相辅相成,以滋养皮肤为主,修复皮肤为辅,并且能补充皮肤所需要的各种营养物质,使皮肤得到从内到外的全面调理,逐渐恢复美白光彩。 In short prescription ingredients complement each other, mainly in order to nourish the skin, repair skin supplement, and can add a variety of nutrients required for the skin, the skin to fully recuperate from the inside to the outside, and gradually restore luster white.

具体实施方式 detailed description

[0029] 下面结合实施例对本发明做进一步的描述。 [0029] The following embodiments in conjunction with embodiments of the present invention will be further described. [0030] 本发明的甘油、蜂蜜为市售。 [0030] Glycerol present invention, are commercially available honey.

[0031] 实施例1 [0031] Example 1

[0032] 1.1菊花提取液的制备: [0032] 1.1 Preparation of Chrysanthemum extract:

[0033] 称取菊花20g,置容器中,加热70°C,第1次加7倍量水,提取1.5h,第2次加6倍量水,提取1.2h,第3次加6倍量水,提取lh,每次用3层纱布滤过,合并滤液,加热浓缩至菊花重量的3倍体积(g/ml),用3层纱布滤过,待用。 [0033] Chrysanthemum weighed 20g, the storage container and heated 70 ° C, 1 plus the first seven times the amount of water, extracting 1.5h, 2nd 6 times the amount of water and extracted 1.2H, 3rd plus 6 times water, extraction LH, each with 3 layers of gauze filtration, the combined filtrate was heated and concentrated to 3 volumes (g / ml) by weight of chrysanthemum, with 3 layers of gauze filtration and set aside.

[0034] 1.2丹参提取液的制备: [0034] 1.2 Preparation of Salvia miltiorrhiza extract:

[0035] 称取丹参20g,置回流提取器中,加热65°C,第1次加12倍量75%乙醇,提取1.5h,第2次加8倍量75%乙醇,提取lh,第3次加8倍量75%乙醇,提取lh,每次用3层纱布滤过,合并滤液,加热浓缩至丹参重量的2倍体积(g/ml),用3层纱布滤过,待用。 [0035] Salvia weighed 20g, opposed reflux extractor, heated 65 ° C, 1 plus the first 12-fold amount of 75% ethanol, extraction 1.5h, 2nd 8 times amount 75% ethanol, extraction LH, 3 times 8 times the amount of 75% ethanol, extraction LH, each with 3 layers of gauze filtration, the combined filtrates were concentrated to a heated 2-fold volume (g / ml) by weight of Salvia, with 3 layers of gauze filtration and set aside.

[0036] 1.3虎杖提取液的制备: [0036] 1.3 Preparation of Japanese knotweed extract:

[0037] 称取虎杖35g,置回流提取器中,加热75°C,第1次加12倍量75%乙醇,提取1.2h,第2次加10倍量75%乙醇,提取lh,第3次加8倍量75%乙醇,提取lh,每次用3层纱布滤过,合并滤液,加热浓缩至虎杖重量的3倍体积(g/ml),用3层纱布滤过,待用。 [0037] Polygonum cuspidatum weighed 35g, opposed reflux extractor, heated 75 ° C, 1 plus the first 12-fold amount of 75% ethanol, extraction 1.2H, 2nd with 10 times the amount of 75% ethanol, extraction LH, 3 times 8 times the amount of 75% ethanol, extraction LH, each with 3 layers of gauze filtration, the combined filtrate was heated and concentrated to 3 volumes (g / ml) by weight of Polygonum cuspidatum, with 3 layers of gauze filtration and set aside.

[0038] 1.4 一种除痘的天然皂的制备方法 [0038] 1.4 Preparation of one kind of natural soap Chudou

[0039] a)称取椰子油9g、棕榈油15g、芥花油6g、乳木果油3g、蜂腊0.8g、玉米油5g、甜杏仁油15g、亚麻籽油3g于烧杯中,置于60°C的水浴锅中让固体油融化,得油溶液A ; [0039] a) Weigh coconut oil 9g, palm oil 15g, canola oil 6g, 3g shea butter, beeswax 0.8g, corn oil 5g, sweet almond oil 15g, 3g linseed oil in a beaker, put of 60 ° C water bath for melting solid oil allows to obtain an oil solution a;

