CN107541364A - Mo Luohai bud camellia handmade soaps through desensitization process and preparation method thereof - Google Patents
Mo Luohai bud camellia handmade soaps through desensitization process and preparation method thereof Download PDFInfo
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- 239000000344 soap Substances 0.000 title claims abstract description 49
- 235000018597 common camellia Nutrition 0.000 title claims abstract description 48
- 238000000034 method Methods 0.000 title claims abstract description 17
- 238000000586 desensitisation Methods 0.000 title claims abstract description 16
- 230000008569 process Effects 0.000 title claims abstract description 15
- 240000001548 Camellia japonica Species 0.000 title claims description 39
- 238000002360 preparation method Methods 0.000 title claims description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 29
- 239000000843 powder Substances 0.000 claims abstract description 27
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- 239000003921 oil Substances 0.000 claims abstract description 14
- 235000019198 oils Nutrition 0.000 claims abstract description 14
- 239000010495 camellia oil Substances 0.000 claims abstract description 12
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- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 11
- 241000209507 Camellia Species 0.000 claims abstract description 9
- 239000003240 coconut oil Substances 0.000 claims abstract description 9
- 235000019864 coconut oil Nutrition 0.000 claims abstract description 9
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- 235000019438 castor oil Nutrition 0.000 claims abstract description 8
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Landscapes
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to a kind of Mo Luohai bud camellia handmade soaps through desensitization process, it is bound up according to mass fraction by following component:15 25 parts of camellia oil, 8 15 parts of grape-kernel oil, 5 10 parts of castor oil, 15 20 parts of coconut oil, 15 20 parts of palm oil, 14 20 parts of deionized water, 8 12 parts of sodium hydroxide, 38 parts of Mo Luohai buds powder, 2 10 parts of tea seed extract solution, 0.1 0.5 parts of essence；The handmade soap adds Mo Luohai buds powder and completely desensitization tea seed extract solution so that handmade soap of the invention has the effect of antipruritic, anti-inflammation, gentle, lubrication, anti-aging.
Description
Technical field
The present invention relates to a kind of camellia handmade soap, particularly a kind of Mo Luohai bud camellia handmade soaps through desensitization process.
Background technology
The production of soap product has a long history, and about with regard to useful grease and contains carbonic acid at B.C. 2500
The plant ass of potassium produces potash soap, and the record of wool is washed with this soap, since 19th century, due to Leblanc soda ash production method
Development, makes the production of soap enter industrialized stage, now, as the improvement of people's living standards, people are for thing
The requirement also more and more higher of matter life, soap products at present on the market are different, but wherein most all containing substantial amounts of chemistry
Product, there is side effect and injury to skin, and people use rear dry skin, and easy allergy.
As a kind of natural agents, tea seed powder but has anaphylactogen so that allergy sufferers pruitus, plays erythema so that tea
Seed powder class product can not largely use tea seed powder raw material；So solving the allergen issue of tea seed powder, it can just cause tea seed powder class
Product can preferably import market.
The content of the invention
One of mesh of the present invention is to overcome existing tea seed extract solution allergic problem, there is provided a kind of Mo Luohai through desensitization process
Bud camellia handmade soap, the handmade soap have the effect of anti-inflammatory, anti-acne.
The two of the mesh of the present invention are to provide the preparation method of the above-mentioned Mo Luohai bud camellia handmade soaps through desensitization process.This hair
Bright technical scheme is：
A kind of Mo Luohai bud camellia handmade soaps through desensitization process, it is made up according to mass fraction meter of following component：Camellia oil
15-25 parts, 8-15 parts of grape-kernel oil, castor oil 5-10 parts, coconut oil 15-20 parts, palm oil 15-20 parts, deionized water 14-
20 parts, sodium hydroxide 8-12 parts, Mo Luohai bud powder 3-8 parts, tea seed extract solution 2-10 parts, essence 0.1-0.5 parts.
The preferred 3-6 parts of wherein described tea seed extract solution, dosage is too high to make soap too soft, and easily becomes sour, and dosage is too low
There is no anti-inflammatory effects.
