CN106265277B - Shampoo for children and preparation method thereof - Google Patents
Shampoo for children and preparation method thereof Download PDFInfo
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- CN106265277B CN106265277B CN201610766224.2A CN201610766224A CN106265277B CN 106265277 B CN106265277 B CN 106265277B CN 201610766224 A CN201610766224 A CN 201610766224A CN 106265277 B CN106265277 B CN 106265277B
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/37—Esters of carboxylic acids
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
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- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/892—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a hydroxy group, e.g. dimethiconol
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- A61Q5/02—Preparations for cleaning the hair
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Abstract
The invention discloses a kind of shampoo for children and preparation method thereof, the shampoo for children is prepared by following raw materials: water, laureth sodium sulfovinate, ethylene glycol distearyl acid, coconut oleoyl amine MEA, betaines surfactant, sodium chloride, dimethiconol, dimethyl silicone polymer, carbomer, hydrolyze sericin, tip edge bladder-wrack extract, yellow tang extract, pierce Asparagus toxiformis (Delile) Coll et Harv extract, sorbierite, essence, ammonia-terminated polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride, sodium hydroxide, methylchloroisothiazandnone, methylisothiazolinone, Phenoxyethanol, tetra- sodium of EDTA, citric acid.Shampoo for children of the present invention contains a variety of natural components, gives the triple loves of child: Shu Rou, moistening, protection, while helping effectively clean scalp and hair-care, water moistens scalp, and soft brighten the hair silk enables the hair of child is soft and moist to distribute gloss.
Description
Technical field
The present invention relates to daily-use chemical industry technical fields, and in particular to a kind of shampoo for children and preparation method thereof.
Background technique
With the acceleration of human industryization process, pollutant component becomes more and more in atmosphere, for example, vehicle exhaust and
Chemical component contained in haze is extremely complex, so that hair, the scalp to human body also bring more threats.
Shampoo is one of domestic bathing articles.Current market sales of shampoo articles are various in style, quality discrepancy
Also big.Usually only there is washing effect, have a single function.Also, traditional shampoo is added to improve cleaning force and ability of deoiling
A large amount of extremely strong surfactants of alkalinity, foaming agent, the ingredients such as soap base, and the skin of human body be it is weakly acidic, for a long time
Using skin can be stimulated.More seriously, the sebum film of skin can be also destroyed.Once lose sebum film, skin be easy to by
To external injury.
Shampoo for children needs profession to develop, and child skin is delicate, cannot use adult cleaning chemical products, otherwise can injure
Skin, and the chemical substance contained in adult cleaning chemical products will affect children's health.
Summary of the invention
Aiming at the above shortcomings existing in the prior art, the first technical problem to be solved by the present invention is to provide a kind of youngster
Virgin shampoo.
The two of the technical issues of solution of the invention are to provide a kind of preparation method of shampoo for children.
Object of the present invention is to what is be achieved through the following technical solutions:
A kind of shampoo for children is prepared by following raw materials: water, laureth sodium sulfovinate, ethylene glycol distearyl
Acid, coconut oleoyl amine MEA, betaines surfactant, sodium chloride, dimethiconol, dimethyl silicone polymer, card wave
Nurse, hydrolysis sericin, tip edge bladder-wrack extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, sorbierite, essence, ammonia end
Dimethyl silicone polymer, guar hydroxypropyltrimonium ammonium chloride, sodium hydroxide, methylchloroisothiazandnone, methyl-isothiazol
Quinoline ketone, Phenoxyethanol, tetra- sodium of EDTA, citric acid.
