CN106434064B - A kind of transparent soap and preparation method thereof of built-in new fresh seaweed - Google Patents

A kind of transparent soap and preparation method thereof of built-in new fresh seaweed Download PDF

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CN106434064B
CN106434064B CN201610861897.6A CN201610861897A CN106434064B CN 106434064 B CN106434064 B CN 106434064B CN 201610861897 A CN201610861897 A CN 201610861897A CN 106434064 B CN106434064 B CN 106434064B
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phase
acid
extracting solution
transparent soap
seaweed
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CN106434064A (en
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付晓婷
刘楠楠
许加超
高昕
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Ocean University of China
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Ocean University of China
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/06—Inorganic compounds
    • C11D9/08—Water-soluble compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/26—Organic compounds, e.g. vitamins containing oxygen
    • C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/26—Organic compounds, e.g. vitamins containing oxygen
    • C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/26—Organic compounds, e.g. vitamins containing oxygen
    • C11D9/267—Organic compounds, e.g. vitamins containing oxygen containing free fatty acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/38—Products in which the composition is not well defined
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/40—Proteins
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
    • C11D9/444—Dyes; Pigments

Abstract

The invention belongs to daily cosmetics technical fields, and in particular to the transparent soap and preparation method thereof of new fresh seaweed built in one kind.It include marine algae extract, new fresh seaweed, in natural seaweed pigment any one or several combinations.The natural seaweed pigment is obtained from one of brown alga, red algae, green alga or several extractions.The marine algae extract weight percent is 5%-30%.Practical and attractive, moisture-keeping nutrient, natural no stimulation of the invention are a real environmentally protective seaweed transparent soap.Preparation method of the present invention is scientific and reasonable, simple for process, and production cost is low, is suitble to industrialized production.

