CN106265277A - Shampoo for children and preparation method thereof - Google Patents
Shampoo for children and preparation method thereof Download PDFInfo
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- CN106265277A CN106265277A CN201610766224.2A CN201610766224A CN106265277A CN 106265277 A CN106265277 A CN 106265277A CN 201610766224 A CN201610766224 A CN 201610766224A CN 106265277 A CN106265277 A CN 106265277A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/892—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a hydroxy group, e.g. dimethiconol
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- A61K8/898—Polysiloxanes containing atoms other than silicon, carbon, oxygen and hydrogen, e.g. dimethicone copolyol phosphate containing nitrogen, e.g. amodimethicone, trimethyl silyl amodimethicone or dimethicone propyl PG-betaine
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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Abstract
The invention discloses a kind of shampoo for children and preparation method thereof, described shampoo for children is prepared from by following raw material: water, sodium laureth sulfate, ethylene glycol bisthioglycolate stearic acid, coconut oleoyl amine MEA, betaines surfactant, sodium chloride, dimethiconol, polydimethylsiloxane, carbomer, hydrolyzed-silk glue protein, tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, sorbitol, essence, ammonia end polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride, sodium hydroxide, methylchloroisothiazandnone, Methylisothiazolinone, phenoxyethanol, EDTA tetra-sodium, citric acid.Shampoo for children of the present invention, contains multiple natural component, gives child triple love: Shu Rou, moisten, protection, while helping effectively clean scalp and hair-care, water profit scalp, soft bright hair, make that the hair of child is soft and moist distributes gloss.
Description
Technical field
The present invention relates to daily-use chemical industry technical field, be specifically related to a kind of shampoo for children and preparation method thereof.
Background technology
Along with the acceleration of human industryization process, in air, pollutant component becomes more and more, such as vehicle exhaust and
Chemical composition contained in haze is extremely complex, thus hair, the scalp of human body is also brought more threat.
Shampoo is one of domestic bathing articles for use.The shampoo articles for use sold in the market are various in style, quality discrepancy
The biggest.Generally only there is clean result, function singleness.Further, tradition shampoo, in order to improve cleaning force and ability of deoiling, adds
The surfactant that a large amount of alkalescence are extremely strong, foaming agent, the composition such as soap base, and the skin of human body is weakly acidic, for a long time
Use Diazolidinyl Urea.More seriously, the sebum film of skin also can be destroyed.Once losing sebum film, skin is easy to be subject to
To external injury.
Shampoo for children needs specialty to develop, and child skin is tender and lovely, it is impossible to uses the cleaning chemical products of adult, otherwise can injure
Skin, and the chemical substance contained in cleaning chemical products of being grown up can affect children's health.
Summary of the invention
For above-mentioned deficiency present in prior art, one of the technical problem to be solved is to provide a kind of youngster
Virgin shampoo.
Solve the technical problem that the two of the present invention are to provide the preparation method of a kind of shampoo for children.
The present invention seeks to be achieved through the following technical solutions:
A kind of shampoo for children, is prepared from by following raw material: water, sodium laureth sulfate, ethylene glycol bisthioglycolate are stearic
Acid, coconut oleoyl amine MEA, betaines surfactant, sodium chloride, dimethiconol, polydimethylsiloxane, card ripple
Nurse, hydrolyzed-silk glue protein, tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, sorbitol, essence, ammonia end
Polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride, sodium hydroxide, methylchloroisothiazandnone, methyl-isothiazol
Quinoline ketone, phenoxyethanol, EDTA tetra-sodium, citric acid.
A kind of shampoo for children, is prepared from by the raw material of following weight parts: sodium laureth sulfate 45-55 part,
Ethylene glycol bisthioglycolate stearic acid 15-25 part, coconut oleoyl amine MEA 35-45 part, betaines surfactant 45-55 part, sodium chloride 1-
10 parts, dimethiconol 1-10 part, polydimethylsiloxane 1-10 part, carbomer 5-15 part, hydrolyzed-silk glue protein 15-
25 parts, tip edge Fucus Vesiculosus extract 1-10 part, yellow tang extract 1-10 part, thorn Asparagus toxiformis (Delile) Coll et Harv extract 1-10 part, sorbitol 5-
15 parts, ammonia end polydimethylsiloxane 1-10 part, guar hydroxypropyltrimonium ammonium chloride 5-15 part, sodium hydroxide 1-10 part,
Methylchloroisothiazandnone 0.1-1 part, Methylisothiazolinone 0.1-1 part, phenoxyethanol 1-10 part, EDTA tetra-sodium 1-10 part,
Citric acid 1-10 part, essence 0.1-1 part, water 700-900 part.