A kind of shampoo for children is prepared by the raw material of following weight parts: 45-55 parts of laureth sodium sulfovinate,
15-25 parts of ethylene glycol distearyl acid, 35-45 parts of coconut oleoyl amine MEA, 45-55 parts of betaines surfactant, sodium chloride 1-
10 parts, 1-10 parts of dimethiconol, 1-10 parts of dimethyl silicone polymer, 5-15 parts of carbomer, hydrolysis sericin 15-
25 parts, 1-10 parts of tip edge bladder-wrack extract, 1-10 parts of yellow tang extract, thorn 1-10 parts of Asparagus toxiformis (Delile) Coll et Harv extract, sorbierite 5-
15 parts, 1-10 parts of ammonia-terminated polydimethylsiloxane, 5-15 parts of guar hydroxypropyltrimonium ammonium chloride, 1-10 parts of sodium hydroxide,
0.1-1 parts of methylchloroisothiazandnone, 0.1-1 parts of methylisothiazolinone, 1-10 parts of Phenoxyethanol, 1-10 parts of tetra- sodium of EDTA,
1-10 parts of citric acid, 0.1-1 parts of essence, 700-900 parts of water.
Preferably, the essence is vanillic aldehyde, lemon extract, Mint Essence, lavender oil, flavoring rose essence etc..
Preferably, the betaines surfactant is Cocoamidopropyl betaine, 3- sulfopropyl cetyl
One or more mixture in diformazan glycine betaine, oleamide propyl betaine.
It is highly preferred that the betaines surfactant is by Cocoamidopropyl betaine, 3- sulfopropyl hexadecane
Base diformazan glycine betaine, oleamide propyl betaine mix, the Cocoamidopropyl betaine, 3- sulfopropyl cetyl
Diformazan glycine betaine, oleamide propyl betaine mass ratio be (1-3): (1-3): (1-3).
The present invention also provides the preparation methods of above-mentioned shampoo for children, comprising the following steps:
65-85 DEG C is heated water to, laureth sodium sulfovinate, ethylene glycol distearyl are sequentially added under stirring condition
Acid, coconut oleoyl amine MEA, betaines surfactant, dimethiconol, dimethyl silicone polymer, carbomer, ammonia end
Dimethyl silicone polymer, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 45-55 DEG C, are sequentially added
Sorbierite, essence, methylchloroisothiazandnone, methylisothiazolinone, Phenoxyethanol, tetra- sodium of EDTA, citric acid, hydroxide
Sodium, sodium chloride, hydrolysis sericin, tip edge bladder-wrack extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract are stirred
It is even to obtain the final product.
Specifically, in the present invention:
Lemon extract, the lemon extract provided using Shanghai bright moon daily use chemicals Co., Ltd in the embodiment of the present invention.
Cocoamidopropyl betaine, No. CAS: 86438-79-1.
3- sulfopropyl etradecyldimethylamine glycine betaine, No. CAS: 2281-11-0.
Oleamide propyl betaine, No. CAS: 25054-76-6.
Ethylene glycol distearyl acid, No. CAS: 627-83-8.
Dimethiconol, No. CAS: 68938-54-5, it is provided using Dow Corning Corporation in the embodiment of the present invention
Model PMX-1403 dimethiconol.
Dimethyl silicone polymer, No. CAS: 9016-00-6.
Carbomer, No. CAS: 76050-42-5.It is provided in the embodiment of the present invention using U.S. Lu Runbo (former promise reputation) company
Acritamer 940.
Sericin is hydrolyzed, the side of embodiment two in number of patent application 201310511239.0 is used in the embodiment of the present invention
Method preparation.
Ammonia-terminated polydimethylsiloxane, No. CAS: 71750-80-6, the fragrant refined chemical industry in Guangzhou is used in the embodiment of the present invention
The ammonia-terminated polydimethylsiloxane TCN-620 that Co., Ltd provides.
Guar hydroxypropyltrimonium ammonium chloride, No. CAS: 65497-29-2, using Yutai County sea in the embodiment of the present invention
Receive Environmental Protection Technology Co., Ltd offer guar hydroxypropyltrimonium ammonium chloride C-14S.
Phenoxyethanol, i.e. ethylene glycol phenyl ether, No. CAS: 122-99-6.
Laureth sodium sulfovinate, No. CAS: 9004-82-4.It is provided in the embodiment of the present invention using Japanese Kao company
Model EMAL 270S laureth sodium sulfovinate.