[0040] b)称取3g氢氧化钠于烧杯加入蒸馏水16ml,用玻璃棒搅拌待其完全溶解,冷却,得溶液B ; [0040] b) weighed beaker was added 3g of sodium hydroxide in 16ml of distilled water, stirring with a glass rod was dissolved completely, cooled to obtain a solution B;

[0041] c)称取蔗糖9g研成过60目筛的细粉,待用。 [0041] c) 9g of sucrose was weighed and pulverized into a fine powder through a 60 mesh screen and set aside. 取无水乙醇9ml,置烧杯中,将蔗糖细粉加入烧杯中,搅拌使溶解成溶液C ; For anhydrous 9ml, set the beaker, the sucrose powder was added to a beaker and stirred to dissolve into solution C;

[0042] d)将溶液B在搅拌下呈细流状倒入油溶液A中,边加边搅拌,然后将溶液C加入,加入甘油16ml、核桃油4ml、油茶籽油3ml,菊花提取液3ml、虎杖提取液5ml、丹参提取液4ml,与此同时在模具中加入液状石蜡,涂抹均匀,待用。 [0042] d) Solution B was small streams into the oil solution A, with stirring, and then the solution C was added, under stirring 16ml glycerin, walnut oil 4ml, camellia oil 3ml, chrysanthemum extract 3ml , Polygonum cuspidatum extract 5ml, Salvia miltiorrhiza extract 4ml, liquid paraffin was added at the same time in the mold, spread evenly, until use. 搅拌7分钟,待混合液面划8字能清晰可见时,倒入模中,待其凝固,就可以形成所需要的天然皂。 Stirred for 7 minutes until the surface of the mixture, 8 can draw upon clearly visible, was poured into the mold and letting it solidify and form the desired natural soap.

[0043] 实施例2 [0043] Example 2

[0044] 2.1菊花提取液的制备: [0044] 2.1 Preparation of Chrysanthemum extract:

[0045] 称取菊花15g,置容器中,加热65°C,第1次加10倍量水,提取1.5h,第2次加6倍量水,提取1.2h,第3次加6倍量水,提取lh,每次用3层纱布滤过,合并滤液,加热浓缩至菊花重量的4倍体积(g/ml),用3层纱布滤过,待用。 [0045] Chrysanthemum weighed 15g, the storage container and heated 65 ° C, the first time plus 10 times the amount of water, extracting 1.5h, 2nd 6 times the amount of water and extracted 1.2H, 3rd plus 6 times water, extraction LH, each with 3 layers of gauze filtration, the combined filtrate was heated and concentrated to 4 volumes by weight of chrysanthemum (g / ml), with 3 layers of gauze filtration and set aside.

[0046] 2.2丹参提取液的制备: [0046] 2.2 Preparation of Salvia miltiorrhiza extract:

[0047] 称取丹参30g,置回流提取器中,加热65°C,第1次加12倍量70%乙醇,提取lh,第2次加8倍量75%乙醇,提取lh,第3次加8倍量70%乙醇,提取lh,每次用3层纱布滤过,合并滤液,加热浓缩至丹参重量的2倍体积(g/ml),用3层纱布滤过,待用。 [0047] Weigh Salvia 30g, opposed reflux extractor, heated 65 ° C, the first time increment 12 times the 70% ethanol extraction LH, 2nd add 8 times amount 75% ethanol, extraction LH, 3rd 8 times the amount of the 70% ethanol extraction LH, each with 3 layers of gauze filtration, the combined filtrates were concentrated to a heated 2-fold volume (g / ml) by weight of Salvia, with 3 layers of gauze filtration and set aside.

[0048] 2.3虎杖提取液的制备: [0048] 2.3 Preparation of Japanese knotweed extract:

[0049] 称取虎杖30g,置回流提取器中,加热75°C第1次加12倍量70%乙醇,提取1.2h,第2次加10倍量70%乙醇,提取lh,第3次加8倍量70%乙醇,提取lh,每次用3层纱布滤过,合并滤液,加热浓缩至虎杖重量的3倍体积(g/ml),用3层纱布滤过,待用。 [0049] Polygonum cuspidatum weighed 30g, opposed reflux extractor, heated 75 ° C 1st 12 times the amount of added 70% ethanol extraction 1.2H, 2nd plus 10 times the amount of 70% ethanol extraction LH, 3rd 8 times the amount of the 70% ethanol extraction LH, each with 3 layers of gauze filtration, the combined filtrate was heated and concentrated to 3 volumes (g / ml) by weight of Polygonum cuspidatum, with 3 layers of gauze filtration and set aside.