Preferably, described tea seed extraction liquid and preparation method thereof comprises the following steps：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through the eye mesh screen of 30 mesh -100, obtains camellia seed
Powder；
（4）Heat extraction：By step（3）Obtained camellia seed powder and deionized water mixing, mixed proportion 1:（3-10）, it is heated to 60
DEG C -100 DEG C, mixing speed is 20-60 revs/min, after stirring 40-60 minutes, adds adsorbent, and adsorbent addition is and tea
The weight ratio of seed powder is（1-2）：10, heating-up temperature is 60 DEG C -100 DEG C, and mixing time is 20-30 minutes, mixing speed 20-
60 revs/min, sedimentation centrifuge filters to get filtrate；Described adsorbent is activated carbon and atlapulgite, and described decolorising agent is
Activated carbon and atlapulgite, adsorption specific surface area 1000m2/g-1500m2/ g, is calculated with part by weight, activated carbon：Atlapulgite=
1：（3-10）.
（5）It is refined：By step（4）The filtrate addition filtrate 1%-6% of acquisition（Percentage by weight）Diatomite, pass through blade mistake
Filter filters, and obtains clarification camellia seed extract solution.
Preferred 4-7 parts of dosage of wherein described Mo Luohai bud powder, dosage is too high to make soap too soft, and easily becomes sour, and use
Measuring too low does not have anti-inflammatory effects.
The preparation method of Mo Luohai bud camellia handmade soaps of the invention through desensitization process, comprises the following steps:
（a）Under normal temperature, NaOH solids are dissolved with low temperature deionized water in a container, make it be in clear or white solution,
It is 30-50 DEG C to control temperature；
（b）In another container, camellia oil, grape-kernel oil, castor oil, coconut oil, palm fibre are put into the greases such as oil and mixed in proportion, is added
Thermal agitation is transparent to whole fat clarifications；
（c）Will（a）It is slowly added to（b）Keeping temperature be less than 35-45 DEG C mixing, be sufficiently stirred, up to soap lye close to or up
It is slight sticky；
（d）The additives such as Mo Luohai buds powder, tea seed extract solution, essence are separately added into, are again stirring for uniformly；
（e）When soap lye sticky hanging wire, mould is poured into, is incubated, after standing 24-48 h, the demoulding；
（f）Hung in shady and cool, ventilation, the place dried, continue curing to 6 weeks, be packaged into finished product, you can use.
Beneficial effects of the present invention：Using tea oil as main vegetable fat material matching Mo Luohai buds powder and tea seed extract solution
Handmade soap, there is extraordinary anti-inflammatory, the effect such as gently releive, lubricate the skin and muscle, especially suitable for sensitivity and dry skin.
Primary raw material used in the present invention is described as follows：
Camellia seed：It is the fruit of tea oil tree；Tea oil tree is the main woody oleiferous plants tree in China, is described as " east tree ", belongs to camellia
Section's Camellia evergreen dungarunga, it is the distinctive woody vegetable oil resource in China；3-6 meters of the height of tree, the diameter of a cross-section of a tree trunk 1.3 meters above the ground is up to 24-30 lis
Rice, smooth bark is taupe.Tea oil tree list leaf alternate, flower are both sexes white, and October, Post flowering was until fruit between October next year
Can be ripe, therefore, tea oil tree has rare flowers and fruits homophyletic phenomenon；Fruit is capsule, is mostly ellipse, has fine, soft fur；Seed
Mostly yellowish-brown, glossy, triangular shape；Tea oil tree is grown in remote mountains, inhales natural nutrient to the greatest extent, evergreen longevity, the age of tree up to 200 years with
On.
Camellia oil：Camellia seed kernel is through cleaning, air-drying（Temperature is less than 100 DEG C）, shelling, seed selection sterilization after, at 20-50 DEG C
Obtained by being squeezed, active material enriches, generally about containing vitamin E 200mg/Kg, sterol 30mg/Kg, squalene
100mg/Kg。
Grape-kernel oil：Grape-kernel oil has two kinds of very important elements, linolenic acid and proanthocyanidin.Linolenic acid can be with
Free radical is resisted, anti-aging, help absorbs vitamin C and E, strengthens the elasticity of the circulatory system, reduces the injury of ultraviolet, protects
Collagen in skin, improve venous engorgement and oedema, prevent melanin deposition.Proanthocyanidin has protection blood vessel elasticity, protects
Skin afflicting with great suffering torment from ultraviolet is protected, prevents the destruction of collagenous fibres and elastomer, skin is kept due elasticity and is opened
Power, skin sagging and wrinkle is avoided to produce.Grape-kernel oil penetration is strong, salubrious non-greasy, is easily absorbed by the skin, any skin quality
It is applicable.