Coconut oleoyl amine MEA, i.e. Coconut Fatty Acid Monoethanolamide, No. CAS: 68140-00-1.Four are used in the embodiment of the present invention
The FS600-CMEA Coconut Fatty Acid Monoethanolamide (being free of glycerol) that Chuan Hua language Fine Chemical Co., Ltd provides.
Tetra- sodium of EDTA, i.e. tetrasodium ethylenediamine tetraacetate, No. CAS: 64-02-8.
Sodium chloride, No. CAS: 7647-14-5.
Citric acid, No. CAS: 77-92-9.
Sodium hydroxide, No. CAS: 1310-73-2.
Methylchloroisothiazandnone, No. CAS: 26172-55-4.
Methylisothiazolinone, No. CAS: 2682-20-4.
Sorbierite, also known as D- D-sorbite, No. CAS: 50-70-4.
Tip edge bladder-wrack extract, English name: Fucus Serratus Extrac, from Boulez Brittany area
Tip edge bladder-wrack, locals are known as " gold seaweed ".The algae extract has reinforcing fiber archaeocyte vigor, and protection mitochondria is thin
Born of the same parents promote cutaneous respiration, bring powerful moisture-keeping efficacy for skin, and Cucumber Extract water storage function also can promote regeneration, increase
Cell viability restores skin life, promotes the metabolism of skin, effectively antagonizes free radical, confrontation cell senescence, discharges simultaneously
Active-energy improves dry, prevention microgroove, wrinkle generates, delay skin aging.Tip edge bladder-wrack extract can be prepared or be purchased
It can buy, preparation method can be conventional water extraction or alcohol extracting method, such as according to solid-liquid after tip edge bladder-wrack is cleaned and crush
Immersing mass fraction than (g/ml) 1:10-1:30 is to impregnate 8-12h in 95% ethyl alcohol, be heated to reflux 4-6h, cooling, is filtered, will
After filtrate concentration, it is lyophilized into powder.Tip edge bladder-wrack extract used in the present invention is bought from Nanjing Ze Lang medicine section
Skill Co., Ltd, the 1g tip edge bladder-wrack extract that specification 10:1, i.e. 10g tip edge bladder-wrack are extracted.
Yellow tang extract, English name: Ascophyllum Nodosum Extract, have it is antitumor, antiviral,
Antibacterial eliminates free radical, anti-oxidation efficacy.Yellow tang extract can be prepared or is commercially available, and preparation method can be conventional
Water extraction or alcohol extracting method, for example immerse mass fraction according to solid-to-liquid ratio (g/ml) 1:10-1:30 after yellow tang is cleaned and crush
Cooling to impregnate 8-12h, being heated to reflux 4-6h in 95% ethyl alcohol, filtering after filtrate is concentrated, is lyophilized into powder.The present invention
Used in yellow tang extract be purchase from Xi'an all places Biotechnology Co., Ltd, specification 10:1, i.e. 10g yellow tang
The 1g yellow tang extract extracted.
Pierce Asparagus toxiformis (Delile) Coll et Harv marine algae extract, English name: Asparagopsis Armata Extract is rich in activated silica, energy
Effectively optimization skin cell metabolism has skin reconstruction, lipolysis, resists oedema, skin quality moisture-keeping efficacy.Pierce Asparagus toxiformis (Delile) Coll et Harv
Marine algae extract can be prepared or is commercially available, and preparation method can be conventional water extraction or alcohol extracting method, for example will pierce Haimen
It is to impregnate 8-12h in 95% ethyl alcohol that winter seaweed, which immerses mass fraction according to solid-to-liquid ratio (g/ml) 1:10-1:30 after cleaning and crush,
It is heated to reflux 4-6h, cooling, filtering after filtrate is concentrated, is lyophilized into powder.Thorn Asparagus toxiformis (Delile) Coll et Harv seaweed used in the present invention mentions
Taking object is beautiful (EXSYMOL) company in purchase self-love west, the 1g that specification 10:1, i.e. 10g thorn Asparagus toxiformis (Delile) Coll et Harv marine algae extract extract
Pierce Asparagus toxiformis (Delile) Coll et Harv marine algae extract.