Preferably, described essence is vanillin, Fructus Citri Limoniae essence, Mint Essence, lavandula angustifolia essence, rose essence etc..
Preferably, described betaines surfactant is cocamido propyl betaine, 3-sulfopropyl cetyl
The mixture of one or more in diformazan glycine betaine, oleamide CAB.
It is highly preferred that described betaines surfactant is by cocamido propyl betaine, 3-sulfopropyl hexadecane
Base diformazan glycine betaine, oleamide CAB mix, described cocamido propyl betaine, 3-sulfopropyl cetyl
Diformazan glycine betaine, the mass ratio of oleamide CAB are (1-3): (1-3): (1-3).
Present invention also offers the preparation method of above-mentioned shampoo for children, comprise the following steps:
Heat water to 65-85 DEG C, under stirring condition, be sequentially added into sodium laureth sulfate, ethylene glycol bisthioglycolate tristearin
Acid, coconut oleoyl amine MEA, betaines surfactant, dimethiconol, polydimethylsiloxane, carbomer, ammonia end
Polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 45-55 DEG C, sequentially add
Sorbitol, essence, methylchloroisothiazandnone, Methylisothiazolinone, phenoxyethanol, EDTA tetra-sodium, citric acid, hydroxide
Sodium, sodium chloride, hydrolyzed-silk glue protein, tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract stirring mixing are all
Even and get final product.
Concrete, in the present invention:
Fructus Citri Limoniae essence, uses the Fructus Citri Limoniae essence that Shanghai bright moon daily use chemicals company limited provides in the embodiment of the present invention.
Cocamido propyl betaine, No. CAS: 86438-79-1.
3-sulfopropyl etradecyldimethylamine glycine betaine, No. CAS: 2281-11-0.
Oleamide CAB, No. CAS: 25054-76-6.
Ethylene glycol bisthioglycolate stearic acid, No. CAS: 627-83-8.
Dimethiconol, No. CAS: 68938-54-5, the embodiment of the present invention use Dow Corning Corporation provide
Model is PMX-1403 dimethiconol.
Polydimethylsiloxane, No. CAS: 9016-00-6.
Carbomer, No. CAS: 76050-42-5.The embodiment of the present invention use U.S. Lu Runbo (former promise reputation) company provide
Acritamer 940.
Hydrolyzed-silk glue protein, uses the side of embodiment two in number of patent application 201310511239.0 in the embodiment of the present invention
Prepared by method.
Ammonia end polydimethylsiloxane, No. CAS: 71750-80-6, the embodiment of the present invention uses the fragrant refined chemical industry in Guangzhou
The ammonia end polydimethylsiloxane TCN-620 that company limited provides.
Guar hydroxypropyltrimonium ammonium chloride, No. CAS: 65497-29-2, the embodiment of the present invention uses sea, Yutai County
Receive Environmental Protection Technology Co., Ltd provide guar hydroxypropyltrimonium ammonium chloride C-14S.
Phenoxyethanol, i.e. ethylene glycol phenyl ether, No. CAS: 122-99-6.
Sodium laureth sulfate, No. CAS: 9004-82-4.The embodiment of the present invention use Japanese Kao company provide
The sodium laureth sulfate that model is EMAL 270S.
Coconut oleoyl amine MEA, i.e. Coconut Fatty Acid Monoethanolamide, No. CAS: 68140-00-1.The embodiment of the present invention uses four
The FS600-CMEA Coconut Fatty Acid Monoethanolamide (without glycerol) that Chuan Hua language Fine Chemical Co., Ltd provides.
EDTA tetra-sodium, i.e. tetrasodium ethylenediamine tetraacetate, No. CAS: 64-02-8.
Sodium chloride, No. CAS: 7647-14-5.
Citric acid, No. CAS: 77-92-9.
Sodium hydroxide, No. CAS: 1310-73-2.
Methylchloroisothiazandnone, No. CAS: 26172-55-4.