Castor oil：Castor oil system derives from Ricinus Communis seed, and it is non-dry type, sticky, it is generally colourless or
Light yellow oil；Function containing mitigation and greasy skin, distinctive castor-oil plant acid alcohol have special soft effect to hair skin, can manufactured
Foam is more and has the perfumed soap of transparent feel, can help to maintain the fragrance of essential oil, essence, also easily solution in it is other it is oily in, so
It is well suited for being used as super fat soap.
Coconut oil：Coconut oil is the indispensable glyceride stock of perfumed soap, and produces natural acid, fatty alcohol and surface
The raw material of activating agent；It can increase the rich of foam with coconut oil soapmaking, strengthen cleaning effect.
Palm oil：Palm oil is also known as brown oily, brown skin oil, and the grease extracted by pericarp in oil palm fruit, is non-drying oil.In right amount
Collocation can increase finished product hardness in the formula of handmade soap, be that handmade soap is more stable, effectively extend the resting period.
Mo Luohai bud powder：Mo Luohai buds are also known as emperor's dish, scientific name corchorus olitorius；In the famous pharmacopeia in China《Dictionary of medicinal plant》
Deng the medicinal description for having jute and false jute in ancient books and records, but not yet take in the medicinal record of corchorus olitorius；Jute enters in China
The history of medicine at least also has more than thousand, early in the Song Dynasty《Bencao Tujing》In have been described " for example weak and narrow point of roundpod jute leaf, stem side,
High four or five chi, chrysanthemum are raw sub small into room such as flax angle.Tender leaf is edible, very sweet cunning, profit large intestine ", China's traditional medicine is recognized
For roundpod jute leaf is bitter in taste, temperature；Enter the heart, liver two passes through；There are regulating qi-flowing for relieving pain, the function such as removing toxic substances apocenosis and hemostasis.Mineral in Mo Luohai buds
Element and vitamin content are high, the juice in Mo Luohai bud-leafs have to skin gently releive, lubricate, anti-aging and other effects.
Sodium hydroxide：As the alkali reacted with fat saponification.
Deionized water：Refer to eliminate the pure water in after ionic species impurity, International Organization for standardization ISO/TC 147 is advised
Fixed " deionization " is defined as：" deionized water is complete or incompletely removes ionic species." using the method system of RO counter-infiltrations
Take, the anion and cation gone using ion exchange resin in water removal.
Essence：The smell of finished product is adjusted, is allowed to pleasant comfortable.
Embodiment
Tea seed extract solution used in embodiment, it is made up of following processing step：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through 50 eye mesh screens, obtains camellia seed powder；
（4）Heat extraction：By step（3）Obtained camellia seed powder and deionized water mixing, mixed proportion 1:6,70 DEG C are heated to, is stirred
Speed is mixed as 40 revs/min, after stirring 50 minutes, adds adsorbent, adsorbent addition is to be with the weight ratio of tea seed powder
1.5：10, heating-up temperature is 65 DEG C, and mixing time is 25 minutes, and mixing speed is 40 revs/min, and sedimentation centrifuge, which filters, to be filtered
Liquid；Described adsorbent is activated carbon and atlapulgite, and average adsorption specific surface area is respectively 1200m2/ g and 1300m2/ g, with
Part by weight calculates, activated carbon：Atlapulgite=1：4.
（5）It is refined：By step（4）The filtrate addition diatomite of filtrate 4% of acquisition, is filtered by leaf-type filter, obtained clear
Clear camellia seed extract solution.
Real above-mentioned tea seed extract solution is subjected to patch test, patch test results are without allergic reaction；Method of testing is as follows:
Step 1：The gauze of four thickness is cut into a diameter of 1cm circle with scissors, totally 8, draws 25uL's respectively with liquid-transfering gun
Tea seed extract solution, is dropped on circular gauze, and blank is done with deionized water；
Step 2：The gripping of gauze tweezers is placed on subject（To tea seed extract solution allergy sufferers）At anteflexion arm, adhesive tape is used
Fix, start timing；
Step 3：Torn after 48h adhesive tape, and observe the reaction of skin at gauze covering immediately.