Shampoo for children of the present invention contains a variety of natural components, gives the triple loves of child: Shu Rou, moistening, protection, side
While helping effectively clean scalp and hair-care, water moistens scalp, and soft brighten the hair silk enables the hair of child is soft and moist to distribute gloss.
Specific embodiment
The present invention will be further explained with reference to the examples below, as described below, is only to preferable implementation of the invention
Example, not limits the present invention, any person skilled in the art is possibly also with the disclosure above
Technology contents be changed to the equivalent embodiment changed on an equal basis.Without departing from the concept of the present invention, according to the present invention
Technical spirit any simple modification or equivalent variations that following embodiment is made, fall within the scope of protection of the present invention.
Embodiment 1
Shampoo for children raw material (parts by weight): 50 parts of laureth sodium sulfovinate, ethylene glycol distearyl sour 20 parts, cocounut oil
40 parts of amide MEA, 51 parts of betaines surfactant, 5 parts of sodium chloride, 3 parts of dimethiconol, poly dimethyl silicon
2 parts of oxygen alkane, 7 parts of carbomer, 20 parts of sericin of hydrolysis, 4 parts of tip edge bladder-wrack extract, 4 parts of yellow tang extract, thorn Haimen
4 parts of winter extract, 10 parts of sorbierite, 2 parts of ammonia-terminated polydimethylsiloxane, 10 parts of guar hydroxypropyltrimonium ammonium chloride, hydrogen
2 parts of sodium oxide molybdena, 0.15 part of methylchloroisothiazandnone, 0.15 part of methylisothiazolinone, 3 parts of Phenoxyethanol, tetra- sodium 1.2 of EDTA
Part, 4 parts of citric acid, 0.18 part of lemon extract, 800 parts of water.
The betaines surfactant is by Cocoamidopropyl betaine, 3- sulfopropyl etradecyldimethylamine beet
Alkali, oleamide propyl betaine are that 1:1:1 is uniformly mixed to obtain in mass ratio.
The preparation method of above-mentioned shampoo for children, comprising the following steps:
75 DEG C are heated water to, laureth sodium sulfovinate, ethylene glycol two are sequentially added under 500 revs/min of stirring conditions
Stearic acid, coconut oleoyl amine MEA, betaines surfactant, dimethiconol, dimethyl silicone polymer, carbomer,
Ammonia-terminated polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 48 DEG C, are sequentially added
Sorbierite, lemon extract, methylchloroisothiazandnone, methylisothiazolinone, Phenoxyethanol, tetra- sodium of EDTA, citric acid, hydrogen-oxygen
Change sodium, sodium chloride, hydrolysis sericin, tip edge bladder-wrack extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract to be stirred
Uniformly.Obtain the shampoo for children of embodiment 1.
Embodiment 2
Shampoo for children raw material (parts by weight): 50 parts of laureth sodium sulfovinate, ethylene glycol distearyl sour 20 parts, cocounut oil
40 parts of amide MEA, 51 parts of betaines surfactant, 5 parts of sodium chloride, 3 parts of dimethiconol, poly dimethyl silicon
2 parts of oxygen alkane, 7 parts of carbomer, hydrolysis 20 parts of sericin, 6 parts of tip edge bladder-wrack extract, 6 parts of yellow tang extract, sorbierite
10 parts, 2 parts of ammonia-terminated polydimethylsiloxane, 10 parts of guar hydroxypropyltrimonium ammonium chloride, 2 parts of sodium hydroxide, methyl chloride it is different
0.15 part of thiazolinone, 0.15 part of methylisothiazolinone, 3 parts of Phenoxyethanol, 1.2 parts of tetra- sodium of EDTA, 4 parts of citric acid, lemon
0.18 part of essence, 800 parts of water.
The betaines surfactant is by Cocoamidopropyl betaine, 3- sulfopropyl etradecyldimethylamine beet
Alkali, oleamide propyl betaine are that 1:1:1 is uniformly mixed to obtain in mass ratio.