[0050] 2.4 一种除痘的天然皂的制备方法[0051] a)称取椰子油8g、棕榈油17g、芥花油7g、乳木果油3g、蜂腊5g、玉米油5g、甜杏仁油12g、亚麻籽油4g于烧杯中。 [0050] 2.4 Preparation of natural soap of one kind of Acne [0051] a) Weigh coconut oil 8g, 17g palm oil, canola oil 7g, shea butter 3g, beeswax 5g, corn oil 5g, sweet almond oil 12g, 4g linseed oil in a beaker. 置于60°C的水浴锅中让固体油融化,得油溶液A ; Placed in waterbath of 60 ° C to melt so that a solid oil to give an oil solution A;

[0052] b)称取3g氢氧化钠于烧杯加入蒸馏水16ml。 [0052] b) was weighed into a beaker of sodium hydroxide was added 3g of distilled water 16ml. 用玻璃棒轻轻搅拌待其完全溶解,冷却,得溶液B ; Gently stirring with a glass rod was dissolved completely, cooled to obtain a solution B;

[0053] c)称取蔗糖9g研成过60目筛的细粉,待用。 [0053] c) 9g of sucrose was weighed and pulverized into a fine powder through a 60 mesh screen and set aside. 取无水乙醇9ml,置烧杯中,将蔗糖细粉加入烧杯中,搅拌使溶解成溶液C ; For anhydrous 9ml, set the beaker, the sucrose powder was added to a beaker and stirred to dissolve into solution C;

[0054] d)将溶液B在搅拌下呈细流状倒入油溶液A中,边加边搅拌,然后将溶液C加入,加入甘油16ml、核桃油4ml、油茶籽油3ml、菊花提取液4ml、虎杖提取液3ml、丹参提取液5ml,与此同时在模具中加入液状石蜡,涂抹均匀,待用。 [0054] d) Solution B was small streams into the oil solution A, with stirring, was then added to the solution C, was added with stirring 16ml glycerol, 4ml walnut oil, camellia oil 3ml, chrysanthemum extract 4ml , Polygonum cuspidatum extract 3ml, Salvia miltiorrhiza extract 5ml, liquid paraffin was added at the same time in the mold, spread evenly, until use. 搅拌6分钟,待混合液面划8字能清晰可见时,倒入模中,待其凝固,就可以形成所需要的除痘的天然皂。 Stirred for 6 minutes until the mixture is classified, 8 surface can be seen clearly when, poured into molds, let it solidify and form the desired Chudou natural soap.

[0055] 实施例3 [0055] Example 3

[0056] 实施例1、2的理化指标如下: [0056] Examples 1 and 2 of the physical and chemical indicators are as follows:

[0057] 3.1 性状 [0057] 3.1 Characters

[0058] 本品为硬度适宜,泡沫丰富,稳定性好,气味芬芳,半透明,细腻均匀的淡黑色天然皂。 [0058] The product is suitable hardness foam, good stability, fragrant, translucent, pale black fine uniform natural soap.

[0059] 3.2 PH 值检查 [0059] 3.2 PH value check

[0060] 取本品用PH试纸测量,测得值为7-8。 [0060] PH test paper of this product measured, the measured value of 7-8.

[0061] 3.3室温放置实验 Placing [0061] 3.3 Experimental rt

[0062] 将实例1、2所制的除痘的天然皂,室温考察6个月,稳定性好,用后感觉无变化,气味无变化。 [0062] Examples 1 and 2 will be made of natural soap Acne, for six months at room temperature inspection, good stability, no change feeling after use, no change in odor.

[0063] 3.4刺激性实验、过敏性实验 [0063] 3.4 Experimental irritation, allergic experiment

[0064] 小白鼠背部剪去毛,分别涂抹实例1、2制备的除痘的天然皂于剪去毛的部位,和没涂部位进行比较,结果没有刺激性和过敏反应。 [0064] Mice cut back hair were applied examples 1 and 2 prepared Chudou natural soap to cut hair portion, and had been coated parts were compared, no irritation and allergic reactions. 取实例I所制的除痘的天然皂涂于志愿者(20-60岁,100人)手面上,过30分钟后观察,均没出现发红,发疹,起泡现象。 Acne prepared from example I was applied to natural soaps volunteers (20-60 years old, 100) surfaces of the hand, observed after 30 minutes, it was no redness, rash, blistering.