Methylisothiazolinone, No. CAS: 2682-20-4.
Sorbitol, also known as D-Sorbitol, No. CAS: 50-70-4.
Tip edge Fucus Vesiculosus extract, English name: Fucus Serratus Extrac, derive from Boulez Brittany area
Tip edge Fucus Vesiculosus, locals is referred to as " gold Sargassum ".This algae extract has reinforcing fiber archeocyte vigor, and protective wire plastochondria is thin
Born of the same parents, promote dermal respiration, bring powerful moisture-keeping efficacy, Cucumber Extract water storage function for skin, also can promote tissue regeneration, increase
Cell viability recovers skin life, promotes the metabolism of skin, is effective against free radical, antagonism cell senescence, discharges simultaneously
Active-energy, improvement is dried, prevention microgroove, wrinkle produce, delay skin aging.Tip edge Fucus Vesiculosus extract can be prepared or purchase
Can buy, preparation method can be conventional water extraction or alcohol extracting method, according to solid-liquid after such as being cleaned and crush by tip edge Fucus Vesiculosus
Immersing mass fraction than (g/ml) 1:10-1:30 is in 95% ethanol, soaks 8-12h, is heated to reflux 4-6h, and cooling is filtered, will
After filtrate concentrates, it is lyophilized into powder.Tip edge Fucus Vesiculosus extract used in the present invention is to buy from Nanjing Ze Lang medicine section
Skill company limited, specification is 10:1, i.e. the 1g tip edge Fucus Vesiculosus extract that 10g tip edge Fucus Vesiculosus extracts.
Yellow tang extract, English name: Ascophyllum Nodosum Extract, have antitumor, antiviral,
Antibacterial, elimination free radical, anti-oxidation efficacy.Yellow tang extract can be prepared or be commercially available, and preparation method can be conventional
Water extraction or alcohol extracting method, after such as yellow tang being cleaned and crush according to solid-to-liquid ratio (g/ml) 1:10-1:30 immerse mass fraction
It is in 95% ethanol, soaks 8-12h, be heated to reflux 4-6h that cooling is filtered, after filtrate being concentrated, is lyophilized into powder.The present invention
Used in yellow tang extract be to buy from Xi'an incomparably bio tech ltd, specification is 10:1, i.e. 10g yellow tang
The 1g yellow tang extract extracted.
Thorn Asparagus toxiformis (Delile) Coll et Harv Sargassum extract, English name: Asparagopsis Armata Extract, rich in activated silica, energy
Effectively optimize skin cell metabolism, there is skin reconstruction, steatolysis, opposing edema, skin quality moisture-keeping efficacy.Thorn Asparagus toxiformis (Delile) Coll et Harv
Sargassum extract can be prepared or be commercially available, and preparation method can be conventional water extraction or alcohol extracting method, such as will sting Haimen
It is in 95% ethanol that winter Sargassum immerses mass fraction according to solid-to-liquid ratio (g/ml) 1:10-1:30 after cleaning and crush, and soaks 8-12h,
It is heated to reflux 4-6h, cooling, filter, after filtrate being concentrated, be lyophilized into powder.Thorn Asparagus toxiformis (Delile) Coll et Harv Sargassum used in the present invention carries
Taking thing is to buy beautiful (EXSYMOL) company in west of regarding for oneself, and specification is 10:1, i.e. the 1g that 10g thorn Asparagus toxiformis (Delile) Coll et Harv Sargassum extract extracts
Thorn Asparagus toxiformis (Delile) Coll et Harv Sargassum extract.
Shampoo for children of the present invention, contains multiple natural component, gives child triple love: Shu Rou, moist, protection, side
While helping effectively clean scalp and hair-care, water profit scalp, soft bright hair, make that the hair of child is soft and moist distributes gloss.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further, the following stated, is only the preferable enforcement to the present invention
Example, not does the restriction of other forms to the present invention, and any those skilled in the art are possibly also with the disclosure above
Technology contents be changed to the Equivalent embodiments that changes on an equal basis.Every without departing from the present invention program content, according to the present invention
Technical spirit any simple modification that following example are done or equivalent variations, all fall within protection scope of the present invention.