Description

A kind of transparent soap and preparation method thereof of built-in new fresh seaweed
Technical field
The invention belongs to daily cosmetics technical fields, and in particular to the transparent soap of new fresh seaweed built in one kind.
Background technique
With the development and improvement of living standard of entire society, requirement of the people to cleaning products is also higher and higher, special It is not the safety of product, it is desirable to which this kind of detergent product has good cleaning effect, while requiring again not damaged to skin. Traditional soap, cleaning force is good, but pH value is generally higher (pH=9-11), and irritation is larger, and beautiful and moisture retention is poor, therefore beauty Seeing seaweed transparent soap that is practical and having both natural moisture preserving will be liked by people.
Transparent soap is the big type in soap, with its transparency highlight product quality, it is pure, beautiful with it is advanced, Liking for consumer is increasingly obtained.Presently commercially available transparent soap generally adds a large amount of artificial essence, colorant, preservative Deng the activity substance content of skin care is few, and is color dullness mostly, the problems such as rare addition inner matter.China's marine algae resource is rich Richness, wherein have economic value there are about more than 100 kinds.Contain protein needed by human, fat, carbohydrate, more in seaweed Kind vitamin and minerals, nutritive value are abundant.New fresh seaweed, marine algae extract and seaweed pigment are added to energy in transparent soap Better nursing skin plays cleaning nutrition, beautiful moist effect.
The present invention in view of the shortcomings of the prior art, by attaching marine algae extract, improves chemicals and preservative The natural pigment that stimulation, built-in new fresh seaweed and addition extract from seaweed itself keeps it safe, beautiful and practical, and auxiliary adds Add sodium alginate, allantoin, jasmine extracting solution and apple extracting solution etc., enhances its nourishing and moisturizing, nontoxic non-stimulated effect.
Summary of the invention
In order to solve the above-mentioned technical problem, The technical solution adopted by the invention is as follows: the present invention is former for product on the market Expect that chemicals content is more, moistens the problems such as trophism is poor, ornamental value is poor, the transparent soap of new fresh seaweed built in one kind, nothing are provided Artificial color, preservative, and built-in seaweed, the seaweed transparent soap for adding seaweed active constituent and natural pigment have beautiful real With, cleaning maintenance the effect of.
In order to solve the above technical problems, the present invention provides seaweed transparent soap, bulk pharmaceutical chemicals include marine algae extract, fresh In seaweed, natural seaweed pigment any one or several combinations.
Wherein, above-mentioned natural seaweed pigment is obtained from one of brown alga, red algae, green alga or several extractions.
Wherein, the weight percent of above-mentioned marine algae extract is 5%-30%.
Preferably, the invention also includes the compositions of following weight percent: jasmine extracting solution 0.5%-3%, apple extract Liquid 0.5%-3%.
Wherein, the preparation process of the marine algae extract is as follows: (1) after rinsing seaweed well, drying crushes to obtain algae Powder；
(2) 1g algae powder is uniformly mixed with the distilled water of 10-200mL, in 30-60 DEG C of oscillation 6-24h；
(3) step (2) concussion liquid is centrifuged at revolving speed 4000r/min 15min, removes bottom precipitation, obtains liquid Marine algae extract sample.
Wherein, the preparation process of the natural seaweed pigment is as follows: after fresh seaweed is cleaned up, with 1-3 times Deionized water is impregnated, is smashed to pieces, vibrating 10-48h, is taken out after being ultrasonically treated 30-120min, is filtered out residue, obtain natural seaweed Pigment.
The present invention also provides the preparation methods of the transparent soap of fresh seaweed new built in one kind, comprising the following steps:
(1) successively by propylene glycol 6%-20%, glycerol 10%-30%, surfactant 0%-10%, stearic acid 10%- 20%, palmitinic acid 1%-10%, myristic acid 2%-10%, lauric acid 0.1%-10%, basic grease 0%-30% are in 70-90 DEG C heating, be allowed to be completely dissolved, obtain A phase；
(2) sodium hydroxide 1%-8%, sugar 1%-10%, alcohol 1%-8%, citric acid are sequentially added in another container 0.1%-5%, deionized water 5-20% dissolve at 70-75 DEG C, obtain B phase；
(3) by sodium alginate 0.1%-2%, allantoin 0.1%-2%, jasmine extracting solution 0.5%-3%, apple extracting solution 0.5%-3%, marine algae extract 5%-30% are mixed to get C phase；
(4) B is added in A phase, after being saponified 20-100min at 70-85 DEG C, cools to 60 DEG C, C phase is added, then 0.01%-3% natural seaweed pigment is added, after mixing evenly reverse mould, clean new fresh seaweed is first put into mold bottom, slowly Soap lye is poured into mold, is demoulded after waiting to be cooled be hardened；
(5) to get finished product after being placed 3-7 days at aeration-drying.
Wherein, the surfactant is sodium lauroyl sarcosine, cocounut oil acyl glycine potassium and cocamidopropyl propyl amide beet One or several kinds of combination in alkali, the basic grease are coconut oil, Sweet Almond Oil, olive oil, palm oil and oenothera biennis One or several kinds of combination in oil.
Preferably, the preparation method of the transparent soap of new fresh seaweed built in above-mentioned one kind, further comprising the steps of:
(1) successively by propylene glycol 6%, glycerol 20%, cocounut oil acyl glycine potassium 10%, stearic acid 8%, palmitinic acid 1%, meat Myristic acid 4%, lauric acid 2%, coconut oil 4%, olive oil 4% are heated at 70-90 DEG C, are allowed to be completely dissolved, are obtained A phase；
(2) sodium hydroxide 4%, sugared 4%, alcohol 2%, citric acid 1%, deionized water are sequentially added in another container 18.5% dissolves at 70-75 DEG C, obtains B phase；
(3) sodium alginate 0.1%, allantoin 0.3%, jasmine extracting solution 0.5%, apple extracting solution 0.5%, seaweed are mentioned Object 10% is taken to be mixed to get C phase；