The preparation method of above-mentioned shampoo for children, comprising the following steps:
75 DEG C are heated water to, laureth sodium sulfovinate, ethylene glycol two are sequentially added under 500 revs/min of stirring conditions
Stearic acid, coconut oleoyl amine MEA, betaines surfactant, dimethiconol, dimethyl silicone polymer, carbomer,
Ammonia-terminated polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 48 DEG C, are sequentially added
Sorbierite, lemon extract, methylchloroisothiazandnone, methylisothiazolinone, Phenoxyethanol, tetra- sodium of EDTA, citric acid, hydrogen-oxygen
Change sodium, sodium chloride, hydrolysis sericin, tip edge bladder-wrack extract, yellow tang extract to be uniformly mixed.Obtain embodiment
2 shampoo for children.
Embodiment 3
Shampoo for children raw material (parts by weight): 50 parts of laureth sodium sulfovinate, ethylene glycol distearyl sour 20 parts, cocounut oil
40 parts of amide MEA, 51 parts of betaines surfactant, 5 parts of sodium chloride, 3 parts of dimethiconol, poly dimethyl silicon
2 parts of oxygen alkane, 7 parts of carbomer, 20 parts of sericin of hydrolysis, 6 parts of tip edge bladder-wrack extract, thorn 6 parts of Asparagus toxiformis (Delile) Coll et Harv extract, sorb
10 parts of alcohol, 2 parts of ammonia-terminated polydimethylsiloxane, 10 parts of guar hydroxypropyltrimonium ammonium chloride, 2 parts of sodium hydroxide, methyl chloride
0.15 part of isothiazolinone, 0.15 part of methylisothiazolinone, 3 parts of Phenoxyethanol, 1.2 parts of tetra- sodium of EDTA, 4 parts of citric acid, lemon
0.18 part of lemon essence, 800 parts of water.
The betaines surfactant is by Cocoamidopropyl betaine, 3- sulfopropyl etradecyldimethylamine beet
Alkali, oleamide propyl betaine are that 1:1:1 is uniformly mixed to obtain in mass ratio.
The preparation method of above-mentioned shampoo for children, comprising the following steps:
75 DEG C are heated water to, laureth sodium sulfovinate, ethylene glycol two are sequentially added under 500 revs/min of stirring conditions
Stearic acid, coconut oleoyl amine MEA, betaines surfactant, dimethiconol, dimethyl silicone polymer, carbomer,
Ammonia-terminated polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 48 DEG C, are sequentially added
Sorbierite, lemon extract, methylchloroisothiazandnone, methylisothiazolinone, Phenoxyethanol, tetra- sodium of EDTA, citric acid, hydrogen-oxygen
Change sodium, sodium chloride, hydrolysis sericin, tip edge bladder-wrack extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract to be uniformly mixed.Implemented
The shampoo for children of example 3.
Embodiment 4
Shampoo for children raw material (parts by weight): 50 parts of laureth sodium sulfovinate, ethylene glycol distearyl sour 20 parts, cocounut oil
40 parts of amide MEA, 51 parts of betaines surfactant, 5 parts of sodium chloride, 3 parts of dimethiconol, poly dimethyl silicon
2 parts of oxygen alkane, 7 parts of carbomer, 20 parts of sericin of hydrolysis, 6 parts of yellow tang extract, thorn 6 parts of Asparagus toxiformis (Delile) Coll et Harv extract, sorbierite 10
Part, 2 parts of ammonia-terminated polydimethylsiloxane, 10 parts of guar hydroxypropyltrimonium ammonium chloride, 2 parts of sodium hydroxide, the different thiophene of methyl chloride
0.15 part of oxazoline ketone, 0.15 part of methylisothiazolinone, 3 parts of Phenoxyethanol, 1.2 parts of tetra- sodium of EDTA, 4 parts of citric acid, lemonene
0.18 part, 800 parts of water of essence.
The betaines surfactant is by Cocoamidopropyl betaine, 3- sulfopropyl etradecyldimethylamine beet
Alkali, oleamide propyl betaine are that 1:1:1 is uniformly mixed to obtain in mass ratio.