Embodiment 1
Shampoo for children raw material (weight portion): sodium laureth sulfate 50 parts, ethylene glycol bisthioglycolate stearic acid 20 parts, cocos nucifera oil
Amide MEA 40 parts, 51 parts of betaines surfactant, 5 parts of sodium chloride, dimethiconol 3 parts, poly dimethyl silicon
2 parts of oxygen alkane, carbomer 7 parts, hydrolyzed-silk glue protein 20 parts, tip edge Fucus Vesiculosus extract 4 parts, yellow tang extract 4 parts, thorn Haimen
Winter extract 4 parts, sorbitol 10 parts, ammonia end polydimethylsiloxane 2 parts, guar hydroxypropyltrimonium ammonium chloride 10 parts, hydrogen
Sodium oxide 2 parts, methylchloroisothiazandnone 0.15 part, Methylisothiazolinone 0.15 part, phenoxyethanol 3 parts, EDTA tetra-sodium 1.2
Part, citric acid 4 parts, Fructus Citri Limoniae essence 0.18 part, 800 parts of water.
Described betaines surfactant is by cocamido propyl betaine, 3-sulfopropyl etradecyldimethylamine Radix Betae
Alkali, oleamide CAB are uniformly mixed for 1:1:1 in mass ratio and obtain.
The preparation method of above-mentioned shampoo for children, comprises the following steps:
Heat water to 75 DEG C, under 500 revs/min of stirring conditions, be sequentially added into sodium laureth sulfate, ethylene glycol bisthioglycolate
Stearic acid, coconut oleoyl amine MEA, betaines surfactant, dimethiconol, polydimethylsiloxane, carbomer,
Ammonia end polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 48 DEG C, sequentially add
Sorbitol, Fructus Citri Limoniae essence, methylchloroisothiazandnone, Methylisothiazolinone, phenoxyethanol, EDTA tetra-sodium, citric acid, hydrogen-oxygen
Change sodium, sodium chloride, hydrolyzed-silk glue protein, tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract stirring mixing
Uniformly.Obtain the shampoo for children of embodiment 1.
Embodiment 2
Shampoo for children raw material (weight portion): sodium laureth sulfate 50 parts, ethylene glycol bisthioglycolate stearic acid 20 parts, cocos nucifera oil
Amide MEA 40 parts, 51 parts of betaines surfactant, 5 parts of sodium chloride, dimethiconol 3 parts, poly dimethyl silicon
2 parts of oxygen alkane, carbomer 7 parts, hydrolyzed-silk glue protein 20 parts, tip edge Fucus Vesiculosus extract 6 parts, yellow tang extract 6 parts, sorbitol
10 parts, ammonia end polydimethylsiloxane 2 parts, guar hydroxypropyltrimonium ammonium chloride 10 parts, sodium hydroxide 2 parts, methyl chloride different
Thiazolinone 0.15 part, Methylisothiazolinone 0.15 part, phenoxyethanol 3 parts, 1.2 parts of EDTA tetra-sodium, citric acid 4 parts, Fructus Citri Limoniae
0.18 part of essence, 800 parts of water.
Described betaines surfactant is by cocamido propyl betaine, 3-sulfopropyl etradecyldimethylamine Radix Betae
Alkali, oleamide CAB are uniformly mixed for 1:1:1 in mass ratio and obtain.
The preparation method of above-mentioned shampoo for children, comprises the following steps:
Heat water to 75 DEG C, under 500 revs/min of stirring conditions, be sequentially added into sodium laureth sulfate, ethylene glycol bisthioglycolate
Stearic acid, coconut oleoyl amine MEA, betaines surfactant, dimethiconol, polydimethylsiloxane, carbomer,
Ammonia end polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 48 DEG C, sequentially add
Sorbitol, Fructus Citri Limoniae essence, methylchloroisothiazandnone, Methylisothiazolinone, phenoxyethanol, EDTA tetra-sodium, citric acid, hydrogen-oxygen
Change sodium, sodium chloride, hydrolyzed-silk glue protein, tip edge Fucus Vesiculosus extract, yellow tang extract are uniformly mixed.Obtain embodiment
The shampoo for children of 2.