(4) B is added in A phase, after being saponified 20min at 70-85 DEG C, cools to 60 DEG C, C phase is added, is added 0.1% natural seaweed pigment, reverse mould, is first put into mold bottom for clean new fresh seaweed, slowly into mold after mixing evenly Soap lye is poured into, is demoulded after waiting to be cooled be hardened；
(5) to get finished product after being placed 3 days at aeration-drying.
The invention has the advantages that:
New fresh seaweed built in transparent soap produced by the invention adds natural seaweed pigment, can prepare containing new fresh seaweed and The seaweed transparent soap of color multiplicity, with beautiful and practical feature.The present invention contains tangleweed extract, comprising more Phenol, polysaccharide, protein etc., and marine alga natural pigment is added, it is not necessarily to chemical preservative and artificial color, there is nutrition to moisten, temperature With non-stimulated effect, crowd suitable for different sexes, age and skin quality.Practical and attractive, moisture-keeping nutrient, natural nothing of the invention Stimulation is a real environmentally protective seaweed transparent soap.Preparation method of the present invention is scientific and reasonable, simple for process, production It is at low cost, it is suitble to industrialized production.
Specific embodiment
The present invention in view of the shortcomings of the prior art, by attaching marine algae extract, improves chemicals and preservative The natural pigment that stimulation, built-in new fresh seaweed and addition extract from seaweed itself keeps it safe, beautiful and practical, and auxiliary adds Add sodium alginate, allantoin, jasmine extracting solution and apple extracting solution etc., enhances its nourishing and moisturizing, nontoxic non-stimulated effect.
Below according to by embodiment, the present invention will be described in detail.
Specific embodiment:
Embodiment 1:
1. group cost implementation seaweed transparent soap ingredient and its weight percent are:
A phase: propylene glycol 6%, glycerol 20%, cocounut oil acyl glycine potassium 10%, stearic acid 8%, palmitinic acid 1%, nutmeg Sour 4%, lauric acid 2%, coconut oil 4%, olive oil 4%；
B phase: sodium hydroxide 4%, sugared 4%, alcohol 2%, citric acid 1%, deionized water 18.5%；
C phase: sodium alginate 0.1%, allantoin 0.3%, jasmine extracting solution 0.5%, apple extracting solution 0.5%, seaweed mention Take object 10%；
2. technical process:
(1) successively by propylene glycol 6%, glycerol 20%, cocounut oil acyl glycine potassium 10%, stearic acid 8%, palmitinic acid 1%, meat Myristic acid 4%, lauric acid 2%, coconut oil 4%, olive oil 4% are heated at 75 DEG C, are allowed to be completely dissolved, are obtained A phase；
(2) 4%, sugar 4%, alcohol 2%, citric acid 1%, deionized water 18.5% are sequentially added in another container 75 It is dissolved at DEG C, obtains B phase；
(3) sodium alginate 0.1%, allantoin 0.3%, jasmine extracting solution 0.5%, apple extracting solution 0.5%, seaweed are mentioned Object 10% is taken to be mixed to get C phase；
(4) B is added in A phase, after being saponified 20min at 70 DEG C, after cooling to 60 DEG C, C phase is added, adds 0.1% natural seaweed pigment, reverse mould, is first put into mold bottom for clean new fresh seaweed, slowly into mold after mixing evenly Soap lye is poured into, is demoulded after waiting to be cooled be hardened；
(5) it after being placed 3 days at aeration-drying, that is, can be used.
The preparation method of marine algae extract among the above:
(1) after rinsing sargassum fusifome well, drying crushes to obtain algae powder, 1g algae powder is uniformly mixed with the water of 20mL, keeps Temperature is extracted 24 hours under oscillating condition at 30 DEG C.
(2) step (2) concussion liquid is centrifuged at revolving speed 4000r/min 15min, removes bottom precipitation, obtains seaweed Extract.
Among the above, built-in new fresh seaweed is selected:
Fresh sargassum fusifome is slightly cleaned with sterile pure water, and after keeping free from admixture, slightly drying makes dry tack free, chooses breakage Blade, guarantee overall beautiful, be put into superclean bench stand-by.
Among the above, the extraction of natural seaweed pigment:
After fresh sargassum fusifome is cleaned up, is impregnated with 1 times of deionized water, smashs to pieces, vibrates 12h, with ultrasonic treatment It is taken out after 30min, filters out residue, obtain natural brown alga pigment.
Embodiment 2:
1. group cost implementation seaweed transparent soap ingredient and its weight percent are:
A phase: propylene glycol 10%, glycerol 15%, cocounut oil acyl glycine potassium 5%, sodium lauroyl sarcosine 2%, coconut oleoyl amine Propyl betaine 2%, stearic acid 4%, palmitinic acid 1%, myristic acid 2%, lauric acid 3%, coconut oil 6%, olive oil 4%, Sweet Almond Oil 4%；
B phase: sodium hydroxide 6%, sugared 8%, alcohol 5%, citric acid 2%, deionized water 6.4%；
C phase: sodium alginate 0.2%, allantoin 0.1%, jasmine extracting solution 1%, apple extracting solution 1%, marine algae extract 12%；
2. technical process:
(1) successively by propylene glycol 10%, glycerol 15%, cocounut oil acyl glycine potassium 5%, sodium lauroyl sarcosine 2%, cocounut oil Amido propyl betaine 2%, stearic acid 4%, palmitinic acid 1%, myristic acid 2%, lauric acid 3%, coconut oil 6%, olive oil 4%, Sweet Almond Oil 4% is heated at 70 DEG C, is allowed to be completely dissolved, is obtained A phase；
(2) sodium hydroxide 6%, sugared 8%, alcohol 5%, citric acid 2%, deionized water are sequentially added in another container 6.4% dissolves at 70 DEG C, obtains B phase；
(3) by sodium alginate 0.2%, allantoin 0.1%, jasmine extracting solution 1%, apple extracting solution 1%, marine algae extract 12% is mixed to get C phase；
(4) B is added in A phase, after being saponified 20min at 85 DEG C, after cooling to 60 DEG C, C phase is added, adds 0.3% natural seaweed pigment, reverse mould, is first put into mold bottom for clean new fresh seaweed, slowly into mold after mixing evenly Soap lye is poured into, is demoulded after waiting to be cooled be hardened；
(5) it after being placed 5 days at aeration-drying, that is, can be used.
The preparation method of marine algae extract among the above:
(1) after rinsing tawny daylily algae well, drying crushes to obtain algae powder, 1g algae powder is uniformly mixed with the water of 100mL, keeps Temperature is extracted 24 hours under oscillating condition at 60 DEG C.