The preparation method of above-mentioned shampoo for children, comprising the following steps:
75 DEG C are heated water to, laureth sodium sulfovinate, ethylene glycol two are sequentially added under 500 revs/min of stirring conditions
Stearic acid, coconut oleoyl amine MEA, betaines surfactant, dimethiconol, dimethyl silicone polymer, carbomer,
Ammonia-terminated polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 48 DEG C, are sequentially added
Sorbierite, lemon extract, methylchloroisothiazandnone, methylisothiazolinone, Phenoxyethanol, tetra- sodium of EDTA, citric acid, hydrogen-oxygen
Change sodium, sodium chloride, hydrolysis sericin, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract to be uniformly mixed.Obtain embodiment 4
Shampoo for children.
Embodiment 5
Substantially the same manner as Example 1, difference is only in that: the betaines surfactant is by 3- sulfopropyl 16
Alkyl-dimethyl glycine betaine, oleamide propyl betaine are that 1:1 is uniformly mixed to obtain in mass ratio.Obtain the youngster of embodiment 5
Virgin shampoo.
Embodiment 6
Substantially the same manner as Example 1, difference is only in that: the betaines surfactant is by cocamidopropyl propyl amide
Glycine betaine, oleamide propyl betaine are that 1:1 is uniformly mixed to obtain in mass ratio.Obtain the shampoo for children of embodiment 6.
Embodiment 7
Substantially the same manner as Example 1, difference is only in that: the betaines surfactant is by cocamidopropyl propyl amide
Glycine betaine, 3- sulfopropyl etradecyldimethylamine glycine betaine are that 1:1 is uniformly mixed to obtain in mass ratio.Obtain embodiment 7
Shampoo for children.
Test case 1
According to method disclosed in " foundation and application study of the anti-dandruff effect detection evaluation method of shampoo " to embodiment
Shampoo made from 1-7 carries out inhibition zone diameter test, evaluates anti-dandruff effect of shampoo product.Inhibition zone diameter is got over
Greatly, anti-dandruff effect is better.Test data is shown in Table 1.
Wherein, " foundation and application study of the anti-dandruff effect detection evaluation method of shampoo ", where, Wang Tan, Jia Zebao, flood
Know roc, Peng Jin, research and development department of Si Bao daily use chemicals Co., Ltd, household chemicals science, o. 11th in 2009.
Table 1: anti-dandruff efficacy test tables of data
Inhibition zone diameter, mm | |
Embodiment 1 | 23.5 |
Embodiment 2 | 18.7 |
Embodiment 3 | 19.5 |
Embodiment 4 | 18.8 |
Embodiment 5 | 20.2 |
Embodiment 6 | 19.6 |
Embodiment 7 | 20.1 |
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (tip edge bladder-wrack extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv
Extract compounding) anti-dandruff effect is substantially better than embodiment 2-4 (tip edge bladder-wrack extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv mentions
Take both any compounding in object);Comparing embodiment 1 and embodiment 5-7, embodiment 1 (Cocoamidopropyl betaine, 3- sulphur third
Base etradecyldimethylamine glycine betaine, oleamide propyl betaine compounding) anti-dandruff effect is substantially better than embodiment 5-7 (coconut oleoyl amine
Propyl betaine, 3- sulfopropyl etradecyldimethylamine glycine betaine, both any compounding in oleamide propyl betaine).
Test case 2
By shampoo for children made from embodiment 1-7, carried out respectively with dark brown vial it is filling, open wide bottle cap, be placed in
Preservation 90 days under 40 DEG C of environment temperature, 85% environment of relative humidity, staphylococcus aureus (ATCC 6538) bacterium colony is then carried out
Sum test, measures referring to GBT 4789.2-2008 microbiological test of food hygiene total plate count.Specific test result is shown in Table
2。
Table 2: total plate count tests table
S. aureus colonies sum, cfu/g | |
Embodiment 1 | 253 |
Embodiment 2 | 783 |
Embodiment 3 | 767 |
Embodiment 4 | 763 |
Embodiment 5 | 572 |
Embodiment 6 | 584 |
Embodiment 7 | 559 |
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (tip edge bladder-wrack extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv
Extract compounding) antiseptic property be substantially better than embodiment 2-4 (tip edge bladder-wrack extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv mention
Take both any compounding in object);Comparing embodiment 1 and embodiment 5-7, embodiment 1 (Cocoamidopropyl betaine, 3- sulphur third
Base etradecyldimethylamine glycine betaine, oleamide propyl betaine compounding) antiseptic property is substantially better than embodiment 5-7 (coconut oleoyl amine
Propyl betaine, 3- sulfopropyl etradecyldimethylamine glycine betaine, both any compounding in oleamide propyl betaine).