Embodiment 3
Shampoo for children raw material (weight portion): sodium laureth sulfate 50 parts, ethylene glycol bisthioglycolate stearic acid 20 parts, cocos nucifera oil
Amide MEA 40 parts, 51 parts of betaines surfactant, 5 parts of sodium chloride, dimethiconol 3 parts, poly dimethyl silicon
2 parts of oxygen alkane, carbomer 7 parts, hydrolyzed-silk glue protein 20 parts, tip edge Fucus Vesiculosus extract 6 parts, thorn Asparagus toxiformis (Delile) Coll et Harv extract 6 parts, Pyrusussuriensis
Alcohol 10 parts, ammonia end polydimethylsiloxane 2 parts, guar hydroxypropyltrimonium ammonium chloride 10 parts, sodium hydroxide 2 parts, methyl chloride
Isothiazolone 0.15 part, Methylisothiazolinone 0.15 part, phenoxyethanol 3 parts, 1.2 parts of EDTA tetra-sodium, citric acid 4 parts, lemon
0.18 part of lemon essence, 800 parts of water.
Described betaines surfactant is by cocamido propyl betaine, 3-sulfopropyl etradecyldimethylamine Radix Betae
Alkali, oleamide CAB are uniformly mixed for 1:1:1 in mass ratio and obtain.
The preparation method of above-mentioned shampoo for children, comprises the following steps:
Heat water to 75 DEG C, under 500 revs/min of stirring conditions, be sequentially added into sodium laureth sulfate, ethylene glycol bisthioglycolate
Stearic acid, coconut oleoyl amine MEA, betaines surfactant, dimethiconol, polydimethylsiloxane, carbomer,
Ammonia end polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 48 DEG C, sequentially add
Sorbitol, Fructus Citri Limoniae essence, methylchloroisothiazandnone, Methylisothiazolinone, phenoxyethanol, EDTA tetra-sodium, citric acid, hydrogen-oxygen
Change sodium, sodium chloride, hydrolyzed-silk glue protein, tip edge Fucus Vesiculosus extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract are uniformly mixed.Implemented
The shampoo for children of example 3.
Embodiment 4
Shampoo for children raw material (weight portion): sodium laureth sulfate 50 parts, ethylene glycol bisthioglycolate stearic acid 20 parts, cocos nucifera oil
Amide MEA 40 parts, 51 parts of betaines surfactant, 5 parts of sodium chloride, dimethiconol 3 parts, poly dimethyl silicon
2 parts of oxygen alkane, carbomer 7 parts, hydrolyzed-silk glue protein 20 parts, yellow tang extract 6 parts, thorn Asparagus toxiformis (Delile) Coll et Harv extract 6 parts, sorbitol 10
Part, ammonia end polydimethylsiloxane 2 parts, guar hydroxypropyltrimonium ammonium chloride 10 parts, sodium hydroxide 2 parts, the different thiophene of methyl chloride
Oxazoline ketone 0.15 part, Methylisothiazolinone 0.15 part, phenoxyethanol 3 parts, 1.2 parts of EDTA tetra-sodium, citric acid 4 parts, NINGMENGXIANG
Essence 0.18 part, 800 parts of water.
Described betaines surfactant is by cocamido propyl betaine, 3-sulfopropyl etradecyldimethylamine Radix Betae
Alkali, oleamide CAB are uniformly mixed for 1:1:1 in mass ratio and obtain.
The preparation method of above-mentioned shampoo for children, comprises the following steps:
Heat water to 75 DEG C, under 500 revs/min of stirring conditions, be sequentially added into sodium laureth sulfate, ethylene glycol bisthioglycolate
Stearic acid, coconut oleoyl amine MEA, betaines surfactant, dimethiconol, polydimethylsiloxane, carbomer,
Ammonia end polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 48 DEG C, sequentially add
Sorbitol, Fructus Citri Limoniae essence, methylchloroisothiazandnone, Methylisothiazolinone, phenoxyethanol, EDTA tetra-sodium, citric acid, hydrogen-oxygen
Change sodium, sodium chloride, hydrolyzed-silk glue protein, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract are uniformly mixed.Obtain embodiment 4
Shampoo for children.
Embodiment 5
Substantially the same manner as Example 1, differ only in: described betaines surfactant is by 3-sulfopropyl 16
Alkyl-dimethyl glycine betaine, oleamide CAB are uniformly mixed for 1:1 in mass ratio and obtain.Obtain the youngster of embodiment 5
Virgin shampoo.
Embodiment 6
Substantially the same manner as Example 1, differ only in: described betaines surfactant is by cocamidopropyl propyl amide
Glycine betaine, oleamide CAB are uniformly mixed for 1:1 in mass ratio and obtain.Obtain the shampoo for children of embodiment 6.