(2) it is centrifuged 15min under the conditions of 4000r/min, obtains marine algae extract.
Among the above, built-in new fresh seaweed is selected:
New fresh laver is slightly cleaned with sterile pure water, and after keeping free from admixture, slightly drying makes dry tack free, chooses breakage Blade, guarantee is overall beautiful, is put into superclean bench stand-by.
Among the above, the extraction of natural seaweed pigment:
It after respectively cleaning up fresh seaweed, tawny daylily algae, impregnated with 1 times of deionized water, smash to pieces, vibrate 36h, with super It is taken out after sonication 30min, filters out residue, obtain the natural seaweed pigment of natural red algae, brown alga pigment.
Embodiment 3:
1. forming seaweed transparent soap ingredient and its weight percent of the present invention is:
A phase: propylene glycol 10%, glycerol 10%, cocounut oil acyl glycine potassium 6%, sodium lauroyl sarcosine 2%, stearic acid 5%, palmitinic acid 5%, myristic acid 1%, lauric acid 3%, olive oil 4%, Sweet Almond Oil 4%；
B phase: sodium hydroxide 5%, sugared 4%, alcohol 5%, citric acid 4%, deionized water 8.2%；
C phase: sodium alginate 0.1%, allantoin 0.2%, jasmine extracting solution 0.5%, apple extracting solution 2%, seaweed are extracted Object 20%；
2. technical process:
(1) by propylene glycol 10%, glycerol 10%, cocounut oil acyl glycine potassium 6%, sodium lauroyl sarcosine 2%, stearic acid 5%, palmitinic acid 5%, myristic acid 1%, lauric acid 3%, olive oil 4%, Sweet Almond Oil 4% are heated at 70 DEG C, are allowed to complete Dissolution, obtains A phase；
(2) sodium hydroxide 5%, sugared 4%, alcohol 5%, citric acid 4%, deionized water are sequentially added in another container 8.2% dissolves at 70 DEG C, obtains B phase；
(3) sodium alginate 0.1%, allantoin 0.2%, jasmine extracting solution 0.5%, apple extracting solution 2%, seaweed are extracted Object 20% is mixed to get C phase；
(4) B is added in A phase, after being saponified 100min at 75 DEG C, after cooling to 60 DEG C, C phase is added, adds 1% natural seaweed pigment, reverse mould, is first put into mold bottom for clean new fresh seaweed after mixing evenly, slowly falls into mold Enter soap lye, is demoulded after waiting to be cooled be hardened；
(2) it after being placed 7 days at aeration-drying, that is, can be used.
3. the preparation method of marine algae extract:
(1) after rinsing sea grape well, drying crushes to obtain algae powder, 1g algae powder is uniformly mixed with the water of 50mL, keeps Temperature is extracted 24 hours under oscillating condition at 40 DEG C.
(2) it is centrifuged 15min under the conditions of 4000r/min, obtains sample.
4. new fresh seaweed built in is selected:
Fresh sea grape is slightly cleaned with sterile pure water, and after keeping free from admixture, slightly drying makes dry tack free, chooses breakage Blade, guarantee overall beautiful, be put into superclean bench stand-by.
5. the extraction of natural seaweed pigment:
After respectively cleaning up fresh sea grape, Yi Guzao, sargassum fusifome, impregnated, smashed to pieces with 2 times of deionized waters, 12h is vibrated, with being taken out after ultrasonic treatment 60min, residue is filtered out, obtains the extracting solution of natural green-alga, red algae, brown alga pigment.
The quality evaluation of embodiment 4, above-described embodiment
1. using effect is tested: by the product of above-mentioned preparation, being respectively issued to 15 testers and compare use.Tester It is cleaned in the same manner using when sample, every kind of sample uses 2 weeks.Tester according to oneself feel comment Point.Standards of grading take ten point system, and 1 point worst, and 10 points best, and the better score more high effect the better.
2. foaming power and foam stability test: with reference to the reality in " preparation of mild foam mildy wash and its performance study " Proved recipe method, not Pei Zhi mass percentage be 10% each product solution 3mL, be placed in 50mL tool plug graduated cylinder in, add distilled water dilute It releases to 15mL, covers, acutely shake 10 times, immediate record foam volume (mL), record foam volume again after 10min.It repeats Measurement 3 times, is averaged.
3. organoleptic indicator: being tested according to the soap body appearance and smell test method of " QB/T 1913-2004 transparent soap ".
4. transparency detects: referring to " moulding mechanism and production method of transparent (translucent) soap ", use standard visual acuity chart (GB11533), transparency is five points corresponding to see the smallest " E " word of standard logarithmic visual acuity chart clearly with twenty-twenty vision person range estimation Score value (L) indicates that the more big then transparency of L value is better, and when L >=5.0 are translucent soap, L >=5.3 are transparent soap.
5. experimental result:
The test of 5.1 cleaning force:
5.2 foaming powers and foam stability test:
Index Initial volume (mL) Volume (mL) after 10min
Embodiment 1 41.01 38.01
Embodiment 2 45.00 35.01
Embodiment 3 38.49 31.65
5.3 organoleptic indicators: it is tested according to the soap body appearance and smell test method of " QB/T 1913-2004 transparent soap ".
Index Soap body appearance Smell
Embodiment 1 Color quality is uniform, transparency is good Meet regulation odor type
Embodiment 2 Color quality is uniform, transparency is good Meet regulation odor type
Embodiment 3 Color quality is uniform, transparency is good Meet regulation odor type
The detection of 5.4 transparencies:
Above-mentioned test result shows new fresh seaweed built in the transparent soap in the present invention, color multiplicity, existing general perfumed soap Cleaning force, and the effect of have the aesthetical properties of transparent soap, also have both nourishing and moisturizing, preparation method is simple, and pollution is few, is a kind of Transparent soap environmentally protective, nutrition is practical.
The above is only highly preferred embodiment of the present invention, is not intended to limit the present invention in any form, and is appointed What those skilled in the art, without departing from the scope of the technical proposal of the invention, using in the method for the disclosure above Appearance makes many possible changes and modifications to technical solution of the present invention, is all within the protection scope of the claims.