Claims (4)
1. a kind of shampoo for children, which is characterized in that be prepared by the raw material of following weight parts: laureth sodium sulfovinate
45-55 parts, 15-25 parts of ethylene glycol distearyl acid, 35-45 parts of coconut oleoyl amine MEA, 45-55 parts of betaines surfactant,
1-10 parts of sodium chloride, 1-10 parts of dimethiconol, 1-10 parts of dimethyl silicone polymer, 5-15 parts of carbomer, hydrolyzed-silk
15-25 parts of glue protein, 1-10 parts of tip edge bladder-wrack extract, 1-10 parts of yellow tang extract, thorn 1-10 parts of Asparagus toxiformis (Delile) Coll et Harv extract,
5-15 parts of sorbierite, 1-10 parts of ammonia-terminated polydimethylsiloxane, 5-15 parts of guar hydroxypropyltrimonium ammonium chloride, sodium hydroxide
1-10 parts, 0.1-1 parts of methylchloroisothiazandnone, 0.1-1 parts of methylisothiazolinone, 1-10 parts of Phenoxyethanol, tetra- sodium of EDTA
1-10 parts, 1-10 parts of citric acid, 0.1-1 parts of essence, 700-900 parts of water.
2. shampoo for children as described in claim 1, it is characterised in that: the betaines surfactant is cocounut oil acyl
Amine propyl betaine, 3- sulfopropyl etradecyldimethylamine glycine betaine, mixture one or more in oleamide propyl betaine.
3. shampoo for children as claimed in claim 2, it is characterised in that: the betaines surfactant is by cocounut oil acyl
Amine propyl betaine, 3- sulfopropyl etradecyldimethylamine glycine betaine, oleamide propyl betaine mix, the coconut oleoyl amine
Propyl betaine, 3- sulfopropyl etradecyldimethylamine glycine betaine, oleamide propyl betaine mass ratio be (1-3): (1-3):
(1-3)。
4. the preparation method of shampoo for children as claimed in any one of claims 1-3, which is characterized in that including following step
It is rapid:
65-85 DEG C is heated water to, laureth sodium sulfovinate, ethylene glycol distearyl acid, coconut palm are sequentially added under stirring condition
Oleamide MEA, betaines surfactant, dimethiconol, dimethyl silicone polymer, carbomer, ammonia end poly- two
Methylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 45-55 DEG C, are sequentially added sorb
Alcohol, essence, methylchloroisothiazandnone, methylisothiazolinone, Phenoxyethanol, tetra- sodium of EDTA, citric acid, sodium hydroxide, chlorine
Change sodium, hydrolysis sericin, tip edge bladder-wrack extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract to be uniformly mixed i.e.
?.
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CN107669552B (en) * | 2017-10-31 | 2019-08-16 | 思拓科(上海)生物科技股份有限公司 | Organic baby's shampoo |
CN107913230A (en) * | 2017-11-27 | 2018-04-17 | 曾万祥 | A kind of ginger juice albumen conserves shampoo |
CN107822975A (en) * | 2017-11-29 | 2018-03-23 | 桂林华诺威生物科技有限公司 | A kind of draft collagen shampoo |
CN108125804A (en) * | 2018-01-29 | 2018-06-08 | 南阳师范学院 | A kind of antibacterial light shampoo paste and preparation method thereof |
CN115813819A (en) * | 2022-12-03 | 2023-03-21 | 福建省梦娇兰日用化学品有限公司 | Children shampoo free of silicone oil and preparation method thereof |
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