Embodiment 7
Substantially the same manner as Example 1, differ only in: described betaines surfactant is by cocamidopropyl propyl amide
Glycine betaine, 3-sulfopropyl etradecyldimethylamine glycine betaine are uniformly mixed for 1:1 in mass ratio and obtain.Obtain embodiment 7
Shampoo for children.
Test case 1
According to the method disclosed in " foundation of shampoo anti-dandruff effect detection evaluation methodology and applied research " to embodiment
The shampoo that 1-7 prepares carries out inhibition zone diameter test, is evaluated anti-dandruff effect of shampoo product.Inhibition zone diameter is more
Greatly, anti-dandruff effect is the best.Test data are shown in Table 1.
Wherein, " foundation of shampoo anti-dandruff effect detection evaluation methodology and applied research ", where, Wang Tan, Jia Zebao, flood
Dawn roc, Peng Jin, research and development department of Si Bao daily use chemicals company limited, household chemicals science, o. 11th in 2009.
Table 1: anti-dandruff efficacy test tables of data
Inhibition zone diameter, mm | |
Embodiment 1 | 23.5 |
Embodiment 2 | 18.7 |
Embodiment 3 | 19.5 |
Embodiment 4 | 18.8 |
Embodiment 5 | 20.2 |
Embodiment 6 | 19.6 |
Embodiment 7 | 20.1 |
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv
Extract compound) anti-dandruff effect be substantially better than embodiment 2-4 (tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv carry
Take in thing arbitrarily that the two is compounding);Comparing embodiment 1 and embodiment 5-7, embodiment 1 (cocamido propyl betaine, 3-sulphur third
Base etradecyldimethylamine glycine betaine, oleamide CAB are compounding) anti-dandruff effect is substantially better than embodiment 5-7 (coconut oleoyl amine
In CAB, 3-sulfopropyl etradecyldimethylamine glycine betaine, oleamide CAB, arbitrarily the two is compounding).
Test case 2
Shampoo for children embodiment 1-7 prepared, carries out fill with dark brown vial respectively, opens wide bottle cap, is placed in
Preservation 90 days under ambient temperature 40 DEG C, relative humidity 85% environment, then carries out staphylococcus aureus (ATCC 6538) bacterium colony
Sum test, measures with reference to GBT 4789.2-2008 microbiological test of food hygiene total plate count.Concrete test result is shown in Table
2。
Table 2: total plate count test table
S. aureus colonies sum, cfu/g | |
Embodiment 1 | 253 |
Embodiment 2 | 783 |
Embodiment 3 | 767 |
Embodiment 4 | 763 |
Embodiment 5 | 572 |
Embodiment 6 | 584 |
Embodiment 7 | 559 |
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv
Extract compound) antiseptic property be substantially better than embodiment 2-4 (tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv carry
Take in thing arbitrarily that the two is compounding);Comparing embodiment 1 and embodiment 5-7, embodiment 1 (cocamido propyl betaine, 3-sulphur third
Base etradecyldimethylamine glycine betaine, oleamide CAB are compounding) antiseptic property is substantially better than embodiment 5-7 (coconut oleoyl amine
In CAB, 3-sulfopropyl etradecyldimethylamine glycine betaine, oleamide CAB, arbitrarily the two is compounding).
Claims (5)
1. a shampoo for children, it is characterised in that be prepared from by following raw material: water, sodium laureth sulfate, second two
The acid of alcohol distearyl, coconut oleoyl amine MEA, betaines surfactant, sodium chloride, dimethiconol, poly dimethyl silicon
Oxygen alkane, carbomer, hydrolyzed-silk glue protein, tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract, sorbitol,
Essence, ammonia end polydimethylsiloxane, guar hydroxypropyltrimonium ammonium chloride, sodium hydroxide, methylchloroisothiazandnone, first
Base isothiazolone, phenoxyethanol, EDTA tetra-sodium, citric acid.