Claims (5)

1. a kind of transparent soap, which is characterized in that transparent soap ingredient and its weight percent are:
A phase: propylene glycol 6%, glycerol 20%, cocounut oil acyl glycine potassium 10%, stearic acid 8%, palmitinic acid 1%, myristic acid 4%, lauric acid 2%, coconut oil 4%, olive oil 4%；
B phase: sodium hydroxide 4%, sugared 4%, alcohol 2%, citric acid 1%, deionized water 18.5%；
C phase: sodium alginate 0.1%, allantoin 0.3%, jasmine extracting solution 0.5%, apple extracting solution 0.5%, marine algae extract 10%；
Natural seaweed pigment 0.1%.
2. a kind of transparent soap, which is characterized in that transparent soap ingredient and its weight percent are:
A phase: propylene glycol 10%, glycerol 15%, cocounut oil acyl glycine potassium 5%, sodium lauroyl sarcosine 2%, cocamidopropyl propyl amide Glycine betaine 2%, stearic acid 4%, palmitinic acid 1%, myristic acid 2%, lauric acid 3%, coconut oil 6%, olive oil 4%, sweet tea apricot Benevolence oil 4%；
B phase: sodium hydroxide 6%, sugared 8%, alcohol 5%, citric acid 2%, deionized water 6.4%；
C phase: sodium alginate 0.2%, allantoin 0.1%, jasmine extracting solution 1%, apple extracting solution 1%, marine algae extract 12%；
Natural seaweed pigment 0.3%.
3. a kind of transparent soap, which is characterized in that transparent soap ingredient and its weight percent are:
A phase: propylene glycol 10%, glycerol 10%, cocounut oil acyl glycine potassium 6%, sodium lauroyl sarcosine 2%, stearic acid 5%, palm fibre Palmitic acid acid 5%, myristic acid 1%, lauric acid 3%, olive oil 4%, Sweet Almond Oil 4%；
B phase: sodium hydroxide 5%, sugared 4%, alcohol 5%, citric acid 4%, deionized water 8.2%；
C phase: sodium alginate 0.1%, allantoin 0.2%, jasmine extracting solution 0.5%, apple extracting solution 2%, marine algae extract 20%；
Natural seaweed pigment 1%.
4. a kind of preparation method of transparent soap as claimed in any one of claims 1-3, which is characterized in that specifically include following Step:
(1) successively propylene glycol, glycerol, surfactant, stearic acid, palmitinic acid, myristic acid, lauric acid, basic grease are existed 70-90 DEG C of heating, is allowed to be completely dissolved, obtains A phase；
(2) sodium hydroxide, sugar, alcohol, citric acid, deionized water are sequentially added in another container to dissolve at 70-75 DEG C, are obtained To B phase；
(3) sodium alginate, allantoin, jasmine extracting solution, apple extracting solution, marine algae extract are mixed to get C phase；
(4) B is added in A phase, after being saponified 20-100min at 70-85 DEG C, cools to 60 DEG C, C phase is added, adds Natural seaweed pigment, reverse mould, slowly pours into soap lye into mold after mixing evenly, demoulds after waiting to be cooled be hardened；
(5) to get finished product after being placed 3-7 days at aeration-drying；
The surfactant be it is a kind of in sodium lauroyl sarcosine, cocounut oil acyl glycine potassium and Cocoamidopropyl betaine or Several combination of person, the basic grease are combinations one or several kinds of in coconut oil, Sweet Almond Oil and olive oil.
5. a kind of preparation method of transparent soap as claimed in claim 4, which is characterized in that specifically includes the following steps:
(1) successively by propylene glycol 6%, glycerol 20%, cocounut oil acyl glycine potassium 10%, stearic acid 8%, palmitinic acid 1%, nutmeg Acid 4%, lauric acid 2%, coconut oil 4%, olive oil 4% are heated at 70-90 DEG C, are allowed to be completely dissolved, are obtained A phase；
(2) sodium hydroxide 4%, sugared 4%, alcohol 2%, citric acid 1%, deionized water 18.5% are sequentially added in another container It is dissolved at 70-75 DEG C, obtains B phase；
(3) by sodium alginate 0.1%, allantoin 0.3%, jasmine extracting solution 0.5%, apple extracting solution 0.5%, marine algae extract 10% is mixed to get C phase；
(4) B is added in A phase, after being saponified 20min at 70-85 DEG C, cools to 60 DEG C, C phase is added, is added 0.1% day Right seaweed pigment, reverse mould, slowly pours into soap lye into mold after mixing evenly, demoulds after waiting to be cooled be hardened；
(5) to get finished product after being placed 3 days at aeration-drying.
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CN108498392A (en) * 2017-05-22 2018-09-07 太仓市神英中草药专业合作社 A kind of Chinese herbal medicine facial cleanser