[0065] 3.5除痘的天然皂祛痘效果考察 [0065] 3.5 Effect Acne Acne natural soaps Investigation

[0066] 选取100名16-26岁年龄段患有不同程度青春痘的人作为试用对象,任意分成两组,分别用实施例1、2制备的天然皂洗脸,每天两次,使用时间为三个月。 [0066] One hundred 16-26 years of age who suffer from varying degrees of acne as a trial subject, arbitrarily divided into two groups, wash with natural soap prepared in Examples 1 and 2 embodiment, twice daily, three time months. 其中实施例1,50例中,男28例,女22例。 Examples Examples 1,50, 28 males and 22 females which embodiment. 实施例2,50例中男24例,女26例。 Example 2.50 Example 24 males, 26 females embodiment.

[0067] 效果标准:显效,治愈85% ;有效,治愈50% ;无效,皮肤无明显改善。 [0067] The performance criteria: markedly effective, 85% cure; effective cure 50%; invalid, no significant improvement in the skin.

[0068] 表1祛痘实验结果 [0068] The results in Table 1 Acne

[0069] [0069]

I显效(人)I有效(人)I无效(人)I总有效率(%) I markedly (people) I effectively (person) I invalid (person) I total efficiency (%)

实例I & 20 5 90 Example I & 20 5 90

实例2 22 26 2 96 Example 22226296

Claims (5)