2. a shampoo for children, it is characterised in that be prepared from by the raw material of following weight parts: sodium laureth sulfate
45-55 part, ethylene glycol bisthioglycolate stearic acid 15-25 part, coconut oleoyl amine MEA 35-45 part, betaines surfactant 45-55 part,
Sodium chloride 1-10 part, dimethiconol 1-10 part, polydimethylsiloxane 1-10 part, carbomer 5-15 part, hydrolyzed-silk
Glue protein 15-25 part, tip edge Fucus Vesiculosus extract 1-10 part, yellow tang extract 1-10 part, thorn Asparagus toxiformis (Delile) Coll et Harv extract 1-10 part,
Sorbitol 5-15 part, ammonia end polydimethylsiloxane 1-10 part, guar hydroxypropyltrimonium ammonium chloride 5-15 part, sodium hydroxide
1-10 part, methylchloroisothiazandnone 0.1-1 part, Methylisothiazolinone 0.1-1 part, phenoxyethanol 1-10 part, EDTA tetra-sodium
1-10 part, citric acid 1-10 part, essence 0.1-1 part, water 700-900 part.
3. shampoo for children as claimed in claim 1 or 2, it is characterised in that: described betaines surfactant is coconut palm
In oleamide CAB, 3-sulfopropyl etradecyldimethylamine glycine betaine, oleamide CAB, one or more is mixed
Compound.
4. shampoo for children as claimed in claim 3, it is characterised in that: described betaines surfactant is by cocos nucifera oil acyl
Amine CAB, 3-sulfopropyl etradecyldimethylamine glycine betaine, oleamide CAB mix, described coconut oleoyl amine
CAB, 3-sulfopropyl etradecyldimethylamine glycine betaine, the mass ratio of oleamide CAB are (1-3): (1-3):
(1-3)。
5. the preparation method of the shampoo for children as according to any one of claim 1-4, it is characterised in that include following step
Rapid:
Heat water to 65-85 DEG C, under stirring condition, be sequentially added into sodium laureth sulfate, ethylene glycol bisthioglycolate stearic acid, coconut palm
Oleamide MEA, betaines surfactant, dimethiconol, polydimethylsiloxane, carbomer, ammonia end poly-two
Methylsiloxane, guar hydroxypropyltrimonium ammonium chloride are uniformly mixed, and are cooled to 45-55 DEG C, sequentially add Pyrusussuriensis
Alcohol, essence, methylchloroisothiazandnone, Methylisothiazolinone, phenoxyethanol, EDTA tetra-sodium, citric acid, sodium hydroxide, chlorine
Change sodium, hydrolyzed-silk glue protein, tip edge Fucus Vesiculosus extract, yellow tang extract, thorn Asparagus toxiformis (Delile) Coll et Harv extract are uniformly mixed i.e.
?.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107669552A (en) * | 2017-10-31 | 2018-02-09 | 思拓科(上海)生物科技股份有限公司 | Organic baby's shampoo |
CN107822975A (en) * | 2017-11-29 | 2018-03-23 | 桂林华诺威生物科技有限公司 | A kind of draft collagen shampoo |
CN107913230A (en) * | 2017-11-27 | 2018-04-17 | 曾万祥 | A kind of ginger juice albumen conserves shampoo |
CN108125804A (en) * | 2018-01-29 | 2018-06-08 | 南阳师范学院 | A kind of antibacterial light shampoo paste and preparation method thereof |
CN115813819A (en) * | 2022-12-03 | 2023-03-21 | 福建省梦娇兰日用化学品有限公司 | Children shampoo free of silicone oil and preparation method thereof |
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CN103720637A (en) * | 2014-01-22 | 2014-04-16 | 云南龙润茶科技有限公司 | Natural plant shampoo and hair conditioner and preparation methods thereof |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107669552A (en) * | 2017-10-31 | 2018-02-09 | 思拓科(上海)生物科技股份有限公司 | Organic baby's shampoo |
CN107913230A (en) * | 2017-11-27 | 2018-04-17 | 曾万祥 | A kind of ginger juice albumen conserves shampoo |
CN107822975A (en) * | 2017-11-29 | 2018-03-23 | 桂林华诺威生物科技有限公司 | A kind of draft collagen shampoo |
CN108125804A (en) * | 2018-01-29 | 2018-06-08 | 南阳师范学院 | A kind of antibacterial light shampoo paste and preparation method thereof |
CN115813819A (en) * | 2022-12-03 | 2023-03-21 | 福建省梦娇兰日用化学品有限公司 | Children shampoo free of silicone oil and preparation method thereof |
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