Embodiment 1
Handmade soap preparation method is as follows：Weigh 180 grams of coconut oil, 180 grams of palm oil, after heating for dissolving, add 200 grams of tea oil,
90 grams of grape-kernel oil, 70 grams of castor oil, after stirring, weigh 100 grams of sodium hydroxides and be dissolved in 180 grams of deionized waters, stir
After uniformly, it is slowly added in grease, lasting stirring, treats that saponification is abundant, when material body is in thread, weighs Mo Luohai bud powder 30g, add
50 grams of above-mentioned tea seed extract solutions, are stirring evenly and then adding into soap lye, add 2 grams of essence, reverse mould after stirring, go out after shaping
Mould, soap is supported to complete curing, obtains handmade soap.
Embodiment 2-7
Embodiment 2-5 handmade soap, its preparation process condition is substantially with embodiment 1, the simply bar such as reaction raw materials and proportion scale
Part is slightly different, specifically as listed in table 1.
The embodiment 1-5 of table 1, comparative example 1-2 Mo Luohai bud camellia handmade soap preparation methods
。
Comparative example 3
Comparative example 3 eliminates Mo Luohai bud powder on the basis of embodiment 1, and tea seed extract solution dosage is 80 grams, other with implementing
Example 1 is identical.
Comparative example 4
Comparative example 4 eliminates tea seed extract solution on the basis of embodiment 1, and Mo Luohai bud powder dosage is 80 grams, other with implementing
Example 1 is identical.
After handmade soap obtained by embodiment 1-5 comparative examples 1-4 is stood into 48 hours, depanning, it is placed at shady and cool ventilation, the
Detect weekly within one month and test its pH value every January, when pH is reduced to below 10.5, tests it and moisten moisturizing, repair acne
Print.
Its functional attributes test result of handmade soap obtained by the embodiment 1-5 of table 2, comparative example 1-4
。
Its functional attributes of handmade soap obtained by embodiment 1-5, comparative example 1-4 and the test side used in physical and chemical index test
Method has：
（1）The method of testing for moistening performance of keeping humidity is tested for hand skin, and specific method is as follows：
By the Mo Luohai bud camellia handmade soaps obtained by embodiment 1-5, comparative example 1-4, got blisters with the net of getting blisters drenched, treat foam
It is fully abundant when can not be further added by, hand is rinsed with clear water, record was rinsed to the clean time, untill not glutinous soapy feeling, was used
Clean towel water purification beads, the back of the hand portion moisture value is detected with digital skin moisture detector after half an hour（Note：Using by hand
The back of the hand portion moisture value will be detected before hand by soaping, and be recorded）；Statistical result such as table 3.
The embodiment 1-5 of table 3, comparative example 1-4 Mo Luohai bud camellia handmade soap trial effect mean scores tables
。
From table 3, it can be seen that moisture retention effect of the present invention is good.
Embodiment 1-5, comparative example 1-4 Mo Luohai bud camellias handmade soap reparation acne print effect testing method are as follows：
Embodiment 1-5, comparative example 1-4 Mo Luohai bud camellia handmade soaps are chosen into 20 triers for having acne print respectively, try out 3
Individual month, count rehabilitation situation quantity, statistical conditions such as table 4.
The camellia handmade soap of table 4 repairs the number of effects statistical form of acne print
。
Claims (7)
1. a kind of Mo Luohai bud camellia handmade soaps through desensitization process, it is made up according to mass fraction meter of following component：Camellia
Oily 15-25 parts, 8-15 parts of grape-kernel oil, castor oil 5-10 parts, coconut oil 15-20 parts, palm oil 15-20 parts, deionized water
14-20 parts, sodium hydroxide 8-12 parts, Mo Luohai bud powder 3-8 parts, tea seed extract solution 2-10 parts, essence 0.1-0.5 parts.
2. a kind of Mo Luohai bud camellia handmade soaps through desensitization process according to claim 1, it is characterised in that described
Tea seed extract solution dosage is 3-6 parts.