  1. 1.一种除痘的天然皂,其特征在于:94g除痘的天然皂中含有以下物质:乳木果油 1-1Og芥花油 1-1Og玉米油 1-1Og椰子油 2-19g甜杏仁油 1-16g棕榈油 8.3-22g蜂蜡 0.8-1lg亚麻籽油 1- 5g氢氧化钠 3 - Sg蒸馏水 1-19ml蔗糖 6-18g水乙醇 6_20ml甘油 IO-2 Om I核桃油 1-5ml油茶籽油 1-5ml菊花提取液 l_5ml虎杖提取液 1-5ml丹参提取液 l-5ml。 A natural soap Acne, wherein: 94g Chudou natural soap contains the following substances: shea butter 1-1Og 1-1Og canola oil, corn oil, coconut oil 2-19g sweet almond 1-1Og palm oil 1-16g 8.3-22g linseed oil, beeswax 0.8-1lg 1- 5g of sodium hydroxide 3 - Sg distilled water, ethanol 6_20ml 1-19ml sucrose 6-18g glycerol IO-2 Om I camellia seed oil walnut oil 1-5ml 1-5ml l_5ml chrysanthemum extract of Polygonum cuspidatum extract 1-5ml Salvia extract l-5ml.
  2. 2.根据权利要求1所述的一种除痘的天然皂,其特征在于:所述的菊花提取液通过以下方法制备: 称取菊花一定量,置容器中,加热60-85°C,第1次加7-14倍量水,提取l_2h,第5-10倍量水,提取l_2h,第3次加4-8倍量水,提取0.5_lh,每次用3层纱布滤过,合并滤液,加热浓缩至菊花重量的1-4倍体积(g/ml),用3层纱布滤过,待用。 2. According to one Chudou natural soap according to claim 1, wherein: said daisy extract prepared by the following method: Weigh chrysanthemum certain amount, the storage container and heated 60-85 ° C, of 1 plus 7-14 times the amount of water and extracted l_2h, 5-10 times the amount of water, extraction l_2h, 3rd 4-8 times the amount of water added, extracted 0.5_lh, each with 3 layers of gauze filtration, the filtrate was combined heated and concentrated to 1-4 volumes of chrysanthemum weight (g / ml), with 3 layers of gauze filtration and set aside.
  3. 3.根据权利要求1所述的一种除痘的天然皂,其特征在于:所述的丹参提取液通过以下方法制备: 称取丹参一定量,置回流提取器中,加热50-85°C第1次加7-14倍量50-85%乙醇,提取l_2h,第2次加5-10倍量50-85%乙醇,提取l_2h,第3次加4_8倍量50-85%乙醇,提0.5-lh,每次用3层纱布滤过,合并滤液,加热浓缩至丹参重量的1-4倍体积(g/ml),用3层纱布滤过,待用。 3. According to one Chudou natural soap according to claim 1, wherein: said Danshen extract was prepared by the following method: Weigh a quantity of Salvia, set reflux extractor, heated 50-85 ° C 1st added 7-14 times the amount of 50-85% ethanol, extraction l_2h, 2nd added 5-10 times the amount of 50-85% ethanol, extraction l_2h, 3rd 4_8 times the amount of 50-85% added ethanol extract 0.5-lh, each with 3 layers of gauze filtration, the combined filtrate was heated and concentrated to 1-4 times the volume (g / ml) by weight of Salvia, with 3 layers of gauze filtration and set aside.
  4. 4.根据权利要求1所述的一种除痘的天然皂,其特征在于:所述的虎杖提取液通过以下方法制备: 称取虎杖一定量,置回流提取器中,加热60-80°C第1次加6-15倍量50-85%乙醇,提取1-2h,第2次加8-10倍量50-85%乙醇,提取l_2h,第3次加7_12倍量50-85%乙醇,提取1-2h,每次用3层纱布滤过,合并滤液,加热浓缩至虎杖重量的1-5倍体积(g/ml),用3层纱布滤过,待用。 4. According to one Chudou natural soap according to claim 1, wherein: said Polygonum cuspidatum extract prepared by the following method: Weigh a quantity of Polygonum cuspidatum, set reflux extractor, heated 60-80 ° C 1 plus an amount of 50-85% ethanol, 6-15 times, extraction 1-2h, 2nd added 8-10 times the amount of 50-85% ethanol, extraction l_2h, 3rd times the amount of 50-85% added ethanol 7_12 extracting 1-2h, each with 3 layers of gauze filtration, the combined filtrate was heated and concentrated to 1-5 volumes of Polygonum cuspidatum weight (g / ml), with 3 layers of gauze filtration and set aside.
  5. 5.权利要求1所述的一种除痘的天然皂的制备方法,包括以下步骤: a)称取椰子油2-19g、棕榈油3-22g、芥花油l_10g、乳木果油l_10g、蜂腊0.8_llg、玉米油l-10g、甜杏仁油l_16g,亚麻籽油l_5g于烧杯中置于60-95°C的水浴锅中让固体油融化,得油溶液A ; b)称取3-8g氢氧化钠于烧杯加入蒸馏水l_19ml,搅拌使其溶解,冷却,得溶液B ; c)称取蔗糖6-18g,研成过60-80目筛的细粉;取无水乙醇6-20ml,置于烧杯中,将蔗糖细粉加入烧杯中,搅拌使其溶解; d)将溶液B在搅拌下呈细流状倒入油溶液A中,边加边搅拌,然后将溶液C加入,加入甘油10-20ml、核桃油l_5ml、油茶籽油l_5ml,菊花提取液l_5ml、虎杖提取液l_5ml、丹参提取液l-5ml,与此同时在模具中加入液状石蜡,涂抹均匀,待用;搅拌5-10分钟,待混合液面划8字能清晰可见时,倒入模中,待其凝固,即可。 The method of preparing a natural soap Acne according claim 1, comprising the following steps: a) Weigh coconut oil 2-19g, 3 - 22 g palm oil, canola oil l_10g, shea butter l_10g, beeswax 0.8_llg, corn oil l-10g, sweet almond oil l_16g, linseed oil l_5g beaker was placed in 60-95 ° C water bath to melt the solid oil allows to obtain an oil solution a; b) Weigh 3- 8g of sodium hydroxide was added to a beaker of distilled water l_19ml, stirring to dissolve, cooled to obtain a solution B; c) sucrose weighed 6-18g, research into a fine powder through a 60-80 mesh sieve; anhydrous ethanol 6-20ml, placed in a beaker, sucrose powder into a beaker and dissolved with stirring; D) and the solution was poured into small streams B oil solution A under stirring, with stirring, and then the solution C was added, glycerin 10-20ml, walnut oil l_5ml, camellia oil l_5ml, chrysanthemum extract l_5ml, Polygonum cuspidatum extract l_5ml, Salvia miltiorrhiza extract l-5ml, liquid paraffin was added at the same time in the mold, spread evenly, aside; stirring 5-10 minutes, until the mixture, 8 can draw upon the surface clearly visible, was poured into the mold and letting it solidify to.
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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103893095A (en) * 2014-04-09 2014-07-02 湖南山田有机农业有限公司 Face cream containing camellia seed oil
CN104327980A (en) * 2014-11-17 2015-02-04 绵阳原香农业科技有限公司 Shea butter soap
CN105273877A (en) * 2015-10-22 2016-01-27 周庆莉 Vitality invigorating toilet soap
CN105316135A (en) * 2015-11-09 2016-02-10 重庆琥珀茶油有限公司 Tea-seed-oil acne-removing facial soap
CN105316136A (en) * 2015-11-09 2016-02-10 重庆琥珀茶油有限公司 Camellia seed shampoo soap
CN105331467A (en) * 2015-12-10 2016-02-17 贵州芳阳特产有限公司 Soap and preparation method thereof
CN105779175A (en) * 2016-04-06 2016-07-20 江苏耐雀生物工程技术有限公司 Natural handmade soap with acne removing function and preparation method of natural handmade soap
CN105779172A (en) * 2014-12-15 2016-07-20 朱玉霖 Bingposanyan ancient soap and preparation method therefor
CN106085656A (en) * 2016-06-21 2016-11-09 陆锦满 Dendrobium officinale beautifying fancy soap
CN106350319A (en) * 2016-08-29 2017-01-25 骆志明 Ground face washing soap with traditional Chinese medicines and effects of removing acne and diminishing inflammation
CN106381242A (en) * 2016-08-29 2017-02-08 杭州素妍化妆品有限公司 Flaxseed oil handmade soap and preparation method thereof