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Publication number Priority date Publication date Assignee Title
JP2011157489A (en) * 2010-02-01 2011-08-18 Kyoko Inami Caulerpa lentillifera soap and process for producing the same
CN102978048A (en) * 2012-11-16 2013-03-20 广州伊凡生物科技有限公司 Weakly acidic transparent soap and preparation method thereof
CN104371861A (en) * 2013-08-15 2015-02-25 青岛鹏远康华天然产物有限公司 Seaweed health soap and making method thereof
KR20150049112A (en) * 2013-10-29 2015-05-08 (주)제주사랑농수산 A Soap Composition Containing Algae Fabrics
CN105062731A (en) * 2015-08-20 2015-11-18 广州栋方生物科技股份有限公司 Fermented-shea-butter amino acid transparent soap

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011157489A (en) * 2010-02-01 2011-08-18 Kyoko Inami Caulerpa lentillifera soap and process for producing the same
CN102978048A (en) * 2012-11-16 2013-03-20 广州伊凡生物科技有限公司 Weakly acidic transparent soap and preparation method thereof
CN104371861A (en) * 2013-08-15 2015-02-25 青岛鹏远康华天然产物有限公司 Seaweed health soap and making method thereof
KR20150049112A (en) * 2013-10-29 2015-05-08 (주)제주사랑농수산 A Soap Composition Containing Algae Fabrics
CN105062731A (en) * 2015-08-20 2015-11-18 广州栋方生物科技股份有限公司 Fermented-shea-butter amino acid transparent soap

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