3. a kind of Mo Luohai bud camellia handmade soaps through desensitization process according to claim 1, it is characterised in that described
Tea seed extraction liquid and preparation method thereof comprises the following steps：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through the eye mesh screen of 30 mesh -100, obtains camellia seed
Powder；
（4）Heat extraction：By step（3）Obtained camellia seed powder and deionized water mixing, mixed proportion 1:（3-10）, it is heated to 60
DEG C -100 DEG C, mixing speed is 20-60 revs/min, after stirring 40-60 minutes, adds adsorbent, and adsorbent addition is and tea
The weight ratio of seed powder is（1-2）：10, heating-up temperature is 60 DEG C -100 DEG C, and mixing time is 20-30 minutes, mixing speed 20-
60 revs/min, sedimentation centrifuge filters to get filtrate；
（5）It is refined：By step（4）The 1-6% diatomite of the filtrate addition filtrate weight of acquisition, is filtered by leaf-type filter, obtained
Camellia seed extract solution must be clarified.
A kind of 4. Mo Luohai bud camellia handmade soaps through desensitization process according to claim 3, it is characterised in that step
（4）Described adsorbent is activated carbon and atlapulgite, is calculated with part by weight, activated carbon：Atlapulgite is 1：（3-10）.
A kind of 5. Mo Luohai bud camellia handmade soaps through desensitization process according to claim 3, it is characterised in that step
（4）Described bleaching agent activated carbon and atlapulgite, adsorption specific surface area are 1000-1500m2/g。
6. a kind of Mo Luohai bud camellia handmade soaps through desensitization process according to claim 1, it is characterised in that described
The dosage of Mo Luohai bud powder is 4-7 parts.
7. a kind of preparation method of the Mo Luohai bud camellia handmade soaps through desensitization process, its feature exist according to claim 1
In comprising the following steps:
（a）Under normal temperature, NaOH solids are dissolved with low temperature deionized water in a container, make it be in clear or white solution,
It is 30-50 DEG C to control temperature；
（b）In another container, camellia oil, grape-kernel oil, castor oil, coconut oil, palm fibre are put into oil and mixed in proportion, heating stirring
It is transparent to whole fat clarifications；
（c）Will（a）It is slowly added to（b）Keeping temperature be less than 35-45 DEG C mixing, be sufficiently stirred, up to soap lye close to or up
It is slight sticky；
（d）Mo Luohai buds powder, tea seed extract solution, essence are separately added into, is again stirring for uniformly；
（e）When soap lye sticky hanging wire, mould is poured into, is incubated, after standing 24-48h, the demoulding；
（f）Hung in shady and cool, ventilation, the place dried, continue curing to 6 weeks, be packaged into finished product, you can use.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102229637A (en) * | 2011-04-18 | 2011-11-02 | 浙江久晟茶业发展有限公司 | Process for extracting tea saponin by using membrane separation and concentration |
| CN104974866A (en) * | 2015-07-20 | 2015-10-14 | 永安市泽恩医疗器械有限公司 | Tea seed essence soap and preparation method |
| CN106109327A (en) * | 2016-07-29 | 2016-11-16 | 广州莫洛海芽化妆品有限公司 | A kind of Mo Luohai bud extracting solution and preparation method and application |
| KR20170036397A (en) * | 2015-09-24 | 2017-04-03 | 최정란 | Composition for Functional Hard Shampoo Soap having Activity of Anti-Oxidant Anti-Microbial and Method for Soap Using Thereof |
| CN107164120A (en) * | 2017-03-24 | 2017-09-15 | 广州伊颜溢美生物科技有限公司 | A kind of pure plant hair soap and preparation method thereof |
-
2017
- 2017-10-18 CN CN201710972978.8A patent/CN107541364A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102229637A (en) * | 2011-04-18 | 2011-11-02 | 浙江久晟茶业发展有限公司 | Process for extracting tea saponin by using membrane separation and concentration |
| CN104974866A (en) * | 2015-07-20 | 2015-10-14 | 永安市泽恩医疗器械有限公司 | Tea seed essence soap and preparation method |
| KR20170036397A (en) * | 2015-09-24 | 2017-04-03 | 최정란 | Composition for Functional Hard Shampoo Soap having Activity of Anti-Oxidant Anti-Microbial and Method for Soap Using Thereof |
| CN106109327A (en) * | 2016-07-29 | 2016-11-16 | 广州莫洛海芽化妆品有限公司 | A kind of Mo Luohai bud extracting solution and preparation method and application |
| CN107164120A (en) * | 2017-03-24 | 2017-09-15 | 广州伊颜溢美生物科技有限公司 | A kind of pure plant hair soap and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 宋丽雅等: "《化妆品植物功效添加剂的研究与开发》", 30 September 2011, 中国轻工业出版社 * |
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