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CN1422644A (en) * 2001-12-06 2003-06-11 高大海 Skin-beauty capsule
CN100528176C (en) * 2003-11-26 2009-08-19 岐黄药业科技投资有限责任公司 Chinese traditional medicinal composition for treating acne
CN102864045A (en) * 2012-09-27 2013-01-09 皖南医学院 Glittering transparent skincare nutritious soap and preparation method thereof
CN102908479A (en) * 2012-09-01 2013-02-06 韩乃巍 Traditional Chinese medicine for treating lung wind blood heat type acne

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CN1422644A (en) * 2001-12-06 2003-06-11 高大海 Skin-beauty capsule
CN100528176C (en) * 2003-11-26 2009-08-19 岐黄药业科技投资有限责任公司 Chinese traditional medicinal composition for treating acne
CN102908479A (en) * 2012-09-01 2013-02-06 韩乃巍 Traditional Chinese medicine for treating lung wind blood heat type acne
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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103893095A (en) * 2014-04-09 2014-07-02 湖南山田有机农业有限公司 Face cream containing camellia seed oil
CN104327980A (en) * 2014-11-17 2015-02-04 绵阳原香农业科技有限公司 Shea butter soap
CN105779172A (en) * 2014-12-15 2016-07-20 朱玉霖 Bingposanyan ancient soap and preparation method therefor
CN105273877A (en) * 2015-10-22 2016-01-27 周庆莉 Vitality invigorating toilet soap
CN105316135A (en) * 2015-11-09 2016-02-10 重庆琥珀茶油有限公司 Tea-seed-oil acne-removing facial soap
CN105316136A (en) * 2015-11-09 2016-02-10 重庆琥珀茶油有限公司 Camellia seed shampoo soap
CN105331467A (en) * 2015-12-10 2016-02-17 贵州芳阳特产有限公司 Soap and preparation method thereof
CN105779175A (en) * 2016-04-06 2016-07-20 江苏耐雀生物工程技术有限公司 Natural handmade soap with acne removing function and preparation method of natural handmade soap
CN106085656A (en) * 2016-06-21 2016-11-09 陆锦满 Dendrobium officinale beautifying fancy soap
CN106350319A (en) * 2016-08-29 2017-01-25 骆志明 Ground face washing soap with traditional Chinese medicines and effects of removing acne and diminishing inflammation
CN106381242A (en) * 2016-08-29 2017-02-08 杭州素妍化妆品有限公司 Flaxseed oil handmade soap and preparation method thereof

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